CN106758356A - Colouring method of the alizarin to dacron - Google Patents

Colouring method of the alizarin to dacron Download PDF

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Publication number
CN106758356A
CN106758356A CN201611089815.7A CN201611089815A CN106758356A CN 106758356 A CN106758356 A CN 106758356A CN 201611089815 A CN201611089815 A CN 201611089815A CN 106758356 A CN106758356 A CN 106758356A
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CN
China
Prior art keywords
alizarin
carbon tetrachloride
dacron
phenol
dyeing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201611089815.7A
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Chinese (zh)
Inventor
卢明
胡睿敏
刘欣
刘萍
刘一萍
蒲青霞
董倩
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Southwest University
Original Assignee
Southwest University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Southwest University filed Critical Southwest University
Priority to CN201611089815.7A priority Critical patent/CN106758356A/en
Publication of CN106758356A publication Critical patent/CN106758356A/en
Pending legal-status Critical Current

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Classifications

    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/34General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/62General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds with sulfate, sulfonate, sulfenic or sulfinic groups
    • D06P1/621Compounds without nitrogen
    • D06P1/622Sulfonic acids or their salts
    • D06P1/625Aromatic
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P3/00Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
    • D06P3/34Material containing ester groups
    • D06P3/52Polyesters

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Coloring (AREA)

Abstract

The invention provides a kind of alizarin to the colouring method of dacron, the method comprises the following steps:Alizarin is dissolved in carbon tetrachloride/phenol mixed solution, surfactant sodium dodecyl base benzene sulfonic acid sodium salt is added, clear solution is obtained under ultrasound;During dacron put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC dyeing.This staining technique need not be modified to alizarin, not use high-temperature dyeing, and fabric color fastness is high after dyeing.

Description

Colouring method of the alizarin to dacron
Technical field
The present invention relates to a kind of textile dyeing technical field, and in particular to a kind of dyeing side of alizarin to dacron Method.
Background technology
Alizarin is a kind of typical mordant dyes.Can be extracted from madder root.Early in before 3500, alizarin just the Central Asia, Egyptian, Europe and China are used as orchil.Alizarin is red acicular crystal, is practically insoluble in water, used as natural plant Thing dyestuff is used to make the red textile of hot flame.Alizarin is used for dyeing and the stamp of cotton, and hunting pink is obtained during with aluminium mordant, Feux rouges brown is obtained during with chromium stain matchmaker, purple is obtained during with iron mordant, gold-tinted is obtained during tin mordanting agent red.But it is alizarin Element is difficult the directly synthetic fibers such as upper dye terylene.
The content of the invention
In order that the effective dyed polyester textiles of alizarin, the present invention is adopted the following technical scheme that.
A kind of alizarin comprises the following steps to the colouring method of dacron:(1)Phenol is dissolved in carbon tetrachloride;(2) Alizarin is dissolved in carbon tetrachloride/phenol mixed solution, surfactant sodium dodecyl base benzene sulfonic acid sodium salt is added, under ultrasound To clear solution;(3)During dacron put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC, 5 ~ 30min of insulation dyeing; (4)Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Further, the carbon tetrachloride of described carbon tetrachloride/phenol mixed solution and the mass ratio of phenol are 1:0.1~ 3。
Further, described surfactant sodium dodecyl base benzene sulfonic acid sodium salt and the matter of carbon tetrachloride/phenol mixed solution Amount is than being 1:2000~8000.
Further, described alizarin and the mass ratio of carbon tetrachloride/phenol mixed solution are 1:200~4000.
The beneficial effects of the present invention are, it is not necessary to alizarin is modified, high-temperature dyeing is not used, fabric color after dyeing Fastness is high.
Specific embodiment
The present invention is described in detail below in conjunction with specific embodiment.It should be noted that the skill described in following embodiments The combination of art feature or technical characteristic be not construed as it is isolated, they can be mutually combined so as to reach preferably Technique effect.
Embodiment 1
Alizarin is as follows to the colouring method detailed step of dacron:
(1)20g phenol is dissolved in 180g carbon tetrachloride;
(2)1g alizarins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.04g surfactant sodium dodecyls are added Base benzene sulfonic acid sodium salt, clear solution is obtained under ultrasound;
(3)During 10g dacrons are put into above-mentioned dye liquor, vibration is heated to 60oC, insulation dyeing 30min;
(4)Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Embodiment 2
Alizarin is as follows to the colouring method detailed step of dacron:
(1)300g phenol is dissolved in 100g carbon tetrachloride;
(2)0.3g alizarins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.08g surfactants 12 are added Sodium alkyl benzene sulfonate, clear solution is obtained under ultrasound;
(3)During 10g dacrons are put into above-mentioned dye liquor, vibration is heated to 30oC, insulation dyeing 30min;
(4)Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Embodiment 3
Alizarin is as follows to the colouring method detailed step of dacron:
(1)50g phenol is dissolved in 250g carbon tetrachloride;
(2)1g alizarins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.06g surfactant sodium dodecyls are added Base benzene sulfonic acid sodium salt, clear solution is obtained under ultrasound;
(3)During 10g dacrons are put into above-mentioned dye liquor, vibration is heated to 50oC, insulation dyeing 10min;
(4)Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Embodiment 4
Alizarin is as follows to the colouring method detailed step of dacron:
(1)200g phenol is dissolved in 200g carbon tetrachloride;
(2)0.9g alizarins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.01g surfactants 12 are added Sodium alkyl benzene sulfonate, clear solution is obtained under ultrasound;
(3)During 10g dacrons are put into above-mentioned dye liquor, vibration is heated to 40oC, insulation dyeing 15min;
(4)Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Although having been presented for some embodiments of the present invention herein, it will be appreciated by those of skill in the art that Without departing from the spirit of the invention, the embodiments herein can be changed.Above-described embodiment be it is exemplary, no Should be using the embodiments herein as the restriction of interest field of the present invention.

