CN105518187B - 生产大块硅碳化物的方法 - Google Patents
生产大块硅碳化物的方法 Download PDFInfo
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- CN105518187B CN105518187B CN201480049097.3A CN201480049097A CN105518187B CN 105518187 B CN105518187 B CN 105518187B CN 201480049097 A CN201480049097 A CN 201480049097A CN 105518187 B CN105518187 B CN 105518187B
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- Prior art keywords
- silicon carbide
- seed
- crucible
- precursor
- silicon
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- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B23/00—Single-crystal growth by condensing evaporated or sublimed materials
- C30B23/02—Epitaxial-layer growth
- C30B23/06—Heating of the deposition chamber, the substrate or the materials to be evaporated
- C30B23/066—Heating of the material to be evaporated
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B23/00—Single-crystal growth by condensing evaporated or sublimed materials
- C30B23/02—Epitaxial-layer growth
- C30B23/025—Epitaxial-layer growth characterised by the substrate
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
- C30B29/10—Inorganic compounds or compositions
- C30B29/36—Carbides
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Crystallography & Structural Chemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910967962.7A CN110670124B (zh) | 2013-09-06 | 2014-09-05 | 生产大块硅碳化物的方法 |
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201361874597P | 2013-09-06 | 2013-09-06 | |
| US61/874,597 | 2013-09-06 | ||
| PCT/US2014/054255 WO2015035140A1 (en) | 2013-09-06 | 2014-09-05 | Method for producing bulk silicon carbide |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910967962.7A Division CN110670124B (zh) | 2013-09-06 | 2014-09-05 | 生产大块硅碳化物的方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105518187A CN105518187A (zh) | 2016-04-20 |
| CN105518187B true CN105518187B (zh) | 2019-11-08 |
Family
ID=52624259
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201480049097.3A Active CN105518187B (zh) | 2013-09-06 | 2014-09-05 | 生产大块硅碳化物的方法 |
| CN201910967962.7A Active CN110670124B (zh) | 2013-09-06 | 2014-09-05 | 生产大块硅碳化物的方法 |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910967962.7A Active CN110670124B (zh) | 2013-09-06 | 2014-09-05 | 生产大块硅碳化物的方法 |
Country Status (7)
| Country | Link |
|---|---|
| US (2) | US10801126B2 (enExample) |
| JP (1) | JP6487446B2 (enExample) |
| KR (1) | KR102266585B1 (enExample) |
| CN (2) | CN105518187B (enExample) |
| DE (1) | DE112014004096T5 (enExample) |
| TW (2) | TWI654346B (enExample) |
| WO (1) | WO2015035140A1 (enExample) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE112014004056T5 (de) | 2013-09-06 | 2016-06-02 | Gtat Corporation | Verfahren und Apparatur zur Herstellung von Massen-Siliciumcarbid aus einem Siliciumcarbid-Vorläufer |
| US11846038B2 (en) * | 2018-08-30 | 2023-12-19 | Senic Inc. | Method of growing semi-insulating silicon carbide single crystal using dopant coated with a carbon-based material |
| CN109402731B (zh) * | 2018-10-17 | 2021-01-15 | 福建北电新材料科技有限公司 | 一种高纯半绝缘碳化硅晶体生长装置及其方法 |
| JP2020189756A (ja) * | 2019-05-17 | 2020-11-26 | 信越半導体株式会社 | 結晶成長装置及び結晶成長方法 |
| EP3760766B1 (en) | 2019-07-03 | 2022-03-09 | SiCrystal GmbH | System for efficient manufacturing of a plurality of high-quality semiconductor single crystals, and method of manufacturing same |
| EP3760765B1 (en) * | 2019-07-03 | 2022-03-16 | SiCrystal GmbH | System for horizontal growth of high-quality semiconductor single crystals, and method of manufacturing same |
| JP7434802B2 (ja) * | 2019-10-30 | 2024-02-21 | 株式会社レゾナック | 結晶成長装置及び結晶成長方法 |
| CN112160025B (zh) * | 2020-08-27 | 2021-07-16 | 露笑新能源技术有限公司 | 一种基于晶体炉的加热组件结构 |
| US20220251725A1 (en) * | 2021-02-09 | 2022-08-11 | National Chung Shan Institute Of Science And Technology | Method of growing on-axis silicon carbide single crystal by regulating silicon carbide source material in size |
| CN113652750B (zh) * | 2021-08-18 | 2022-07-12 | 山东天岳先进科技股份有限公司 | 具有环形形貌的碳化硅晶体及其制备方法和制得的衬底 |
| CN116716655B (zh) * | 2023-06-14 | 2024-04-02 | 通威微电子有限公司 | 生长高质量碳化硅晶体的装置、方法及碳化硅晶体 |
