CN106758335A - Colouring method of the Acetylshikonin to wool fabric - Google Patents

Colouring method of the Acetylshikonin to wool fabric Download PDF

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Publication number
CN106758335A
CN106758335A CN201611088964.1A CN201611088964A CN106758335A CN 106758335 A CN106758335 A CN 106758335A CN 201611088964 A CN201611088964 A CN 201611088964A CN 106758335 A CN106758335 A CN 106758335A
Authority
CN
China
Prior art keywords
acetylshikonin
carbon tetrachloride
wool fabric
phenol
dyeing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201611088964.1A
Other languages
Chinese (zh)
Inventor
卢明
周菁
赵振云
刘萍
刘一萍
刘欣
胡睿敏
蒲青霞
董倩
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Southwest University
Original Assignee
Southwest University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Southwest University filed Critical Southwest University
Priority to CN201611088964.1A priority Critical patent/CN106758335A/en
Publication of CN106758335A publication Critical patent/CN106758335A/en
Pending legal-status Critical Current

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Classifications

    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/62—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds with sulfate, sulfonate, sulfenic or sulfinic groups
    • D06P1/621—Compounds without nitrogen
    • D06P1/622—Sulfonic acids or their salts
    • D06P1/625—Aromatic
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
    • D06P3/02—Material containing basic nitrogen
    • D06P3/04—Material containing basic nitrogen containing amide groups
    • D06P3/14—Wool

Abstract

The invention provides a kind of Acetylshikonin to the colouring method of wool fabric, the method comprises the following steps：Acetylshikonin is dissolved in carbon tetrachloride/phenol mixed solution, surfactant sodium dodecyl base benzene sulfonic acid sodium salt is added, clear solution is obtained under ultrasound；During wool fabric put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC dyeing.This staining technique need not be modified to Acetylshikonin, not use high-temperature dyeing, and fabric color fastness is high after dyeing.

Description

Colouring method of the Acetylshikonin to wool fabric
Technical field
The present invention relates to a kind of textile dyeing technical field, and in particular to a kind of dye of Acetylshikonin to wool fabric Color method.
Background technology
Acetylshikonin is primarily present in Asian puccoon root also known as Acetyl-shikonin, is naphthalene Quinone Pigments, aubergine needle-like knot It is brilliant.The hydrophobicity side switch of Acetylshikonin is long, therefore water-soluble poor, typically can be using the method for first mordant dyeing to cellulose Fabric is dyeed.Being compatible with the environment property of Acetylshikonin is good, is harmful to human health.But Acetylshikonin is to wool Deng protein fibre, directly upper dye is poor, and color fastness is poor.
The content of the invention
In order that the effective dyeing wool fabric of Acetylshikonin, the present invention is adopted the following technical scheme that.
A kind of Acetylshikonin comprises the following steps to the colouring method of wool fabric：（1）Phenol is dissolved in carbon tetrachloride In；（2）Acetylshikonin is dissolved in carbon tetrachloride/phenol mixed solution, surfactant sodium dodecyl base benzene sulphur is added Sour sodium, clear solution is obtained under ultrasound；（3）During wool fabric put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC, is incubated 5 ~ 30min of dyeing；（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Further, the carbon tetrachloride of described carbon tetrachloride/phenol mixed solution and the mass ratio of phenol are 1:0.1~ 3。
Further, described surfactant sodium dodecyl base benzene sulfonic acid sodium salt and the matter of carbon tetrachloride/phenol mixed solution Amount is than being 1:2000~8000.
Further, described Acetylshikonin and the mass ratio of carbon tetrachloride/phenol mixed solution are 1:200~4000.
The beneficial effects of the present invention are, it is not necessary to Acetylshikonin is modified, high-temperature dyeing is not used, after dyeing Fabric color fastness is high.
Specific embodiment
The present invention is described in detail below in conjunction with specific embodiment.It should be noted that the skill described in following embodiments The combination of art feature or technical characteristic be not construed as it is isolated, they can be mutually combined so as to reach preferably Technique effect.
Embodiment 1
Acetylshikonin is as follows to the colouring method detailed step of wool fabric：
（1）20g phenol is dissolved in 180g carbon tetrachloride；
（2）1g Acetylshikonins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.04g surfactants are added Neopelex, clear solution is obtained under ultrasound；
（3）During 10g wool fabrics are put into above-mentioned dye liquor, vibration is heated to 60oC, insulation dyeing 30min；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Embodiment 2
Acetylshikonin is as follows to the colouring method detailed step of wool fabric：
（1）300g phenol is dissolved in 100g carbon tetrachloride；
（2）0.1g Acetylshikonins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.08g surface-actives are added Agent neopelex, clear solution is obtained under ultrasound；
（3）During 10g wool fabrics are put into above-mentioned dye liquor, vibration is heated to 30oC, insulation dyeing 30min；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Embodiment 3
Acetylshikonin is as follows to the colouring method detailed step of wool fabric：
（1）50g phenol is dissolved in 250g carbon tetrachloride；
（2）1g Acetylshikonins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.06g surfactants are added Neopelex, clear solution is obtained under ultrasound；
（3）During 10g wool fabrics are put into above-mentioned dye liquor, vibration is heated to 50oC, insulation dyeing 10min；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Embodiment 4
Acetylshikonin is as follows to the colouring method detailed step of wool fabric：
（1）200g phenol is dissolved in 200g carbon tetrachloride；
（2）0.7g Acetylshikonins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.01g surface-actives are added Agent neopelex, clear solution is obtained under ultrasound；
（3）During 10g wool fabrics are put into above-mentioned dye liquor, vibration is heated to 40oC, insulation dyeing 15min；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Although having been presented for some embodiments of the present invention herein, it will be appreciated by those of skill in the art that Without departing from the spirit of the invention, the embodiments herein can be changed.Above-described embodiment be it is exemplary, no Should be using the embodiments herein as the restriction of interest field of the present invention.

