CN106758333A - Colouring method of the shikonin to bafta - Google Patents
Colouring method of the shikonin to bafta Download PDFInfo
- Publication number
- CN106758333A CN106758333A CN201611088956.7A CN201611088956A CN106758333A CN 106758333 A CN106758333 A CN 106758333A CN 201611088956 A CN201611088956 A CN 201611088956A CN 106758333 A CN106758333 A CN 106758333A
- Authority
- CN
- China
- Prior art keywords
- shikonin
- carbon tetrachloride
- bafta
- phenol
- dyeing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/62—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds with sulfate, sulfonate, sulfenic or sulfinic groups
- D06P1/621—Compounds without nitrogen
- D06P1/622—Sulfonic acids or their salts
- D06P1/625—Aromatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/58—Material containing hydroxyl groups
- D06P3/60—Natural or regenerated cellulose
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Coloring (AREA)
Abstract
The invention provides a kind of shikonin to the colouring method of bafta, the method comprises the following steps：Shikonin is dissolved in carbon tetrachloride/phenol mixed solution, surfactant sodium dodecyl base benzene sulfonic acid sodium salt is added, clear solution is obtained under ultrasound；During bafta put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC dyeing.This staining technique need not be modified to shikonin, not use high-temperature dyeing, and fabric color fastness is high after dyeing.
Description
Technical field
The present invention relates to a kind of textile dyeing technical field, and in particular to a kind of dyeing side of shikonin to bafta
Method.
Background technology
Shikonin, is primarily present in Asian puccoon root, is naphthoquinone derivatives, shiny red acicular crystal.The hydrophobicity of shikonin
Side switch is long, therefore water-soluble poor, cellulose base fiber fabric can typically be dyeed using the method for first mordant dyeing.Asian puccoon
Being compatible with the environment property of quinone is good, is harmful to human health.But shikonin is to cellulose fibres such as cottons, and directly upper dye is poor, and color jail
Degree is poor.
The content of the invention
In order that the effective dyed cotton fabric of shikonin, the present invention is adopted the following technical scheme that.
A kind of shikonin comprises the following steps to the colouring method of bafta：（1）Phenol is dissolved in carbon tetrachloride；（2）
Shikonin is dissolved in carbon tetrachloride/phenol mixed solution, surfactant sodium dodecyl base benzene sulfonic acid sodium salt is added, under ultrasound
Obtain clear solution；（3）During bafta put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC, 5 ~ 30min of insulation dyeing；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Further, the carbon tetrachloride of described carbon tetrachloride/phenol mixed solution and the mass ratio of phenol are 1:0.1~
3。
Further, described surfactant sodium dodecyl base benzene sulfonic acid sodium salt and the matter of carbon tetrachloride/phenol mixed solution
Amount is than being 1:2000~8000.
Further, described shikonin and the mass ratio of carbon tetrachloride/phenol mixed solution are 1:200~4000.
The beneficial effects of the present invention are, it is not necessary to shikonin is modified, high-temperature dyeing is not used, fabric after dyeing
Color fastness is high.
Specific embodiment
The present invention is described in detail below in conjunction with specific embodiment.It should be noted that the skill described in following embodiments
The combination of art feature or technical characteristic be not construed as it is isolated, they can be mutually combined so as to reach preferably
Technique effect.
Embodiment 1
Shikonin is as follows to the colouring method detailed step of bafta：
（1）20g phenol is dissolved in 180g carbon tetrachloride；
（2）1g shikonins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.04g surfactants 12 are added
Sodium alkyl benzene sulfonate, clear solution is obtained under ultrasound；
（3）During 10g baftas are put into above-mentioned dye liquor, vibration is heated to 60oC, insulation dyeing 30min；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Embodiment 2
Shikonin is as follows to the colouring method detailed step of bafta：
（1）300g phenol is dissolved in 100g carbon tetrachloride；
（2）0.1g shikonins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.08g surfactants ten are added
Dialkyl benzene sulfonic acids sodium, clear solution is obtained under ultrasound；
（3）During 10g baftas are put into above-mentioned dye liquor, vibration is heated to 30oC, insulation dyeing 30min；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Embodiment 3
Shikonin is as follows to the colouring method detailed step of bafta：
（1）50g phenol is dissolved in 250g carbon tetrachloride；
（2）0.6g shikonins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.06g surfactants ten are added
Dialkyl benzene sulfonic acids sodium, clear solution is obtained under ultrasound；
（3）During 10g baftas are put into above-mentioned dye liquor, vibration is heated to 50oC, insulation dyeing 10min；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Embodiment 4
Shikonin is as follows to the colouring method detailed step of bafta：
（1）200g phenol is dissolved in 200g carbon tetrachloride；
（2）0.8g shikonins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.01g surfactants ten are added
Dialkyl benzene sulfonic acids sodium, clear solution is obtained under ultrasound；
（3）During 10g baftas are put into above-mentioned dye liquor, vibration is heated to 40oC, insulation dyeing 15min；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Although having been presented for some embodiments of the present invention herein, it will be appreciated by those of skill in the art that
Without departing from the spirit of the invention, the embodiments herein can be changed.Above-described embodiment be it is exemplary, no
Should be using the embodiments herein as the restriction of interest field of the present invention.
