CN105256604A - Method for dyeing textile by using traditional Chinese medicine - Google Patents
Method for dyeing textile by using traditional Chinese medicine Download PDFInfo
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- CN105256604A CN105256604A CN201510516345.7A CN201510516345A CN105256604A CN 105256604 A CN105256604 A CN 105256604A CN 201510516345 A CN201510516345 A CN 201510516345A CN 105256604 A CN105256604 A CN 105256604A
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Abstract
The invention provides a method for dyeing a textile by using a traditional Chinese medicine. The method comprises the following steps: a, preparation of dye liquor: a step of taking the traditional Chinese medicine and treating the traditional Chinese medicine so as to obtain the dye liquor; b, pretreatment of a fabric: a step of adding sodium bicarbonate into warm water, carrying out uniform mixing, adding the fabric for soaking and then washing the fabric with water so as to obtain a to-be-dyed fabric; c, dyeing: a step of soaking the to-be-dyed fabric obtained in the step b in to the dye liquor prepared in the step a, carrying out heating to 80 to 95 DEG C, maintaining the temperature for 10 to 25 min, then carrying out cooling for 0 to 10 min, taking out the fabric, putting the fabric into the dye liquor as the temperature of the dye liquor decreases to 35 to 60 DEG C, heating the dye liquor to 80 to 95 DEG C and maintaining the temperature for 10 min; d, taking-out of the fabric: a step of taking out the fabric as the dye liquor is cooled to a temperature no less than 50 DEG C; and e, cleaning and drying so as to obtain the fabric dyed with the traditional Chinese medicine. The method for dyeing the textile by using the traditional Chinese medicine is simple, enables the dyed textile to have stable quality, has low cost, is widely applicable to dyeing plants and animals or mineral dyeing and has wide market prospects.
Description
Technical field
The invention belongs to textile dyeing field, be specifically related to one " Chinese medicine dye " method.
Background technology
Current, the textile dyeing overwhelming majority uses chemical synthetic dye, though easy to use, also produces serious seondary effect to human health and ecological environment.Research shows, has kind more than 100 to commonly use chemical synthetic dye and likely produces carcinogen, and the textiles of 20 number of chemical synthetic dyestuffs dyeing has skin stimulates generation irritated, and chemical synthetic dye also produces a large amount of pollution to environment in process of production.Enhancing along with mankind's environmental consciousness and the attention to own health, people invest healthy free of contamination natural dye sight again.
Natural dye generally derives from plant, animal and mineral matter, based on vegetable colour.Vegetable colour extracts from the root of plant, stem, leaf and fruit, as: indigo, madder, Asian puccoon, safflower, mulberry, tea etc.; Animal dye number is less, mainly takes from shellfish and kermes polypide, as: worm (purple) glue, alkermes, kermes etc.; Mineral dye is the colored inorganic material extracted from mineral, as chrome yellow, ultramarine, manganese brown etc.It is found that the pigment of the microorganism generations such as bacterium, fungi, mould also can be used as the source of natural dye in recent years.
It is the colouring method of Chinese tradition that vegetable colour dyes to textiles, and health environment-friendly, uses with a long history.Also pertinent literature is had to report the colouring method of vegetable colour at present, as: relaxation (relaxation etc., the application of domestic and international natural plant dye and current situation, hosiery industry, 2009,53:P75-78) report pigment classification, dye class and the color of natural plant dye; Extract the method for natural dye; The colouring method of natural dye.
The method of the extraction natural dye of report comprises traditional aqueous extraction method, alcohol dipping method, supercritical ultrasonics technology, adds dispersant method and freeze-drying.Wherein, traditional water-boiling method plant is contaminated material to pulverize, soak, boil, filter, and obtains dye liquor.It is that the dye material of pulverizing is put into closed container that alcohol dipping method is extracted, and adds 95% ethanolic solution and floods and poured out by solution for some hours; Pour the ethanol of same concentrations again into, again flood; So repeatedly twice, finally all solution is mixed, filter, both can be used as dye liquor.Supercritical ultrasonics technology is processed in supersonic generator dye material and water, and elimination residue after cooling, filtrate concentrate drying, obtains dye liquor.Adding dispersant method is joined in traditional dye liquor by dispersant, and make the original dyestuff that solubility is lower in water form comparatively stable dispersion, dye granule is dispersed.Freeze-drying is Vacuum Freezing & Drying Technology, belongs to lyophilization, is freezed in advance by water-containing materials, then makes it a kind of method distilled under vacuum conditions.
