CN106758346A - Colouring method of the sorphoranone to bafta - Google Patents

Colouring method of the sorphoranone to bafta Download PDF

Info

Publication number
CN106758346A
CN106758346A CN201611089289.4A CN201611089289A CN106758346A CN 106758346 A CN106758346 A CN 106758346A CN 201611089289 A CN201611089289 A CN 201611089289A CN 106758346 A CN106758346 A CN 106758346A
Authority
CN
China
Prior art keywords
sorphoranone
dmso
dimethyl sulfoxide
bafta
phenol
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201611089289.4A
Other languages
Chinese (zh)
Inventor
卢明
赵振云
周菁
刘萍
刘一萍
李兰倩
樊涛
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Southwest University
Original Assignee
Southwest University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Southwest University filed Critical Southwest University
Priority to CN201611089289.4A priority Critical patent/CN106758346A/en
Publication of CN106758346A publication Critical patent/CN106758346A/en
Pending legal-status Critical Current

Links

Classifications

    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/62—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds with sulfate, sulfonate, sulfenic or sulfinic groups
    • D06P1/621—Compounds without nitrogen
    • D06P1/622—Sulfonic acids or their salts
    • D06P1/625—Aromatic
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
    • D06P3/58—Material containing hydroxyl groups
    • D06P3/60—Natural or regenerated cellulose

Landscapes

  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Coloring (AREA)

Abstract

The invention provides a kind of sorphoranone to the colouring method of bafta, the method comprises the following steps：Sorphoranone is dissolved in dimethyl sulfoxide (DMSO)/phenol mixed solution, surfactant sodium dodecyl base benzene sulfonic acid sodium salt is added, clear solution is obtained under ultrasound；During bafta put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC dyeing.This staining technique need not be modified to sorphoranone, not use high-temperature dyeing, and fabric color fastness is high after dyeing.

