CN108498380A - A kind of hops facial mask and preparation method thereof - Google Patents
A kind of hops facial mask and preparation method thereof Download PDFInfo
- Publication number
- CN108498380A CN108498380A CN201810537191.3A CN201810537191A CN108498380A CN 108498380 A CN108498380 A CN 108498380A CN 201810537191 A CN201810537191 A CN 201810537191A CN 108498380 A CN108498380 A CN 108498380A
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- Prior art keywords
- hops
- facial mask
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
Abstract
The invention discloses a kind of hops facial masks, including hops extracting solution 6%~10%, polyvinyl acetate lotion 8~12%, polyvinyl alcohol 8~12%, olive oil 2~4%, glycerine or propylene glycol 6%~8%, zinc oxide 6~8%, kaolin 5~6%, ethyl alcohol 3~4%, Purified Water 40~50%, fragrance 1~3% and preservative 1~3%.The invention also discloses the preparation methods of hops facial mask, first soak polyvinyl alcohol with ethyl alcohol, and kaolin, zinc oxide, Purified Water mixing is added；Mixed solution is heated, then hops extracting solution, polyvinyl acetate lotion, olive oil and other compositions are added, after stirring is stood；Glycerine or propylene glycol, fragrance and preservative are added, paste facial mask is made.Hops facial mask has anti-inflammatory, antibacterial, moisturizing, block, crease-resistant and other effects, and hops constituents extracting method is effective, and facial mask preparation method is simple.
Description
Technical field
The present invention relates to a kind of skin care item, more particularly to a kind of hops facial mask and preparation method thereof.
Background technology
Facial mask market has become that China's daily use chemicals industry is fastest-rising one of to segment market at present.Facial mask utilizes and is covered in face
The of short duration time in portion is temporarily isolating extraneous air and pollution, improves skin temperature and expansion pore, promote sweat gland secretion with it is new
Old metabolism makes skin oxygen content rise.In the prior art be used for beauty mask product there are many shortcomings, soaking effects
Difference, hard texture are applied uncomfortable on the face, and chemical additive is more, be easy it is hardened be hardened, not environmentally can not pollution degradation environment etc..With
The development of medical cosmetology industry, application of the natural active matter in cosmetics becomes a kind of new trend.Hops
It is that the active ingredient of hops is introduced into cosmetics by Chinese herbal medicine cultivated plant range in China, has complied with cosmetics and returned
Return natural trend, while pollution-free, without side-effects, the exploitation for the development in traditional Chinese medicine cosmetics product and market is played
Positive reference role.
The ingredient of hops includes mainly hop oil, hop resin, polyphenols etc..Polyphenol in hops is carried
It takes, such as common tea polyphenols, water can be used as solvent.However, polyphenol can with the substance in plant, such as protein,
The compound that the formation such as polysaccharide are stablized, Extraction solvent not only needs have good dissolubility to polyphenol, and being also required to will be more
The hydrogen bond of phenolic compound is broken, to improve the recovery rate of alcohols.Extraction using water as polyphenol, required energy consumption is big, when
Between it is long, efficiency is low.Compound of polysaccharide is usually with free state and combination in hops, mainly with the phase interaction of hydrogen bond and group
With condensing together and existing mechanical crushing method is difficult that cell is carried out to effectively broken, chemical disruption methods, for example, by using dilute
Acid or diluted alkaline can make polysaccharide that degradation occur and change its space structure, it is caused to lose activity, thus these methods are difficult to obtain
Ideal extraction effect.
Invention content
In view of the above-mentioned defects in the prior art, the present invention provides a kind of hops facial mask and preparation method thereof, the beer
Flower facial mask has anti-inflammatory, antibacterial, moisturizing, block, crease-resistant and other effects, and the dispersion of facial mask appearance is uniform, easily applies exhibition, fine and smooth, and fragrance is bright
Aobvious, viscosity is appropriate, skin wet, good absorbing, and hops constituents extracting method is effective, and facial mask preparation method is simple.
