CN104027293B - A kind of skin-lightening cosmetic and preparation method thereof - Google Patents
A kind of skin-lightening cosmetic and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a kind of skin-lightening cosmetics and preparation method thereof.The present invention is that mainly have rice bran extract, gadol extract, ginkgo biloba p.e, tea polyphenols, lemon juice concentrate, chitosan, kudzu root extract, konjaku powder, floral disc of sunflower extract, sunflower seed benevolence extract, gleditsia sinensis benevolence, hemicellulose, honey using various plants composition as primary raw material；In addition, also containing a small amount of glycerine, 1,3 propylene glycol, saualane, Sodium Hyaluronate, carbomer, triethanolamine, allantoin, nano-titanium dioxide, collagen protein powder, antiseptic, the different monooctyl ester of ferulic acid and glutathione.The composition can be used in whitening formula, has effects that skin whitening, moisturizing, antibacterial anti-inflammatory, removes free radical, inhibit melanin to be formed, inhibit dopachrome interconvertible enzyme and tyrosinase activity.
Description
Technical field
The present invention relates to natural products to utilize field, and in particular to a kind of skin-lightening cosmetic and preparation method thereof.
Background technology
It is everyone person's character to pursue beautiful appearance, and the state of skin and appearance are wherein important composition portions
Part, healthy and pale skin is that everybody is pursued.For this purpose, the demand to skin-lightening cosmetic occupies always various cosmetics demands
First of.The product that national daily use chemicals industry is related to whitening at present accounts for one third, and there are more than 3800 daily chemical industry, every family in China
Whitening product is no less than 10 sections substantially, and some even accounts for product proportion 80%, and just there is more than 1300 cosmetics life in only Guangdong Province
Produce enterprise.
Skin histology is the first layer protective barrier of people, and broad sense can be divided into epidermis, corium and subcutaneous tissue.The face of skin
Color is mainly determined according to quantity, size and distribution containing melanin in Skin Cell.
The problem of for skin-whitening, depends primarily on the ability of melanocyte synthesis of melanin.In the epidermis base of people
Bottom iuntercellular, is dispersed with melanocyte, and the tyrosinase that it contains can be by oxidizing tyrosine at polysaccharide, and tyrosinase is
A kind of polyphenol enzyme, belongs to redox enzymes, and centre can finally generate melanin using a series of metabolic process.
Melanin production is more, and skin is pitch-darker；Conversely, then skin is more pale.Tyrosinase has unique dual catalytic work(
Can, it is the key enzyme of B16 cell in organism, the aging with people has substantial connection.Its abnormal overexpression can lead to human body
Pigmentation disease.Tyrosinase inhibitor can treat common chromatodermatosis such as freckle, yellowish-brown at present
Spot, senile plaque.So the ursin in popular skin-lightening cosmetic, vitamin C derivatives, kojic acid and its spreading out currently on the market
Chinese medical extracts such as biology, green-tea extract, licorice etc. are tyrosinase inhibitor, mainly by inhibiting junket ammonia
The activity of sour enzyme and reach inhibition B16 cell, and then play skin whitening effect.
In a kind of lightening compositions of patent CN201010214873.4, a kind of lightening compositions, the composition are disclosed
Contain mulberry bark extract, camomile extract, gadol extract, grape seed extract, licorice, the extraction of chicken mulberry
Object, ursin, kojic dipalmitate, niacinamide, tetrahydro curcumin, moisturizer and preservative, effective whitening in the invention
Ingredient can inhibit the activity of tyrosinase, block melanin transport, inhibit melanin to be formed, can be used for skin-lightening cosmetic
In, safely and effectively.In a kind of whitening plant extract combinations of patent CN201310210916.5 and its answering in cosmetics
In, a kind of plant composition with whitening function and its application in skin-lightening cosmetic, the plant of the invention are disclosed
Composition is extracted by mulberry bark extract, licorice, peony extract, Flos Bombacis Malabarici extract, angelica extract, the root bark of tree peony
Object compounds.The plant composition of the invention can be used in whitening formula, has and inhibits tyrosinase activity, removes free radical
With the function of skin whitening.In a kind of skin-lightening cosmetics of patent CN201210511695.0 and preparation method thereof, one is disclosed
Kind skin-lightening cosmetic, the composition by weight percentage, are made of the following raw material：50~70wt% cucumber seeds oil, 15~
25wt% St. john's worts oil, 15~25wt% pot marigold oils, preparation method are：By 50~70wt% cucumber seeds oil, 15~25wt%
St. john's wort oil, 15~25wt% pot marigold oils, mix at a temperature of 20~25 DEG C, stir evenly to get product；U.S. of the invention
Albefaction cosmetic, is made by crude vegetal, green, safety, non-stimulated to skin.
