CN103451965A - Natural dyeing method of yellow modal fabric - Google Patents
Natural dyeing method of yellow modal fabric Download PDFInfo
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- CN103451965A CN103451965A CN2013103824649A CN201310382464A CN103451965A CN 103451965 A CN103451965 A CN 103451965A CN 2013103824649 A CN2013103824649 A CN 2013103824649A CN 201310382464 A CN201310382464 A CN 201310382464A CN 103451965 A CN103451965 A CN 103451965A
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- Prior art keywords
- washing
- modal fabric
- natural
- yellow
- modal
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- 239000004744 fabric Substances 0.000 title claims abstract description 49
- 238000004043 dyeing Methods 0.000 title claims abstract description 26
- 238000000034 method Methods 0.000 title claims abstract description 24
- 238000005406 washing Methods 0.000 claims abstract description 51
- 239000000975 dye Substances 0.000 claims abstract description 22
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 13
- SEBIKDIMAPSUBY-ARYZWOCPSA-N Crocin Chemical compound C([C@H]1O[C@H]([C@@H]([C@@H](O)[C@@H]1O)O)OC(=O)C(C)=CC=CC(C)=C\C=C\C=C(/C)\C=C\C=C(C)C(=O)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO[C@H]2[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O2)O)O1)O)O[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O SEBIKDIMAPSUBY-ARYZWOCPSA-N 0.000 claims abstract description 12
- 239000009627 gardenia yellow Substances 0.000 claims abstract description 12
- 238000010438 heat treatment Methods 0.000 claims abstract description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 8
- 238000010992 reflux Methods 0.000 claims abstract description 7
- 238000001035 drying Methods 0.000 claims abstract description 6
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 30
- 239000003795 chemical substances by application Substances 0.000 claims description 15
- 238000009413 insulation Methods 0.000 claims description 10
- 238000010792 warming Methods 0.000 claims description 10
- 244000111489 Gardenia augusta Species 0.000 claims description 6
- 235000018958 Gardenia augusta Nutrition 0.000 claims description 6
- 238000002203 pretreatment Methods 0.000 claims description 6
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 5
- 229940037003 alum Drugs 0.000 claims description 5
- 239000013527 degreasing agent Substances 0.000 claims description 5
- 238000000605 extraction Methods 0.000 claims description 5
- 238000010298 pulverizing process Methods 0.000 claims description 5
- 238000002791 soaking Methods 0.000 claims description 5
- 238000004040 coloring Methods 0.000 abstract description 4
- 229930182559 Natural dye Natural products 0.000 abstract description 2
- 230000000694 effects Effects 0.000 abstract description 2
- 230000007613 environmental effect Effects 0.000 abstract description 2
- 239000000978 natural dye Substances 0.000 abstract description 2
- 240000001972 Gardenia jasminoides Species 0.000 abstract 1
- 230000001105 regulatory effect Effects 0.000 description 3
- 229920003043 Cellulose fiber Polymers 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 229920000742 Cotton Polymers 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 238000009987 spinning Methods 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
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- Coloring (AREA)
Abstract
The invention discloses a natural dyeing method of a yellow modal fabric. The natural dyeing method comprises six stages as follows: pretreatment, drying, dyeing, water washing, color fixing and after finishing, wherein a natural gardenia yellow dye made from gardenia and ethanol through heating reflux is adopted in the dyeing process; water washing is carried out twice at different temperatures in the water washing stage, so that the coloring fastness of the dye is guaranteed. The natural dyeing method provided by the invention has the advantages that on one hand, the method of dyeing the modal fabric by using the natural dye can not cause pollution to the environment and has no harm on the human body, and also is in accordance with the color styles of nature, simplicity and elegance of the modal fabric, and therefore, the ecological environmental protection performance of the modal fabric is improved, the additional value of the modal fabric products is greatly increased, the requirements of people for healthy clothes are met and great practical value of the method is reflected, and on the other hand, the effects of quick coloring and even and stable color are achieved.
Description
Technical field
The present invention relates to the dyeing and finishing technology of fabric, relate in particular to a kind of natural dyeing method of yellow modal fabric.
