CN102220705A - Method for dying silk fabric by using natural dye of Suaeda salsa - Google Patents
Method for dying silk fabric by using natural dye of Suaeda salsa Download PDFInfo
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- CN102220705A CN102220705A CN 201110111540 CN201110111540A CN102220705A CN 102220705 A CN102220705 A CN 102220705A CN 201110111540 CN201110111540 CN 201110111540 CN 201110111540 A CN201110111540 A CN 201110111540A CN 102220705 A CN102220705 A CN 102220705A
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- suaeda salsa
- mordant
- dying
- natural dye
- silk fabric
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Abstract
The invention relates to a method for dying silk fabric by using natural dye of Suaeda salsa, comprising the following steps of: preparing a natural dye solution of Suaeda salsa with concentration of 10-20% (o.w.f), wherein the dying temperature is 40-60 DEG C, the bath ratio is 1: 20-50, the pH value of the dye solution is 2-4, and the dying time is 30-90 min; fetching a mordant solution with concentration of 2-10% (o.w.f), wherein the mordant temperature is 40-100 DEG C, and the mordant time is 30-90 min; or dying and adding mordants and the natural dye solution of the Suaeda salsa before the silk fabric is added to the natural dye solution of the Suaeda salsa or after the silk fabric is added to the natural dye solution of the Suaeda salsa. The method adopts the existing fabric dying device to directly dye without adding another device or increasing cost; the silk fabric after dying in the method is colorful and has good washing fastness and rubbing fastness; moreover, the method is suitable for industrial production without toxicity, harm and pollution, and has good application prospect.
Description
Technical field
This method that the dyeing extract that relates to plant self is used on textiles is specifically related to the method that the Suaeda salsa natural dye dyes on silk fabric.
Background technology
In recent years, because the influence of environmental problem and energy problem, people are tending towards pursuing continuable, and are eco-friendly and the human health advantageous method produced dyestuff.The exploitation natural dye is the general trend that the world uses the dyestuff development, natural dye is meant and obtains from plant, animal or mineral resources, seldom or not pass through the dyestuff of chemical process, a lot of natural dyes have safe and reliable, the tone nature, near advantages such as natural materials, natural, multi-functional is the trend of dyestuff development.
Alkali paulin (Suaeda salsa) saline land, tender seedling claims " wolf tail bar ", often is called " HAIYINGCAI ", " alkali wormwood artemisia ", " salt wormwood artemisia ", annual herb, stem is upright, cylindrical, up to 30～100 centimetres, Hua Dansheng or 2～3 have handle to cluster on the short handle of axil, the group's of being umbrella, perianth is the five-pointed star shape in the fruit phase, and normally March in time, early and middle ten days all can be emerged to early June, and epigeal cotyledon is scarlet.Be the florescence 7～August, and be productive phase 9～October, November the initial seed full maturity.Plant is red as fire when ripe, has ornamental value.Be typical halophytes, its cultivation technique is more extensive, mainly is distributed in northeast, northwest, North China and Henan, Shandong, Jiangsu, zhejiang and other places.The fluffy commodity of alkali is good, and the fluffy plant type of alkali is attractive in appearance, and the refined title of " emerald coral " is arranged; Fresh and tender cauline leaf is nutritious, has special seafood flavor, and mouthfeel is good.Cure mainly dyspepsia stagnation, heating etc. and cut to be used as medicine.Be a kind of fabulous wild plant resource of doing feed, medicine, food etc., containing huge ecology, economic and social benefit.
Ripe saline land alkali paulin stem, leaf take on a red color, and are rich in a large amount of natural colouring matters.Publication number is that CN101204217A and publication number are that the patent of CN101747663A was carried out research and report to extraction method of natural pigments in the alkali paulin saline land, and the pigment of extraction mainly is used in food service industry with the form of food coloring.Up to the present, the research that fabric dyes is not appeared in the newspapers as natural dye with the Suaeda salsa extract.
Summary of the invention
Technical problem to be solved by this invention provides the method for a kind of Suaeda salsa natural dye to silk fabric, and this method utilization has the direct dyeing of textile dyeing equipment now, does not increase equipment, does not increase cost; Silk fabric lovely luster through the present invention's dyeing has good washing fastness and fastness to rubbing, is suitable for suitability for industrialized production, and is nontoxic, harmless, pollution-free, has a good application prospect.
