CN106758336A - The method that sulfuretin dyes silk fabric - Google Patents
The method that sulfuretin dyes silk fabric Download PDFInfo
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- CN106758336A CN106758336A CN201611088965.6A CN201611088965A CN106758336A CN 106758336 A CN106758336 A CN 106758336A CN 201611088965 A CN201611088965 A CN 201611088965A CN 106758336 A CN106758336 A CN 106758336A
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- ethanol
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- phenol
- sulfuretin
- silk fabric
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- 239000004744 fabric Substances 0.000 title claims abstract description 28
- 238000000034 method Methods 0.000 title claims abstract description 14
- 239000000975 dye Substances 0.000 title claims description 8
- RGNXWPVNPFAADO-NSIKDUERSA-N sulfuretin Chemical compound O1C2=CC(O)=CC=C2C(=O)\C1=C\C1=CC=C(O)C(O)=C1 RGNXWPVNPFAADO-NSIKDUERSA-N 0.000 title claims 7
- RGNXWPVNPFAADO-UHFFFAOYSA-N sulfuretin Natural products O1C2=CC(O)=CC=C2C(=O)C1=CC1=CC=C(O)C(O)=C1 RGNXWPVNPFAADO-UHFFFAOYSA-N 0.000 title claims 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 53
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims abstract description 21
- 238000004043 dyeing Methods 0.000 claims abstract description 19
- 239000000243 solution Substances 0.000 claims abstract description 15
- 239000011259 mixed solution Substances 0.000 claims abstract description 12
- 239000004094 surface-active agent Substances 0.000 claims abstract description 9
- 238000002604 ultrasonography Methods 0.000 claims description 5
- 238000009413 insulation Methods 0.000 claims 1
- SESFRYSPDFLNCH-UHFFFAOYSA-N benzyl benzoate Chemical compound C=1C=CC=CC=1C(=O)OCC1=CC=CC=C1 SESFRYSPDFLNCH-UHFFFAOYSA-N 0.000 abstract description 14
- 229960002903 benzyl benzoate Drugs 0.000 abstract description 7
- 238000002525 ultrasonication Methods 0.000 abstract 1
- 241000208223 Anacardiaceae Species 0.000 description 1
- 244000115658 Dahlia pinnata Species 0.000 description 1
- 235000012040 Dahlia pinnata Nutrition 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 244000020551 Helianthus annuus Species 0.000 description 1
- 235000003222 Helianthus annuus Nutrition 0.000 description 1
- 241000538804 Lethrinus haematopterus Species 0.000 description 1
- 229930182559 Natural dye Natural products 0.000 description 1
- 240000003152 Rhus chinensis Species 0.000 description 1
- 235000014220 Rhus chinensis Nutrition 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000009967 direct dyeing Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000000978 natural dye Substances 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 230000003595 spectral effect Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/651—Compounds without nitrogen
- D06P1/65106—Oxygen-containing compounds
- D06P1/65125—Compounds containing ester groups
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
本发明提供了一种硫黄菊素染色丝绸织物的方法，该方法包括如下步骤：将硫黄菊素溶解于乙醇/苯酚混合溶液中，再加入表面活性剂苯甲酸苄酯，超声下得到透明溶液；将丝绸织物投入到上述染液中，振荡加热至30~60ºC染色。本染色技术不需要对硫黄菊素进行改性，不采用高温染色，染色后织物色牢度高。The invention provides a method for dyeing silk fabrics with thiomethrin. The method comprises the following steps: dissolving thiomethrin in an ethanol/phenol mixed solution, adding a surfactant benzyl benzoate, and obtaining a transparent solution under ultrasonication; Put the silk fabric into the above dyeing solution, vibrate and heat to 30~60ºC for dyeing. This dyeing technology does not need to modify thiocyanin, does not use high temperature dyeing, and the color fastness of the dyed fabric is high.
Description
技术领域technical field
本发明涉及一种纺织品染色技术领域，具体涉及一种硫黄菊素染色丝绸织物的方法。The invention relates to the technical field of textile dyeing, in particular to a method for dyeing silk fabrics with thiomethrin.
背景技术Background technique
硫黄菊素是从漆树科黄栌属木材和向日葵属及大丽花属黄色变种植物中提取的一种化学成分。硫黄菊素是一种传统的天然染料，在不同的光谱光源照射下，会产生色差现象，在烛光下为显光辉的赤色，在阳光下呈带红光的黄色，使得这种黄色成为中国皇帝的专用服色。但是硫黄菊素对丝绸等蛋白质纤维直接上染较差，且色牢度较差。Thiofantrin is a chemical component extracted from the wood of the genus Sumac and the yellow varietal plants of the genus Sunflower and Dahlia in the family Anacardiaceae. Thiofanthrin is a traditional natural dye. Under different spectral light sources, it will produce chromatic aberration. It is bright red under candlelight, and reddish yellow under sunlight, making this yellow color the color of the Chinese emperor. special clothing color. However, thiamethrin is poor in direct dyeing of protein fibers such as silk, and its color fastness is poor.
