CN106758359A - Colouring method of the sulfuretin to silk fabric - Google Patents
Colouring method of the sulfuretin to silk fabric Download PDFInfo
- Publication number
- CN106758359A CN106758359A CN201611089839.2A CN201611089839A CN106758359A CN 106758359 A CN106758359 A CN 106758359A CN 201611089839 A CN201611089839 A CN 201611089839A CN 106758359 A CN106758359 A CN 106758359A
- Authority
- CN
- China
- Prior art keywords
- sulfuretin
- carbon tetrachloride
- silk fabric
- phenol
- dyeing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/62—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds with sulfate, sulfonate, sulfenic or sulfinic groups
- D06P1/621—Compounds without nitrogen
- D06P1/622—Sulfonic acids or their salts
- D06P1/625—Aromatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention provides a kind of sulfuretin to the colouring method of silk fabric, the method comprises the following steps：Sulfuretin is dissolved in carbon tetrachloride/phenol mixed solution, surfactant sodium dodecyl base benzene sulfonic acid sodium salt is added, clear solution is obtained under ultrasound；During silk fabric put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC dyeing.This staining technique need not be modified to sulfuretin, not use high-temperature dyeing, and fabric color fastness is high after dyeing.
Description
Technical field
The present invention relates to a kind of textile dyeing technical field, and in particular to a kind of dyeing of sulfuretin to silk fabric
Method.
Background technology
Sulfuretin be from Anacardiaceae smoke tree belong to timber and Helianthus and dahlia yellow cultivars in extract
A kind of chemical composition.Sulfuretin is a kind of traditional natural dye, under different spectroscopic light source irradiations, aberration can be produced to show
As being to show brilliant redness of the skin or complexion under candle light, in the sun in red shade yellow so that this yellow turns into the special of Chinese emperors
Use the style and colour of clothes.But sulfuretin is to protein fibres such as silks, and directly upper dye is poor, and color fastness is poor.
The content of the invention
In order that sulfuretin effectively dyes silk fabric, the present invention is adopted the following technical scheme that.
A kind of sulfuretin comprises the following steps to the colouring method of silk fabric：（1）Phenol is dissolved in carbon tetrachloride
In；（2）Sulfuretin is dissolved in carbon tetrachloride/phenol mixed solution, surfactant sodium dodecyl base benzene sulfonic acid is added
Sodium, clear solution is obtained under ultrasound；（3）During silk fabric put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC, insulation dye
5 ~ 30min of color；（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Further, the carbon tetrachloride of described carbon tetrachloride/phenol mixed solution and the mass ratio of phenol are 1:0.1~
3。
Further, described surfactant sodium dodecyl base benzene sulfonic acid sodium salt and the matter of carbon tetrachloride/phenol mixed solution
Amount is than being 1:2000~8000.
Further, described sulfuretin and the mass ratio of carbon tetrachloride/phenol mixed solution are 1:200~4000.
The beneficial effects of the present invention are, it is not necessary to sulfuretin is modified, high-temperature dyeing is not used, knitted after dyeing
Look for fastness high.
Specific embodiment
The present invention is described in detail below in conjunction with specific embodiment.It should be noted that the skill described in following embodiments
The combination of art feature or technical characteristic be not construed as it is isolated, they can be mutually combined so as to reach preferably
Technique effect.
Embodiment 1
Sulfuretin is as follows to the colouring method detailed step of silk fabric：
（1）20g phenol is dissolved in 180g carbon tetrachloride；
（2）0.4g sulfuretins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.04g surfactants are added
Neopelex, clear solution is obtained under ultrasound；
（3）During 10g silk fabrics are put into above-mentioned dye liquor, vibration is heated to 60oC, insulation dyeing 30min；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Embodiment 2
Sulfuretin is as follows to the colouring method detailed step of silk fabric：
（1）300g phenol is dissolved in 100g carbon tetrachloride；
（2）0.1g sulfuretins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.08g surfactants are added
Neopelex, clear solution is obtained under ultrasound；
（3）During 10g silk fabrics are put into above-mentioned dye liquor, vibration is heated to 30oC, insulation dyeing 30min；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Embodiment 3
Sulfuretin is as follows to the colouring method detailed step of silk fabric：
（1）50g phenol is dissolved in 250g carbon tetrachloride；
（2）1g sulfuretins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.06g surfactants ten are added
Dialkyl benzene sulfonic acids sodium, clear solution is obtained under ultrasound；
（3）During 10g silk fabrics are put into above-mentioned dye liquor, vibration is heated to 50oC, insulation dyeing 10min；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Embodiment 4
Sulfuretin is as follows to the colouring method detailed step of silk fabric：
（1）200g phenol is dissolved in 200g carbon tetrachloride；
（2）0.8g sulfuretins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.01g surfactants are added
Neopelex, clear solution is obtained under ultrasound；
（3）During 10g silk fabrics are put into above-mentioned dye liquor, vibration is heated to 40oC, insulation dyeing 15min；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Although having been presented for some embodiments of the present invention herein, it will be appreciated by those of skill in the art that
Without departing from the spirit of the invention, the embodiments herein can be changed.Above-described embodiment be it is exemplary, no
Should be using the embodiments herein as the restriction of interest field of the present invention.
