CN104274371A - Method for extracting lupulus and application of extracting solution of lupulus - Google Patents
Method for extracting lupulus and application of extracting solution of lupulus Download PDFInfo
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- CN104274371A CN104274371A CN201410515336.1A CN201410515336A CN104274371A CN 104274371 A CN104274371 A CN 104274371A CN 201410515336 A CN201410515336 A CN 201410515336A CN 104274371 A CN104274371 A CN 104274371A
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Abstract
The invention relates to the field of natural product extraction and in particular relates to a method for extracting lupulus and application of an extracting solution of the lupulus. The method for extracting the lupulus comprises the following steps: (1) inputting the ground and dried lupulus powder into an extraction tube through a feeding hole of an ultrasonic extractor by virtue of a quantification feeder, heating an extraction solvent, and inputting the solvent into the extraction tube through a residue discharging end of the ultrasonic extractor; (2) performing countercurrent ultrasonic extraction on the lupulus powder and the extraction solvent in the extraction tube of the ultrasonic extractor under normal pressure for 20-50 minutes; (3) discharging the residues through the residue discharge opening of the ultrasonic extractor after the ultrasonic extraction is finished, and discharging the separation solution through a liquid outlet of the ultrasonic extractor; and (4) adding a separating agent into the separation solution, performing desolvation treatment, thereby obtaining the lupulus extracting solution. According to the lupulus extraction process disclosed by the invention, the process is easy to operate, the extracted product is stable in quality, the solvent can be recycled, and the extraction cost is low.
Description
Technical field
The present invention relates to field of natural product extraction, be specifically related to a kind of extracting method of Flos lupuli (Flos Humuli Lupuli) and the application of extracting solution thereof.
Background technology
Flos lupuli (Flos Humuli Lupuli) is containing wherein having .alpha.-bitter acid, IsoHopCO2N. .beta.-bitter acid etc.; Tens kinds of active component such as myrcene, Humuleno, linalool, Fols lupuli alcohol, tannin, chromocor compound, choline, fructose, sucrose, glucose, thus have very strong pharmacological action, as antibacterial, antiinflammatory, antioxidation, sedation.Flos lupuli (Flos Humuli Lupuli) is mainly used in making beer and pharmaceutical field, applies very few in cosmetics, temporarily also without application in hair articles for use.
Scalp is the soft tissue be covered in outside skull, and mostly, pressure disorderly with hormone secretion greatly, excessive combing, frequent feed high lipid food can cause scalp fat secretion superfluous, if it is improper to nurse, adds life and notice that the people of oily hair the most easily becomes seborrheic alopecia not.Healthy scalp ecological environment is maintained by the balance of finance, credits and materials: oils and fats, flora, metabolic balance.Skin fat secretion is unbalance right overhead, and scalp fuel-displacedly will become greasy; When scalp flora environment is unbalance, harmful bacteria grows in a large number, just there will be the phenomenon of head pruritus; And scalp stratum corneum is too fast, comes off and just form dandruff.Scalp pomade, head pruritus, dandruff are many, hair is done, alopecia etc. are the unbalance scalp problems caused of scalp ecological environment.Scalp is human body second thin skin skin, faster than face 6 times of its aging rate, faster than health skin 12 times.Scalp is thinner than facial skin, but responsive than facial skin, equally needs to look after.
In the prior art, from the method that Flos lupuli (Flos Humuli Lupuli) extracts, main employing supercritical extraction, acid-base neutralization again separate mode extracts.The deficiency that these extracting method exist can only extract a kind of composition each time, operation is wasted time and energy, and complex process, extraction ratio is low besides, and some technique also needs, by raw material pelletize, to cause extraction Quality Down, the unstable product quality extracted, also have Extraction solvent consumption high, environmental pollution is large, causes extraction cost high.
Summary of the invention
Technical problem to be solved by this invention is to provide a kind of extracting method of Flos lupuli (Flos Humuli Lupuli).
Another object of the present invention is to provide the application of the extracting solution of said extracted method gained.
