CN109044935A - A kind of mildly clean micella makeup remover and its production technology - Google Patents

A kind of mildly clean micella makeup remover and its production technology Download PDF

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Publication number
CN109044935A
CN109044935A CN201811246234.9A CN201811246234A CN109044935A CN 109044935 A CN109044935 A CN 109044935A CN 201811246234 A CN201811246234 A CN 201811246234A CN 109044935 A CN109044935 A CN 109044935A
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parts
skin
micella
makeup remover
agent
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CN109044935B (en
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楼彪
张川
石蓓君
从云玲
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Hangzhou Weikela Investment Co., Ltd.
Yu Qiongfei
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When Johnson Chemical (hangzhou) Ltd By Share Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36Carboxylic acids; Salts or anhydrides thereof
    • A61K8/365Hydroxycarboxylic acids; Ketocarboxylic acids
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36Carboxylic acids; Salts or anhydrides thereof
    • A61K8/368Carboxylic acids; Salts or anhydrides thereof with carboxyl groups directly bound to carbon atoms of aromatic rings
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/39Derivatives containing from 2 to 10 oxyalkylene groups
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • AHUMAN NECESSITIES
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    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/14Preparations for removing make-up
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
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    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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Abstract

The invention discloses a kind of mild clean micella makeup remover and its production technologies.Micella makeup remover includes the component of following parts by weight: 1.0-10 parts of PEG-8 caprylic/capric glyceride type;0.5-5 parts of butanediol;0.5-5 parts of glycerol;0.002-2 parts of skin conditioning agent;0.5-5 parts of antibacterial agent;0.0011-0.0015 parts of pH adjusting agent;85-95 parts of water;The skin conditioning agent includes at least one of the first skin conditioning agent, Second Skin conditioner;First skin conditioning agent is made of bermuda lily bulb extract, sodium benzoate, citric acid;The Second Skin conditioner is made of propylene glycol, calendula extract, Second Skin conditioner with water.Micella makeup remover of the invention can also also have effects that maintenance to skin while mildly being removed ornaments and formal dress to skin, achieve the effect that soft and moist moisturizing skin.

Description

A kind of mildly clean micella makeup remover and its production technology
Technical field
The present invention relates to makeup removing product technical fields, more specifically, it relates to a kind of mild clean micella makeup remover And its production technology.
Background technique
Now with increased popularity of the color make-up in urban woman life, makeup removing is also necessarily as the most key of skin care One step.Therefore, also higher and higher for the requirement of makeup removal products, it is not only required to rapid cleaning, deep-pollution-removing, also requires temperature It does not stimulate.
The Chinese patent that existing application publication number is CN108113922A, data of publication of application is on June 5th, 2018 discloses A kind of makeup remover composition, is made of the raw material of following mass fraction: 11-14 parts of lecithin, 8-13 parts of camomile extract, 7-10 parts of disodium ethylene diamine tetraacetate, 10-12 parts of glycerol, 3-5 parts of cocinic acid sucrose ester, 6-8 parts of lanolin, polyvinyl alcohol 12-15 parts, 4-7 parts of olive oil, 1-3 parts of methyl isopropyl thiazolinone, 2-5 parts of zinc gluconate, 2-4 parts of tea tree ethereal oil, polyoxy second 9-12 parts of alkene sorbitan monolaurate, 25-35 parts of deionized water.
Although the prior art can play the effect of the color make-up on certain cleaning skin, the lecithin that wherein contains, coconut palm Seed oil acid sucrose ester, lanolin, polyoxyethylene sorbitan monolaurate are grease type organic principle, in use, part oil Rouge can enter between intracellular or cell, be used for a long time, and will cause that pore is coarse, dirty easily to enter in coarse pore, from And easily cause the infection and acne of skin;Also it can cause dry skin and coarse phenomenon.
Summary of the invention
It is unloaded in view of the deficienciess of the prior art, the first purpose of this invention is to provide a kind of mild clean micella Adornment water can also also have effects that maintenance to skin while mildly being removed ornaments and formal dress to skin, reach the effect of soft and moist moisturizing skin Fruit.
Second object of the present invention is to provide a kind of production technology of mild clean micella makeup remover, can make to obtain Micella makeup remover keep the validity of adding ingredient as much as possible.
To realize above-mentioned first purpose, the present invention provides the following technical scheme that
A kind of mild clean micella makeup remover, the component including following parts by weight:
1.0-10 parts of PEG-8 caprylic/capric glyceride type;
0.5-5 parts of butanediol;
0.5-5 parts of glycerol;
0.002-2 parts of skin conditioning agent;
0.5-5 parts of antibacterial agent;
0.0011-0.0015 parts of pH adjusting agent;
85-95 parts of water;
The skin conditioning agent includes at least one of the first skin conditioning agent, Second Skin conditioner;First skin Conditioner is made of bermuda lily bulb extract, sodium benzoate, citric acid;The Second Skin conditioner is by propylene glycol, gold Small cup flower extract, Second Skin conditioner are formed with water.