For skin-lightening cosmetic, China has abundant animal and plant resource, modern biotechnology can be made full use of to carry
The active constituent in animals and plants, the research of comprehensive lightening mechanism, then scientific compatibility are taken, is brought out the best in each other, can be obtained various natural
Cosmetics, to achieve the effect that skin whitening, this is to the abundant of China's whitening cosmetic product and pushes China's cosmetic industry all
It has important practical significance.
In above-mentioned patented method, use raw material for rice bran extract, ginkgo biloba p.e, tea polyphenols, lemon juice, shell
Glycan, kudzu root extract, konjaku powder, floral disc of sunflower extract, sunflower seed benevolence extract, gleditsia sinensis benevolence, hemicellulose and
The animal and plant extracts reflex such as honey there are no report with skin-lightening cosmetic is prepared at the national level by document and patent retrieval
Road.
Existing skin-lightening cosmetic is primarily present problems with and defect：
（1）There is the irritation to skin in part skin-lightening cosmetic, because often containing acid, alkali, salt, table in skin-lightening cosmetic
The chemically ingredient such as face activating agent.These chemical substances act on after mucous membrane of skin, organ etc. through often causing irritation skin
Skin lesion, also known as irritation contact dermatitis, are a kind of most commonly seen skin lesion and skin caused by skin-lightening cosmetic
The acute inflammation that part occurs rapidly.In addition, the group branch also in the whitening product of part is deposited in body, can not excrete
It goes, can lead to that blood is unsmooth, aging phenomenon of skin, generate dark sore, color spot, skin sallow, wrinkle increase, relaxation, and skin is new
Old metabolism slows down.It can even be entered by placenta in fetus body, endanger the development of fetal central nervous system, cause harmful effect.
（2）Product stability is low, many anti-oxidant chemical efficiency ingredients of skin-lightening cosmetic, all carries one or several insatiable hungers
And double bond, these functional components because its stronger reproducibility can play the effect of inhibition melanin in skin, but are being made
When cosmetics finished product, then because its exposure in air more than the moon even a couple of days, just under the action ofs oxygen, light, metal ion etc. not
Saturated bond deactivation, loses whitening active, to keep whitening effect poor.
（3）Whitening approach is single, and melanin is generated by the chemical reaction of a series of complex, can have a plurality of approach to press down
Make its generation.And the whitening product overwhelming majority on Cosmetic Market is and every only based on tyrosinase inhibitor at present
Year finds such new compound with faster speed.But various whitening additives can only all inhibit an approach, and fail complete
Play the role of to face inhibiting melanin.
（4）Existing whitening cosmetic product is to embody effect, intentionally adds a variety of chemical compositions and uses hormone, though to skin
Skin has tender white effect, it is possible to reduce wrinkle, but some Management of Cosmetics Enterprises can add taboo regulated substance in its product（Such as antibiotic
Class）.These contain hormone cosmetics be used for a long time after, can make skin to hormone generate rely in addition systemic damage, one
Denier, which deactivates, there is also the reaction of the hormonal dependents scytitis such as pigmentations such as erythema, papule, exudation, telangiectasis.
According to above-mentioned deficiency, which is mainly improved optimization from the following aspect：
The first, using pure natural on-chemically modified or synthesis composition
It is proved that there is significant white-skinned face function there are many whitening active ingredients, but due to its existing irritation, shakiness
The various defects such as qualitative significantly limit application and effect of product.Therefore, there is preferable white-skinned face function in guarantee product
Under the premise of reduce application to these compounds to the greatest extent, the appearance for causing the above problem can be significantly improved.