Claims (4)
1. colouring method of a kind of sulfuretin to silk fabric, it is characterised in that comprise the following steps：
（1）Phenol is dissolved in carbon tetrachloride；
（2）Sulfuretin is dissolved in carbon tetrachloride/phenol mixed solution, surfactant sodium dodecyl base benzene sulfonic acid is added
Sodium, clear solution is obtained under ultrasound；
（3）During silk fabric put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC, 5 ~ 30min of insulation dyeing；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
2. sulfuretin as claimed in claim 1 is to the colouring method of silk fabric, and described carbon tetrachloride/phenol mixing is molten
The carbon tetrachloride of liquid is 1 with the mass ratio of phenol:0.1~3.
3. sulfuretin as claimed in claim 1 is to the colouring method of silk fabric, described surfactant sodium dodecyl base
Benzene sulfonic acid sodium salt is 1 with the mass ratio of carbon tetrachloride/phenol mixed solution:2000~8000.
4. sulfuretin as claimed in claim 1 is to the colouring method of silk fabric, and described sulfuretin and carbon tetrachloride/
The mass ratio of phenol mixed solution is 1:200~4000.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611089839.2A CN106758359A (en) | 2016-12-01 | 2016-12-01 | Colouring method of the sulfuretin to silk fabric |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611089839.2A CN106758359A (en) | 2016-12-01 | 2016-12-01 | Colouring method of the sulfuretin to silk fabric |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106758359A true CN106758359A (en) | 2017-05-31 |
Family
ID=58914246
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611089839.2A Pending CN106758359A (en) | 2016-12-01 | 2016-12-01 | Colouring method of the sulfuretin to silk fabric |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106758359A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102093744A (en) * | 2009-12-10 | 2011-06-15 | 中国农业科学院植物保护研究所 | Tithonia diversifolia or guayule natural plant dye and preparation method and application thereof |
| CN102677461A (en) * | 2012-05-06 | 2012-09-19 | 南通市鸿基织造有限公司 | Process for producing underwear fabric |
| CN105062130A (en) * | 2015-08-11 | 2015-11-18 | 浙江理工大学 | Preparation method of wild chrysanthemum natural dye and preparation of anti-bacterial textiles adopting wild chrysanthemum natural dye |
| CN105400232A (en) * | 2015-11-16 | 2016-03-16 | 桐乡蓝印花布厂有限公司 | Preparation method of chrysanthemum vegetable dye |
-
2016
- 2016-12-01 CN CN201611089839.2A patent/CN106758359A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102093744A (en) * | 2009-12-10 | 2011-06-15 | 中国农业科学院植物保护研究所 | Tithonia diversifolia or guayule natural plant dye and preparation method and application thereof |
| CN102677461A (en) * | 2012-05-06 | 2012-09-19 | 南通市鸿基织造有限公司 | Process for producing underwear fabric |
| CN105062130A (en) * | 2015-08-11 | 2015-11-18 | 浙江理工大学 | Preparation method of wild chrysanthemum natural dye and preparation of anti-bacterial textiles adopting wild chrysanthemum natural dye |
| CN105400232A (en) * | 2015-11-16 | 2016-03-16 | 桐乡蓝印花布厂有限公司 | Preparation method of chrysanthemum vegetable dye |
Non-Patent Citations (1)
| Title |
|---|
| 赵丰: "《中国古代物质文化史 纺织下》", 31 January 2014, 开明出版社 * |
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Application publication date: 20170531 |
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