CN106758345A - Colouring method of the safflower red pigment to dacron - Google Patents

Colouring method of the safflower red pigment to dacron Download PDF

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Publication number
CN106758345A
CN106758345A CN201611089032.9A CN201611089032A CN106758345A CN 106758345 A CN106758345 A CN 106758345A CN 201611089032 A CN201611089032 A CN 201611089032A CN 106758345 A CN106758345 A CN 106758345A
Authority
CN
China
Prior art keywords
red pigment
dacron
safflower red
carbon tetrachloride
phenol
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201611089032.9A
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Chinese (zh)
Inventor
卢明
刘萍
刘一萍
李兰倩
樊涛
赵振云
周菁
胡睿敏
蒲青霞
董倩
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Southwest University
Original Assignee
Southwest University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Southwest University filed Critical Southwest University
Priority to CN201611089032.9A priority Critical patent/CN106758345A/en
Publication of CN106758345A publication Critical patent/CN106758345A/en
Pending legal-status Critical Current

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Classifications

    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/34General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/62General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds with sulfate, sulfonate, sulfenic or sulfinic groups
    • D06P1/621Compounds without nitrogen
    • D06P1/622Sulfonic acids or their salts
    • D06P1/625Aromatic
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P3/00Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
    • D06P3/34Material containing ester groups
    • D06P3/52Polyesters

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Coloring (AREA)

Abstract

The invention provides a kind of safflower red pigment to the colouring method of dacron, the method comprises the following steps:Safflower red pigment is dissolved in carbon tetrachloride/phenol mixed solution, surfactant sodium dodecyl base benzene sulfonic acid sodium salt is added, clear solution is obtained under ultrasound;During dacron put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC dyeing.This staining technique need not be modified to safflower red pigment, not use high-temperature dyeing, and fabric color fastness is high after dyeing.

Description

Colouring method of the safflower red pigment to dacron
Technical field
The present invention relates to a kind of textile dyeing technical field, and in particular to a kind of dye of safflower red pigment to dacron Color method.
Background technology
Safflower red pigment be the petal with safflower as raw material, the natural pigment for extracting, kermesinus has to russet The crystallization of gloss or crystalline powder, it is water insoluble, can be used for food industry, cosmetics industry(Such as lipstick), dyestuff.Safflower is red The Tang Dynasty is just widely used pigment in ancient times.But safflower red pigment is difficult the directly synthetic fibers such as upper dye terylene.
The content of the invention
In order that the effective dyed polyester textiles of safflower red pigment, the present invention is adopted the following technical scheme that.
A kind of safflower red pigment comprises the following steps to the colouring method of dacron:(1)Phenol is dissolved in carbon tetrachloride In;(2)Safflower red pigment is dissolved in carbon tetrachloride/phenol mixed solution, surfactant sodium dodecyl base benzene sulphur is added Sour sodium, clear solution is obtained under ultrasound;(3)During dacron put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC, is incubated 5 ~ 30min of dyeing;(4)Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Further, the carbon tetrachloride of described carbon tetrachloride/phenol mixed solution and the mass ratio of phenol are 1:0.1~ 3。
Further, described surfactant sodium dodecyl base benzene sulfonic acid sodium salt and the matter of carbon tetrachloride/phenol mixed solution Amount is than being 1:2000~8000.
Further, described safflower red pigment and the mass ratio of carbon tetrachloride/phenol mixed solution are 1:200~4000.
The beneficial effects of the present invention are, it is not necessary to safflower red pigment is modified, high-temperature dyeing is not used, after dyeing Fabric color fastness is high.
Specific embodiment
The present invention is described in detail below in conjunction with specific embodiment.It should be noted that the skill described in following embodiments The combination of art feature or technical characteristic be not construed as it is isolated, they can be mutually combined so as to reach preferably Technique effect.
Embodiment 1
Safflower red pigment is as follows to the colouring method detailed step of dacron:
(1)20g phenol is dissolved in 180g carbon tetrachloride;
(2)1g safflower red pigments are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.04g surfactants are added Neopelex, clear solution is obtained under ultrasound;
(3)During 10g dacrons are put into above-mentioned dye liquor, vibration is heated to 60oC, insulation dyeing 30min;
(4)Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Embodiment 2
Safflower red pigment is as follows to the colouring method detailed step of dacron:
(1)300g phenol is dissolved in 100g carbon tetrachloride;
(2)0.1g safflower red pigments are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.08g surface-actives are added Agent neopelex, clear solution is obtained under ultrasound;
(3)During 10g dacrons are put into above-mentioned dye liquor, vibration is heated to 30oC, insulation dyeing 30min;
(4)Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Embodiment 3
Safflower red pigment is as follows to the colouring method detailed step of dacron:
(1)50g phenol is dissolved in 250g carbon tetrachloride;
(2)0.4g safflower red pigments are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.06g surface-actives are added Agent neopelex, clear solution is obtained under ultrasound;
(3)During 10g dacrons are put into above-mentioned dye liquor, vibration is heated to 50oC, insulation dyeing 10min;
(4)Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Embodiment 4
Safflower red pigment is as follows to the colouring method detailed step of dacron:
(1)200g phenol is dissolved in 200g carbon tetrachloride;
(2)0.9g safflower red pigments are dissolved in above-mentioned carbon tetrachloride/phenol mixed solution, 0.01g surface-actives are added Agent neopelex, clear solution is obtained under ultrasound;
(3)During 10g dacrons are put into above-mentioned dye liquor, vibration is heated to 40oC, insulation dyeing 15min;
(4)Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
Although having been presented for some embodiments of the present invention herein, it will be appreciated by those of skill in the art that Without departing from the spirit of the invention, the embodiments herein can be changed.Above-described embodiment be it is exemplary, no Should be using the embodiments herein as the restriction of interest field of the present invention.