The method of dying silk fabric on the Suaeda salsa natural dye of the present invention comprises:
The Suaeda salsa extract (is gathered stem, the leaf of ripe Suaeda salsa, pulverizing the back drops in the water, the pH value is 5,50 ℃ of following lixiviates were filtered after 20 minutes, with the filtrate concentrate drying of collecting, obtain the dyestuff pulvis, during dyeing pulvis be made into certain density dye liquor) as dyestuff, adopt the mordant dyeing mode to silk fabric carry out pre-matchmaker, with matchmaker or back mordant dyeing look.
Detailed process is: compound concentration is the Suaeda salsa natural dye dye liquor of 10～20% (o.w.f), 40～60 ℃ of dyeing temperatures; bath raio is 1: 20～50; dye liquor pH value 2～4; dyeing time 30～90 minutes; getting concentration is the mordant solution of 2～10% (o.w.f); 40～100 ℃ of dyeing temperatures; 30～90 minutes mordant dyeing time, mordant before silk fabric drops into Suaeda salsa natural dye dye liquor, drop into behind the Suaeda salsa natural dye dye liquor or and add with bathing with Suaeda salsa natural dye dye liquor.
Wherein said o.w.f: heavy to fabric.
Wherein said bath raio: the ratio of fabric quality and solution quality.
Wherein said mordant is: one or more in copper sulphate, frerrous chloride, ferric sulfate, aluminum sulfate, alum, stannous chloride, the zinc sulfate.
The mordant that dyeing is used all has affinity to coloring material and fiber, anchor at fiber surface thereby can form coordinate bond with the metal ion effect of mordant western-style clothes on silk fiber during the Suaeda salsa natural dye dying, increases dyefastness.Simultaneously, use different mordants can also produce different form and aspect.
According to GB/T 3921.1-1997 textile color stability test color fastness to washing; Fabric COLOR FASTNESS test analysis is carried out in the evaluation of GB/T 3920-1997 textile color stability test fastness to rubbing.The colour fastness to rubbing of fabric and color fastness to water all reached and take requirement after result's demonstration was dyed.
Beneficial effect:
(1) the existing textile dyeing equipment direct dyeing of the inventive method utilization does not increase equipment, does not increase cost, is applied to the cleaner production of textile industry, can produce in a large number;
(2) dyeing of the present invention is simple, dyes that back textile dyeing fastness is good, colour-fast, nondiscolouring, favorable reproducibility; Color and luster is natural, graceful, caters to people's pursuing individualityization, diversified requirement;
(3) the inventive method does not exist synthetic dyestuffs to the pollution of environment with to the injury of human body; Can obtain ecology, safe, nontoxic natural dye dying fabric, have suitability for industrialized production and Application Prospect;
(4) saline land the alkali paulin can improve ecological environments such as salt-soda soil, beach ground positive role is arranged, and at feed, medicine, field of food multipurpose is arranged in addition, easily enlarges plantation, can realize large-scale planting.
Concrete enforcement side
Embodiment 1:
The aluminum sulfate of getting concentration 5% (o.w.f) is as mordant; bath raio 1: 50; 90 ℃ of mordant dyeing temperature, and silk fabric is carried out mordant dyeing, and the mordant dyeing time is 60 minutes; take out fabric; the Suaeda salsa natural dye dye liquor of 10% (o.w.f) that puts into dyes, dye liquor pH value 3, bath raio 1: 50; 55 ℃ of dyeing temperatures, dyeing time 30 minutes.
Dye back fabric displaing amaranth, after measured, dye the L value 67.07 of back fabric, a value 23.96, b value-3.53, water-fast 4 grades of the COLOR FASTNESS staining fastnesses of washing, water-fast 3～4 grades of the COLOR FASTNESS variable color fastness of washing; 4～5 grades of dry fastnesses, 3～4 grades of fastness to wet rubbings.
Embodiment 2:
The Suaeda salsa natural dye dye liquor of getting concentration and be 10% (o.w.f) dyes to silk fabric, dye liquor pH value 3; bath raio 1: 50; 55 ℃ of dyeing temperatures, dyeing time 30 minutes dyes the back and takes out fabric; put into mordant dyeing in the aluminum sulfate mordant dyeing of concentration 5% (o.w.f) again; bath raio 1: 50,55 ℃ of mordant dyeing temperature, 90 minutes mordant dyeing time.