The colouring method of the natural dye of report comprises direct staining method, reduction vatting and mordant dyeing etc.Wherein, (1) direct staining method: utilize the pigment of Activities of Some Plants dyestuff good to the solubility of water, dye liquor directly can be adsorbed onto fiber, dyeing flow process is preparation dye liquor → dyeing → washing, drying → soap, wash, drying.For different plants, there is requirement at links such as dyeing temperature, dyeing times, even pH value, such as: the dyeing temperature of tea is 90 DEG C, dyeing time 45min, pH value 4; Rheum officinale dyeing temperature is 80 DEG C, dyeing time 45min, pH value 7; Madder dyeing temperature is more than 80 DEG C, dyeing time 30min, pH value 9; Asian puccoon dyeing temperature is 40-60 DEG C, dyeing time 40min, pH value 3-4; For different plants, the conditional parameter of selection has larger difference.(2) reduction vatting: there is natural colouring matter compound in plant, and in dyeing course, finally form water-fast pigment, as bluegrass.First former dyestuff is reduced before dyeing, contaminate fabric and adopt air oxidation again, make its oxidative color-developing, again become water-fast reducing dye, anchor on fabric.(3) mordant dyeing: some natural plant pigment has good dissolubility to water, in dye liquor, pigment can directly be bonded on fabric, but dyefastness is poor.For improving its dyefastness, usually using mordant and pigment complex coordination to form water-fast compound, anchoring on fiber with this.After mordant dyeing comprises again first mordant dyeing after stain, mordant dyeing after first dyeing, with method such as bath mordant dyeing etc.But, mordant add the dye-uptake and dyefastness that can improve cloth, but introduce new chemical contamination.(4) comprising other decoration method in addition, as utilized the principle of the natural colouring matter in vegetable colour to acid, alkaline different solubility to process fiber, making it set dyeing on fiber, as safflower, root tuber of aromatic turmeric etc.
The document is also pointed out, because the alternative color variety of natural plant dye is less, chromatogram is incomplete; And most plants dyestuff exists the problem of dyefastness difference, even if adopt multiple mordant to be also difficult to address this problem, especially light fastness and soaping fastness, and also traditional mordant great majority are containing heavy metal ion, and what have is put into forbidding list.Traditional natural plant dye dye-uptake is low, and dyeing time is long, has a strong impact on the problems such as the quality of cloth and also limit application in the industrial production.
Summary of the invention
In order to solve the problems of the technologies described above, the object of the present invention is to provide a kind of raising natural dye dye-uptake, high, the not easy to fade natural dye dying method of dyefastness.
The raw material of natural dye of the present invention comes from Chinese medicine (Chineseherbology, TraditionalMateriaMedica), namely tcm theory instruct under for preventing, diagnosing, treat or regulate the medicine of function of human body.The Chinese medicine that natural dye of the present invention is used, comprises autonomic drug, animal drugs, mineral drug; Dry product or fresh goods is included in autonomic drug.The dyes extracted in Chinese medicine technical process is on the textile also called " Chinese medicine dye " by the present invention.
One of the present invention " Chinese medicine dye " method, it comprises the steps:
A, prepare dye liquor: get Chinese medicine, process obtains dye liquor;
B, cloth pre-treatment: in warm water, add sodium bicarbonate, mixing; Add cloth, soak, then with water cleaning, material of dying cloth must be waited;
C, to dye cloth:
The material of dying cloth waited getting step b immerses in dye liquor described in step a, is warming up to 80-95 DEG C, keeps 10-25 minute; Cooling 0-10 minute, takes out cloth;
Treat that dye liquor is cooled to 35-60 DEG C, again put into cloth, be warming up to 80-95 DEG C, keep 10 minutes;
D, be cooled to when being not less than 50 DEG C take out cloth;
E, cleaning, dry, obtain " Chinese medicine dye " cloth.