Claims (4)

1. colouring method of a kind of safflower red pigment to dacron, it is characterised in that comprise the following steps:
(1)Phenol is dissolved in carbon tetrachloride;
(2)Safflower red pigment is dissolved in carbon tetrachloride/phenol mixed solution, surfactant sodium dodecyl base benzene sulphur is added Sour sodium, clear solution is obtained under ultrasound;
(3)During dacron put into above-mentioned dye liquor, vibration is heated to 30 ~ 60oC, 5 ~ 30min of insulation dyeing;
(4)Fabric after dyeing is placed in carbon tetrachloride and is washed, dried under 80oC.
2. safflower red pigment as claimed in claim 1 is to the colouring method of dacron, described carbon tetrachloride/phenol mixing The carbon tetrachloride of solution is 1 with the mass ratio of phenol:0.1~3.
3. safflower red pigment as claimed in claim 1 is to the colouring method of dacron, described surfactant sodium dodecyl Base benzene sulfonic acid sodium salt is 1 with the mass ratio of carbon tetrachloride/phenol mixed solution:2000~8000.
4. safflower red pigment as claimed in claim 1 is to the colouring method of dacron, described safflower red pigment and tetrachloro The mass ratio for changing carbon/phenol mixed solution is 1:200~4000.
CN201611089032.9A 2016-12-01 2016-12-01 Colouring method of the safflower red pigment to dacron Pending CN106758345A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611089032.9A CN106758345A (en) 2016-12-01 2016-12-01 Colouring method of the safflower red pigment to dacron

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201611089032.9A CN106758345A (en) 2016-12-01 2016-12-01 Colouring method of the safflower red pigment to dacron

Publications (1)

Publication Number Publication Date
CN106758345A true CN106758345A (en) 2017-05-31

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201611089032.9A Pending CN106758345A (en) 2016-12-01 2016-12-01 Colouring method of the safflower red pigment to dacron

Country Status (1)

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CN (1) CN106758345A (en)

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101696553A (en) * 2009-10-30 2010-04-21 五邑大学 Method for dying fabrics by color combination of vegetable dyes
CN102061632A (en) * 2010-11-19 2011-05-18 南京工业大学 Dyeing process of natural organic dye extracted from safflowers
CN102295839A (en) * 2011-06-29 2011-12-28 新疆奥斯曼生物资源有限公司 Preparation method of carhamus tincwrius L. haematochrome

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101696553A (en) * 2009-10-30 2010-04-21 五邑大学 Method for dying fabrics by color combination of vegetable dyes
CN102061632A (en) * 2010-11-19 2011-05-18 南京工业大学 Dyeing process of natural organic dye extracted from safflowers
CN102295839A (en) * 2011-06-29 2011-12-28 新疆奥斯曼生物资源有限公司 Preparation method of carhamus tincwrius L. haematochrome

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
何瑾馨: "《染料化学第2版》", 31 October 2016, 中国纺织出版社 *
刘正超: "《染化药剂(下册)》", 30 June 1980, 纺织工业出版社 *
陈英等: "《染整工艺试验教程 第2版》", 31 March 2016, 中国纺织出版社 *

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Application publication date: 20170531