Technical problem to be solved by this invention is achieved by the following technical programs:
An extracting method for Flos lupuli (Flos Humuli Lupuli), comprises following steps:
(1) the dried Flos lupuli (Flos Humuli Lupuli) powder of pulverizing is input in extraction tube by quantitative feeder by the charging aperture of ultrasonic extractor, Extraction solvent is input in extraction tube through heating by the deslagging end of ultrasonic extractor simultaneously;
(2) hop power and Extraction solvent are carried out adverse current supersound extraction 20-50 minute under normal pressure in the extraction tube of ultrasonic extractor;
(3) after completing supersound extraction, discharge material slag by the slag-drip opening of ultrasonic extractor, discharge separating medium by the leakage fluid dram of ultrasonic extractor;
(4) separating medium is added in separating medium, then obtains Flos lupuli (Flos Humuli Lupuli) extracting solution through carrying out precipitation treatment.
Flos lupuli (Flos Humuli Lupuli) powder is through screening, remove impurity, is crushed to 50-80 object hop power powder.
Further, described separating medium is at least one in water, glycerol, butanediol, pentanediol.
Further, described Flos lupuli (Flos Humuli Lupuli) powder and the feed weight of Extraction solvent are than being 1:2 ~ 1:10.
Further, described Extraction solvent is at least one in water, ethanol, methanol, acetone, petroleum ether, normal hexane.
Further, the carrying out precipitation treatment in described step (4) is evaporated at 50 ~ 70 DEG C by the separating medium containing separating medium, and air pressure is-0.1 ~ 0Mpa, makes extracting solution evaporation and concentration to the 30-50% of separating medium volume.
The Flos lupuli (Flos Humuli Lupuli) extracting solution of extracting method gained of the present invention effectively can suppress the activity of 5α-reductase, can suppress the fat secretion of scalp, reduces because fat secretion crosses Sheng and produces seborrheic dermatitis.Flos lupuli (Flos Humuli Lupuli) extracting solution also has antibacterial effect.The generation of the dandruff is because the amount reproduction of chlosma on scalp causes the cuticular hyperplasia of scalp, thus impels corneocyte extremely to come off with the form of white or Lycoperdon polymorphum Vitt squama, and this squama come off is the dandruff.Flos lupuli (Flos Humuli Lupuli) extracting solution suppresses the activity of chlosma, makes it normally not breed, decreases the decomposition of corneocyte, thus slow down the generation of the dandruff.And Flos lupuli (Flos Humuli Lupuli) extracting solution is also improved the microcirculation of vascular system and skin, Flos lupuli (Flos Humuli Lupuli) extracting solution is by promoting that neovascularization strengthens blood vessel defensive ability/resistance ability restructuring scalp capillary system, capillary tube is the main portions that blood and surrounding tissue carry out mass exchange, the reparation of blood capillary improves exchange capacity, thus makes scalp cells more vigourous.
The application of Flos lupuli (Flos Humuli Lupuli) extracting solution in scalp essence of said extracted method gained.
A kind of scalp essence, comprises the component of following percentage by weight:
Surfactant 0.5 ~ 10%; Thickening agent 0.1 ~ 3%; Wetting agent 0.5 ~ 10%; Additive 0.01 ~ 5%; Flos lupuli (Flos Humuli Lupuli) extracting solution 0.5 ~ 10%; Anti-sensitizer 0.1 ~ 1%; Antiseptic 0 ~ 1.5%; Surplus is water.
Surfactant selected by the present invention is described surfactant is hexadecyltrimethylammonium chloride, octadecyl trimethyl ammonium chloride, Cremophor RH40, polyoxyethylene (80) sorbic alcohol laurate, at least one in sorbitol glycosides polyoxyethylene (20) ether monolaurate.
Surfactant is formed can be reduced interfacial tension by hydrophilic and oleophilic two group, has the effect of emulsifying and solubilising, and the present invention is hexadecyltrimethylammonium chloride cationic surfactant and Cremophor RH40 non-ionic surface active agent preferably.Cationic surfactant is that its molecule is water-soluble ionize after, the hydrophilic group be connected with lipophilic group is positively charged surfactant, quaternary cationics good water solubility, not only acidproof but also alkaline-resisting and great majority have bactericidal action.Due to hair and scalp surface electronegative, its electric charge can be neutralized with quaternary cationics, therefore have good antistatic property.Quaternary cationics can form hydrophobic oil film in scalp surface, makes scalp have level and smooth effect.Non-ionic surface active agent Cremophor RH40 has the effect of solubilising, solubilising part can be insoluble in the oily matter of water.