Wherein, in step a, described dye liquor by Chinese medicine boiling, filtration preparation, also can be prepared by the following method:
1) get Chinese medicine dry product, pulverize, add water, be warming up to 80-95 DEG C, keep 20 minutes;
2) be cooled to 60 DEG C, add water; Be warming up to 80-95 DEG C again, keep 10 minutes;
3) be cooled to 60 DEG C, add water; Be warming up to 80-95 DEG C again, keep 6 minutes;
4) the elimination dregs of a decoction, obtain dye liquor;
Preferably, get Chinese medicine 1.5 parts, add water for 3 times and be respectively 400 parts, 50 parts, 50 parts; The temperature added water is 4-20 DEG C;
Described Chinese medicine is plant, animal drugs dry product or mineral drug.
Wherein, in step a, the preparation method of described dye liquor is:
Get Chinese medicine, making beating, soaks, and filters; Filtrate decocts, and obtains dye liquor;
Preferably, get Chinese medicine 1 part, making beating, adds 8 parts of water soakings 3 days, filters; Filtrate decocts 30 minutes, obtains dye liquor;
Described Chinese medicine is plant, animal drugs fresh goods.
Wherein, in step b, described cloth is silkworm real silk, spinning cotton or silk flosssilk wadding cloth.
Wherein, in step b, described warm water is the water of 20-40 DEG C.
Wherein, in step c, described in the process of dying cloth, add cold water 1-3 time before being warming up to 80-95 DEG C; A water can be added for silkworm real silk; 2-3 water can be added for spinning cotton or silk flosssilk wadding cloth; Described cold water to be temperature the be water of 4-20 DEG C, the object at every turn adding cold water makes high temperature abrupt temperature drop, to reach fixation object.
Wherein, after steps d, also comprise fixation step.
Wherein, the method for described fixation is:
With grape wine in dye liquor after taking out cloth, stir and evenly mix, put into cloth, sealing 3-5 hour; And/or the cloth taken out be immersed in containing salt 20-30g/L the aqueous solution in 3-10 minute.
Wherein, in step e, described drying for directly to dry or when cloth moisture is 50-90%, 130-250 DEG C of baking 1-5 minute.
Wherein, described Chinese medicine is barberry, Yellow Fructus Gardeniae, safflower, bush, the sophora bud, Chinese gall, bush and/or ochre.
The present invention's " Chinese medicine dye " technique is simple, constant product quality, cost is low, be widely used in dyeing plant, animal or mineral dyeing, such as barberry, Yellow Fructus Gardeniae, Flos Carthami, ochre etc., abundant raw material source, good with the compatibility of environment, biodegradable, simultaneously due to during the active component existed in Chinese medicine is attached to and dyes cloth, effect that Chinese medicine is intrinsic can be played, as barberry has effect of heat-clearing, dampness removing, the loose stasis of blood, Yellow Fructus Gardeniae has effect of heat-clearing, purging intense heat, cool blood, and Flos Carthami has effect of activating blood to promote menstruation, stasis-dispelling and pain-killing.
The present invention's " Chinese medicine dye ", except routine dye silkworm real silk, is also applicable to the textiles that other is dissimilar, as spinning cotton, silk flosssilk wadding cloth etc.; The inventive method colour tone nature, color fastness are high, good light stability, and stuff coloring evenly, is not faded; In the present invention's " Chinese medicine dye " process, in conjunction with knot dyeing, textiles multiple patterns and color change can also be given, make Color have very strong aesthetic; In addition, the present invention does not need to add mordant, just can reach outstanding Color by means of only specific technological process and parameter, and environment friendly and pollution-free, consumer can use safely; The inventive method is applicable to large-scale industrial production, has very wide market prospects.
Obviously, according to foregoing of the present invention, according to ordinary technical knowledge and the customary means of this area, not departing under the present invention's above-mentioned basic fundamental thought prerequisite, the amendment of other various ways, replacement or change can also be made.
The detailed description of the invention of form by the following examples, is described in further detail foregoing of the present invention again.But this should be interpreted as that the scope of the above-mentioned theme of the present invention is only limitted to following example.All technology realized based on foregoing of the present invention all belong to scope of the present invention.
