CN106702773A - Method for dyeing wool fabric with gardenin - Google Patents
Method for dyeing wool fabric with gardenin Download PDFInfo
- Publication number
- CN106702773A CN106702773A CN201611089821.2A CN201611089821A CN106702773A CN 106702773 A CN106702773 A CN 106702773A CN 201611089821 A CN201611089821 A CN 201611089821A CN 106702773 A CN106702773 A CN 106702773A
- Authority
- CN
- China
- Prior art keywords
- gardenin
- dyeing
- ethanol
- wool fabric
- phenol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/651—Compounds without nitrogen
- D06P1/65106—Oxygen-containing compounds
- D06P1/65125—Compounds containing ester groups
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
- D06P3/14—Wool
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Coloring (AREA)
Abstract
The invention provides a method for dyeing wool fabric with gardenin. The method comprises the following steps: dissolving gardenin in an ethanol/phenol mixed solution; adding a surfactant, namely benzyl benzoate, and obtaining a transparent solution under ultrasonic action; putting the wool fabric into the dyeing liquid; and oscillating and heating to 30-60 DEG C for dyeing. In the dyeing technology, the gardenin is not modified, high-temperature dyeing is not adopted, and the dyed fabric has high color fastness.
Description
Technical field
The present invention relates to a kind of textile dyeing technical field, and in particular to a kind of side of gardenin dyeing wool fabric
Method.
Background technology
Gardenin is a kind of natural pigment extracted from madder wort cape jasmine, is flavone compound.Gardenin can
The depth yellow for obtaining different tones is dyeed with different mordant dyeing agent.Gardenin yellow plant dye most widely used since being Qin Han
Material.But gardenin is to protein fibres such as wools, and directly upper dye is poor, and color fastness is poor.
The content of the invention
In order that the effective dyeing wool fabric of gardenin, the present invention is adopted the following technical scheme that.
A kind of method of gardenin dyeing wool fabric, comprises the following steps：（1）Phenol is dissolved in ethanol；（2）By Cape jasmine
Sub- element is dissolved in ethanol/phenol mixed solution, adds surfactant Ergol, and clear solution is obtained under ultrasound；
（3）During wool fabric put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC, 5 ~ 30min of insulation dyeing；（4）To be knitted after dyeing
Thing is placed in ethanol and washs, and is dried under 80oC.
Further, the ethanol of described ethanol/phenol mixed solution and the mass ratio of phenol are 1:0.1~3.
Further, described surfactant Ergol is 1 with the mass ratio of ethanol/phenol mixed solution:
2000~8000。
Further, described gardenin and the mass ratio of ethanol/phenol mixed solution are 1:200~4000.
The beneficial effects of the present invention are, it is not necessary to gardenin is modified, high-temperature dyeing is not used, fabric after dyeing
Color fastness is high.
Specific embodiment
The present invention is described in detail below in conjunction with specific embodiment.It should be noted that the skill described in following embodiments
The combination of art feature or technical characteristic be not construed as it is isolated, they can be mutually combined so as to reach preferably
Technique effect.
Embodiment 1
The method detailed step of gardenin dyeing wool fabric is as follows：
（1）20g phenol is dissolved in 180g ethanol；
（2）0.1g gardenins are dissolved in above-mentioned ethanol/phenol mixed solution, 0.04g surfactant benzoic acid is added
Benzyl ester, clear solution is obtained under ultrasound；
（3）During 10g wool fabrics are put into above-mentioned dye liquor, vibration is heated to 60oC, insulation dyeing 30min；
（4）Fabric after dyeing is placed in ethanol and is washed, dried under 80oC.