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| JPH06316499A (ja) * | 1993-04-30 | 1994-11-15 | Sharp Corp | 炭化珪素単結晶の製造方法 |
| JP2001294413A (ja) * | 2000-04-11 | 2001-10-23 | Toyota Motor Corp | カーボンナノチューブの製造方法および多孔質SiC材料の製造方法および多孔質SiC材料 |
| CN1570225A (zh) * | 2003-04-24 | 2005-01-26 | 奥克麦蒂克有限公司 | 通过气相淀积制备单晶的设备和方法 |
| CN1717508A (zh) * | 2003-07-31 | 2006-01-04 | Si晶体股份公司 | 用于有气体可渗透坩埚壁的ain单晶生产的方法和设备 |
| CN101061262A (zh) * | 2004-10-04 | 2007-10-24 | 格里公司 | 低1c螺旋位错3英寸碳化硅晶片 |
| WO2008014446A2 (en) * | 2006-07-28 | 2008-01-31 | Caracal, Inc. | Sintered metal components for crystal growth reactors |
| CN101580964A (zh) * | 2008-05-12 | 2009-11-18 | 中国科学院物理研究所 | 一种用于生长高质量碳化硅晶体的籽晶托 |
| JP2009280431A (ja) * | 2008-05-21 | 2009-12-03 | Bridgestone Corp | 炭化珪素単結晶の製造方法 |
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| CN102187019A (zh) * | 2008-10-15 | 2011-09-14 | 新日本制铁株式会社 | 碳化硅单晶和碳化硅单晶晶片 |
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| CN102596804A (zh) * | 2009-09-15 | 2012-07-18 | Ii-Vi有限公司 | SiC单晶的升华生长 |
| CN202440568U (zh) * | 2012-01-17 | 2012-09-19 | 山东天岳先进材料科技有限公司 | 一种用于生长碳化硅晶棒的石墨坩埚 |
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-
2014
- 2014-09-05 CN CN201480049097.3A patent/CN105518187B/zh active Active
- 2014-09-05 KR KR1020167008933A patent/KR102266585B1/ko active Active
- 2014-09-05 DE DE112014004096.7T patent/DE112014004096T5/de active Pending
- 2014-09-05 JP JP2016540410A patent/JP6487446B2/ja active Active
- 2014-09-05 CN CN201910967962.7A patent/CN110670124B/zh active Active
- 2014-09-05 US US14/478,432 patent/US10801126B2/en active Active
- 2014-09-05 WO PCT/US2014/054255 patent/WO2015035140A1/en not_active Ceased
- 2014-09-09 TW TW103130958A patent/TWI654346B/zh active
- 2014-09-09 TW TW108100545A patent/TWI690627B/zh active
-
2020
- 2020-10-09 US US17/067,040 patent/US11505876B2/en active Active
Patent Citations (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH06316499A (ja) * | 1993-04-30 | 1994-11-15 | Sharp Corp | 炭化珪素単結晶の製造方法 |
| JP2001294413A (ja) * | 2000-04-11 | 2001-10-23 | Toyota Motor Corp | カーボンナノチューブの製造方法および多孔質SiC材料の製造方法および多孔質SiC材料 |
| CN1570225A (zh) * | 2003-04-24 | 2005-01-26 | 奥克麦蒂克有限公司 | 通过气相淀积制备单晶的设备和方法 |
| CN1717508A (zh) * | 2003-07-31 | 2006-01-04 | Si晶体股份公司 | 用于有气体可渗透坩埚壁的ain单晶生产的方法和设备 |
| CN101061262A (zh) * | 2004-10-04 | 2007-10-24 | 格里公司 | 低1c螺旋位错3英寸碳化硅晶片 |
| WO2008014446A2 (en) * | 2006-07-28 | 2008-01-31 | Caracal, Inc. | Sintered metal components for crystal growth reactors |
| CN101580964A (zh) * | 2008-05-12 | 2009-11-18 | 中国科学院物理研究所 | 一种用于生长高质量碳化硅晶体的籽晶托 |
| JP2009280431A (ja) * | 2008-05-21 | 2009-12-03 | Bridgestone Corp | 炭化珪素単結晶の製造方法 |
| CN102187019A (zh) * | 2008-10-15 | 2011-09-14 | 新日本制铁株式会社 | 碳化硅单晶和碳化硅单晶晶片 |
| WO2010111473A1 (en) * | 2009-03-26 | 2010-09-30 | Ii-Vi Incorporated | Sic single crystal sublimation growth method and apparatus |
| CN102596804A (zh) * | 2009-09-15 | 2012-07-18 | Ii-Vi有限公司 | SiC单晶的升华生长 |
| CN101985773A (zh) * | 2009-11-05 | 2011-03-16 | 新疆天科合达蓝光半导体有限公司 | 一种籽晶处理方法和生长碳化硅单晶的方法 |
| CN102414349A (zh) * | 2009-11-30 | 2012-04-11 | 住友电气工业株式会社 | 制造单晶的方法 |
| CN102134743A (zh) * | 2009-12-25 | 2011-07-27 | 株式会社电装 | 碳化硅单结晶的制造装置和制造方法 |
| CN102534763A (zh) * | 2012-01-17 | 2012-07-04 | 山东天岳先进材料科技有限公司 | 一种物理气相沉积法生长大尺寸碳化硅单晶的石墨坩埚及其应用 |
| CN202440568U (zh) * | 2012-01-17 | 2012-09-19 | 山东天岳先进材料科技有限公司 | 一种用于生长碳化硅晶棒的石墨坩埚 |
Also Published As
| Publication number | Publication date |
|---|---|
| TW201920784A (zh) | 2019-06-01 |
| US10801126B2 (en) | 2020-10-13 |
| CN110670124A (zh) | 2020-01-10 |
| TW201522726A (zh) | 2015-06-16 |
| WO2015035140A1 (en) | 2015-03-12 |
| JP6487446B2 (ja) | 2019-03-20 |
| TWI654346B (zh) | 2019-03-21 |
| US20210032770A1 (en) | 2021-02-04 |
| CN110670124B (zh) | 2021-07-30 |
| US20150068445A1 (en) | 2015-03-12 |
| KR102266585B1 (ko) | 2021-06-18 |
| US11505876B2 (en) | 2022-11-22 |
| DE112014004096T5 (de) | 2016-06-23 |
| TWI690627B (zh) | 2020-04-11 |
| KR20160050086A (ko) | 2016-05-10 |
| JP2016531836A (ja) | 2016-10-13 |
| CN105518187A (zh) | 2016-04-20 |
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