Accompanying drawing explanation
Fig. 1 is the fresh chromosome of barberry;
Fig. 2 is that barberry soaks figure;
Fig. 3 is the barberry dye liquor figure prepared;
Fig. 4 is unseasoned silkworm real silk cloth figure after barberry dyeing;
Fig. 5 is the silkworm real silk cloth finished figure after barberry dyeing;
Fig. 6 is Yellow Fructus Gardeniae powder figure;
Fig. 7 is the silkworm real silk cloth figure in Yellow Fructus Gardeniae dyeing course;
Fig. 8 is that silkworm real silk cloth is adding sealed picture in Yellow Fructus Gardeniae dye liquor vinous;
Fig. 9 is unseasoned silkworm real silk cloth figure after Yellow Fructus Gardeniae dyeing;
Figure 10 is the silkworm real silk cloth finished figure after Yellow Fructus Gardeniae dyeing;
Figure 11 is the silkworm real silk cloth finished figure after ochre dyeing;
Figure 12 is the silkworm real silk cloth finished figure after ochre dyeing;
Figure 13 has cleaned undyed spinning cotton cloth figure;
Figure 14 is the spinning cotton cloth finished figure after Yellow Fructus Gardeniae dyeing;
Figure 15 is the silk floss cloth cloth finished figure after barberry dyeing.
Detailed description of the invention
Be described further with embodiment below, but the present invention is not limited to these embodiments.
The present invention's experiment material used is as follows:
Stainless-steel pan, glass, vial, measurement instrument, thermometer, measuring cup, electronic platform balance, measuring spoon, mortar, pulverizer, plastic bag, plastic glove, long bamboo chopsticks, slip through the net, filter cloth, electric oven, electric iron, permanent hair styling plate; Sodium bicarbonate(edible), edible salt, grape wine.
Embodiment 1 〝 Chinese medicine dye of the present invention 〞 method
〝 Chinese medicine of the present invention dye 〞 method may be used for the dyeing of silkworm real silk cloth, Chinese medicine used with barberry (having another name called copper acupuncture, soulie barberry bark) fresh goods for example.
One, colouring method:
1, prepare dye liquor: root (see Fig. 1) 500g getting barberry fresh goods, making beating, adds 4000mL water, soaks three days (see Fig. 2); Then use the filter cloth elimination dregs of a decoction, liquid stainless-steel pan is boiled 30 minutes, obtain dye liquor (see Fig. 3);
2, cloth preliminary treatment: with the water of 30 DEG C, puts after 10g sodium bicarbonate(edible) stirs evenly, adds the white silkworm real silk cloth of fabric width 2 meters, length 5 meters, to soak after 30 minutes with water cleaning, must wait material of dying cloth;
3, get material of waiting to dye cloth and evenly put into dye liquor, keep 25 minutes at 80-95 DEG C, cloth is taken out;
Treat that dye liquor temperature is reduced to 35 DEG C, again cloth is put into pot, keep 10 minutes at 80-95 DEG C, take out cloth;
4, when dye liquor temperature is reduced to 50 DEG C, in dye liquor, pour 5g grape wine into, after stirring evenly, again put into cloth, will the dye liquor plastic bag sealing 3-5 hour of cloth be put into, take out cloth;
5, cloth to be immersed in the aqueous solution containing salt 30g/L 5 minutes, then to remove cloth loose colour (see Fig. 4) with water cleaning;
6, dry in the air cloth, when cloth moisture is 50%, toasts 1 minute with electric heater, obtains " Chinese medicine dye " cloth.
Two, Color evaluation
Cloth finished product (see Fig. 5) after dyeing, can smell light Chinese medicine fragrance, can taste slight bitter taste.Cloth after dyeing is carried out soaping, Ultraviolet radiation test.
Result shows, the cloth after dyeing is through alkaline soap washing, Ultraviolet radiation color fast after 24 hours, colour-fast.
Embodiment 2 〝 Chinese medicine dye of the present invention 〞 method
〝 Chinese medicine dye 〞 method of the present invention may be used for the dyeing of silkworm real silk cloth, and Chinese medicine used is for Yellow Fructus Gardeniae dry product.