Embodiment 2
The method detailed step of gardenin dyeing wool fabric is as follows：
（1）300g phenol is dissolved in 100g ethanol；
（2）1g gardenins are dissolved in above-mentioned ethanol/phenol mixed solution, 0.08g surfactant Benzyl Benzoates are added
Ester, clear solution is obtained under ultrasound；
（3）During 10g wool fabrics are put into above-mentioned dye liquor, vibration is heated to 30oC, insulation dyeing 30min；
（4）Fabric after dyeing is placed in ethanol and is washed, dried under 80oC.
Embodiment 3
The method detailed step of gardenin dyeing wool fabric is as follows：
（1）50g phenol is dissolved in 250g ethanol；
（2）0.2g gardenins are dissolved in above-mentioned ethanol/phenol mixed solution, 0.06g surfactant benzoic acid is added
Benzyl ester, clear solution is obtained under ultrasound；
（3）During 10g wool fabrics are put into above-mentioned dye liquor, vibration is heated to 50oC, insulation dyeing 10min；
（4）Fabric after dyeing is placed in ethanol and is washed, dried under 80oC.
Embodiment 4
The method detailed step of gardenin dyeing wool fabric is as follows：
（1）200g phenol is dissolved in 200g ethanol；
（2）0.6g gardenins are dissolved in above-mentioned ethanol/phenol mixed solution, 0.01g surfactant benzoic acid is added
Benzyl ester, clear solution is obtained under ultrasound；
（3）During 10g wool fabrics are put into above-mentioned dye liquor, vibration is heated to 40oC, insulation dyeing 15min；
（4）Fabric after dyeing is placed in ethanol and is washed, dried under 80oC.
Although having been presented for some embodiments of the present invention herein, it will be appreciated by those of skill in the art that
Without departing from the spirit of the invention, the embodiments herein can be changed.Above-described embodiment be it is exemplary, no
Should be using the embodiments herein as the restriction of interest field of the present invention.
Claims (4)
1. a kind of method of gardenin dyeing wool fabric, it is characterised in that comprise the following steps：
（1）Phenol is dissolved in ethanol；
（2）Gardenin is dissolved in ethanol/phenol mixed solution, surfactant Ergol is added, under ultrasound
To clear solution；
（3）During wool fabric put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC, 5 ~ 30min of insulation dyeing；
（4）Fabric after dyeing is placed in ethanol and is washed, dried under 80oC.
2. the method for gardenin dyeing wool fabric as claimed in claim 1, the ethanol of described ethanol/phenol mixed solution
It is 1 with the mass ratio of phenol:0.1~3.
3. the method for gardenin dyeing wool fabric as claimed in claim 1, described surfactant Ergol with
The mass ratio of ethanol/phenol mixed solution is 1:2000~8000.
4. the method for gardenin dyeing wool fabric as claimed in claim 1, described gardenin mixes molten with ethanol/phenol
The mass ratio of liquid is 1:200~4000.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611089821.2A CN106702773A (en) | 2016-12-01 | 2016-12-01 | Method for dyeing wool fabric with gardenin |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611089821.2A CN106702773A (en) | 2016-12-01 | 2016-12-01 | Method for dyeing wool fabric with gardenin |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106702773A true CN106702773A (en) | 2017-05-24 |
Family
ID=58934429
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611089821.2A Pending CN106702773A (en) | 2016-12-01 | 2016-12-01 | Method for dyeing wool fabric with gardenin |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106702773A (en) |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102383321A (en) * | 2011-09-07 | 2012-03-21 | 浙江理工大学 | Method for improving light fastness of natural dye stuff dyed fabrics |