Thickening agent selected by the present invention is hydroxyethyl-cellulose, hydroxypropyl emthylcellulose, styrene/acrylic (ester) copolymer, at least one in carbomer.
In order to make system more stable and improve the outward appearance of system; the present invention preferably selects hydroxyethyl-cellulose as thickening agent, and hydroxyethyl-cellulose has good thickening, suspension, dispersion, emulsifying, bonding, film forming, protection moisture and provides the characteristics such as protecting colloid.Hydroxyethyl-cellulose can provide enough suspension dynamics for system, and comfortable skinfeel, can form the protecting film that one deck prevents moisture content from volatilizing on scalp top layer.
Wetting agent selected by the present invention is glycerol, propylene glycol, 1.3-butanediol, D-panthenol, hyaluronate sodium, at least one in pyrrolidone sodium carboxylate.
Wetting agent is human body self secretion natural moisture preserving component, because its natural performance has good affinity and moisture retention to skin, gives the care that scalp is natural, strengthens the resistance that scalp stimulates to external world, play the effect of prevention.Pyrrolidone sodium carboxylate of the present invention (PCA-sodium) is a kind of nature moisturizing factor (Natural Moisturizing Factor, NMF), has excellent hygroscopicity, gives scalp comfort and moisture feeling, increases flexibility and elasticity.Even if in higher concentrations, little to skin and oculomucous stimulation, colorless and odorless, is stable at low temperature and high temperature, can biodegradation rapidly.D-panthenol is the precursor of vitamin B5, therefore also known as dexpanthenol, promotes the metabolism of human body protein, fat, saccharide, keeps skin and mucosa, improves hair luster, improve immunity, prevent the generation of disease; At cosmetic industry: deeply permeate scalp, the growth of scalp irritation cell, promotes wound healing, plays antiinflammation.And propylene glycol has hygroscopicity, good performance of keeping humidity can be provided, pin the moisture content in scalp, increase flexibility and the elasticity of scalp.
Additive of the present invention is benzotriazole butylphenol sodium sulfonate, at least one in three (tetramethyl hydroxy piperidine alcohol) citrate.It can resist the injury of ultraviolet to scalp cells, delays the aging of scalp cells.
Described anti-sensitizer is at least one in bisabolol, plant sterol anti-sensitizer; wherein preferably use preferred bisabolol; bisabolol is as active component with protection and nursing allergic skin, and bisabolol reaches the stimulation suppressing external substance thin to scalp by suppressing the generation of leukotriene B4.
The present invention's antiseptic used is that the conventional antiseptic of the art all can realize the present invention.
The present invention has following beneficial effect:
Flos lupuli (Flos Humuli Lupuli) extraction process of the present invention, technological operation is simple, and the constant product quality of extraction, can to recycled solvent, and extraction cost is low.Scalp essence of the present invention is by adding the Flos lupuli (Flos Humuli Lupuli) extracting solution of extracting method gained of the present invention; use natural, safety, gentleness and the high cosmetic material of purity; strengthen scalp resistance; from a variety of causes causing scalp problems; add the both effectiveness compositions such as corresponding wetting agent, additive, active matter and anti-sensitizer; natural barrier action is played to scalp skin care; can make scalp moisten, moisturizing, fat secretion balance; supplement scalp and produce required nutrient; improve scalp growing environment, promote scalp health growth.
Detailed description of the invention
Below in conjunction with embodiment, the present invention will be described in detail, and embodiment is only the preferred embodiment of the present invention, is not limitation of the invention.
embodiment 1
An extracting method for Flos lupuli (Flos Humuli Lupuli), comprises following steps:
(1) the dried Flos lupuli (Flos Humuli Lupuli) powder of pulverizing is input in extraction tube by quantitative feeder by the charging aperture of ultrasonic extractor, Extraction solvent is input in extraction tube through heating by the deslagging end of ultrasonic extractor simultaneously; Wherein Extraction solvent is the mixture of water and ethanol, and the volume ratio of water and ethanol is 3:1, and Flos lupuli (Flos Humuli Lupuli) powder is 1:3 with the feed weight ratio of Extraction solvent.