Hops facial mask in the present invention, is specifically made from the following raw materials in parts by weight：Hops extracting solution 6%~
10%, polyvinyl acetate lotion 8~12%, polyvinyl alcohol 8~12%, olive oil 2~4%, glycerine or propylene glycol 6%~
8%, zinc oxide 6~8%, kaolin 5~6%, ethyl alcohol 3~4%, Purified Water 40~50%, fragrance 1~3% and preservative 1~
3%.
Further, in hops facial mask can also contain vitamin C 1~2%, vitamin E 1~2%, hexadecanol 2~
3% and lanolin 3~4%.
Further, lupulus extract includes polyphenols, flavonoids and polysaccharide compound.
Further, lupulus extract includes at least one of Hop polyphenols or tannic acid, further includes that isopentene group is looked into
Youngster's ketone, at least one of flavonols or flavonoid glycoside.
Further, lupulus extract may also include protein, fat, cellulose and trace element.
The invention also discloses a kind of method being used to prepare above-mentioned hops facial mask, this method includes：It will gather first
Vinyl alcohol is soaked with ethyl alcohol, and kaolin, zinc oxide, Purified Water mixing is added；Mixed solution is heated to 75 DEG C~80 DEG C, then will
It after hops extracting solution, polyvinyl acetate lotion, olive oil and other compositions are added, is uniformly mixed, stands 12~15
Hour；Glycerine or propylene glycol, fragrance and preservative are added, stirs evenly and paste facial mask is made.
Further, wherein the extracting method of hops extracting solution is：After sample is crushed, 40 mesh sieve is crossed；It takes suitable
The sample of amount, is added into organic solvent；It is filtered after a certain period of time using being heated to reflux device and extracting, obtains Polyphenols
Compound.
Further, the organic solvent concentration that uses of extraction polyphenol compound is the compound of 55%~60% acetone and water
System, reaction temperature are 60~65 DEG C, solid-liquid ratio 1：15~1：18, extraction time is 80~100 minutes.
Further, the organic solvent that uses of extraction flavonoids compound is the compound of a concentration of 40~50% ethyl alcohol and water
System, reaction temperature are 60~65 DEG C, solid-liquid ratio 1：20, extraction time is 90~120 minutes.
Further, the organic solvent for extracting polysaccharose substance is the compound system of a concentration of 65~70% ethyl alcohol and water,
Reaction temperature is 70~75 DEG C, solid-liquid ratio 1：20~1：25, extraction time is 100~120 minutes.
The present invention can realize following advantageous effect compared with prior art：
Facial mask containing hop components, hops contain natural wine aroma, can reduce the dosage of natural flavor；Simultaneously
With anti-inflammatory, antibacterial, moisturizing, block, crease-resistant and other effects, and the skin diseases such as acne, blackhead, seborrhea can be prevented；In addition
The plant polyphenol of extraction can prevent the oxide of peroxidating unsaturated fatty acid, have very strong antitumor, anti-oxidant, antibacterial,
Eliminate the functions such as interior free yl.
The extracting method of polyphenols in the present invention can carry out polyphenol good dissolving, and effectively realize more
The hydrogen bond of phenolic compound is broken, to improve the recovery rate of alcohols；The extraction of flavones can be extracted effectively in hops
Distinctive compound isopentenyl base looks into youngster's ketone, and at low cost, and flavonoids extraction efficiency is high, and extract quality is good, prevents flavones
Phenomena such as extraction process is degraded.Extraction method of polysaccharides in the present invention can effectively destroy between sugar chain and other substances
Covalent bond, novel technology for extracting is simple and convenient, extraction efficiency is high.
Description of the drawings
Fig. 1 is the influential effect experimental result that different ethanol concentration extracts hop polyphenols
Fig. 2 is the influential effect experimental result that different feed liquid compares hop polyphenols extraction
Specific implementation mode
Below in conjunction with specific embodiment, the present invention is described in further detail.