Claims (4)
1. colouring method of a kind of shikonin to bafta, it is characterised in that comprise the following steps：
（1）Phenol is dissolved in carbon tetrachloride；
（2）Shikonin is dissolved in carbon tetrachloride/phenol mixed solution, surfactant sodium dodecyl base benzene sulfonic acid is added
Sodium, clear solution is obtained under ultrasound；
（3）During bafta put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC, 5 ~ 30min of insulation dyeing；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
2. shikonin as claimed in claim 1 is to the colouring method of bafta, described carbon tetrachloride/phenol mixed solution
Carbon tetrachloride is 1 with the mass ratio of phenol:0.1~3.
3. shikonin as claimed in claim 1 is to the colouring method of bafta, described surfactant sodium dodecyl base benzene sulphur
Sour sodium is 1 with the mass ratio of carbon tetrachloride/phenol mixed solution:2000~8000.
4. to the colouring method of bafta, described shikonin and carbon tetrachloride/phenol are mixed shikonin as claimed in claim 1
The mass ratio for closing solution is 1:200~4000.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611088956.7A CN106758333A (en) | 2016-12-01 | 2016-12-01 | Colouring method of the shikonin to bafta |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611088956.7A CN106758333A (en) | 2016-12-01 | 2016-12-01 | Colouring method of the shikonin to bafta |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106758333A true CN106758333A (en) | 2017-05-31 |
Family
ID=58913311
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611088956.7A Pending CN106758333A (en) | 2016-12-01 | 2016-12-01 | Colouring method of the shikonin to bafta |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106758333A (en) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101148826A (en) * | 2007-09-30 | 2008-03-26 | 无锡汇罗新材料科技有限公司 | Technique for dyeing purified cotton yarn by vegetable dye |
| CN101666044A (en) * | 2008-09-03 | 2010-03-10 | 上海市长宁区少年科技指导站 | Application of alkannin serving as dye |
| CN101914305A (en) * | 2010-08-11 | 2010-12-15 | 常州大学 | Extraction of natural gromwell dye and application thereof |
| CN103103822A (en) * | 2012-11-15 | 2013-05-15 | 沈阳洪达信息科技有限公司 | Natural purple cotton fabric |
| CN104088167A (en) * | 2014-07-04 | 2014-10-08 | 常州大学 | Method for improving color depth and light fastness of natural dye-dyed fabric |
-
2016
- 2016-12-01 CN CN201611088956.7A patent/CN106758333A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101148826A (en) * | 2007-09-30 | 2008-03-26 | 无锡汇罗新材料科技有限公司 | Technique for dyeing purified cotton yarn by vegetable dye |
| CN101666044A (en) * | 2008-09-03 | 2010-03-10 | 上海市长宁区少年科技指导站 | Application of alkannin serving as dye |
| CN101914305A (en) * | 2010-08-11 | 2010-12-15 | 常州大学 | Extraction of natural gromwell dye and application thereof |
| CN103103822A (en) * | 2012-11-15 | 2013-05-15 | 沈阳洪达信息科技有限公司 | Natural purple cotton fabric |
| CN104088167A (en) * | 2014-07-04 | 2014-10-08 | 常州大学 | Method for improving color depth and light fastness of natural dye-dyed fabric |
Non-Patent Citations (1)
| Title |
|---|
| 巩梦婷: "古文献修复中染色配纸的研究", 《中国优秀硕士学位论文全文数据库信息科技辑》 * |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170531 |