The second, the composition for generating stimulation to skin is not added, and ensures its safety
Stimulate sex chromosome mosaicism for existing for the whitening active ingredients of part, can in prescription more additions it is pure natural, it is mild and in
Property animal and plant extracts, make product while reaching white-skinned face function, irritation reduce, be really achieved the mesh of safe whitening
's.
Third, combination different approaches, comprehensive skin whitening
Whitening active ingredients are subjected to scientific composition, it is multi-pronged, inhibit melanogenesis from different approaches, is finally reached complete
The purpose of face whitening.By inhibiting melanin production, inhibits melanin to transmit, smash the approach such as melanin and cleaning cortex to reach
To the purpose of skin whitening.
Invention content
The purpose of the present invention is obtain one kind by using Yunnan and some living resources extracts of other local characteristics
Skin-lightening cosmetic nonirritant to human skin, whitening effect is good, safe, the cosmetics press the hundred of composition gross mass
Score meter contains rice bran extract 3-5%, gadol extract 0.2-1%, ginkgo biloba p.e 0.2-1%, lemon juice 0.2-
0.5%, chitosan 0.2-2%, kudzu root extract 0.2-1%, konjaku powder 0.2-2%, floral disc of sunflower extract 0.3-2%, Xiang
Althea seed kernel extract 0.3-2%, gleditsia sinensis benevolence 0.5-3%, hemicellulose 0.3-2%, honey 0.3-2%.
Also contain other auxiliary materials in the present composition, constituent and its mass percent are：Rice bran extract 3-
5%, gadol extract 0.2-1%, ginkgo biloba p.e 0.2-1%, tea polyphenols 0.02-0.4%, lemon juice 0.4-2%, shell are poly-
Sugared 0.2-2%, kudzu root extract 0.2-1%, konjaku powder 0.2-2%, floral disc of sunflower extract 0.3-2%, sunflower seed benevolence carry
Take object 0.3-2%, gleditsia sinensis benevolence 0.5-3%, hemicellulose 0.3-2%, honey 0.3-2%, glycerine 2-5%, 1,3- propylene glycol 2-4%, angle
Shark alkane 2-6%, Sodium Hyaluronate 0.05-2%, carbomer 0.5-1.0%, triethanolamine 0.5-1.0%, allantoin 0.1-0.3%, two
The different monooctyl ester 0.1-2% of titanium oxide 0.1-1%, collagen protein powder 0.8-3%, antiseptic 0.1-0.2%, ferulic acid, glutathione 1-2%,
Remaining as water.
Sunflower seed benevolence extract is by after immature sunflower seed benevolence drying and crushing, with ethyl alcohol, methanol in the present invention
Or acetone reflux extracts crushed material, extracting solution is made after being concentrated and dried, and the mass percent concentration of ethyl alcohol, methanol or acetone is
70-80%。
The sunflower seed floral disc extract is after being in florescence immature floral disc of sunflower drying and crushing, to use second
Alcohol, methanol or acetone reflux extract crushed material, and extracting solution is made after being concentrated and dried, ethyl alcohol, methanol or acetone mass percent
A concentration of 30-50%.
Heretofore described rice bran extract, gadol extract, ginkgo biloba p.e, tea polyphenols, chitosan, pueraria lobata
Extract, konjaku powder, gleditsia sinensis benevolence, honey, glycerine, 1,3- propylene glycol, saualane, Sodium Hyaluronate, carbomer, three ethyl alcohol
The different monooctyl ester of amine, allantoin, titanium dioxide, collagen protein powder, antiseptic, ferulic acid, glutathione are conventional commercial product.
Heretofore described lemon juice be lemon juicing after filter to get filtrate.
Heretofore described hemicellulose can by it is commercially available or with reference to Zhang Baikun, Zhang Meiyun et al. in periodical " Heilungkiang
The method separation and Extraction described in document " hemicellulose extractive technique and Development of Comprehensive Utilization " in papermaking ".