Dye back fabric displaing amaranth, after measured, dye the L value 69.17 of back fabric, a value 20.62, b value 1.65, water-fast 3～4 grades of the COLOR FASTNESS staining fastnesses of washing, water-fast 3～4 grades of the COLOR FASTNESS variable color fastness of washing; 4 grades of dry fastnesses, 3～4 grades of fastness to wet rubbings.
Embodiment 3:
The dye liquor that is made into the aluminum sulfate of the Suaeda salsa natural dye and 5% (o.w.f) of 10% (o.w.f) dyes dye liquor pH value 3, bath raio 1: 50,55 ℃ of dyeing temperatures, dyeing time 90 minutes to silk fabric.
Dye back fabric displaing amaranth, after measured, dye the L value 73.28 of back fabric, a value 19.04, b value 1.92, water-fast 4 grades of the COLOR FASTNESS staining fastnesses of washing, water-fast 3～4 grades of the COLOR FASTNESS variable color fastness of washing; 4～5 grades of dry fastnesses, 3～4 grades of fastness to wet rubbings.
Embodiment 4:
The ferrous sulfate of getting concentration 5% (o.w.f) is as mordant; bath raio 1: 50; 90 ℃ of mordant dyeing temperature, and silk fabric is carried out mordant dyeing, and the mordant dyeing time is 60 minutes; take out fabric; the Suaeda salsa natural dye dye liquor of 10% (o.w.f) that puts into dyes, dye liquor pH value 3, bath raio 1: 50; 55 ℃ of dyeing temperatures, dyeing time 30 minutes.
Dye the back fabric and show yellowish-brown, after measured, dye the L value 60.32 of back fabric, a value 9.94, b value 12.24, water-fast 4 grades of the COLOR FASTNESS staining fastnesses of washing, water-fast 3～4 grades of the COLOR FASTNESS variable color fastness of washing; 4 grades of dry fastnesses, 3～4 grades of fastness to wet rubbings.
Claims (3)
1. the method for dying silk fabric on the Suaeda salsa natural dye is characterized in that, may further comprise the steps:
Compound concentration is the Suaeda salsa natural dye dye liquor of 10～20% (o.w.f), 40～60 ℃ of dyeing temperatures; bath raio is 1: 20～50; dye liquor pH value 2～4; dyeing time 30～90 minutes, getting concentration is the mordant solution of 2～10% (o.w.f), 40～100 ℃ of mordant dyeing temperature; 30～90 minutes mordant dyeing time, mordant drops into the forward and backward or bath interpolation together of Suaeda salsa natural dye dye liquor at silk fabric.
Wherein said o.w.f: heavy to fabric.
Wherein said bath raio: the ratio of fabric quality and solution quality.
2. the method for dying silk fabric on the Suaeda salsa natural dye according to claim 1 is characterized in that, described mordant is one or more in copper sulphate, frerrous chloride, ferric sulfate, aluminum sulfate, alum, stannous chloride, the zinc sulfate.
