CN106758334A - The method of Acetylshikonin dyed cotton fabric - Google Patents
The method of Acetylshikonin dyed cotton fabric Download PDFInfo
- Publication number
- CN106758334A CN106758334A CN201611088961.8A CN201611088961A CN106758334A CN 106758334 A CN106758334 A CN 106758334A CN 201611088961 A CN201611088961 A CN 201611088961A CN 106758334 A CN106758334 A CN 106758334A
- Authority
- CN
- China
- Prior art keywords
- acetylshikonin
- ethanol
- phenol
- dyeing
- cotton fabric
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/651—Compounds without nitrogen
- D06P1/65106—Oxygen-containing compounds
- D06P1/65125—Compounds containing ester groups
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/58—Material containing hydroxyl groups
- D06P3/60—Natural or regenerated cellulose
Abstract
The invention provides a kind of method of Acetylshikonin dyed cotton fabric, the method comprises the following steps：Acetylshikonin is dissolved in ethanol/phenol mixed solution, surfactant Ergol is added, clear solution is obtained under ultrasound；During bafta put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC dyeing.This staining technique need not be modified to Acetylshikonin, not use high-temperature dyeing, and fabric color fastness is high after dyeing.
Description
Technical field
The present invention relates to a kind of textile dyeing technical field, and in particular to a kind of side of Acetylshikonin dyed cotton fabric
Method.
Background technology
Acetylshikonin is primarily present in Asian puccoon root also known as Acetyl-shikonin, is naphthalene Quinone Pigments, aubergine needle-like knot
It is brilliant.The hydrophobicity side switch of Acetylshikonin is long, therefore water-soluble poor, typically can be using the method for first mordant dyeing to cellulose
Fabric is dyeed.Being compatible with the environment property of Acetylshikonin is good, is harmful to human health.But Acetylshikonin is to cotton etc.
Directly upper dye is poor for cellulose fibre, and color fastness is poor.
The content of the invention
In order that the effective dyed cotton fabric of Acetylshikonin, the present invention is adopted the following technical scheme that.
A kind of method of Acetylshikonin dyed cotton fabric, comprises the following steps：（1）Phenol is dissolved in ethanol；（2）Will
Acetylshikonin is dissolved in ethanol/phenol mixed solution, adds surfactant Ergol, obtains transparent under ultrasound
Solution；（3）During bafta put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC, 5 ~ 30min of insulation dyeing；（4）Will dyeing
Fabric is placed in ethanol and washs afterwards, is dried under 80oC.
Further, the ethanol of described ethanol/phenol mixed solution and the mass ratio of phenol are 1:0.1~3.
Further, described surfactant Ergol is 1 with the mass ratio of ethanol/phenol mixed solution:
2000~8000。
Further, described Acetylshikonin and the mass ratio of ethanol/phenol mixed solution are 1:200~4000.
The beneficial effects of the present invention are, it is not necessary to Acetylshikonin is modified, high-temperature dyeing is not used, after dyeing
Fabric color fastness is high.
Specific embodiment
The present invention is described in detail below in conjunction with specific embodiment.It should be noted that the skill described in following embodiments
The combination of art feature or technical characteristic be not construed as it is isolated, they can be mutually combined so as to reach preferably
Technique effect.
Embodiment 1
The method detailed step of Acetylshikonin dyed cotton fabric is as follows：
（1）20g phenol is dissolved in 180g ethanol；
（2）1g Acetylshikonins are dissolved in above-mentioned ethanol/phenol mixed solution, 0.04g surfactant benzene first is added
Acid benzyl ester, clear solution is obtained under ultrasound；
（3）During 10g baftas are put into above-mentioned dye liquor, vibration is heated to 60oC, insulation dyeing 30min；
（4）Fabric after dyeing is placed in ethanol and is washed, dried under 80oC.
Embodiment 2
The method detailed step of Acetylshikonin dyed cotton fabric is as follows：
（1）300g phenol is dissolved in 100g ethanol；
（2）0.1g Acetylshikonins are dissolved in above-mentioned ethanol/phenol mixed solution, 0.08g surfactant benzene is added
Benzyl formate, clear solution is obtained under ultrasound；
（3）During 10g baftas are put into above-mentioned dye liquor, vibration is heated to 30oC, insulation dyeing 30min；
（4）Fabric after dyeing is placed in ethanol and is washed, dried under 80oC.