Background technology
The raw material of Modal fibre is to originate from European spinney, through special spinning technique, is made after making wooden slurries, and be a kind of cellulose fibre, belong to cellulose fibre together so the same with cotton, be pure natural fabric.The model product is because the good flexibility that has of itself and good hygroscopicity but the poor characteristics of its fabric stiffness are used in the production of underwear now mostly.But also just because of modal fabric, it is famous with the natural green feature of environmental protection, chemical dye mostly used at present dyes, not only brought dyeing waste water, some chemical dye also forms potential threat to health, the style natural, simple for the modal fabric of underwear production with major part can not bring out the best in each other, and reduced to a certain extent its surcharge.
Therefore, need a kind of new technical scheme to address the above problem.
Summary of the invention
Goal of the invention: in order to solve the existing problem of prior art, the invention provides a kind of
Technical scheme: for achieving the above object, the natural dyeing method of a kind of yellow modal fabric of the present invention comprises the following steps:
(1) pre-treatment: the hydrogen peroxide solution that is 30% with mass fraction by modal fabric soaks 35-45min, adds in addition degreaser 0.5-1.0g/L, and soaking temperature is 80-100 ℃, has soaked after washing;
(2) dry: will be dried through the modal fabric of washing, temperature 70-80 ℃, dry to 7-8 and become dry;
(3) dyeing: at 20-25 ℃, the modal fabric after drying is entered to water, bath raio is 1:15-1:25, and adjusting pH is 6-6.5, be warming up to 35-45 ℃, add natural gardenia yellow dye 3%(o.w.f), anti-creasing agent 2-4g/L, be down to room temperature after insulation 15-20min and keep 15-20min, take out washing;
(4) washing: washing is divided into two stages, at first carries out hot wash, and wash temperature is 70-80 ℃, and wash time is 10-20min, then carries out common washing, and washing temperature is room temperature, and washing time is 20-30min;
(5) fixation: the modal fabric after washing is reentered into to dye vat, and bath raio is 1:15-1:25, adds citric acid and color-fixing agent, and wherein citric acid adding amount is 1-2g/L, and the color-fixing agent addition is 3-5g/L, is warming up to 50-60 ℃ of insulation 25-35min;
(6) after, arrange: the modal fabric after the taking-up fixation, carry out loose formula stoving process stentering forming under 80-90 ℃.
Further, in described step (3), the natural gardenia yellow dye is that the cape jasmine 20g that gets pulverizing uses the ethanol of 50%-60% at 70-100 ℃ of lower heating and refluxing extraction 5-6h, the alum solution that adds 13-16g/L in phegma, heating 30-40min is uniformly mixed and makes under 40-50 ℃.
Further, the described speed that is uniformly mixed is 600-800r/min.
Beneficial effect: the natural dyeing method of a kind of yellow modal fabric provided by the present invention, comprise pre-treatment, dry, dyeing, washing, six stages of fixation and rear arrangement, wherein dyeing takes the natural gardenia yellow dye made from cape jasmine and alcohol heating reflux to carry out, and in the washing in washing stage twice different temperatures successively, guaranteed the colouring fastness of dyestuff, the method that one aspect of the present invention utilizes natural dye to be dyeed to modal fabric can be to environment, also harmless, with its nature of modal fabric, simple, graceful color style brings out the best in each other, increased its eco-environmental prote, greatly improve the modal fabric value-added content of product, meet the demand of people to healthy clothing, there is very strong practical value, there is on the other hand colouring fast, the effect that color is uniform and stable.