Another object of the present invention is to provide a kind of preparation method of skin-lightening cosmetic, includes the following steps：
（1）Glycerine, rice bran extract and 1,3- propylene glycol is added in Sodium Hyaluronate, allantoin, the different monooctyl ester of ferulic acid
It mixes in oil phase, stirs and evenly mixs for use；
（2）By gadol extract, ginkgo biloba p.e, tea polyphenols, kudzu root extract, floral disc of sunflower extract, to
Day althea seed kernel extract, titanium dioxide, collagen protein powder and glutathione mixing, by solid-to-liquid ratio 1：The ratio of 5-15 is in mixture
Water is added to stir 30-120min, mixing speed 50-500r/min, for use；
（3）After konjaku powder and hemicellulose are mixed, by solid-to-liquid ratio 1：The ratio of 5-15 adds water and adds in the mixture
Heat to temperature is that 70-90 DEG C of stirring is for use to being completely dissolved, mixing speed 50-200r/min；
（4）After gleditsia sinensis benevolence is dried, it is milled to more than 200 mesh, by solid-to-liquid ratio 1：The ratio of 5-15 is put into 40-50 DEG C of warm water
Middle to impregnate 24 hours or more, filtering and collecting filter liquid is for use；
（5）Chitosan lemon juice is pressed into solid-to-liquid ratio 1：2-6 fully dissolves, for use；
（6）By step（2）, step（3）, step（4）And step（5）Step is added in the mixture of middle acquisition（1）In it is mixed
It closes in object, is uniformly mixed under the conditions of speed of agitator 30-400r/min；
（7）In step（6）Saualane is added in the mixture of acquisition to stir evenly, then adds carbomer and three ethyl alcohol
Amine is uniformly mixed, and is eventually adding honey and antiseptic, is added surplus water and is uniformly mixed；
（8）By step（7）The mixture of middle acquisition is pumped into homogenizer, is vacuumized in -0.04--0.08MPa, stirring, equal
After matter 5-10min, homogenizer rotating speed be 1000-3000r/min；
（9）To step（8）The mixture of middle acquisition carries out closed ageing at normal temperatures, and digestion time 12-36h has been aged
At rear up to skin-lightening cosmetic.
The advantages of the method for the present invention and technique effect：
1, the product obtained in the present invention makes sunflower, rice bran, rhodiola root, ginkgo leaf, lemon, chitosan, pueraria lobata, evil spirit
The animal and plant extracts such as taro, gleditsia sinensis, hemicellulose and honey obtain high value added utilization, are a kind of natural whiting cosmetics.
2, heretofore described cosmetics and preparation method thereof are with technique is relatively simple, cost is relatively low, compound emulsion
Feature with obvious effects afterwards, safety is good.
3, the cosmetics can be used as the whitening products such as lotion, essence, lotion.
Specific implementation mode
Below by embodiment, invention is further described in detail, but the scope of the present invention is not limited in described
Hold, the method used unless otherwise specified in embodiment is conventional method, and the reagent used is routine unless otherwise specified
Commercial reagent.
Embodiment 1：This skin-lightening cosmetic constituent and its mass percent are rice bran extract 3%, gadol extract
0.2%, ginkgo biloba p.e 0.2%, tea polyphenols 0.02%, lemon juice 0.8%, chitosan 0.2%, kudzu root extract 0.2%, konjaku
Fine powder 0.2%, floral disc of sunflower extract 0.3%, sunflower seed benevolence extract 0.3%, gleditsia sinensis benevolence 0.5%, hemicellulose 0.3%, bee
Honey 0.3%, glycerine 2%, 1,3- propylene glycol 2%, saualane 2%, Sodium Hyaluronate 0.1%, carbomer 0.5%, triethanolamine 0.5%, urine
The different monooctyl ester 2% of Bursin 0.1%, titanium dioxide 0.1%, collagen protein powder 0.8%, antiseptic Phenoxyethanol 0.1%, ferulic acid, gluathione
Peptide 1%, remaining as water.