Description

Colouring method of the sorphoranone to bafta
Technical field
The present invention relates to a kind of textile dyeing technical field, and in particular to a kind of dyeing side of sorphoranone to bafta Method.
Background technology
Pigment composition in sophora flower is graveoline, also known as sorphoranone.Sorphoranone belongs to flavone derivative.Sorphoranone difficulty is insoluble Yu Shui, be in bright colors, the weld that fastness is excellent, being compatible with the environment property is good, is harmful to human health.But sorphoranone pair Directly upper dye is poor for the cellulose fibres such as cotton, and color fastness is poor.
The content of the invention
In order that the effective dyed cotton fabric of sorphoranone, the present invention is adopted the following technical scheme that.
A kind of sorphoranone comprises the following steps to the colouring method of bafta：（1）Phenol is dissolved in dimethyl sulfoxide (DMSO)； （2）Sorphoranone is dissolved in dimethyl sulfoxide (DMSO)/phenol mixed solution, surfactant sodium dodecyl base benzene sulfonic acid sodium salt is added, Clear solution is obtained under ultrasound；（3）During bafta put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC, and insulation dyeing 5 ~ 30min；（4）Fabric after dyeing is placed in dimethyl sulfoxide (DMSO) and is washed, dried under 80oC.
Further, the dimethyl sulfoxide (DMSO) of described dimethyl sulfoxide (DMSO)/phenol mixed solution and the mass ratio of phenol are 1: 0.1~3。
Further, described surfactant sodium dodecyl base benzene sulfonic acid sodium salt and dimethyl sulfoxide (DMSO)/phenol mixed solution Mass ratio is 1:2000~8000.
Further, described sorphoranone and the mass ratio of dimethyl sulfoxide (DMSO)/phenol mixed solution are 1:200~4000.
The beneficial effects of the present invention are, it is not necessary to sorphoranone is modified, high-temperature dyeing is not used, fabric after dyeing Color fastness is high.
Specific embodiment
The present invention is described in detail below in conjunction with specific embodiment.It should be noted that the skill described in following embodiments The combination of art feature or technical characteristic be not construed as it is isolated, they can be mutually combined so as to reach preferably Technique effect.
Embodiment 1
Sorphoranone is as follows to the colouring method detailed step of bafta：
（1）20g phenol is dissolved in 180g dimethyl sulfoxide (DMSO)s；
（2）1g sorphoranones are dissolved in above-mentioned dimethyl sulfoxide (DMSO)/phenol mixed solution, 0.04g surfactants ten are added Dialkyl benzene sulfonic acids sodium, clear solution is obtained under ultrasound；
（3）During 10g baftas are put into above-mentioned dye liquor, vibration is heated to 60oC, insulation dyeing 30min；
（4）Fabric after dyeing is placed in dimethyl sulfoxide (DMSO) and is washed, dried under 80oC.
Embodiment 2
Sorphoranone is as follows to the colouring method detailed step of bafta：
（1）300g phenol is dissolved in 100g dimethyl sulfoxide (DMSO)s；
（2）0.8g sorphoranones are dissolved in above-mentioned dimethyl sulfoxide (DMSO)/phenol mixed solution, 0.08g surfactants are added Neopelex, clear solution is obtained under ultrasound；
（3）During 10g baftas are put into above-mentioned dye liquor, vibration is heated to 30oC, insulation dyeing 30min；
（4）Fabric after dyeing is placed in dimethyl sulfoxide (DMSO) and is washed, dried under 80oC.
Embodiment 3
Sorphoranone is as follows to the colouring method detailed step of bafta：
（1）50g phenol is dissolved in 250g dimethyl sulfoxide (DMSO)s；
（2）0.1g sorphoranones are dissolved in above-mentioned dimethyl sulfoxide (DMSO)/phenol mixed solution, 0.06g surfactants are added Neopelex, clear solution is obtained under ultrasound；
（3）During 10g baftas are put into above-mentioned dye liquor, vibration is heated to 50oC, insulation dyeing 10min；
（4）Fabric after dyeing is placed in dimethyl sulfoxide (DMSO) and is washed, dried under 80oC.
Embodiment 4
Sorphoranone is as follows to the colouring method detailed step of bafta：
（1）200g phenol is dissolved in 200g dimethyl sulfoxide (DMSO)s；
（2）0.4g sorphoranones are dissolved in above-mentioned dimethyl sulfoxide (DMSO)/phenol mixed solution, 0.01g surfactants are added Neopelex, clear solution is obtained under ultrasound；
（3）During 10g baftas are put into above-mentioned dye liquor, vibration is heated to 40oC, insulation dyeing 15min；
（4）Fabric after dyeing is placed in dimethyl sulfoxide (DMSO) and is washed, dried under 80oC.
Although having been presented for some embodiments of the present invention herein, it will be appreciated by those of skill in the art that Without departing from the spirit of the invention, the embodiments herein can be changed.Above-described embodiment be it is exemplary, no Should be using the embodiments herein as the restriction of interest field of the present invention.

Claims (4)

1. colouring method of a kind of sorphoranone to bafta, it is characterised in that comprise the following steps：
（1）Phenol is dissolved in dimethyl sulfoxide (DMSO)；
（2）Sorphoranone is dissolved in dimethyl sulfoxide (DMSO)/phenol mixed solution, surfactant sodium dodecyl base benzene sulfonic acid is added Sodium, clear solution is obtained under ultrasound；
（3）During bafta put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC, 5 ~ 30min of insulation dyeing；
（4）Fabric after dyeing is placed in dimethyl sulfoxide (DMSO) and is washed, dried under 80oC.
2. sorphoranone as claimed in claim 1 is to the colouring method of bafta, described dimethyl sulfoxide (DMSO)/phenol mixed solution The mass ratio of dimethyl sulfoxide (DMSO) and phenol be 1:0.1~3.
3. sorphoranone as claimed in claim 1 is to the colouring method of bafta, described surfactant sodium dodecyl base benzene sulphur Sour sodium is 1 with the mass ratio of dimethyl sulfoxide (DMSO)/phenol mixed solution:2000~8000.
4. sorphoranone as claimed in claim 1 is to the colouring method of bafta, described sorphoranone and dimethyl sulfoxide (DMSO)/phenol The mass ratio of mixed solution is 1:200~4000.
CN201611089289.4A 2016-12-01 2016-12-01 Colouring method of the sorphoranone to bafta Pending CN106758346A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611089289.4A CN106758346A (en) 2016-12-01 2016-12-01 Colouring method of the sorphoranone to bafta