Hops facial mask includes hops extracting solution 6%~10% in the present embodiment, and polyvinyl acetate lotion 8~
12%, polyvinyl alcohol 8~12%, olive oil 2~4%, glycerine or propylene glycol 6%~8%, zinc oxide 6~8%, kaolin 5~
6%, ethyl alcohol 3~4%, Purified Water 40~50% can also contain suitable fragrance and preservative.Can also it contain in hops facial mask
Vitamin C 1~2%, vitamin E 1~2%, hexadecanol 2~3% and lanolin 3~4%.
The preparation method of hops facial mask is first to soak polyvinyl alcohol with ethyl alcohol, and kaolin is added, zinc oxide, refines
After water mixing, mixed solution is heated to 75 DEG C~80 DEG C, then by hops extracting solution, polyvinyl acetate lotion, olive oil
And after other compositions are added, be uniformly mixed, 12~15 hours are stood, glycerine or propylene glycol, fragrance and preservative are added,
It stirs evenly and paste facial mask is made.
Lupulus extract includes polyphenols, flavonoids and polysaccharide compound etc..Polyphenols such as hops
Polyphenol can have fungistatic effect to various bacteria, have the function of preventing scytitis；Such as contain tannic acid, skin can be improved
The blood circulation of part.Flavone compound such as isopentene group looks into youngster's ketone, flavonols and flavonoid glycoside, can play radioresistance and town
Quiet effect has stronger anti-corrosion function and inoxidizability.Lupulus extract may also include protein, fat, cellulose and
Trace element etc. can promote the absorption of skin, improve the function of skin.
The extracting method of polyphenol compound is in hops：After sample is crushed, 40 mesh sieve is crossed.Take suitable sample
Product are added into organic solvent.It is filtered after a certain period of time using being heated to reflux device and extracting, obtains Polyphenols chemical combination
Object.The acetone that the organic solvent concentration of phenolic compound is 55%~60% is extracted in the present invention, remaining as water, reaction temperature is
60~65 DEG C, solid-liquid ratio 1：15~1：18, extraction time is 80~100 minutes, and extracted amount can reach 36~45mg/g.
Different solvents see the table below the influential effect experimental result that hop polyphenols extract, as can be seen from the table acetone 55%
~60% acetone and the compound system of water are most suitable for the extraction of hop polyphenols, the followed by compound system of second alcohol and water, and
It is simple worst using the extraction effect of water.
The condition that flavones is extracted in hops is to use concentration of alcohol for 40~50%, remaining as water, reaction temperature 60
~65 DEG C, solid-liquid ratio 1：20, extraction time is 90~120 minutes, and extracted amount can reach 65~70mg/g.
Different ethanol concentration and different feed liquid compare the influential effect of hop polyphenols extraction experimental result is shown in Fig. 1 and Fig. 2,
It can be seen that from attached drawing, be 40~50% in concentration of alcohol, solid-liquid ratio 1：When 20, the extracted amount of flavones increases.
The condition of polysaccharose substance is to use concentration of alcohol for 65~70%, and remaining as water, reaction temperature is 70~75 DEG C,
Solid-liquid ratio is 1：20~1：25, extraction time is 90~120 minutes, and polysaccharide crude extract can reach 40~50%.
Detection of Stability is carried out to facial mask, the drying time of facial mask is moderate, is 1153 ± 30s, is conducive to nutritional ingredient
It absorbs, while preventing loss of moist, moistening effect can be played.Facial mask under normal temperature state pH value be neutrality, meet country about
The correlation standard of facial mask.The equal no significant difference of facial mask color and luster under high temperature and low-temperature condition, the facial mask under apocarpy
Property is stablized.Through sensory testing, the dispersion of facial mask appearance is uniform, easily applies exhibition, and fine and smooth, fragrance is apparent, and viscosity is appropriate, and skin is wet
Profit, infiltration rate are moderate.Facial mask is coated on experimenter's the back of the hand, is observed after 12 hours, experimenter's the back of the hand is more moist, no hair
It is red, rash is played, it is non-stimulated to skin phenomena such as pain, allergy, and be not susceptible to be layered, oil slick phenomenon.