The specific embodiment
Below in conjunction with specific embodiment, the present invention is further described:
Embodiment 1:
A kind of natural dyeing method of yellow modal fabric is characterized in that comprising the following steps:
(1) pre-treatment: the hydrogen peroxide solution that is 30% with mass fraction by modal fabric soaks 35min, adds in addition degreaser 0.5g/L, and soaking temperature is 80 ℃, has soaked after washing;
(2) dry: will be dried through the modal fabric of washing, temperature 70 C, dry to 7 one-tenth and do;
(3) dyeing: at 20 ℃, the modal fabric after drying is entered to water, bath raio is 1:15, and regulating pH is 6, is warming up to 35 ℃, adds natural gardenia yellow dye 3%(o.w.f), anti-creasing agent 2g/L, be down to room temperature after insulation 15min and keep 15min, takes out washing; Wherein the natural gardenia yellow dye is the cape jasmine 20g that gets pulverizing with 50% ethanol at 70 ℃ of lower heating and refluxing extraction 6h, adds the alum solution of 13g/L in phegma, and heating 40min is uniformly mixed and makes with the speed of 600r/min under 40 ℃.
(4) washing: washing is divided into two stages, at first carries out hot wash, and wash temperature is 70 ℃, and wash time is 10min, then carries out common washing, and washing temperature is room temperature, and washing time is 20min;
(5) fixation: the modal fabric after washing is reentered into to dye vat, and bath raio is 1:15, adds citric acid and color-fixing agent, and wherein citric acid adding amount is 1g/L, and the color-fixing agent addition is 3g/L, is warming up to 50 ℃ of insulation 25min;
(6) after, arrange: the modal fabric after the taking-up fixation, carry out loose formula stoving process stentering forming under 80 ℃.
Embodiment 2:
A kind of natural dyeing method of yellow modal fabric is characterized in that comprising the following steps:
(1) pre-treatment: the hydrogen peroxide solution that is 30% with mass fraction by modal fabric soaks 45min, adds in addition degreaser 1.0g/L, and soaking temperature is 100 ℃, has soaked after washing;
(2) dry: will be dried through the modal fabric of washing, 80 ℃ of temperature, dry to 8 one-tenth and do;
(3) dyeing: at 25 ℃, the modal fabric after drying is entered to water, bath raio is 1:25, and regulating pH is 6.5, is warming up to 45 ℃, adds natural gardenia yellow dye 3%(o.w.f), anti-creasing agent 4g/L, be down to room temperature after insulation 20min and keep 20min, takes out washing; Wherein the natural gardenia yellow dye is the cape jasmine 20g that gets pulverizing with 60% ethanol at 100 ℃ of lower heating and refluxing extraction 5h, adds the alum solution of 16g/L in phegma, and heating 30min is uniformly mixed and makes with the speed of 800r/min under 50 ℃.
(4) washing: washing is divided into two stages, at first carries out hot wash, and wash temperature is 80 ℃, and wash time is 20min, then carries out common washing, and washing temperature is room temperature, and washing time is 30min;
(5) fixation: the modal fabric after washing is reentered into to dye vat, and bath raio is 1:25, adds citric acid and color-fixing agent, and wherein citric acid adding amount is 2g/L, and the color-fixing agent addition is 5g/L, is warming up to 60 ℃ of insulation 35min;
(6) after, arrange: the modal fabric after the taking-up fixation, carry out loose formula stoving process stentering forming under 90 ℃.
Embodiment 3:
A kind of natural dyeing method of yellow modal fabric is characterized in that comprising the following steps:
(1) pre-treatment: the hydrogen peroxide solution that is 30% with mass fraction by modal fabric soaks 40min, adds in addition degreaser 0.8g/L, and soaking temperature is 90 ℃, has soaked after washing;
(2) dry: will be dried through the modal fabric of washing, 75 ℃ of temperature, dry to 7.5 one-tenth and do;
(3) dyeing: at 23 ℃, the modal fabric after drying is entered to water, bath raio is 1:20, and regulating pH is 6.3, is warming up to 40 ℃, adds natural gardenia yellow dye 3%(o.w.f), anti-creasing agent 3g/L, be down to room temperature after insulation 18min and keep 18min, takes out washing; Wherein the natural gardenia yellow dye is the cape jasmine 20g that gets pulverizing with 55% ethanol at 70 ℃ of lower heating and refluxing extraction 5.5h, adds the alum solution of 15g/L in phegma, and heating 35min is uniformly mixed and makes with the speed of 700r/min under 45 ℃.
