CN106758338A - Colouring method of the alizarin to bafta - Google Patents

Colouring method of the alizarin to bafta Download PDF

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Publication number
CN106758338A
CN106758338A CN201611089016.XA CN201611089016A CN106758338A CN 106758338 A CN106758338 A CN 106758338A CN 201611089016 A CN201611089016 A CN 201611089016A CN 106758338 A CN106758338 A CN 106758338A
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CN
China
Prior art keywords
alizarin
dmso
dimethyl sulfoxide
bafta
phenol
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201611089016.XA
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Chinese (zh)
Inventor
刘萍
刘一萍
刘欣
胡睿敏
蒲青霞
董倩
卢明
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Southwest University
Original Assignee
Southwest University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Southwest University filed Critical Southwest University
Priority to CN201611089016.XA priority Critical patent/CN106758338A/en
Publication of CN106758338A publication Critical patent/CN106758338A/en
Pending legal-status Critical Current

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Classifications

    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/34General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/62General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds with sulfate, sulfonate, sulfenic or sulfinic groups
    • D06P1/621Compounds without nitrogen
    • D06P1/622Sulfonic acids or their salts
    • D06P1/625Aromatic
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P3/00Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
    • D06P3/58Material containing hydroxyl groups
    • D06P3/60Natural or regenerated cellulose

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Coloring (AREA)

Abstract

The invention provides a kind of alizarin to the colouring method of bafta, the method comprises the following steps:Alizarin is dissolved in dimethyl sulfoxide (DMSO)/phenol mixed solution, surfactant sodium dodecyl base benzene sulfonic acid sodium salt is added, clear solution is obtained under ultrasound;During bafta put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC dyeing.This staining technique need not be modified to alizarin, not use high-temperature dyeing, and fabric color fastness is high after dyeing.

Description

Colouring method of the alizarin to bafta
Technical field
The present invention relates to a kind of textile dyeing technical field, and in particular to a kind of colouring method of alizarin to bafta.
Background technology
Alizarin is a kind of typical mordant dyes.Can be extracted from madder root.Early in before 3500, alizarin just the Central Asia, Egyptian, Europe and China are used as orchil.Alizarin is red acicular crystal, is practically insoluble in water, used as natural plant Thing dyestuff is used to make the red textile of hot flame.Hunting pink is obtained during alizarin aluminium mordant, obtains red during with chromium stain matchmaker Light brown, obtains purple during with iron mordant, gold-tinted is obtained during tin mordanting agent red.But alizarin is to cellulose fibres such as cottons Directly upper dye is poor, and color fastness is poor.
The content of the invention
In order that the effective dyed cotton fabric of alizarin, the present invention is adopted the following technical scheme that.
A kind of alizarin comprises the following steps to the colouring method of bafta:(1)Phenol is dissolved in dimethyl sulfoxide (DMSO);(2) Alizarin is dissolved in dimethyl sulfoxide (DMSO)/phenol mixed solution, surfactant sodium dodecyl base benzene sulfonic acid sodium salt is added, under ultrasound Obtain clear solution;(3)During bafta put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC, 5 ~ 30min of insulation dyeing; (4)Fabric after dyeing is placed in dimethyl sulfoxide (DMSO) and is washed, dried under 80oC.
Further, the dimethyl sulfoxide (DMSO) of described dimethyl sulfoxide (DMSO)/phenol mixed solution and the mass ratio of phenol are 1: 0.1~3。
Further, described surfactant sodium dodecyl base benzene sulfonic acid sodium salt and dimethyl sulfoxide (DMSO)/phenol mixed solution Mass ratio is 1:2000~8000.
Further, described alizarin and the mass ratio of dimethyl sulfoxide (DMSO)/phenol mixed solution are 1:200~4000.
The beneficial effects of the present invention are, it is not necessary to alizarin is modified, high-temperature dyeing is not used, fabric color after dyeing Fastness is high.
Specific embodiment
The present invention is described in detail below in conjunction with specific embodiment.It should be noted that the skill described in following embodiments The combination of art feature or technical characteristic be not construed as it is isolated, they can be mutually combined so as to reach preferably Technique effect.
Embodiment 1
Alizarin is as follows to the colouring method detailed step of bafta:
(1)20g phenol is dissolved in 180g dimethyl sulfoxide (DMSO)s;
(2)0.8g alizarins are dissolved in above-mentioned dimethyl sulfoxide (DMSO)/phenol mixed solution, 0.04g surfactants ten are added Dialkyl benzene sulfonic acids sodium, clear solution is obtained under ultrasound;
(3)During 10g baftas are put into above-mentioned dye liquor, vibration is heated to 60oC, insulation dyeing 30min;
(4)Fabric after dyeing is placed in dimethyl sulfoxide (DMSO) and is washed, dried under 80oC.
Embodiment 2
Alizarin is as follows to the colouring method detailed step of bafta:
(1)300g phenol is dissolved in 100g dimethyl sulfoxide (DMSO)s;
(2)0.1g alizarins are dissolved in above-mentioned dimethyl sulfoxide (DMSO)/phenol mixed solution, 0.08g surfactants ten are added Dialkyl benzene sulfonic acids sodium, clear solution is obtained under ultrasound;
(3)During 10g baftas are put into above-mentioned dye liquor, vibration is heated to 30oC, insulation dyeing 30min;
(4)Fabric after dyeing is placed in dimethyl sulfoxide (DMSO) and is washed, dried under 80oC.
Embodiment 3
Alizarin is as follows to the colouring method detailed step of bafta:
(1)50g phenol is dissolved in 250g dimethyl sulfoxide (DMSO)s;
(2)0.7g alizarins are dissolved in above-mentioned dimethyl sulfoxide (DMSO)/phenol mixed solution, 0.06g surfactants ten are added Dialkyl benzene sulfonic acids sodium, clear solution is obtained under ultrasound;
(3)During 10g baftas are put into above-mentioned dye liquor, vibration is heated to 50oC, insulation dyeing 10min;
(4)Fabric after dyeing is placed in dimethyl sulfoxide (DMSO) and is washed, dried under 80oC.
Embodiment 4
Alizarin is as follows to the colouring method detailed step of bafta:
(1)200g phenol is dissolved in 200g dimethyl sulfoxide (DMSO)s;
(2)1g alizarins are dissolved in above-mentioned dimethyl sulfoxide (DMSO)/phenol mixed solution, 0.01g surfactants 12 are added Sodium alkyl benzene sulfonate, clear solution is obtained under ultrasound;
(3)During 10g baftas are put into above-mentioned dye liquor, vibration is heated to 40oC, insulation dyeing 15min;
(4)Fabric after dyeing is placed in dimethyl sulfoxide (DMSO) and is washed, dried under 80oC.
Although having been presented for some embodiments of the present invention herein, it will be appreciated by those of skill in the art that Without departing from the spirit of the invention, the embodiments herein can be changed.Above-described embodiment be it is exemplary, no Should be using the embodiments herein as the restriction of interest field of the present invention.

