CN103603213A - Method for dyeing cotton fabrics through vegetable dyes - Google Patents
Method for dyeing cotton fabrics through vegetable dyes Download PDFInfo
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- CN103603213A CN103603213A CN201310618223.XA CN201310618223A CN103603213A CN 103603213 A CN103603213 A CN 103603213A CN 201310618223 A CN201310618223 A CN 201310618223A CN 103603213 A CN103603213 A CN 103603213A
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Abstract
The invention provides a method for dyeing cotton fabrics through vegetable dyes. The method comprises the following steps: (1) extracting vegetable dyes from vegetable raw materials; (2) adding vegetable dyes which account for 25-50 percent of the weight of the cotton fabrics into the cotton fabrics for dyeing, wherein a weight bath ratio of dyeing is 1: (10-50), regulating a pH value of a dyeing solution to be 4-6, wherein the dye bath temperature is 30-70 DEG C, and the dyeing time is 0.5-4 hours; (3) adding a mordant into the dyed cotton fabrics for mordanting, wherein the amount of the mordant is 1/3-1/2 of the weight of the vegetable dyes, the weight bath ratio is 1: (10-50), regulating the pH value of the dyeing solution to be 4-6, the dye bath temperature is 30-70 DEG C, and the dyeing time is 0.5-4 hours; and (4) soaping, washing and drying the mordanted cotton fabrics. The method is safe and environment-friendly, the dyed cotton fabrics are high in dyeing color fastness and difficult to fade and discolor, and the dyed color is soft and natural.
Description
Technical field
The invention belongs to printing technology field, be specifically related to a kind of method with vegetable colour dyeing cotton fabric.Background technology
Vegetable colour dyeing is mainly to utilize the partial pigment such as bark, leaf, root, fruit, flower, stem and the method that dyes.From the dyeing of vegetable colour, some natural plant pigment has good dissolubility to water, and dye liquor is directly on set fabric, thereby and some phytochrome need to mordant with it complex coordination make it fixing on fabric.Also have some fabric pigments water insoluble, need to utilize them different and anchor on fiber to the solution degree of acid, alkaline solution.Vegetable colour and technique environmental protection thereof, be healthy dyestuff, and the compatibility of most plants dyestuff and ecological environment is good, biodegradable, and toxicity is lower, produces the raw material of these dyestuffs and can regenerate.Vegetable colour is nontoxic, and skin, without anaphylaxis and carcinogenic, is had to good biodegradability and Environmental compatibility.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of method of vegetable colour dyeing cotton fabric.
Technical scheme provided by the invention is a kind of method of vegetable colour dyeing cotton fabric, it is characterized in that: comprise the following steps:
1) plant material is pulverized, the ratio that is 1:10～50 in solid-liquid ratio adds clear water in plant material, at 10～30 ℃, extracts 0.5～1h, and by extracting liquid filtering, filtrate is concentrated, the dry vegetable colour that is;
2) get on the vegetable colour that COTTON FABRIC adds its weight 25～50% and dye, the weight bath raio of above dying is 1:10～50, and regulating dye liquor pH value is 4～6, and dye bath temperature is 30～70 ℃, and dyeing time is 0.5～4 hour;
3) add mordant to carry out mordant dyeing the COTTON FABRIC of dying on, mordant consumption is 1/3～1/2 of vegetable colour weight, and weight bath raio is 1:10～50, and regulating the pH value of dye liquor is 4～6, and dye bath temperature is 30～70 ℃, and dyeing time is 0.5～4 hour;
4) the good COTTON FABRIC of mordant dyeing is soaped, washing and oven dry.
Above-mentioned steps 3) mordant described in is alum.
Above-mentioned plant material is hispid arthraxon, cape jasmine or sophora flower.
The present invention utilizes plant material to dye to COTTON FABRIC, has plant material aboundresources, a little nontoxic, and is conducive to the reasonable utilization of resource.Meanwhile, dyefastness is good, and Exposure to Sunlight is colour-fast, the nondiscolouring of soaping, and even dyeing, color and luster is soft, simple and unsophisticated, nature.
The specific embodiment
The present invention is further elaborated for following specific embodiment, but not as a limitation of the invention.