| CN102953186A (en) * | 2012-09-27 | 2013-03-06 | 杭州翔盛高强纤维材料股份有限公司 | Ultra high molecular weight polyethylene fiber dyeing device and method |
| CN103174041A (en) * | 2013-04-12 | 2013-06-26 | 祝洪哲 | Method for low-temperature ultrasonic dyeing and soaping of short fiber by using Chinese herbal medicine plant dye |
| CN103215831A (en) * | 2013-04-19 | 2013-07-24 | 江阴职业技术学院 | Polyester/sorona mixed fabric disperse dye one-bath process dyeing method |
| CN104088170A (en) * | 2014-07-21 | 2014-10-08 | 天津天绿健科技有限公司 | Method for dyeing wool by use of natural dyestuff-gardenia yellow |
| CN105648799A (en) * | 2016-01-25 | 2016-06-08 | 苏州印丝特纺织数码科技有限公司 | Neutral leveling agent for dyeing wool fiber with acid dye |
-
2016
- 2016-12-01 CN CN201611089821.2A patent/CN106702773A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102383321A (en) * | 2011-09-07 | 2012-03-21 | 浙江理工大学 | Method for improving light fastness of natural dye stuff dyed fabrics |
| CN102953186A (en) * | 2012-09-27 | 2013-03-06 | 杭州翔盛高强纤维材料股份有限公司 | Ultra high molecular weight polyethylene fiber dyeing device and method |
| CN103174041A (en) * | 2013-04-12 | 2013-06-26 | 祝洪哲 | Method for low-temperature ultrasonic dyeing and soaping of short fiber by using Chinese herbal medicine plant dye |
| CN103215831A (en) * | 2013-04-19 | 2013-07-24 | 江阴职业技术学院 | Polyester/sorona mixed fabric disperse dye one-bath process dyeing method |
| CN104088170A (en) * | 2014-07-21 | 2014-10-08 | 天津天绿健科技有限公司 | Method for dyeing wool by use of natural dyestuff-gardenia yellow |
| CN105648799A (en) * | 2016-01-25 | 2016-06-08 | 苏州印丝特纺织数码科技有限公司 | Neutral leveling agent for dyeing wool fiber with acid dye |
Non-Patent Citations (1)
| Title |
|---|
| 范洪琼等: "《基础化学》", 31 August 2018 * |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106702773A (en) | Method for dyeing wool fabric with gardenin | |
| CN106758353A (en) | Colouring method of the gardenin to wool fabric | |
| CN106702769A (en) | Method for dyeing silk fabrics with gardenin | |
| CN106592268A (en) | Method for dyeing polyester fabric with gardenin | |
| CN106702788A (en) | Method for dyeing polyester fabrics by using gardenin | |
| CN106758335A (en) | Colouring method of the Acetylshikonin to wool fabric | |
| CN106544896A (en) | The method of gardenin dyed cotton fabric | |
| CN106702771A (en) | Method for dyeing polyester textile by rutamine | |
| CN106702772A (en) | Method for dyeing silk fabric with rutin | |
| CN106702774A (en) | Method for dyeing silk fabric by utilizing acetylshikonin | |
| CN106702768A (en) | Method for dyeing silk fabric by using curcumin | |
| CN106702770A (en) | Dyeing method of shikonin on polyester fabric | |
| CN106702775A (en) | Method for dyeing polyester fabric through alizarin | |
| CN106592271A (en) | Method of using safflower red to dye wool fabric | |
| CN106758363A (en) | The method of Acetylshikonin dyeing wool fabric | |
| CN106555343A (en) | The method of sorphoranone dyeing wool fabric | |
| CN106638052A (en) | Method for dyeing cotton fabric with rutamine | |
| CN106758339A (en) | The method of shikonin dyed polyester textiles | |
| CN106544897A (en) | The method of shikonin dyeing wool fabric | |
| CN106544890A (en) | Colouring method of the gardenin to bafta | |
| CN106638029A (en) | Method for dyeing cotton fabric through acetyl shikonin | |
| CN106544899A (en) | The method that shikonin dyes silk fabric | |
| CN106758354A (en) | The method of shikonin dyed cotton fabric | |
| CN106758340A (en) | Colouring method of the sorphoranone to wool fabric | |
| CN106758362A (en) | The method of curcumin dyeing wool fabric |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20170524 |
|
| WD01 | Invention patent application deemed withdrawn after publication |