Claims (4)

1. colouring method of a kind of Acetylshikonin to wool fabric, it is characterised in that comprise the following steps：
（1）Phenol is dissolved in carbon tetrachloride；
（2）Acetylshikonin is dissolved in carbon tetrachloride/phenol mixed solution, surfactant sodium dodecyl base benzene sulphur is added Sour sodium, clear solution is obtained under ultrasound；
（3）During wool fabric put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC, 5 ~ 30min of insulation dyeing；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
2. Acetylshikonin as claimed in claim 1 is to the colouring method of wool fabric, described carbon tetrachloride/phenol mixing The carbon tetrachloride of solution is 1 with the mass ratio of phenol:0.1~3.
3. Acetylshikonin as claimed in claim 1 is to the colouring method of wool fabric, described surfactant sodium dodecyl Base benzene sulfonic acid sodium salt is 1 with the mass ratio of carbon tetrachloride/phenol mixed solution:2000~8000.
4. Acetylshikonin as claimed in claim 1 is to the colouring method of wool fabric, described Acetylshikonin and tetrachloro The mass ratio for changing carbon/phenol mixed solution is 1:200~4000.
CN201611088964.1A 2016-12-01 2016-12-01 Colouring method of the Acetylshikonin to wool fabric Pending CN106758335A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611088964.1A CN106758335A (en) 2016-12-01 2016-12-01 Colouring method of the Acetylshikonin to wool fabric

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201611088964.1A CN106758335A (en) 2016-12-01 2016-12-01 Colouring method of the Acetylshikonin to wool fabric

Publications (1)

Publication Number Publication Date
CN106758335A true CN106758335A (en) 2017-05-31

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201611088964.1A Pending CN106758335A (en) 2016-12-01 2016-12-01 Colouring method of the Acetylshikonin to wool fabric

Country Status (1)

Country Link
CN (1) CN106758335A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113106584A (en) * 2021-04-08 2021-07-13 江南织造府(宁波)线业有限公司 Method for preparing woven yarn by using worsted leftovers

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104088167A (en) * 2014-07-04 2014-10-08 常州大学 Method for improving color depth and light fastness of natural dye-dyed fabric
CN105908530A (en) * 2016-05-18 2016-08-31 江苏阳光股份有限公司 One-bath dyeing process for wool Sorna fabric
CN105970672A (en) * 2016-05-18 2016-09-28 江苏阳光股份有限公司 Process for dyeing wool-cotton worsted fabric with vegetable dye

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104088167A (en) * 2014-07-04 2014-10-08 常州大学 Method for improving color depth and light fastness of natural dye-dyed fabric
CN105908530A (en) * 2016-05-18 2016-08-31 江苏阳光股份有限公司 One-bath dyeing process for wool Sorna fabric
CN105970672A (en) * 2016-05-18 2016-09-28 江苏阳光股份有限公司 Process for dyeing wool-cotton worsted fabric with vegetable dye

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
韩晓俊等: "媒染剂在天然染料对毛织物染色中的作用", 《毛纺科技》 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113106584A (en) * 2021-04-08 2021-07-13 江南织造府(宁波)线业有限公司 Method for preparing woven yarn by using worsted leftovers

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