Claims (4)

1. colouring method of a kind of alizarin to bafta, it is characterised in that comprise the following steps:
(1)Phenol is dissolved in dimethyl sulfoxide (DMSO);
(2)Alizarin is dissolved in dimethyl sulfoxide (DMSO)/phenol mixed solution, surfactant sodium dodecyl base benzene sulfonic acid is added Sodium, clear solution is obtained under ultrasound;
(3)During bafta put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC, 5 ~ 30min of insulation dyeing;
(4)Fabric after dyeing is placed in dimethyl sulfoxide (DMSO) and is washed, dried under 80oC.
2. alizarin as claimed in claim 1 is to the colouring method of bafta, described dimethyl sulfoxide (DMSO)/phenol mixed solution Dimethyl sulfoxide (DMSO) is 1 with the mass ratio of phenol:0.1~3.
3. alizarin as claimed in claim 1 is to the colouring method of bafta, described surfactant sodium dodecyl base benzene sulfonic acid Sodium is 1 with the mass ratio of dimethyl sulfoxide (DMSO)/phenol mixed solution:2000~8000.
4. to the colouring method of bafta, described alizarin mixes alizarin as claimed in claim 1 with dimethyl sulfoxide (DMSO)/phenol The mass ratio of solution is 1:200~4000.
CN201611089016.XA 2016-12-01 2016-12-01 Colouring method of the alizarin to bafta Pending CN106758338A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611089016.XA CN106758338A (en) 2016-12-01 2016-12-01 Colouring method of the alizarin to bafta

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201611089016.XA CN106758338A (en) 2016-12-01 2016-12-01 Colouring method of the alizarin to bafta

Publications (1)

Publication Number Publication Date
CN106758338A true CN106758338A (en) 2017-05-31

Family

ID=58914132

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201611089016.XA Pending CN106758338A (en) 2016-12-01 2016-12-01 Colouring method of the alizarin to bafta

Country Status (1)

Country Link
CN (1) CN106758338A (en)

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101696553A (en) * 2009-10-30 2010-04-21 五邑大学 Method for dying fabrics by color combination of vegetable dyes
CN103174041A (en) * 2013-04-12 2013-06-26 祝洪哲 Method for low-temperature ultrasonic dyeing and soaping of short fiber by using Chinese herbal medicine plant dye

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101696553A (en) * 2009-10-30 2010-04-21 五邑大学 Method for dying fabrics by color combination of vegetable dyes
CN103174041A (en) * 2013-04-12 2013-06-26 祝洪哲 Method for low-temperature ultrasonic dyeing and soaping of short fiber by using Chinese herbal medicine plant dye

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
何瑾馨: "《染料化学 第2版》", 31 October 2016, 中国纺织出版社 *

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Application publication date: 20170531