By using above-mentioned technical proposal, PEG-8 caprylic/capric glyceride type be a kind of nonionic surface active agent and The effect of emulsifier can dissolve the dirt for being attached to skin surface, effectively play makeup removing decontamination.Meanwhile PEG-8 octanoic acid/last of the ten Heavenly stems Acid glycerol esters can be used as moisturizing factor, have good spreadability, so that skin is had smooth but not greasy feeling, to play soft Moisten the effect of skin.
Butanediol, glycerol are small molecule moisturizing ingredient, and good penetrability easily enters skin, and also portable the application In other compositions enter in skin, to play the role of with preferable moisturizing, soft and moist skin, and safety is stingless Swash.Meanwhile butanediol also has the function of antibacterial, sterilization, has anti-inflammatory, calm effect to skin.
In this application, PEG-8 caprylic/capric glyceride type has hydrophilic group and lipophilic group as surfactant.Skin Skin surface layer it is dirty mainly from color make-up product, skin itself grease secretion and external environment in pollutant attachment, PEG-8 Lipophilic group in caprylic/capric glyceride type can wrap dirt, hydrophilic group then facilitate water wash away it is dirty.When PEG-8 is pungent When acid/glycerol decanoate class usage amount is in the use scope of the application, PEG-8 caprylic/capric glyceride type can be formulated In form micella, make remove color make-up effective ratio area it is bigger, and then can more effectively make remove skin surface it is dirty.
In addition, butanediol, glycerol and PEG-8 caprylic/capric glyceride type cooperate, help to make micella makeup remover Mildness is reinforced, and while effective decontamination, skin can also be made to keep water profit, reach preferable soft and moist sense.
It include vitamin and multiple nutritional components, safe nothing in bermuda lily bulb extract in first skin conditioning agent Stimulation.Aspartic acid abundant contained therein has oxidation resistant effect;The ophiopogonpolysaccharide contained is natural moisturizer;Institute The veratramine contained has strong inhibiting effect to tyrosinase, can be with whitening spot-removing.Bermuda lily bulb extract pair as a result, Skin has effects that moisturizing, anti-oxidant and whitening conditioning.
Citric acid can accelerate the update of skin keratin, facilitate skin pore shrink, to skin can play moisturizing, The effect of whitening, improve skin blackspot, it is coarse phenomena such as, thus the effect of playing conditioning to skin.
Sodium benzoate can be converted into benzoic acid in an acidic solution, play and inhibit the growth of the microorganisms such as saccharomycete and bacterium Effect.In this application, the effect of sodium benzoate of less content primarily serves anti-inflammatory, sterilization to skin, to maintain flesh The normal activity of skin cell, the effect of conditioning is played to skin.
In Second Skin conditioner, propylene glycol is soluble in Second Skin conditioner water, has to skin soft and moist, moisturizing Effect.Calendula extract contains lutein and luteole, has the function of delaying senescence.In this application, pot marigold mentions It takes lutein and zeatin in object as the antioxidant haveing excellent performance, anti-aging can be played the role of to skin.Simultaneously Calendula extract also has the function of anti-inflammatory, sterilization to skin.
Wherein, the extracting method of bermuda lily bulb extract, includes the following steps:
S1, by bermuda lily bulb through ultrasonic cleansing, dry, the lustration raw material of acquisition bermuda lily bulb;
S2, by the lustration raw material obtained in step S1 through supercritical CO2Extraction, supercritical CO2The extraction temperature of extraction is 25-38 DEG C, extracting pressure 16-19MPa, extraction time 1.5-2h, CO2Flow is 18-20kg/h, obtains bermuda lily bulb the One extracting solution;
S3 is distilled the first extracting solution of bermuda lily bulb obtained in step S2, obtains bermuda lily bulb extract.
The step of extraction step of calendula extract is with bermuda lily bulb extract is identical.
The main function of antibacterial agent in this application is anti-corrosion, antibacterial, facilitates the micella makeup remover for extending mild moisturizing Service life.
In this application, the micella makeup remover of mild moisturizing makes pH value control in 5.5-5.8 under the action of pH adjusting agent In the range of, skin is not stimulated mildly more.
Water in the application is deionized water.
Further preferably are as follows: the skin conditioning agent is composed of the following parts by weight:
First 0.001-1 parts of skin conditioning agent;0.001-1 parts of Second Skin conditioner.