Embodiment 1
1) hispid arthraxon is pulverized, the ratio that is 1:10 in solid-liquid ratio adds clear water in hispid arthraxon, at 10 ℃, extracts 0.5h, and by extracting liquid filtering, filtrate is concentrated, the dry vegetable colour that is;
2) get on the vegetable colour that COTTON FABRIC adds its weight 25% and dye, the weight bath raio of above dying is 1:10, and regulating dye liquor pH value is 4, and dye bath temperature is 30 ℃, and dyeing time is 0.5 hour;
3) add alum to carry out mordant dyeing the COTTON FABRIC of dying on, alum consumption is 1/3 of vegetable colour weight, and weight bath raio is 1:10, and regulating the pH value of dye liquor is 4, and dye bath temperature is 30 ℃, and dyeing time is 0.5 hour;
4) the good COTTON FABRIC of mordant dyeing is soaped, washing and oven dry.It is 3-4 level that the COTTON FABRIC dyeing is measured to fastness to washing by GB/T3921-2008GB/T3920-2008 method, and colour fastness to rubbing is 3-4 level.
Embodiment 2
1) cape jasmine is pulverized, the ratio that is 1:50 in solid-liquid ratio adds clear water in cape jasmine, at 30 ℃, extracts 1h, and by extracting liquid filtering, filtrate is concentrated, the dry vegetable colour that is;
2) get on the vegetable colour that COTTON FABRIC adds its weight 50% and dye, the weight bath raio of above dying is 1:50, and regulating dye liquor pH value is 6, and dye bath temperature is 70 ℃, and dyeing time is 4 hours;
3) add alum to carry out mordant dyeing the COTTON FABRIC of dying on, alum consumption is 1/2 of vegetable colour weight, and weight bath raio is 1:50, and regulating the pH value of dye liquor is 6, and dye bath temperature is 70 ℃, and dyeing time is 4 hours;
4) the good COTTON FABRIC of mordant dyeing is soaped, washing and oven dry.It is 3-4 level that the COTTON FABRIC dyeing is measured to fastness to washing by GB/T3921-2008GB/T3920-2008 method, and colour fastness to rubbing is 4 grades.
Embodiment 3
1) sophora flower is pulverized, the ratio that is 1:25 in solid-liquid ratio adds clear water in sophora flower, at 20 ℃, extracts 0.8h, and by extracting liquid filtering, filtrate is concentrated, the dry vegetable colour that is;
2) get on the vegetable colour that COTTON FABRIC adds its weight 40% and dye, the weight bath raio of above dying is 1:25, and regulating dye liquor pH value is 5, and dye bath temperature is 50 ℃, and dyeing time is 2 hours;
3) add alum to carry out mordant dyeing the COTTON FABRIC of dying on, alum consumption is 5/12 of vegetable colour weight, and weight bath raio is 1:25, and regulating the pH value of dye liquor is 5, and dye bath temperature is 50 ℃, and dyeing time is 2 hours;
4) the good COTTON FABRIC of mordant dyeing is soaped, washing and oven dry.It is 3-4 level that the COTTON FABRIC dyeing is measured to fastness to washing by GB/T3921-2008GB/T3920-2008 method, and colour fastness to rubbing is 3-4 level.
Embodiment 4
1) hispid arthraxon is pulverized, the ratio that is 1:10 in solid-liquid ratio adds clear water in hispid arthraxon, at 30 ℃, extracts 0.5h, and by extracting liquid filtering, filtrate is concentrated, the dry vegetable colour that is;
2) get on the vegetable colour that COTTON FABRIC adds its weight 50% and dye, the weight bath raio of above dying is 1:10, and regulating dye liquor pH value is 6, and dye bath temperature is 30 ℃, and dyeing time is 4 hours;
3) add alum to carry out mordant dyeing the COTTON FABRIC of dying on, alum consumption is 1/3 of vegetable colour weight, and weight bath raio is 1:50, and regulating the pH value of dye liquor is 4, and dye bath temperature is 70 ℃, and dyeing time is 0.5 hour;
4) the good COTTON FABRIC of mordant dyeing is soaped, washing and oven dry.It is 3-4 level that the COTTON FABRIC dyeing is measured to fastness to washing by GB/T3921-2008GB/T3920-2008 method, and colour fastness to rubbing is 4-5 level.