(2) hop power and Extraction solvent are carried out adverse current supersound extraction 35 minutes in the extraction tube of ultrasonic extractor under normal pressure;
(3) after completing supersound extraction, discharge material slag by the slag-drip opening of ultrasonic extractor, discharge separating medium by the leakage fluid dram of ultrasonic extractor;
(4) be added in separating medium by glycerol, at 60 DEG C, air pressure is evaporate under the condition of-0.1Mpa, makes extracting solution evaporation and concentration to 40% of separating medium volume, obtains Flos lupuli (Flos Humuli Lupuli) extracting solution.
embodiment 2
An extracting method for Flos lupuli (Flos Humuli Lupuli), comprises following steps:
(1) the dried Flos lupuli (Flos Humuli Lupuli) powder of pulverizing is input in extraction tube by quantitative feeder by the charging aperture of ultrasonic extractor, Extraction solvent is input in extraction tube through heating by the deslagging end of ultrasonic extractor simultaneously; Wherein Extraction solvent is the mixture of water and methanol, and the volume ratio of water and methanol is 5:1, and Flos lupuli (Flos Humuli Lupuli) powder is 1:7 with the feed weight ratio of Extraction solvent.
(2) hop power and Extraction solvent are carried out adverse current supersound extraction 30 minutes in the extraction tube of ultrasonic extractor under normal pressure;
(3) after completing supersound extraction, discharge material slag by the slag-drip opening of ultrasonic extractor, discharge separating medium by the leakage fluid dram of ultrasonic extractor;
(4) be added in separating medium by butanediol, at 55 DEG C, air pressure is evaporate under the condition of-0.1Mpa, makes extracting solution evaporation and concentration to 50% of separating medium volume, obtains Flos lupuli (Flos Humuli Lupuli) extracting solution.
embodiment 3
An extracting method for Flos lupuli (Flos Humuli Lupuli), comprises following steps:
(1) the dried Flos lupuli (Flos Humuli Lupuli) powder of pulverizing is input in extraction tube by quantitative feeder by the charging aperture of ultrasonic extractor, Extraction solvent is input in extraction tube through heating by the deslagging end of ultrasonic extractor simultaneously; Wherein Extraction solvent is the mixture of acetone and ethanol, and the volume ratio of acetone and ethanol is 1:1, and Flos lupuli (Flos Humuli Lupuli) powder is 1:9 with the feed weight ratio of Extraction solvent.
(2) hop power and Extraction solvent are carried out adverse current supersound extraction 50 minutes in the extraction tube of ultrasonic extractor under normal pressure;
(3) after completing supersound extraction, discharge material slag by the slag-drip opening of ultrasonic extractor, discharge separating medium by the leakage fluid dram of ultrasonic extractor; Water, glycerol, butanediol, pentanediol
(4) be added in separating medium by separating medium (separating medium is the mixture of water and glycerol, and its volume ratio is 1:1), at 70 DEG C, air pressure is evaporate under the condition of 0Mpa, makes extracting solution evaporation and concentration to 30% of separating medium volume, obtains Flos lupuli (Flos Humuli Lupuli) extracting solution.
embodiment 4
A kind of scalp essence, comprises the component of following percentage by weight:
2% hexadecyltrimethylammonium chloride; 0.2%PEG-40 castor oil hydrogenated; 0.5% hydroxyethyl-cellulose; 0.5%PCA-sodium; 0.5%D-pantothenylol; 0.5% propylene glycol; 0.01% benzotriazole butylphenol sodium sulfonate; 0.01% 3 (tetramethyl hydroxy piperidine alcohol) citrate; The Flos lupuli (Flos Humuli Lupuli) extracting solution of 3% embodiment 1; 0.1% bisabolol; 0.8% phenoxyethanol; 0.2% caprylyl glycol; 100% is complemented to water.