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201611089289.4A CN106758346A (en) 2016-12-01 2016-12-01 Colouring method of the sorphoranone to bafta

Publications (1)

Publication Number Publication Date
CN106758346A true CN106758346A (en) 2017-05-31

Family

ID=58915373

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201611089289.4A Pending CN106758346A (en) 2016-12-01 2016-12-01 Colouring method of the sorphoranone to bafta

Country Status (1)

Country Link
CN (1) CN106758346A (en)

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1966585A (en) * 2006-11-27 2007-05-23 江南大学 Method of extracting and preparing yellow pigment of pagodatree flower
CN101148826A (en) * 2007-09-30 2008-03-26 无锡汇罗新材料科技有限公司 Technique for dyeing purified cotton yarn by vegetable dye
CN105086508A (en) * 2015-10-08 2015-11-25 嘉兴市欣纺纺织品有限公司 Sophora japonica plant dye extraction method and dyeing method through dye

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1966585A (en) * 2006-11-27 2007-05-23 江南大学 Method of extracting and preparing yellow pigment of pagodatree flower
CN101148826A (en) * 2007-09-30 2008-03-26 无锡汇罗新材料科技有限公司 Technique for dyeing purified cotton yarn by vegetable dye
CN105086508A (en) * 2015-10-08 2015-11-25 嘉兴市欣纺纺织品有限公司 Sophora japonica plant dye extraction method and dyeing method through dye

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
何瑾馨: "《染料化学第2版》", 31 October 2016, 中国纺织出版社 *
刘丽芳: "《中药分析实验与指导第2版》", 30 September 2015, 中国医药科技出版社 *
缑菲菲等: "《槐米染色织物色牢度提升方法的研究》", 《染整技术》 *

Similar Documents

Publication Publication Date Title
CN106758346A (en) Colouring method of the sorphoranone to bafta
CN106758335A (en) Colouring method of the Acetylshikonin to wool fabric
CN106758337A (en) Colouring method of the sorphoranone to silk fabric
CN106758340A (en) Colouring method of the sorphoranone to wool fabric
CN106758333A (en) Colouring method of the shikonin to bafta
CN106758347A (en) Colouring method of the Acetylshikonin to silk fabric
CN106758350A (en) Colouring method of the Acetylshikonin to dacron
CN106758353A (en) Colouring method of the gardenin to wool fabric
CN106758365A (en) Colouring method of the curcumin to bafta
CN106555343A (en) The method of sorphoranone dyeing wool fabric
CN106544893A (en) Colouring method of the sorphoranone to dacron
CN106758356A (en) Colouring method of the alizarin to dacron
CN106702772A (en) Method for dyeing silk fabric with rutin
CN106758349A (en) Colouring method of the sulfuretin to bafta
CN106758344A (en) Colouring method of the shikonin to wool fabric
CN106702768A (en) Method for dyeing silk fabric by using curcumin
CN106758354A (en) The method of shikonin dyed cotton fabric
CN106758359A (en) Colouring method of the sulfuretin to silk fabric
CN106702770A (en) Dyeing method of shikonin on polyester fabric
CN106758363A (en) The method of Acetylshikonin dyeing wool fabric
CN106758341A (en) Colouring method of the safflower red pigment to wool fabric
CN106758357A (en) Colouring method of the sulfuretin to wool fabric
CN106702771A (en) Method for dyeing polyester textile by rutamine
CN106638029A (en) Method for dyeing cotton fabric through acetyl shikonin
CN106758338A (en) Colouring method of the alizarin to bafta

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20170531

WD01 Invention patent application deemed withdrawn after publication