One, colouring method
1, dye liquor is prepared: get Yellow Fructus Gardeniae dry fruit, be ground into powder; Be filled with water with stainless-steel pan, get 15g Yellow Fructus Gardeniae powder (see Fig. 6) and pour in pot, add 4000mL water, after powder and water being stirred evenly with long bamboo chopsticks, keep 20 minutes at 80-95 DEG C; When temperature is reduced to 60 DEG C, add the water 500mL of 4-20 DEG C, keep 10 minutes at 80-95 DEG C; When temperature drops to 60 DEG C again, add the water 500mL of 4-20 DEG C, keep 6 minutes at 80-95 DEG C; With the filter screen elimination dregs of a decoction, obtain dye liquor;
2, cloth preliminary treatment: with the water of 30 DEG C, puts after 10g sodium bicarbonate(edible) stirs evenly, adds the white silkworm real silk cloth of fabric width 2 meters, length 5 meters, to soak after 30 minutes with water cleaning, must wait material of dying cloth;
3, material of waiting to dye cloth evenly puts into dye liquor, keeps after 10 minutes at 80-95 DEG C; Build after lid cools 10 minutes naturally, cloth is taken out and spreads out;
Treat that dye liquor temperature is reduced to 60 DEG C, again cloth is put into pot, add the water 500mL of 4-20 DEG C, at 80-95 DEG C, keep 10 minutes (see Fig. 7); When dye liquor temperature is reduced to 50 DEG C, take out cloth;
4, after cloth takes out, in dye liquor, pour 5g grape wine into, after stirring evenly, again put into cloth, will dye liquor plastic bag sealing 3-5 hour (see Fig. 8) of cloth be put into, take out cloth;
5, cloth to be immersed in the aqueous solution containing salt 20g/L 5 minutes, then to remove cloth loose colour (see Fig. 9) with water cleaning, dry, obtain " Chinese medicine dye " cloth.
Two, Color evaluation
Cloth finished product (see Figure 10) after dyeing, is undertaken soaping by the cloth after dyeing, Ultraviolet radiation test.
Result shows, the cloth after dyeing is through alkaline soap washing, Ultraviolet radiation color fast after 24 hours, colour-fast.
Embodiment 3 〝 Chinese medicine dye of the present invention 〞 method
〝 Chinese medicine dye 〞 method of the present invention may be used for the dyeing of silkworm real silk cloth, and Chinese medicine used is for ochre.
One, colouring method
1, dye liquor is prepared: get ochre block, be ground into powder; Be filled with water with stainless-steel pan, get ochre powder 15g and pour in pot, add 4000mL water, after powder and water being stirred evenly with long bamboo chopsticks, keep 20 minutes at 80-95 DEG C; When temperature is reduced to 60 DEG C, add the water 500mL of 4-20 DEG C, keep 10 minutes at 80-95 DEG C; When temperature drops to 60 DEG C again, add the water 500mL of 4-20 DEG C, keep 6 minutes at 80-95 DEG C; With the filter screen elimination dregs of a decoction, obtain dye liquor;
2, cloth preliminary treatment: with the water of 30 DEG C, puts after 10g sodium bicarbonate(edible) stirs evenly, adds the white silkworm real silk cloth of fabric width 2 meters, length 5 meters, to soak after 30 minutes with water cleaning, must wait material of dying cloth;
3, material of waiting to dye cloth evenly puts into dye liquor, keeps 10 minutes at 80-95 DEG C; Build after lid cools 10 minutes naturally, take out cloth and spread out;
Treat that dye liquor temperature is reduced to 60 DEG C, again cloth is put into pot, keep 10 minutes at 80-95 DEG C; When dye liquor temperature is reduced to 50 DEG C, take out cloth;
4, remove cloth loose colour with water cleaning, dry.
Two, Color evaluation
Cloth finished product (see Figure 11, Figure 12) after dyeing, is undertaken soaping by the cloth after dyeing, Ultraviolet radiation test.
Result shows, the cloth after dyeing is through alkaline soap washing, Ultraviolet radiation color fast after 24 hours, colour-fast.