发明内容Contents of the invention
为了使硫黄菊素有效染色丝绸织物，本发明采取如下技术方案。In order to make thiamethrin effectively dye silk fabrics, the present invention adopts the following technical solutions.
一种硫黄菊素染色丝绸织物的方法，包括如下步骤：（1）将苯酚溶于乙醇中；（2）将硫黄菊素溶解于乙醇/苯酚混合溶液中，再加入表面活性剂苯甲酸苄酯，超声下得到透明溶液；（3）将丝绸织物投入到上述染液中，振荡加热至30~60ºC，保温染色5~30min；（4）将染色后织物置于乙醇中洗涤，80ºC下烘干。A method for dyeing silk fabrics with thiomethrin, comprising the steps of: (1) dissolving phenol in ethanol; (2) dissolving thiomethrin in a mixed solution of ethanol/phenol, and then adding surfactant benzyl benzoate , to obtain a transparent solution under ultrasonic; (3) put the silk fabric into the above dyeing solution, oscillate and heat to 30~60ºC, keep it warm for 5~30min; (4) wash the dyed fabric in ethanol, and dry it at 80ºC .
进一步的，所述的乙醇/苯酚混合溶液的乙醇与苯酚的质量比为1:0.1~3。Further, the mass ratio of ethanol to phenol in the ethanol/phenol mixed solution is 1:0.1~3.
进一步的，所述的表面活性剂苯甲酸苄酯与乙醇/苯酚混合溶液的质量比为1:2000~8000。Further, the mass ratio of the surfactant benzyl benzoate to the ethanol/phenol mixed solution is 1:2000-8000.
进一步的，所述的硫黄菊素与乙醇/苯酚混合溶液的质量比为1:200~4000。Further, the mass ratio of the thiomethrin to the ethanol/phenol mixed solution is 1:200~4000.
本发明的有益效果在于，不需要对硫黄菊素进行改性，不采用高温染色，染色后织物色牢度高。The invention has the beneficial effects of not needing to modify the thiamethrin, not adopting high-temperature dyeing, and having high color fastness of the dyed fabric.
具体实施方式detailed description
下文将结合具体实施例详细描述本发明。应当注意的是，下述实施例中描述的技术特征或者技术特征的组合不应当被认为是孤立的，它们可以被相互组合从而达到更好的技术效果。The present invention will be described in detail below in conjunction with specific embodiments. It should be noted that the technical features or combinations of technical features described in the following embodiments should not be regarded as isolated, and they can be combined with each other to achieve better technical effects.
实施例1Example 1
硫黄菊素染色丝绸织物的方法详细步骤如下：The detailed steps of the method for dyeing silk fabrics with thiomethrin are as follows:
（1）将20g苯酚溶于180g乙醇中；(1) Dissolve 20g of phenol in 180g of ethanol;
（2）将0.4g硫黄菊素溶解于上述乙醇/苯酚混合溶液中，再加入0.04g表面活性剂苯甲酸苄酯，超声下得到透明溶液；(2) Dissolve 0.4g of thiamethrin in the above ethanol/phenol mixed solution, then add 0.04g of surfactant benzyl benzoate, and obtain a transparent solution under ultrasound;
（3）将10g丝绸织物投入到上述染液中，振荡加热至60ºC，保温染色30min；(3) Put 10g of silk fabric into the above dyeing solution, vibrate and heat to 60ºC, and keep it warm for 30 minutes;
（4）将染色后织物置于乙醇中洗涤，80ºC下烘干。(4) Wash the dyed fabric in ethanol and dry at 80ºC.
实施例2Example 2
硫黄菊素染色丝绸织物的方法详细步骤如下：The detailed steps of the method for dyeing silk fabrics with thiomethrin are as follows:
（1）将300g苯酚溶于100g乙醇中；(1) Dissolve 300g phenol in 100g ethanol;
（2）将0.1g硫黄菊素溶解于上述乙醇/苯酚混合溶液中，再加入0.08g表面活性剂苯甲酸苄酯，超声下得到透明溶液；(2) Dissolve 0.1g of thiamethrin in the above ethanol/phenol mixed solution, then add 0.08g of surfactant benzyl benzoate, and obtain a transparent solution under ultrasound;
（3）将10g丝绸织物投入到上述染液中，振荡加热至30ºC，保温染色30min；(3) Put 10g of silk fabric into the above dyeing solution, vibrate and heat to 30ºC, and keep it warm for 30min;
（4）将染色后织物置于乙醇中洗涤，80ºC下烘干。(4) Wash the dyed fabric in ethanol and dry at 80ºC.