The preparation method of the said goods is as follows：
（1）Glycerine 2%, rice bran extraction is added in Sodium Hyaluronate 0.1%, allantoin 0.1% and the different monooctyl ester 0.1% of ferulic acid
In the mixing oil phase of object 3% and 1,3-PD 2%, stir and evenly mix for use；
（2）By gadol extract 0.2%, ginkgo biloba p.e 0.2%, tea polyphenols 0.02%, kudzu root extract 0.2%, to
Day sunflower disk extract 0.3%, sunflower seed benevolence extract 0.3%, nano-titanium dioxide 0.1%, collagen protein powder 0.8% and paddy Guang
Sweet peptide 1% is added to the container, then presses solid-to-liquid ratio 1：15 are added water, under conditions of low whipping speed 50r/min, time 30min, stir
It mixes uniformly for use；
（3）Konjaku powder 0.2% and hemicellulose 0.3% are added to the container, then press solid-to-liquid ratio 1：15 are added water, then add
Heat to temperature is 70 ° of С, and under conditions of mixing speed 50r/min, time 10min, stirring is for use to being completely dissolved；
（4）After taking gleditsia sinensis benevolence 0.5% to dry, 300 mesh are milled to, solid-to-liquid ratio 1 is pressed in 40 ° of С warm water：15 impregnate, the time
It is 24 hours, for use with 200 mesh filter screen filtering and collecting filter liquids；
（5）Take chitosan 0.2% with lemon juice 0.8% by solid-to-liquid ratio 1：4 fully dissolvings, after it is for use；
（6）By step 2）, step 3）, step 4）With step 5）Step 1 is added in the solution or mixture of middle acquisition）In
It mixes in oil phase, is uniformly mixed at time 0.5h, speed of agitator 30r/min；
（7）In step 6）Saualane 2% is added in the mixture of middle acquisition to be uniformly mixed, adds carbomer 0.5%
It is uniformly mixed with triethanolamine 0.5%；
（9）In step 8）Honey 0.3% and antiseptic Phenoxyethanol 0.1% are added in the mixture of middle acquisition, then adds surplus
Remaining water is uniformly mixed；
（10）By step 9）The mixture of middle acquisition is pumped into homogenizer, is vacuumized in -0.04MPa, stirring, homogeneous 5min
Afterwards, homogenizer rotating speed is 1000r/min；
（11）To step 10）The mixture of middle acquisition carries out closed ageing, digestion time 12h at normal temperatures, and ageing is completed
After can be obtained a kind of skin-lightening cosmetic.
The index of correlation after using the present embodiment method is measured using common detection methods, wherein tyrosine enzyme activity
Property assay method use Mushroom tyrosinase DOPA rate oxidizing process, respectively with spectrophotometry measure superoxide anion from
By the scavenging effect of base and to Hydroxyl Radical Scavenging, specific targets data are as follows：
| Experimental project | Tyrosinase vigor inhibits | Scavenging effect to ultra-oxygen anion free radical | To hydroxyl radical free radical scavenging effect |
| Inhibiting rate（%） | 85.8 | 34.6 | 53.2 |
In addition, to its PFA value (sun care preparations long wave ultraviolet protection index) and spf value（Sun protection factor）It is surveyed
Fixed, PFA values and spf value are respectively PFA values 7, SPF15.
Testing result shows that the skin-lightening cosmetic, which is used for a long time, can effectively inhibit the activity of tyrosinase and remove freely
The effect of base effectively slows down the aggregate velocity of melanin, and the absorption and antitan agent to ultraviolet light have good effect, simultaneously
Also have the function of moisturizing, moisturizing, skin care and brilliant white, and there is safety and nonirritant to human skin.
Claims (7)
1. a kind of skin-lightening cosmetic, it is characterised in that contain based on the percentage of composition gross mass：Rice bran extract 3~5%,
Gadol extract 0.2~1%, ginkgo biloba p.e 0.2~1%, tea polyphenols 0.02~0.4%, lemon juice 0.4~2%, shell are poly-
Sugar 0.2~2%, kudzu root extract 0.2~1%, konjaku powder 0.2~2%, floral disc of sunflower extract 0.3~2%, sunflower seed
Benevolence extract 0.3~2%, gleditsia sinensis benevolence 0.5~3%, hemicellulose 0.3~2%, honey 0.3~2%, glycerine 2~5%, 1,3- the third two
Alcohol 2~4%, saualane 2~6%, Sodium Hyaluronate 0.05~2%, carbomer 0.5~1.0%, triethanolamine 0.5~1.0%, allantois
The different monooctyl ester of element 0.1~0.3%, titanium dioxide 0.1~1%, collagen protein powder 0.8~3%, antiseptic 0.1~0.2%, ferulic acid 0.1
~2%, glutathione 1~2%, remaining as water.