3. the method for dying silk fabric on the Suaeda salsa natural dye according to claim 1 is characterized in that, cleans after the dyeing, dehydration, mechanical finishing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110111540 CN102220705A (en) | 2011-04-20 | 2011-04-20 | Method for dying silk fabric by using natural dye of Suaeda salsa |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110111540 CN102220705A (en) | 2011-04-20 | 2011-04-20 | Method for dying silk fabric by using natural dye of Suaeda salsa |
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| CN102220705A true CN102220705A (en) | 2011-10-19 |
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| CN 201110111540 Pending CN102220705A (en) | 2011-04-20 | 2011-04-20 | Method for dying silk fabric by using natural dye of Suaeda salsa |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102535189A (en) * | 2012-02-16 | 2012-07-04 | 武汉纺织大学 | Method for dyeing metachrome silk fabric by using parslane herb dye liquor |
| CN102587154A (en) * | 2012-02-16 | 2012-07-18 | 武汉纺织大学 | Method for dyeing silk fabrics by using purslane dye solution and bath mordant |
| CN104179039A (en) * | 2014-08-25 | 2014-12-03 | 苏州大学 | Method for dyeing silk or silk fabric by aspergillus niger spore powder |
| CN104233862A (en) * | 2013-06-17 | 2014-12-24 | 无锡市东新织造有限公司 | Process for aluminum salt pre-mordanting and after-dyeing for real silk fabric by using henna pigment |
| CN104264454A (en) * | 2014-09-27 | 2015-01-07 | 无锡市东北塘宏良染色厂 | Mordant for textiles |
| CN105780534A (en) * | 2016-03-18 | 2016-07-20 | 河南工程学院 | Process of utilizing Fructus chebulae pigment to dye silk fabric |
| CN106320001A (en) * | 2016-08-19 | 2017-01-11 | 河南工程学院 | Method for dyeing wool by myrobalan pigment |
| CN115045124A (en) * | 2022-05-24 | 2022-09-13 | 江南大学 | High-sensitivity acid-base color-changing silk fabric and preparation method thereof |
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| CN1712634A (en) * | 2005-07-21 | 2005-12-28 | 上海交通大学 | Process for dyeing silk and wool with skullcap |
| CN101204217A (en) * | 2007-12-20 | 2008-06-25 | 山东师范大学 | Method for extracting beet red pigment from Suaeda salsa |
| CN101545216A (en) * | 2009-04-30 | 2009-09-30 | 东华大学 | Dyeing method for common goldenrod herb natural dye |
| CN101914306A (en) * | 2010-08-19 | 2010-12-15 | 浙江理工大学 | Method for preparing photinia fruit natural dye and application of photinia fruit natural dye |
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2011
- 2011-04-20 CN CN 201110111540 patent/CN102220705A/en active Pending
Patent Citations (4)
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| CN1712634A (en) * | 2005-07-21 | 2005-12-28 | 上海交通大学 | Process for dyeing silk and wool with skullcap |
| CN101204217A (en) * | 2007-12-20 | 2008-06-25 | 山东师范大学 | Method for extracting beet red pigment from Suaeda salsa |
| CN101545216A (en) * | 2009-04-30 | 2009-09-30 | 东华大学 | Dyeing method for common goldenrod herb natural dye |
| CN101914306A (en) * | 2010-08-19 | 2010-12-15 | 浙江理工大学 | Method for preparing photinia fruit natural dye and application of photinia fruit natural dye |
Non-Patent Citations (1)
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Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102535189A (en) * | 2012-02-16 | 2012-07-04 | 武汉纺织大学 | Method for dyeing metachrome silk fabric by using parslane herb dye liquor |
| CN102587154A (en) * | 2012-02-16 | 2012-07-18 | 武汉纺织大学 | Method for dyeing silk fabrics by using purslane dye solution and bath mordant |
| CN102535189B (en) * | 2012-02-16 | 2014-06-04 | 武汉纺织大学 | Method for dyeing metachrome silk fabric by using parslane herb dye liquor |
| CN104233862A (en) * | 2013-06-17 | 2014-12-24 | 无锡市东新织造有限公司 | Process for aluminum salt pre-mordanting and after-dyeing for real silk fabric by using henna pigment |
| CN104179039A (en) * | 2014-08-25 | 2014-12-03 | 苏州大学 | Method for dyeing silk or silk fabric by aspergillus niger spore powder |
| CN104179039B (en) * | 2014-08-25 | 2016-01-20 | 苏州大学 | The aspergillus niger spore powder colouring method of a kind of silk or its fabric |
| CN104264454A (en) * | 2014-09-27 | 2015-01-07 | 无锡市东北塘宏良染色厂 | Mordant for textiles |
| CN105780534A (en) * | 2016-03-18 | 2016-07-20 | 河南工程学院 | Process of utilizing Fructus chebulae pigment to dye silk fabric |
| CN105780534B (en) * | 2016-03-18 | 2018-06-05 | 河南工程学院 | The technique dyed using myrobalan's pigment to silk fabric |
| CN106320001A (en) * | 2016-08-19 | 2017-01-11 | 河南工程学院 | Method for dyeing wool by myrobalan pigment |
| CN115045124A (en) * | 2022-05-24 | 2022-09-13 | 江南大学 | High-sensitivity acid-base color-changing silk fabric and preparation method thereof |
| CN115045124B (en) * | 2022-05-24 | 2023-09-08 | 江南大学 | High-sensitivity acid-base color-changing silk fabric and preparation method thereof |
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Application publication date: 20111019 |