The method that embodiment 4 Flos Carthami is dyed cloth
〝 Chinese medicine dye 〞 method of the present invention may be used for the dyeing of spinning cotton, and Chinese medicine used is for Flos Carthami dry product.
One, colouring method
1, dye liquor is prepared: get Flos Carthami dry product, be ground into powder; Be filled with water with stainless-steel pan, get Yellow Fructus Gardeniae powder 15g and pour in pot, add 4000mL water, after powder and water being stirred evenly with long bamboo chopsticks, keep 20 minutes at 80-95 DEG C; When temperature is reduced to 60 DEG C, add the water 500mL of 4-20 DEG C, keep 10 minutes at 80-95 DEG C; When temperature drops to 60 DEG C again, add the water 500mL of 4-20 DEG C, keep 6 minutes at 80-95 DEG C; With the filter screen elimination dregs of a decoction, obtain dye liquor;
2, cloth preliminary treatment: with the water of 30 DEG C, puts after 10g sodium bicarbonate(edible) stirs evenly, adds the spinning cotton of white of fabric width 2 meters, length 5 meters, to soak after 30 minutes with water cleaning, must wait material of dying cloth;
3, material of waiting to dye cloth evenly puts into dye liquor, adds the water 500mL of 4-20 DEG C, after keeping 10 minutes at 80-95 DEG C; Build after lid cools 10 minutes naturally, cloth is taken out and spreads out;
Treat that dye liquor temperature is reduced to 60 DEG C, again cloth is put into pot, add the water 500mL of 4-20 DEG C, keep 10 minutes at 80-95 DEG C; When dye liquor temperature is reduced to 50 DEG C, take out cloth;
4, cloth to be immersed in the aqueous solution containing salt 20g/L 5 minutes, then to remove cloth loose colour with water cleaning;
5, dry in the air cloth, when cloth moisture is 70%, toasts 3 minutes with electric heater, obtains " Chinese medicine dye " cloth.
Two, Color evaluation
Cloth after dyeing is carried out soaping, Ultraviolet radiation test.
Result shows, the cloth after dyeing is through alkaline soap washing, Ultraviolet radiation color fast after 24 hours, colour-fast.
Embodiment 5 〝 Chinese medicine dye of the present invention 〞 method
〝 Chinese medicine dye 〞 method of the present invention may be used for the dyeing of spinning cotton, and Chinese medicine used is for Yellow Fructus Gardeniae dry product.
One, colouring method
1, dye liquor is prepared: get Yellow Fructus Gardeniae dry fruit, be ground into powder; Be filled with water with stainless-steel pan, get 15g Yellow Fructus Gardeniae powder and pour in pot, add 4000mL water, after powder and water being stirred evenly with long bamboo chopsticks, keep 20 minutes at 80-95 DEG C; When temperature is reduced to 60 DEG C, add the water 500mL of 4-20 DEG C, keep 10 minutes at 80-95 DEG C; When temperature drops to 60 DEG C again, add the water 500mL of 4-20 DEG C, keep 6 minutes at 80-95 DEG C; With the filter screen elimination dregs of a decoction, obtain dye liquor;
2, cloth preliminary treatment: with the water of 30 DEG C, puts after 10g sodium bicarbonate(edible) stirs evenly, adds the spinning cotton of white of fabric width 2 meters, length 5 meters, to soak after 30 minutes with water cleaning, must wait material (see Figure 13) of dying cloth;
3, material of waiting to dye cloth evenly puts into dye liquor, adds the water 500mL of 4-20 DEG C, keeps after 10 minutes at 80-95 DEG C; Build after lid cools 10 minutes naturally, cloth is taken out and spreads out;
Treat that dye liquor temperature is reduced to 60 DEG C, again cloth is put into pot, add the water 500mL of 4-20 DEG C, keep 10 minutes at 80-95 DEG C; When dye liquor temperature is reduced to 50 DEG C, take out cloth;
4, after cloth takes out, in dye liquor, pour 5g grape wine into, after stirring evenly, again put into cloth, will the dye liquor plastic bag sealing 3-5 hour of cloth be put into, take out cloth;
5, cloth to be immersed in the aqueous solution containing salt 20g/L 5 minutes, then to remove cloth loose colour with water cleaning;
6, dry in the air cloth, when cloth moisture is 90%, toasts 5 minutes with electric heater, obtains " Chinese medicine dye " cloth.