Claims (3)
1. a method for vegetable colour dyeing cotton fabric, is characterized in that: comprise the following steps:
1) plant material is pulverized, the ratio that is 1:10～50 in solid-liquid ratio adds clear water in plant material, at 10～30 ℃, extracts 0.5～1h, and by extracting liquid filtering, filtrate is concentrated, the dry vegetable colour that is;
2) get on the vegetable colour that COTTON FABRIC adds its weight 25～50% and dye, the weight bath raio of above dying is 1:10～50, and regulating dye liquor pH value is 4～6, and dye bath temperature is 30～70 ℃, and dyeing time is 0.5～4 hour;
3) add mordant to carry out mordant dyeing the COTTON FABRIC of dying on, mordant consumption is 1/3～1/2 of vegetable colour weight, and weight bath raio is 1:10～50, and regulating the pH value of dye liquor is 4～6, and dye bath temperature is 30～70 ℃, and dyeing time is 0.5～4 hour;
4) the good COTTON FABRIC of mordant dyeing is soaped, washing and oven dry.
2. the method for vegetable colour dyeing cotton fabric according to claim 1, is characterized in that: mordant described in step 3) is alum.
3. the method for vegetable colour dyeing cotton fabric according to claim 1, is characterized in that: described plant material is hispid arthraxon, cape jasmine or sophora flower.
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| CN201310618223.XA CN103603213A (en) | 2013-11-28 | 2013-11-28 | Method for dyeing cotton fabrics through vegetable dyes |
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| CN201310618223.XA CN103603213A (en) | 2013-11-28 | 2013-11-28 | Method for dyeing cotton fabrics through vegetable dyes |
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Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104004380A (en) * | 2014-04-30 | 2014-08-27 | 浙江雨兰建材有限公司 | Coating pigment extracted from plants |
| CN104179039A (en) * | 2014-08-25 | 2014-12-03 | 苏州大学 | Method for dyeing silk or silk fabric by aspergillus niger spore powder |
| CN104861737A (en) * | 2015-05-13 | 2015-08-26 | 钱玉梅 | Method for preparing sophora japonica plant dyes |
| CN105086508A (en) * | 2015-10-08 | 2015-11-25 | 嘉兴市欣纺纺织品有限公司 | Sophora japonica plant dye extraction method and dyeing method through dye |
| CN105131644A (en) * | 2015-10-08 | 2015-12-09 | 嘉兴市欣纺纺织品有限公司 | Extracting method and dyeing method for sappan plant dye |
| CN105504867A (en) * | 2016-01-29 | 2016-04-20 | 辽东学院 | Plant-based natural dye for fabrics as well as preparation method and fabric dyeing method of dye |
| CN106544896A (en) * | 2016-12-01 | 2017-03-29 | 西南大学 | The method of gardenin dyed cotton fabric |
| CN106948188A (en) * | 2017-03-24 | 2017-07-14 | 北京工业大学 | Vegetation dye improves color fastness experimental method |
| CN107099168A (en) * | 2017-06-08 | 2017-08-29 | 山东滨州豪盛巾被有限公司 | A kind of extraction of hispid arthraxon dyestuff and colouring method |
| CN107356660A (en) * | 2017-07-21 | 2017-11-17 | 浙江理工大学 | It is a kind of to simulate the method for removing ancient times bafta exogenous strontium |
| CN108929561A (en) * | 2017-05-26 | 2018-12-04 | 天津工业大学 | A kind of preparation method of sedge natural dye and the application in cotton fabric dyeing process |
| CN109575631A (en) * | 2018-11-12 | 2019-04-05 | 苏州工业园区职业技术学院 | A kind of vegetable dye and its dyeing |
| CN115387134A (en) * | 2022-05-31 | 2022-11-25 | 湖南工程学院 | One-bath one-step method for extracting and dyeing vegetable dye pigment and dyeing equipment |