实施例3Example 3
硫黄菊素染色丝绸织物的方法详细步骤如下：The detailed steps of the method for dyeing silk fabrics with thiomethrin are as follows:
（1）将50g苯酚溶于250g乙醇中；(1) Dissolve 50g of phenol in 250g of ethanol;
（2）将1g硫黄菊素溶解于上述乙醇/苯酚混合溶液中，再加入0.06g表面活性剂苯甲酸苄酯，超声下得到透明溶液；(2) Dissolve 1g of thiamethrin in the above ethanol/phenol mixed solution, then add 0.06g of surfactant benzyl benzoate, and obtain a transparent solution under ultrasound;
（3）将10g丝绸织物投入到上述染液中，振荡加热至50ºC，保温染色10min；(3) Put 10g of silk fabric into the above dyeing solution, vibrate and heat to 50ºC, and keep it warm for 10min;
（4）将染色后织物置于乙醇中洗涤，80ºC下烘干。(4) Wash the dyed fabric in ethanol and dry at 80ºC.
实施例4Example 4
硫黄菊素染色丝绸织物的方法详细步骤如下：The detailed steps of the method for dyeing silk fabrics with thiomethrin are as follows:
（1）将200g苯酚溶于200g乙醇中；(1) Dissolve 200g phenol in 200g ethanol;
（2）将0.8g硫黄菊素溶解于上述乙醇/苯酚混合溶液中，再加入0.01g表面活性剂苯甲酸苄酯，超声下得到透明溶液；(2) Dissolve 0.8g of thiamethrin in the above ethanol/phenol mixed solution, then add 0.01g of surfactant benzyl benzoate, and obtain a transparent solution under ultrasound;
（3）将10g丝绸织物投入到上述染液中，振荡加热至40ºC，保温染色15min；(3) Put 10g of silk fabric into the above dye solution, heat it to 40ºC with vibration, and keep it warm for 15 minutes;
（4）将染色后织物置于乙醇中洗涤，80ºC下烘干。(4) Wash the dyed fabric in ethanol and dry at 80ºC.
本文虽然已经给出了本发明的一些实施例，但是本领域的技术人员应当理解，在不脱离本发明精神的情况下，可以对本文的实施例进行改变。上述实施例只是示例性的，不应以本文的实施例作为本发明权利范围的限定。Although some embodiments of the present invention have been given herein, those skilled in the art should understand that the embodiments herein can be changed without departing from the spirit of the present invention. The above-mentioned embodiments are only exemplary, and the embodiments herein should not be used as limitations on the scope of rights of the present invention.
Claims (4)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611088965.6A CN106758336A (en) | 2016-12-01 | 2016-12-01 | The method that sulfuretin dyes silk fabric |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201611088965.6A CN106758336A (en) | 2016-12-01 | 2016-12-01 | The method that sulfuretin dyes silk fabric |
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| CN106758336A true CN106758336A (en) | 2017-05-31 |
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| CN201611088965.6A Pending CN106758336A (en) | 2016-12-01 | 2016-12-01 | The method that sulfuretin dyes silk fabric |
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101148827A (en) * | 2007-09-30 | 2008-03-26 | 无锡汇罗新材料科技有限公司 | Technique for dyeing silk face fabric by vegetable dye |
| CN101696553A (en) * | 2009-10-30 | 2010-04-21 | 五邑大学 | Method for dying fabrics by color combination of vegetable dyes |
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2016
- 2016-12-01 CN CN201611088965.6A patent/CN106758336A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101148827A (en) * | 2007-09-30 | 2008-03-26 | 无锡汇罗新材料科技有限公司 | Technique for dyeing silk face fabric by vegetable dye |
| CN101696553A (en) * | 2009-10-30 | 2010-04-21 | 五邑大学 | Method for dying fabrics by color combination of vegetable dyes |
Non-Patent Citations (3)
| Title |
|---|
| 唐人成等: "《双组分纤维纺织品的染色》", 31 October 2003, 中国纺织出版社 * |
| 宋心远等: "《活性染料染色的理论和实践》", 30 September 1991, 纺织工业出版社 第1版 * |
| 赵丰等著: "《中国古代物质文化史 纺织（下）》", 31 January 2014, 开明出版社 * |
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