Claims (4)

1. colouring method of a kind of alizarin to dacron, it is characterised in that comprise the following steps:
(1)Phenol is dissolved in carbon tetrachloride;
(2)Alizarin is dissolved in carbon tetrachloride/phenol mixed solution, surfactant sodium dodecyl base benzene sulfonic acid sodium salt is added, Clear solution is obtained under ultrasound;
(3)During dacron put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC, 5 ~ 30min of insulation dyeing;
(4)Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
2. alizarin as claimed in claim 1 is to the colouring method of dacron, described carbon tetrachloride/phenol mixed solution Carbon tetrachloride is 1 with the mass ratio of phenol:0.1~3.
3. alizarin as claimed in claim 1 is to the colouring method of dacron, described surfactant sodium dodecyl base benzene sulphur Sour sodium is 1 with the mass ratio of carbon tetrachloride/phenol mixed solution:2000~8000.
4. to the colouring method of dacron, described alizarin mixes alizarin as claimed in claim 1 with carbon tetrachloride/phenol The mass ratio of solution is 1:200~4000.
CN201611089815.7A 2016-12-01 2016-12-01 Colouring method of the alizarin to dacron Pending CN106758356A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611089815.7A CN106758356A (en) 2016-12-01 2016-12-01 Colouring method of the alizarin to dacron

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201611089815.7A CN106758356A (en) 2016-12-01 2016-12-01 Colouring method of the alizarin to dacron

Publications (1)

Publication Number Publication Date
CN106758356A true CN106758356A (en) 2017-05-31

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CN201611089815.7A Pending CN106758356A (en) 2016-12-01 2016-12-01 Colouring method of the alizarin to dacron

Country Status (1)

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CN (1) CN106758356A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109914125A (en) * 2019-02-22 2019-06-21 东华大学 A kind of normal pressure exhaust process of biology base PTT series polyester textile

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1810889A (en) * 2006-02-21 2006-08-02 海澜集团公司 Madder dye extracting process and its usage in dyeing mercerized wool and mercerized wool fabric
CN101696553A (en) * 2009-10-30 2010-04-21 五邑大学 Method for dying fabrics by color combination of vegetable dyes
CN103174041A (en) * 2013-04-12 2013-06-26 祝洪哲 Method for low-temperature ultrasonic dyeing and soaping of short fiber by using Chinese herbal medicine plant dye
CN103215831A (en) * 2013-04-19 2013-07-24 江阴职业技术学院 Polyester/sorona mixed fabric disperse dye one-bath process dyeing method

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1810889A (en) * 2006-02-21 2006-08-02 海澜集团公司 Madder dye extracting process and its usage in dyeing mercerized wool and mercerized wool fabric
CN101696553A (en) * 2009-10-30 2010-04-21 五邑大学 Method for dying fabrics by color combination of vegetable dyes
CN103174041A (en) * 2013-04-12 2013-06-26 祝洪哲 Method for low-temperature ultrasonic dyeing and soaping of short fiber by using Chinese herbal medicine plant dye
CN103215831A (en) * 2013-04-19 2013-07-24 江阴职业技术学院 Polyester/sorona mixed fabric disperse dye one-bath process dyeing method

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
于伯龄: "天然染料等同体——茜素的染色试验", 《印染》 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109914125A (en) * 2019-02-22 2019-06-21 东华大学 A kind of normal pressure exhaust process of biology base PTT series polyester textile
CN109914125B (en) * 2019-02-22 2021-07-20 东华大学 Normal-pressure dip dyeing process of bio-based PTT series polyester fabric

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