2. skin-lightening cosmetic according to claim 1, it is characterised in that：Sunflower seed benevolence extract is by immature to day
After althea seed kernel drying and crushing, crushed material is extracted with ethyl alcohol, methanol or acetone reflux, extracting solution is made after being concentrated and dried, ethyl alcohol, first
The mass percent concentration of alcohol or acetone is 70~80%.
3. skin-lightening cosmetic according to claim 1, it is characterised in that：Sunflower seed floral disc extract is will to be in the florescence not
After ripe floral disc of sunflower drying and crushing, crushed material is extracted with ethyl alcohol, methanol or acetone reflux, extracting solution is made after being concentrated and dried
, the mass percent concentration of ethyl alcohol, methanol or acetone is 30~50%.
4. skin-lightening cosmetic according to claim 1, it is characterised in that：Antiseptic is in hydantoins, Phenoxyethanol, propolis
One kind or arbitrary ratio mixture.
5. skin-lightening cosmetic according to claim 1, it is characterised in that：Rice bran extract, gadol extract, ginkgo leaf carry
Object, tea polyphenols, hemicellulose is taken to need to carry out adsorption bleaching, adsorbing and removing pigment, metal ion and other impurities before use.
6. skin-lightening cosmetic according to claim 5, it is characterised in that：To rice bran extract, gadol extract, ginkgo leaf
Extract, tea polyphenols, hemicellulose carry out adsorption bleaching, are made using carclazyte, activated carbon, macroreticular resin, attapulgite and zeolite
For adsorbent.
7. the preparation method of skin-lightening cosmetic according to claim 1, it is characterised in that including following processing steps：
（1）Sodium Hyaluronate, allantoin, the different monooctyl ester of ferulic acid are added to the mixing of glycerine, rice bran extract and 1,3- propylene glycol
In oil phase, stir and evenly mix for use；
（2）By gadol extract, ginkgo biloba p.e, tea polyphenols, kudzu root extract, floral disc of sunflower extract, sunflower
Seed benevolence extract, titanium dioxide, collagen protein powder and glutathione mixing, by solid-to-liquid ratio 1：5~15 ratio adds in mixture
Water stirs 30~120min, 50~500r/min of mixing speed, for use；
（3）After konjaku powder and hemicellulose are mixed, by solid-to-liquid ratio 1：5~15 ratio adds water and is heated in the mixture
Temperature is that 70~90 DEG C of stirrings are for use to being completely dissolved, 50~200r/min of mixing speed；
（4）After gleditsia sinensis benevolence is dried, it is milled to more than 200 mesh, by solid-to-liquid ratio 1：5~15 ratio is put into 40~50 DEG C of warm water
Impregnate 24 hours or more, filtering and collecting filter liquid is for use；
（5）Chitosan lemon juice is pressed into solid-to-liquid ratio 1：2~6 fully dissolvings, for use；
（6）By step（2）, step（3）, step（4）And step（5）Step is added in the mixture of middle acquisition（1）In mixture
In, it is uniformly mixed under the conditions of 30~400r/min of speed of agitator；
（7）In step（6）Saualane is added in the mixture of acquisition to stir evenly, then adds carbomer and triethanolamine stirs
It mixes uniformly mixed, is eventually adding honey and antiseptic, adds surplus water and be uniformly mixed；
（8）By step（7）The mixture of middle acquisition is pumped into homogenizer, is vacuumized in -0.04~-0.08MPa, stirring, homogeneous 5
~10min, homogenizer rotating speed are 1000~3000r/min；
（9）To step（8）The mixture of middle acquisition carries out closed ageing, 12~36h of digestion time, after the completion of ageing at normal temperatures
Up to skin-lightening cosmetic.
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