Two, Color evaluation
Cloth finished product (see Figure 14) after dyeing, is undertaken soaping by the cloth after dyeing, Ultraviolet radiation test.
Result shows, the cloth after dyeing is through alkaline soap washing, Ultraviolet radiation color fast after 24 hours, colour-fast.
Embodiment 6 〝 Chinese medicine dye of the present invention 〞 method
〝 Chinese medicine dye 〞 method of the present invention may be used for silk flosssilk wadding cloth dyeing, and Chinese medicine used is example with Yellow Fructus Gardeniae (having another name called wood red, stand, fructus gardeniae, branch, yellow chicken, fresh) fresh fruit.
One, colouring method:
1, prepare dye liquor: get Yellow Fructus Gardeniae fresh fruit 500g, making beating, adds 4000mL water, soaks three days; Then use the filter cloth elimination dregs of a decoction, liquid stainless-steel pan is boiled 30 minutes, obtains dye liquor;
2, cloth preliminary treatment: with the water of 30 DEG C, puts after 10g sodium bicarbonate(edible) stirs evenly, adds the white silk cotton of fabric width 2 meters, length 5 meters, to soak after 30 minutes with water cleaning, must wait material of dying cloth;
3, get material of waiting to dye cloth and evenly put into dye liquor, keep 25 minutes at 80-95 DEG C, cloth is taken out;
Treat that dye liquor temperature is reduced to 35 DEG C, again cloth is put into pot, keep 10 minutes at 80-95 DEG C; Take out cloth;
4, when dye liquor temperature is reduced to 50 DEG C, in dye liquor, pour 5g grape wine into, after stirring evenly, again put into cloth, will the dye liquor plastic bag sealing 3-5 hour of cloth be put into, take out cloth;
5, dry in the air cloth, when cloth moisture is 90%, toasts 3 minutes with electric heater, obtains " Chinese medicine dye " cloth.
Two, Color evaluation
Cloth finished product after dyeing is carried out soaping, Ultraviolet radiation test.
Result shows, the cloth after dyeing is through alkaline soap washing, Ultraviolet radiation color fast after 24 hours, colour-fast.
Embodiment 7 〝 Chinese medicine dye of the present invention 〞 method
〝 Chinese medicine of the present invention dye 〞 method may be used for silk flosssilk wadding cloth dyeing, Chinese medicine used with barberry (having another name called copper acupuncture, soulie barberry bark) fresh goods for example.
One, colouring method:
1, prepare dye liquor: the root 500g getting barberry fresh goods pulls an oar, and adds 4000mL water, soak three days; Then use the filter cloth elimination dregs of a decoction, liquid stainless-steel pan is boiled 30 minutes, obtains dye liquor;
2, cloth preliminary treatment: with the water of 30 DEG C, puts after 10g sodium bicarbonate(edible) stirs evenly, adds the white silk cotton of fabric width 2 meters, length 5 meters, to soak after 30 minutes with water cleaning, must wait material of dying cloth;
3, get material of waiting to dye cloth and evenly put into dye liquor, keep 25 minutes at 80-95 DEG C, cloth is taken out;
Treat that dye liquor temperature is reduced to 35 DEG C, again cloth is put into pot, keep 10 minutes at 80-95 DEG C, take out cloth;
4, when dye liquor temperature is reduced to 50 DEG C, in dye liquor, pour 5g grape wine into, after stirring evenly, again put into cloth, will the dye liquor plastic bag sealing 3-5 hour of cloth be put into, take out cloth;
5, cloth to be immersed in the aqueous solution containing salt 30g/L 5 minutes, then to remove cloth loose colour with water cleaning;
6, dry in the air cloth, when cloth moisture is 50%, toasts 1 minute with electric heater, obtains " Chinese medicine dye " cloth.
Two, Color evaluation
Cloth finished product (see Figure 15) after dyeing, can smell light Chinese medicine fragrance, can taste slight bitter taste.Cloth after dyeing is carried out soaping, Ultraviolet radiation test.