By using above-mentioned technical proposal, using the first skin conditioning agent, the Second Skin within the scope of above-mentioned parts by weight Conditioner cooperates, and facilitates the skin conditioning agent for making to be formed and plays better decontamination and moisturizing work in micella makeup remover With, and phenomena such as mildly do not stimulate to skin, be less prone to allergy.
Further preferably are as follows: first skin conditioning agent is (99-99.4) %: 0.5% by following weight percent: Bermuda lily bulb extract, sodium formate, the citric acid composition of (0.1-0.5) %.
By using above-mentioned technical proposal, through research makeup removing effect evaluation test discovery, using above-mentioned weight fraction ratio model The first skin conditioning agent that bermuda lily bulb extract, sodium formate, citric acid in enclosing complement each other to form can play skin To better pore refining, moisturizing, oxidation resistant effect.
Further preferably are as follows: the Second Skin conditioner is 15%: (15-30) %: (55- by following weight percent 70) calendula extract, propylene glycol of %, Second Skin conditioner are formed with water.
By using above-mentioned technical proposal, through research makeup removing effect evaluation test discovery, using above-mentioned weight fraction ratio model The Second Skin conditioner that calendula extract, propylene glycol in enclosing, Second Skin conditioner are complemented each other to form with water, can be right Skin plays the role of better moisturizing, anti-inflammatory, oxidation resistant.
Further preferably are as follows: the antibacterial agent is used by decoyl hydroximic acid, Sensiva SC50,1,2- hexylene glycol, antibacterial agent Butanediol, antibacterial agent are formed with water.
By using above-mentioned technical proposal, decoyl hydroximic acid is organic acid, mild and non-stimulated, also has stronger antibacterial Ability.1,2- hexylene glycol, antibacterial agent butanediol are the dihydric alcohols inhibited to microorganisms such as bacterium and saccharomycete Class.Decoyl hydroximic acid and 1,2- hexylene glycol, antibacterial agent form compound system with butanediol, can achieve the effect that broad-spectrum antiseptic. Sensiva SC50 is anti-corrosion synergist, helps to improve the antibacterial effect of the antibacterial agent in the application.
Therefore, pass through decoyl hydroximic acid, Sensiva SC50,1,2- hexylene glycol, antibacterial agent butanediol, antibacterial agent water It cooperates, facilitates the shelf-life for the micella makeup remover for effectively extending mild moisturizing, and irritation is extremely low, even if contact eye Portion will not cause the excitement of eye.
The antibacterial agent of said components composition is a kind of efficiently mild antibacterial agent, can effectively extend the micella of mild moisturizing The shelf-life of makeup remover also there is extremely low irritation will not cause Ocular irritation even if accidentally contacting eye.
Further preferably are as follows: in the antibacterial agent, decoyl hydroximic acid, Sensiva SC50,1,2- hexylene glycol, antibacterial agent are used Butanediol, antibacterial agent water weight fraction ratio be 1.8: 1: 1.2: 13: 3.
By using above-mentioned technical proposal, through research makeup removing effect evaluation test discovery, using above-mentioned weight fraction ratio Decoyl hydroximic acid, Sensiva SC50,1,2- hexylene glycol, antibacterial agent butanediol, antibacterial agent are cooperated with water, help to mention High entirety
Further preferably are as follows: the pH adjusting agent is arginine.
By using above-mentioned technical proposal, due to contain in the raw material components of the micella makeup remover of mild moisturizing citric acid, One of calendula extract, bermuda lily bulb extract or more than one components, these are with conditioning skin effect Containing acid ingredient or be acid ingredient in component, make the micella makeup remover entirety slant acidity of mild moisturizing, if acid excessive, There can be irritation to skin, skin is made the phenomenon that dyssecretosis occur.And arginine is a kind of basic amino acid, can be used as pH Regulator can effectively neutralize acid ingredient, play the role of adjusting pH, and also there is arginine enhancing skin to strengthen cutin With the function of moisturizing, has effects that certain nursing to skin.