(4) washing: washing is divided into two stages, at first carries out hot wash, and wash temperature is 75 ℃, and wash time is 15min, then carries out common washing, and washing temperature is room temperature, and washing time is 25min;
(5) fixation: the modal fabric after washing is reentered into to dye vat, and bath raio is 1:20, adds citric acid and color-fixing agent, and wherein citric acid adding amount is 1.5g/L, and the color-fixing agent addition is 4g/L, is warming up to 55 ℃ of insulation 30min;
(6) after, arrange: the modal fabric after the taking-up fixation, carry out loose formula stoving process stentering forming under 85 ℃.
Should be understood that, the above specific embodiment only is not used in and limits the scope of the invention for the present invention is described, after having read the present invention, those skilled in the art all fall within the application's claims limited range to the modification of the various equivalent form of values of the present invention.
Claims (3)
1. the natural dyeing method of a yellow modal fabric is characterized in that comprising the following steps:
(1) pre-treatment: the hydrogen peroxide solution that is 30% with mass fraction by modal fabric soaks 35-45min, adds in addition degreaser 0.5-1.0g/L, and soaking temperature is 80-100 ℃, has soaked after washing;
(2) dry: will be dried through the modal fabric of washing, temperature 70-80 ℃, dry to 7-8 and become dry;
(3) dyeing: at 20-25 ℃, the modal fabric after drying is entered to water, bath raio is 1:15-1:25, and adjusting pH is 6-6.5, be warming up to 35-45 ℃, add natural gardenia yellow dye 3%(o.w.f), anti-creasing agent 2-4g/L, be down to room temperature after insulation 15-20min and keep 15-20min, take out washing;
(4) washing: washing is divided into two stages, at first carries out hot wash, and wash temperature is 70-80 ℃, and wash time is 10-20min, then carries out common washing, and washing temperature is room temperature, and washing time is 20-30min;
(5) fixation: the modal fabric after washing is reentered into to dye vat, and bath raio is 1:15-1:25, adds citric acid and color-fixing agent, and wherein citric acid adding amount is 1-2g/L, and the color-fixing agent addition is 3-5g/L, is warming up to 50-60 ℃ of insulation 25-35min;
(6) after, arrange: the modal fabric after the taking-up fixation, carry out loose formula stoving process stentering forming under 80-90 ℃.
2. the natural dyeing method of a kind of yellow modal fabric according to claim 1, it is characterized in that: in described step (3), the natural gardenia yellow dye is that the cape jasmine 20g that gets pulverizing uses the ethanol of 50%-60% at 70-100 ℃ of lower heating and refluxing extraction 5-6h, the alum solution that adds 13-16g/L in phegma, heating 30-40min is uniformly mixed and makes under 40-50 ℃.
3. the natural dyeing method of a kind of yellow modal fabric according to claim 2, it is characterized in that: the described speed that is uniformly mixed is 600-800r/min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310382464.9A CN103451965B (en) | 2013-08-28 | 2013-08-28 | A kind of natural dyeing method of yellow modal fabric |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310382464.9A CN103451965B (en) | 2013-08-28 | 2013-08-28 | A kind of natural dyeing method of yellow modal fabric |
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| CN103451965A true CN103451965A (en) | 2013-12-18 |
| CN103451965B CN103451965B (en) | 2015-08-05 |
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| CN201310382464.9A Active CN103451965B (en) | 2013-08-28 | 2013-08-28 | A kind of natural dyeing method of yellow modal fabric |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103938468A (en) * | 2014-05-12 | 2014-07-23 | 祝一鸣 | Natural plant dyestuff dyeing and finishing processing method for loose cellulose fiber |
| CN103938386A (en) * | 2014-04-25 | 2014-07-23 | 何炽斌 | Production method for dyeing cloth through pure natural dyeing liquid |