embodiment 5
A kind of scalp essence, comprises the component of following percentage by weight:
3% hexadecyltrimethylammonium chloride; 0.5%PEG-40 castor oil hydrogenated; 1% hydroxyethyl-cellulose; 1%PCA-sodium; 1%D-pantothenylol; 1% propylene glycol; 0.03% benzotriazole butylphenol sodium sulfonate; 0.02% 3 (tetramethyl hydroxy piperidine alcohol) citrate; The Flos lupuli (Flos Humuli Lupuli) extracting solution of 5% embodiment 1; 0.15% bisabolol; 0.8% phenoxyethanol; 0.2% caprylyl glycol; 100% is complemented to water.
embodiment 6
A kind of scalp essence, comprises the component of following percentage by weight:
4% hexadecyltrimethylammonium chloride; 1%PEG-40 castor oil hydrogenated; 1.5% hydroxyethyl-cellulose; 1.5%PCA-sodium; 1.5%D-pantothenylol; 1.5% propylene glycol; 0.05% benzotriazole butylphenol sodium sulfonate; 0.03% 3 (tetramethyl hydroxy piperidine alcohol) citrate; The Flos lupuli (Flos Humuli Lupuli) extracting solution of 7% embodiment 1; 0.2% bisabolol; 0.8% phenoxyethanol; 0.2% caprylyl glycol; 100% is complemented to water.
comparative example
A kind of scalp essence, comprises the component of following percentage by weight:
2% hexadecyltrimethylammonium chloride; 0.2%PEG-40 castor oil hydrogenated; 0.5% hydroxyethyl-cellulose; 0.5%PCA-sodium; 0.5%D-pantothenylol; 0.5% propylene glycol; 0.01% benzotriazole butylphenol sodium sulfonate; 0.01% 3 (tetramethyl hydroxy piperidine alcohol) citrate; 0.1% bisabolol; 0.8% phenoxyethanol; 0.2% caprylyl glycol; 100% is complemented to water.
Preparation method of the present invention is conventional configuration and hybrid technology, does not elaborate at this.
The present invention uses in the essence mode of routine, mainly comprises following step:
(1) have one's hair wash rear or can be used for daily scalp care;
(2) product of the present invention of effective dose is used to be coated in scalp equably, soft massage one minute.
Table 1 volunteer is to scalp essence and sample for reference effect assessment mark
Note: volunteer evaluates the assessment result obtained.Moisten moisturizing and conditioning effect: 10 points best, and 0 point the poorest.Wherein, sample for reference 1,2 is commercial like product.
Assessment result shows that essence of the present invention can bring superior moist moisturizing and conditioning effect.
Table 2 volunteer is to the evaluation result of this essence effect
Assessment result shows, scalp essence of the present invention has well moist moisturizing and conditioning effect.
The above embodiment only have expressed embodiments of the present invention; it describes comparatively concrete and detailed; but therefore can not be interpreted as the restriction to the scope of the claims of the present invention; in every case the technical scheme adopting the form of equivalent replacement or equivalent transformation to obtain, all should drop within protection scope of the present invention.
Claims (7)
1. an extracting method for Flos lupuli (Flos Humuli Lupuli), is characterized in that, comprises following steps:
(1) the dried Flos lupuli (Flos Humuli Lupuli) powder of pulverizing is input in extraction tube by quantitative feeder by the charging aperture of ultrasonic extractor, Extraction solvent is input in extraction tube through heating by the deslagging end of ultrasonic extractor simultaneously;
(2) hop power and Extraction solvent are carried out adverse current supersound extraction 20-50 minute under normal pressure in the extraction tube of ultrasonic extractor;
(3) after completing supersound extraction, discharge material slag by the slag-drip opening of ultrasonic extractor, discharge separating medium by the leakage fluid dram of ultrasonic extractor;
(4) separating medium is added in separating medium, then obtains Flos lupuli (Flos Humuli Lupuli) extracting solution through carrying out precipitation treatment.
2. the extracting method of a kind of Flos lupuli (Flos Humuli Lupuli) according to claim 1, is characterized in that, described separating medium is at least one in water, glycerol, butanediol, pentanediol.