The implementation of the present invention is not limited to this, and the above according to the invention is known using the ordinary skill of this field
Knowledge and customary means, under the premise of not departing from above-mentioned basic fundamental thought of the invention, the present invention can also make other a variety of shapes
Modification, replacement or the change of formula, all fall within rights protection scope of the present invention.
Claims (10)
1. a kind of hops facial mask, which is characterized in that be made from the following raw materials in parts by weight：Hops extracting solution 6%~10%,
Polyvinyl acetate lotion 8~12%, polyvinyl alcohol 8~12%, olive oil 2~4%, glycerine or propylene glycol 6%~8%, oxygen
Change zinc 6~8%, kaolin 5~6%, ethyl alcohol 3~4%, Purified Water 40~50%, fragrance 1~3% and preservative 1~3%.
2. hops facial mask according to claim 1, it is characterised in that：Further include in hops facial mask vitamin C 1~
2%, vitamin E 1~2%, hexadecanol 2~3% and lanolin 3~4%.
3. hops facial mask according to claim 1, it is characterised in that：Lupulus extract includes polyphenols, Huang
Ketone and polysaccharide compound.
4. hops facial mask according to claim 3, it is characterised in that：Lupulus extract includes Hop polyphenols or tannic acid
At least one of, further include that isopentene group looks into youngster's ketone, at least one of flavonols or flavonoid glycoside.
5. hops facial mask according to claim 3, it is characterised in that：Lupulus extract may also include protein, fat
Fat, cellulose and trace element.
6. a kind of preparation method about the hops facial mask described in claim 3, it is characterised in that：This method includes：It is first
Polyvinyl alcohol is soaked with ethyl alcohol first, kaolin, zinc oxide, Purified Water mixing is added；Mixed solution is heated to 75 DEG C~80
DEG C, then by hops extracting solution, polyvinyl acetate lotion is uniformly mixed, stands after olive oil and other compositions are added
12~15 hours；Glycerine or propylene glycol, fragrance and preservative are added, stirs evenly and paste facial mask is made.
7. the preparation method of hops facial mask according to claim 6, it is characterised in that：The extraction side of hops extracting solution
Method is：After sample is crushed, 40 mesh sieve is crossed；Suitable sample is taken, is added into organic solvent；It is filled using being heated to reflux
It sets to extract and filter after a certain period of time, obtain polyphenol compound.
8. the preparation method of hops facial mask according to claim 6, it is characterised in that：Polyphenol compound is extracted to use
Organic solvent concentration be 55%~60% acetone and water compound system, reaction temperature is 60~65 DEG C, solid-liquid ratio 1：15
~1：18, extraction time is 80~100 minutes.
9. the preparation method of hops facial mask according to claim 6, it is characterised in that：Flavonoids compound is extracted to use
Organic solvent be a concentration of 40~50% ethyl alcohol and water compound system, reaction temperature be 60~65 DEG C, solid-liquid ratio 1：20,
Extraction time is 90~120 minutes.
10. the preparation method of hops facial mask according to claim 6, it is characterised in that：Extraction polysaccharose substance has
Solvent is the compound system of a concentration of 65~70% ethyl alcohol and water, and reaction temperature is 70~75 DEG C, solid-liquid ratio 1：20~1：
25, extraction time is 100~120 minutes.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201810537191.3A CN108498380A (en) | 2018-05-30 | 2018-05-30 | A kind of hops facial mask and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810537191.3A CN108498380A (en) | 2018-05-30 | 2018-05-30 | A kind of hops facial mask and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
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| CN108498380A true CN108498380A (en) | 2018-09-07 |
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| CN201810537191.3A Pending CN108498380A (en) | 2018-05-30 | 2018-05-30 | A kind of hops facial mask and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114366699A (en) * | 2022-01-17 | 2022-04-19 | 吴俊洁 | Whitening skin cream and preparation process thereof |
| CN115300437A (en) * | 2022-07-09 | 2022-11-08 | 黄斌斌 | Moisturizing and anti-aging skin care composition and preparation method and application thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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Application publication date: 20180907 |
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