Embodiment 3
The method detailed step of Acetylshikonin dyed cotton fabric is as follows：
（1）50g phenol is dissolved in 250g ethanol；
（2）1g Acetylshikonins are dissolved in above-mentioned ethanol/phenol mixed solution, 0.06g surfactant benzene first is added
Acid benzyl ester, clear solution is obtained under ultrasound；
（3）During 10g baftas are put into above-mentioned dye liquor, vibration is heated to 50oC, insulation dyeing 10min；
（4）Fabric after dyeing is placed in ethanol and is washed, dried under 80oC.
Embodiment 4
The method detailed step of Acetylshikonin dyed cotton fabric is as follows：
（1）200g phenol is dissolved in 200g ethanol；
（2）0.7g Acetylshikonins are dissolved in above-mentioned ethanol/phenol mixed solution, 0.01g surfactant benzene is added
Benzyl formate, clear solution is obtained under ultrasound；
（3）During 10g baftas are put into above-mentioned dye liquor, vibration is heated to 40oC, insulation dyeing 15min；
（4）Fabric after dyeing is placed in ethanol and is washed, dried under 80oC.
Although having been presented for some embodiments of the present invention herein, it will be appreciated by those of skill in the art that
Without departing from the spirit of the invention, the embodiments herein can be changed.Above-described embodiment be it is exemplary, no
Should be using the embodiments herein as the restriction of interest field of the present invention.
Claims (4)
1. a kind of method of Acetylshikonin dyed cotton fabric, it is characterised in that comprise the following steps：
（1）Phenol is dissolved in ethanol；
（2）Acetylshikonin is dissolved in ethanol/phenol mixed solution, surfactant Ergol is added, ultrasound
Under obtain clear solution；
（3）During bafta put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC, 5 ~ 30min of insulation dyeing；
（4）Fabric after dyeing is placed in ethanol and is washed, dried under 80oC.
2. the method for Acetylshikonin dyed cotton fabric as claimed in claim 1, the second of described ethanol/phenol mixed solution
Alcohol is 1 with the mass ratio of phenol:0.1~3.
3. the method for Acetylshikonin dyed cotton fabric as claimed in claim 1, described surfactant Ergol
It is 1 with the mass ratio of ethanol/phenol mixed solution:2000~8000.
4. the method for Acetylshikonin dyed cotton fabric as claimed in claim 1, described Acetylshikonin and ethanol/phenol
The mass ratio of mixed solution is 1:200~4000.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611088961.8A CN106758334A (en) | 2016-12-01 | 2016-12-01 | The method of Acetylshikonin dyed cotton fabric |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611088961.8A CN106758334A (en) | 2016-12-01 | 2016-12-01 | The method of Acetylshikonin dyed cotton fabric |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106758334A true CN106758334A (en) | 2017-05-31 |
Family
ID=58914174
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611088961.8A Pending CN106758334A (en) | 2016-12-01 | 2016-12-01 | The method of Acetylshikonin dyed cotton fabric |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106758334A (en) |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101914305A (en) * | 2010-08-11 | 2010-12-15 | 常州大学 | Extraction of natural gromwell dye and application thereof |
| CN103103822A (en) * | 2012-11-15 | 2013-05-15 | 沈阳洪达信息科技有限公司 | Natural purple cotton fabric |
-
2016
- 2016-12-01 CN CN201611088961.8A patent/CN106758334A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101914305A (en) * | 2010-08-11 | 2010-12-15 | 常州大学 | Extraction of natural gromwell dye and application thereof |
| CN103103822A (en) * | 2012-11-15 | 2013-05-15 | 沈阳洪达信息科技有限公司 | Natural purple cotton fabric |
Non-Patent Citations (1)
| Title |
|---|
| 唐人成等: "《双组分纤维纺织品的染色》", 31 October 2003, 中国纺织出版社 * |
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| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20170531 |
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| WD01 | Invention patent application deemed withdrawn after publication |