CN106758347A - Colouring method of the Acetylshikonin to silk fabric - Google Patents
Colouring method of the Acetylshikonin to silk fabric Download PDFInfo
- Publication number
- CN106758347A CN106758347A CN201611089290.7A CN201611089290A CN106758347A CN 106758347 A CN106758347 A CN 106758347A CN 201611089290 A CN201611089290 A CN 201611089290A CN 106758347 A CN106758347 A CN 106758347A
- Authority
- CN
- China
- Prior art keywords
- acetylshikonin
- carbon tetrachloride
- silk fabric
- phenol
- dyeing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/62—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds with sulfate, sulfonate, sulfenic or sulfinic groups
- D06P1/621—Compounds without nitrogen
- D06P1/622—Sulfonic acids or their salts
- D06P1/625—Aromatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Coloring (AREA)
Abstract
The invention provides a kind of Acetylshikonin to the colouring method of silk fabric, the method comprises the following steps：Acetylshikonin is dissolved in carbon tetrachloride/phenol mixed solution, surfactant sodium dodecyl base benzene sulfonic acid sodium salt is added, clear solution is obtained under ultrasound；During silk fabric put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC dyeing.This staining technique need not be modified to Acetylshikonin, not use high-temperature dyeing, and fabric color fastness is high after dyeing.
Description
Technical field
The present invention relates to a kind of textile dyeing technical field, and in particular to a kind of dye of Acetylshikonin to silk fabric
Color method.
Background technology
Acetylshikonin is primarily present in Asian puccoon root also known as Acetyl-shikonin, is naphthalene Quinone Pigments, aubergine needle-like knot
It is brilliant.The hydrophobicity side switch of Acetylshikonin is long, therefore water-soluble poor, typically can be using the method for first mordant dyeing to cellulose
Fabric is dyeed.Being compatible with the environment property of Acetylshikonin is good, is harmful to human health.But Acetylshikonin is to silk
Deng protein fibre, directly upper dye is poor, and color fastness is poor.
The content of the invention
In order that Acetylshikonin effectively dyes silk fabric, the present invention is adopted the following technical scheme that.
A kind of Acetylshikonin comprises the following steps to the colouring method of silk fabric：（1）Phenol is dissolved in carbon tetrachloride
In；（2）Acetylshikonin is dissolved in carbon tetrachloride/phenol mixed solution, surfactant sodium dodecyl base benzene sulphur is added
Sour sodium, clear solution is obtained under ultrasound；（3）During silk fabric put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC, is incubated
5 ~ 30min of dyeing；（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Further, the carbon tetrachloride of described carbon tetrachloride/phenol mixed solution and the mass ratio of phenol are 1:0.1~
3。
Further, described surfactant sodium dodecyl base benzene sulfonic acid sodium salt and the matter of carbon tetrachloride/phenol mixed solution
Amount is than being 1:2000~8000.
Further, described Acetylshikonin and the mass ratio of carbon tetrachloride/phenol mixed solution are 1:200~4000.
The beneficial effects of the present invention are, it is not necessary to Acetylshikonin is modified, high-temperature dyeing is not used, after dyeing
Fabric color fastness is high.
Specific embodiment
The present invention is described in detail below in conjunction with specific embodiment.It should be noted that the skill described in following embodiments
The combination of art feature or technical characteristic be not construed as it is isolated, they can be mutually combined so as to reach preferably
Technique effect.