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| CN101144249A (en) * | 2007-10-19 | 2008-03-19 | 无锡汇罗新材料科技有限公司 | Technique for dyeing pure cotton knitting face fabric by plant dyestuff |
| CN101148826A (en) * | 2007-09-30 | 2008-03-26 | 无锡汇罗新材料科技有限公司 | Technique for dyeing purified cotton yarn by vegetable dye |
| CN101307572A (en) * | 2007-05-15 | 2008-11-19 | 袁慧丽 | Dyeing method of cape jasmine in natural fiber |
| CN102634993A (en) * | 2012-02-01 | 2012-08-15 | 常州美胜生物材料有限公司 | Method for dyeing cotton fibers by using natural dye |
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Patent Citations (4)
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| CN101307572A (en) * | 2007-05-15 | 2008-11-19 | 袁慧丽 | Dyeing method of cape jasmine in natural fiber |
| CN101148826A (en) * | 2007-09-30 | 2008-03-26 | 无锡汇罗新材料科技有限公司 | Technique for dyeing purified cotton yarn by vegetable dye |
| CN101144249A (en) * | 2007-10-19 | 2008-03-19 | 无锡汇罗新材料科技有限公司 | Technique for dyeing pure cotton knitting face fabric by plant dyestuff |
| CN102634993A (en) * | 2012-02-01 | 2012-08-15 | 常州美胜生物材料有限公司 | Method for dyeing cotton fibers by using natural dye |
Cited By (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104004380A (en) * | 2014-04-30 | 2014-08-27 | 浙江雨兰建材有限公司 | Coating pigment extracted from plants |
| CN104004380B (en) * | 2014-04-30 | 2016-06-22 | 浙江雨兰建材有限公司 | A kind of paint pigment extracted from plant |
| CN104179039A (en) * | 2014-08-25 | 2014-12-03 | 苏州大学 | Method for dyeing silk or silk fabric by aspergillus niger spore powder |
| CN104179039B (en) * | 2014-08-25 | 2016-01-20 | 苏州大学 | The aspergillus niger spore powder colouring method of a kind of silk or its fabric |
| CN104861737A (en) * | 2015-05-13 | 2015-08-26 | 钱玉梅 | Method for preparing sophora japonica plant dyes |
| CN105086508A (en) * | 2015-10-08 | 2015-11-25 | 嘉兴市欣纺纺织品有限公司 | Sophora japonica plant dye extraction method and dyeing method through dye |
| CN105131644A (en) * | 2015-10-08 | 2015-12-09 | 嘉兴市欣纺纺织品有限公司 | Extracting method and dyeing method for sappan plant dye |
| CN105504867A (en) * | 2016-01-29 | 2016-04-20 | 辽东学院 | Plant-based natural dye for fabrics as well as preparation method and fabric dyeing method of dye |
| CN106544896A (en) * | 2016-12-01 | 2017-03-29 | 西南大学 | The method of gardenin dyed cotton fabric |
| CN106948188A (en) * | 2017-03-24 | 2017-07-14 | 北京工业大学 | Vegetation dye improves color fastness experimental method |
| CN108929561A (en) * | 2017-05-26 | 2018-12-04 | 天津工业大学 | A kind of preparation method of sedge natural dye and the application in cotton fabric dyeing process |
| CN107099168A (en) * | 2017-06-08 | 2017-08-29 | 山东滨州豪盛巾被有限公司 | A kind of extraction of hispid arthraxon dyestuff and colouring method |
| CN107099168B (en) * | 2017-06-08 | 2019-12-20 | 山东滨州豪盛巾被有限公司 | Hispid arthraxon dye extraction and dyeing method |
| CN107356660A (en) * | 2017-07-21 | 2017-11-17 | 浙江理工大学 | It is a kind of to simulate the method for removing ancient times bafta exogenous strontium |
| CN109575631A (en) * | 2018-11-12 | 2019-04-05 | 苏州工业园区职业技术学院 | A kind of vegetable dye and its dyeing |
| CN115387134A (en) * | 2022-05-31 | 2022-11-25 | 湖南工程学院 | One-bath one-step method for extracting and dyeing vegetable dye pigment and dyeing equipment |
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Application publication date: 20140226 |