3. the extracting method of a kind of Flos lupuli (Flos Humuli Lupuli) according to claim 1, is characterized in that, described Flos lupuli (Flos Humuli Lupuli) powder is 1:2 ~ 1:10 with the feed weight ratio of Extraction solvent.
4. the extracting method of a kind of Flos lupuli (Flos Humuli Lupuli) according to claim 3, is characterized in that, described Extraction solvent is at least one in water, ethanol, methanol, acetone, petroleum ether, normal hexane.
5. the extracting method of a kind of Flos lupuli (Flos Humuli Lupuli) according to claim 1, it is characterized in that, carrying out precipitation treatment in described step (4) is evaporated at 50 ~ 70 DEG C by the separating medium containing separating medium, and air pressure is-0.1 ~ 0Mpa, makes extracting solution evaporation and concentration to the 30-50% of separating medium volume.
6. the application of Flos lupuli (Flos Humuli Lupuli) extracting solution in scalp essence of the extracting method gained of claim 1.
7. a scalp essence, is characterized in that the component comprising following percentage by weight:
Surfactant 0.5 ~ 10%;
Thickening agent 0.1 ~ 3%;
Wetting agent 0.5 ~ 10%;
Additive 0.01 ~ 5%;
The Flos lupuli (Flos Humuli Lupuli) extracting solution 0.5 ~ 10% of claim 1 extracting method gained;
Anti-sensitizer 0.1 ~ 1%;
Antiseptic 0 ~ 1.5%;
Surplus is water.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410515336.1A CN104274371A (en) | 2014-09-30 | 2014-09-30 | Method for extracting lupulus and application of extracting solution of lupulus |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410515336.1A CN104274371A (en) | 2014-09-30 | 2014-09-30 | Method for extracting lupulus and application of extracting solution of lupulus |
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| CN104274371A true CN104274371A (en) | 2015-01-14 |
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| CN201410515336.1A Pending CN104274371A (en) | 2014-09-30 | 2014-09-30 | Method for extracting lupulus and application of extracting solution of lupulus |
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| CN105919899A (en) * | 2016-06-27 | 2016-09-07 | 北京普世安生物科技有限公司 | Hair re-growing nourishing dew and preparation method thereof |
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| CN107890444A (en) * | 2017-11-15 | 2018-04-10 | 惠州兆骐礼品有限公司 | A kind of extracting method of plant society extract and the personal care composition for alleviating inflammation |
| CN108498380A (en) * | 2018-05-30 | 2018-09-07 | 广州市康超信息科技有限公司 | A kind of hops facial mask and preparation method thereof |
| CN108653130A (en) * | 2018-06-14 | 2018-10-16 | 广州植境生物科技有限公司 | A kind of draft Haircare composition containing shrubby sophora extract |
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2014
- 2014-09-30 CN CN201410515336.1A patent/CN104274371A/en active Pending
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105919899A (en) * | 2016-06-27 | 2016-09-07 | 北京普世安生物科技有限公司 | Hair re-growing nourishing dew and preparation method thereof |
| CN107349119A (en) * | 2017-07-25 | 2017-11-17 | 北京斯利安药业有限公司 | A kind of amino acid soap of stabilization and preparation method thereof |
| CN107349119B (en) * | 2017-07-25 | 2020-08-25 | 北京斯利安药业有限公司 | Stable amino acid soap and preparation method thereof |
| CN107890444A (en) * | 2017-11-15 | 2018-04-10 | 惠州兆骐礼品有限公司 | A kind of extracting method of plant society extract and the personal care composition for alleviating inflammation |
| CN107890444B (en) * | 2017-11-15 | 2021-04-27 | 惠州兆婷化妆品有限公司 | Extraction method of plant combined extract and personal care composition for relieving inflammation |
| CN108498380A (en) * | 2018-05-30 | 2018-09-07 | 广州市康超信息科技有限公司 | A kind of hops facial mask and preparation method thereof |
| CN108653130A (en) * | 2018-06-14 | 2018-10-16 | 广州植境生物科技有限公司 | A kind of draft Haircare composition containing shrubby sophora extract |
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Application publication date: 20150114 |