Embodiment 1
Acetylshikonin is as follows to the colouring method detailed step of silk fabric：
（1）20g phenol is dissolved in 180g carbon tetrachloride；
（2）1g Acetylshikonins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.04g surfactants are added
Neopelex, clear solution is obtained under ultrasound；
（3）During 10g silk fabrics are put into above-mentioned dye liquor, vibration is heated to 60oC, insulation dyeing 30min；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Embodiment 2
Acetylshikonin is as follows to the colouring method detailed step of silk fabric：
（1）300g phenol is dissolved in 100g carbon tetrachloride；
（2）0.1g Acetylshikonins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.08g surface-actives are added
Agent neopelex, clear solution is obtained under ultrasound；
（3）During 10g silk fabrics are put into above-mentioned dye liquor, vibration is heated to 30oC, insulation dyeing 30min；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Embodiment 3
Acetylshikonin is as follows to the colouring method detailed step of silk fabric：
（1）50g phenol is dissolved in 250g carbon tetrachloride；
（2）1g Acetylshikonins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.06g surfactants are added
Neopelex, clear solution is obtained under ultrasound；
（3）During 10g silk fabrics are put into above-mentioned dye liquor, vibration is heated to 50oC, insulation dyeing 10min；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Embodiment 4
Acetylshikonin is as follows to the colouring method detailed step of silk fabric：
（1）200g phenol is dissolved in 200g carbon tetrachloride；
（2）0.7g Acetylshikonins are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.01g surface-actives are added
Agent neopelex, clear solution is obtained under ultrasound；
（3）During 10g silk fabrics are put into above-mentioned dye liquor, vibration is heated to 40oC, insulation dyeing 15min；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Although having been presented for some embodiments of the present invention herein, it will be appreciated by those of skill in the art that
Without departing from the spirit of the invention, the embodiments herein can be changed.Above-described embodiment be it is exemplary, no
Should be using the embodiments herein as the restriction of interest field of the present invention.
Claims (4)
1. colouring method of a kind of Acetylshikonin to silk fabric, it is characterised in that comprise the following steps：
（1）Phenol is dissolved in carbon tetrachloride；
（2）Acetylshikonin is dissolved in carbon tetrachloride/phenol mixed solution, surfactant sodium dodecyl base benzene sulphur is added
Sour sodium, clear solution is obtained under ultrasound；
（3）During silk fabric put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC, 5 ~ 30min of insulation dyeing；
（4）Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
2. Acetylshikonin as claimed in claim 1 is to the colouring method of silk fabric, described carbon tetrachloride/phenol mixing
The carbon tetrachloride of solution is 1 with the mass ratio of phenol:0.1~3.
3. Acetylshikonin as claimed in claim 1 is to the colouring method of silk fabric, described surfactant sodium dodecyl
Base benzene sulfonic acid sodium salt is 1 with the mass ratio of carbon tetrachloride/phenol mixed solution:2000~8000.
4. Acetylshikonin as claimed in claim 1 is to the colouring method of silk fabric, described Acetylshikonin and tetrachloro
The mass ratio for changing carbon/phenol mixed solution is 1:200~4000.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611089290.7A CN106758347A (en) | 2016-12-01 | 2016-12-01 | Colouring method of the Acetylshikonin to silk fabric |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611089290.7A CN106758347A (en) | 2016-12-01 | 2016-12-01 | Colouring method of the Acetylshikonin to silk fabric |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106758347A true CN106758347A (en) | 2017-05-31 |
Family
ID=58915300
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611089290.7A Pending CN106758347A (en) | 2016-12-01 | 2016-12-01 | Colouring method of the Acetylshikonin to silk fabric |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106758347A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101358383A (en) * | 2008-09-09 | 2009-02-04 | 东华大学 | Alkanna tinctoria drug loading nano fiber, preparation and application thereof |
| CN101666044A (en) * | 2008-09-03 | 2010-03-10 | 上海市长宁区少年科技指导站 | Application of alkannin serving as dye |
| CN105908530A (en) * | 2016-05-18 | 2016-08-31 | 江苏阳光股份有限公司 | One-bath dyeing process for wool Sorna fabric |
| CN105970672A (en) * | 2016-05-18 | 2016-09-28 | 江苏阳光股份有限公司 | Process for dyeing wool-cotton worsted fabric with vegetable dye |
-
2016
- 2016-12-01 CN CN201611089290.7A patent/CN106758347A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101666044A (en) * | 2008-09-03 | 2010-03-10 | 上海市长宁区少年科技指导站 | Application of alkannin serving as dye |
| CN101358383A (en) * | 2008-09-09 | 2009-02-04 | 东华大学 | Alkanna tinctoria drug loading nano fiber, preparation and application thereof |
| CN105908530A (en) * | 2016-05-18 | 2016-08-31 | 江苏阳光股份有限公司 | One-bath dyeing process for wool Sorna fabric |
| CN105970672A (en) * | 2016-05-18 | 2016-09-28 | 江苏阳光股份有限公司 | Process for dyeing wool-cotton worsted fabric with vegetable dye |
Non-Patent Citations (1)
| Title |
|---|
| 何瑾馨: "《染料化学第2版》", 31 October 2016, 中国纺织出版社 * |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
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| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20170531 |