| CN105332293A (en) * | 2015-10-29 | 2016-02-17 | 南通仙乐色织有限公司 | Dyeing method for improving reactive brilliant blue dyeing stability |
| CN106283723A (en) * | 2016-08-11 | 2017-01-04 | 广东溢达纺织有限公司 | Modified Gardenia Yellow and the method that cation-modified cellulose base fiber fabric is dyeed thereof |
| CN106544890A (en) * | 2016-12-01 | 2017-03-29 | 西南大学 | Colouring method of the gardenin to bafta |
| CN109295757A (en) * | 2018-08-28 | 2019-02-01 | 苏州典传创意科技有限公司 | A kind of natural dye dying method of regenerated fiber fabric |
| CN110592984A (en) * | 2019-10-29 | 2019-12-20 | 青岛雪达集团有限公司 | Dyeing and finishing process of modal blended fabric and method for preparing modal blended tinged fabric by using dyeing and finishing process |
| CN110656512A (en) * | 2019-10-29 | 2020-01-07 | 青岛雪达集团有限公司 | Method for dyeing and finishing modal blended fabric by using natural plant dye |
| CN113832744A (en) * | 2021-10-12 | 2021-12-24 | 广州市当美服饰有限公司 | Environment-friendly clothing dye and application thereof in clothing printing and dyeing |
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Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103938386A (en) * | 2014-04-25 | 2014-07-23 | 何炽斌 | Production method for dyeing cloth through pure natural dyeing liquid |
| CN103938468A (en) * | 2014-05-12 | 2014-07-23 | 祝一鸣 | Natural plant dyestuff dyeing and finishing processing method for loose cellulose fiber |
| CN103938468B (en) * | 2014-05-12 | 2016-01-13 | 祝一鸣 | For the natural plant dye dyeing and finishing processing method of cellulose bulk fibre |
| CN105332293A (en) * | 2015-10-29 | 2016-02-17 | 南通仙乐色织有限公司 | Dyeing method for improving reactive brilliant blue dyeing stability |
| CN106283723A (en) * | 2016-08-11 | 2017-01-04 | 广东溢达纺织有限公司 | Modified Gardenia Yellow and the method that cation-modified cellulose base fiber fabric is dyeed thereof |
| CN106283723B (en) * | 2016-08-11 | 2019-05-14 | 广东溢达纺织有限公司 | Modified Gardenia Yellow and its method that cation-modified cellulose base fiber fabric is dyed |
| CN106544890A (en) * | 2016-12-01 | 2017-03-29 | 西南大学 | Colouring method of the gardenin to bafta |
| CN109295757A (en) * | 2018-08-28 | 2019-02-01 | 苏州典传创意科技有限公司 | A kind of natural dye dying method of regenerated fiber fabric |
| CN110592984A (en) * | 2019-10-29 | 2019-12-20 | 青岛雪达集团有限公司 | Dyeing and finishing process of modal blended fabric and method for preparing modal blended tinged fabric by using dyeing and finishing process |
| CN110656512A (en) * | 2019-10-29 | 2020-01-07 | 青岛雪达集团有限公司 | Method for dyeing and finishing modal blended fabric by using natural plant dye |
| CN113832744A (en) * | 2021-10-12 | 2021-12-24 | 广州市当美服饰有限公司 | Environment-friendly clothing dye and application thereof in clothing printing and dyeing |
| CN113832744B (en) * | 2021-10-12 | 2023-09-19 | 开平市信迪染整厂有限公司 | Environment-friendly clothing dye and application thereof in clothing printing and dyeing |
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| Publication number | Publication date |
|---|---|
| CN103451965B (en) | 2015-08-05 |
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Effective date of registration: 20181220 Address after: 312000 Huibin Road, Ma'an Town, Keqiao District, Shaoxing City, Zhejiang Province, 488 Patentee after: Zhejiang Shaoxing Zhonghuan Printing and Dyeing Co., Ltd. Address before: 212444 Jiangsu, Zhenjiang, Jurong, Hou Hou Town, Gaoping Road, Jurong Road, Hou Bai Zhen Ying Rui printing factory Patentee before: Jurong City Houbai Town Yingrui Print Works |
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Denomination of invention: A natural dyeing method of yellow modal fabric Effective date of registration: 20220424 Granted publication date: 20150805 Pledgee: Bank of Ningbo Co.,Ltd. Shaoxing Branch Pledgor: Zhejiang Shaoxing Zhonghuan Printing and Dyeing Co.,Ltd. Registration number: Y2022330000575 |
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