Result shows, the cloth after dyeing is through alkaline soap washing, Ultraviolet radiation color fast after 24 hours, colour-fast.
To sum up, the present invention's " Chinese medicine dye " technique is simple, constant product quality, cost is low, is widely used in dyeing plant, animal or mineral dyeing, abundant raw material source, good with the compatibility of environment, biodegradable, simultaneously due to during the active component existed in Chinese medicine is attached to and dyes cloth, effect that Chinese medicine is intrinsic can be played.
The present invention's " Chinese medicine dye ", except routine dye silkworm real silk, is also applicable to the textiles that other is dissimilar, as spinning cotton, silk flosssilk wadding cloth etc.; Colour tone nature, color fastness are high, good light stability, and stuff coloring evenly, is not faded; In addition, the present invention does not need to add mordant, just can reach outstanding Color by means of only specific technological process and parameter, and environment friendly and pollution-free, consumer can use safely; The inventive method is applicable to large-scale industrial production, has very wide market prospects.
Claims (10)
1. " Chinese medicine dye " method, it is characterized in that, it comprises the steps:
A, prepare dye liquor: get Chinese medicine, process obtains dye liquor;
B, cloth pre-treatment: in warm water, add sodium bicarbonate, mixing; Add cloth, soak, then with water cleaning, material of dying cloth must be waited;
C, to dye cloth:
The material of dying cloth waited getting step b immerses in dye liquor described in step a, is warming up to 80-95 DEG C, keeps 10-25 minute; Cooling 0-10 minute, takes out cloth;
Treat that dye liquor is cooled to 35-60 DEG C, again put into cloth, be warming up to 80-95 DEG C, keep 10 minutes;
D, be cooled to when being not less than 50 DEG C take out cloth;
E, cleaning, dry, obtain " Chinese medicine dye " cloth.
2. method according to claim 1, is characterized in that, in step a, the preparation method of described dye liquor is:
1) get Chinese medicine, pulverize, add water, be warming up to 80-95 DEG C, keep 20 minutes;
2) be cooled to 60 DEG C, add water; Be warming up to 80-95 DEG C again, keep 10 minutes;
3) be cooled to 60 DEG C, add water; Be warming up to 80-95 DEG C again, keep 6 minutes;
4) the elimination dregs of a decoction, obtain dye liquor;
Preferably, get Chinese medicine 1.5 parts, add water for 3 times and be respectively 400 parts, 50 parts, 50 parts; The temperature added water is 4-20 DEG C;
Described Chinese medicine is plant, animal drugs dry product or mineral drug.
3. method according to claim 1, is characterized in that: in step a, and the preparation method of described dye liquor is:
Get Chinese medicine, making beating, soaks, and filters; Filtrate decocts, and obtains dye liquor;
Preferably, get Chinese medicine 1 part, making beating, adds 8 parts of water soakings 3 days, filters; Filtrate decocts 30 minutes, obtains dye liquor;
Described Chinese medicine is plant, animal drugs fresh goods.
4. method according to claim 1, is characterized in that, in step b, described cloth is silkworm real silk, spinning cotton or silk flosssilk wadding cloth.
5. method according to claim 1, is characterized in that, in step b, described warm water is the water of 20-40 DEG C.
6. method according to claim 1, is characterized in that, in step c, described in the process of dying cloth, add cold water 1-3 time before being warming up to 80-95 DEG C.
7. method according to claim 1, is characterized in that, after steps d, also comprises fixation step.
8. method according to claim 7, is characterized in that, the method for described fixation is:
With grape wine in dye liquor after taking out cloth, stir and evenly mix, put into cloth, sealing 3-5 hour; And/or the cloth taken out be immersed in containing salt 20-30g/L the aqueous solution in 3-10 minute.
9. method according to claim 1, is characterized in that, in step e, described drying for directly to dry or when cloth moisture is 50-90%, 130-250 DEG C of baking 1-5 minute.
10. the method according to claim 1-9 any one, is characterized in that, described Chinese medicine is barberry, Yellow Fructus Gardeniae, safflower, bush, the sophora bud, Chinese gall, bush and/or ochre.
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