To realize above-mentioned second purpose, the present invention provides the following technical scheme that
A kind of production technology of mild clean micella makeup remover, includes the following steps:
Step 1, according to parts by weight, water is weighed, is heated to 100 DEG C, constant temperature 10-20min is cooled to room temperature;
Step 2, according to parts by weight, weigh PEG-8 caprylic/capric glyceride type, antibacterial agent butanediol, glycerol be added to by It is cooled in step 1 in the water of room temperature, is heated to 80-85 DEG C, sufficiently dissolve and mixed to transparent, obtain mixture A;
Step 3, mixture A obtained in step 2 is cooled to 40-50 DEG C, according to parts by weight, weighs the first skin condition Agent, Second Skin conditioner, and be added sequentially in mixture A are sufficiently dissolved and are mixed to transparent, obtain mixture A1;
Step 4, according to parts by weight, weigh antibacterial agent and be added in the mixture A1 obtained by step 3, sufficiently dissolve and mix It is even to transparent, obtain mixture A2;
Step 5, according to parts by weight, arginine is weighed, is added in the mixture A2 obtained by step 4, is sufficiently dissolved and mix It is even, the pH of mixture is adjusted between 5.5-5.8, obtains mixture A3;
Step 6, the mixture A3 obtained by step 5 is cooled to 25-30 DEG C, discharging obtains the micella makeup remover of mild moisturizing.
By using above-mentioned technical proposal, first bermuda lily bulb extract, sodium benzoate, citric acid are mixed respectively equal Even preparation obtains the first skin conditioning agent;Propylene glycol, calendula extract, Second Skin conditioner are uniformly mixed with water and are prepared Obtain Second Skin conditioner;By decoyl hydroximic acid, Sensiva SC50,1,2- hexylene glycol, antibacterial agent butanediol, antibacterial agent With water be uniformly mixed prepare obtain antibacterial agent, then according still further to parts by weight match by previously prepared first skin conditioning agent, Second Skin conditioner, antibacterial agent carry out hybrid manipulation according to step.Such purpose is the micella that can promote mild moisturizing The raw material components of makeup remover mix more evenly, to help preferably to play the mild of makeup remover, moisturizing, the work efficiently removed ornaments and formal dress With.
Further preferably are as follows: in the step 5, when arginine is added, arginine is added while stirring, the speed of stirring is 100-120rpm, adding arginic speed is 0.00115-0.0002 parts/15s.
By using above-mentioned technical proposal, be conducive to be substantially soluble in the arginine being added in the system of liquid phase, to make The pH value of display can be more accurate.
In conclusion the invention has the following advantages:
The first, the micella makeup remover of mild moisturizing provided by the invention can be mild makeup removing so that skin surface cleaning is without residual It stays, wherein butanediol, glycerol, the first skin conditioning agent, Second Skin conditioner have preferable maintenance effect to skin, so that Skin has effects that moisturizing, soft and moist, calm, pore refining of releiving.
The second, the first skin conditioning agent, Second Skin conditioning in the micella makeup remover of mild moisturizing provided by the invention Agent also has effect anti-oxidant, that anti-inflammatory is antibacterial to skin.
Third, the micella makeup remover of mild moisturizing provided by the invention have the characteristics that mild non-stimulated.
Specific embodiment
Invention is further described in detail with reference to embodiments.
Embodiment 1: a kind of mild clean micella makeup remover, included component and its corresponding parts by weight such as table 1 It is shown, and acquisition is made by the steps:
Step 1, water is weighed, is heated to 100 DEG C, constant temperature 10min is cooled to room temperature;
Step 2, weigh PEG-8 caprylic/capric glyceride type, antibacterial agent butanediol, glycerol be added to by step 1 through cooling Into the water of room temperature, 80 DEG C are heated to, sufficiently dissolve and is mixed to transparent, mixture A is obtained;
Step 3, mixture A obtained in step 2 is cooled to 40 DEG C, weighs the first skin conditioning agent, Second Skin conditioner, And be added sequentially in mixture A, sufficiently dissolve and mix to transparent, obtain mixture A1;
Step 4, it weighs antibacterial agent and is added in the mixture A1 obtained by step 3, sufficiently dissolve and mix to transparent, obtain mixed Close object A2;
Step 5, arginine is weighed, is added in the mixture A2 obtained by step 4, when arginine is added, is added while stirring Arginine, the speed of stirring are 100rpm, and adding arginic speed is 0.00115 part/15s, sufficiently dissolves and mixes, and are adjusted The pH of mixture obtains mixture A3 between 5.5;
Step 6, the mixture A3 obtained by step 5 is cooled to 25 DEG C, discharging obtains the micella makeup remover of mild moisturizing.
Wherein, the first skin conditioning agent is extracted by the bermuda lily bulb that weight percent is 99%: 0.5%: 0.5% Object, sodium formate, citric acid composition;Second Skin conditioner is by 15%: 15%: 70% calendula extract, propylene glycol, second Skin conditioning agent is formed with water.
Antibacterial agent by weight fraction ratio be 1.8: 1: 1.2: 13: 3 decoyl hydroximic acid, Sensiva SC50,1,2- oneself two Alcohol, antibacterial agent butanediol, antibacterial agent are formed with water.
Embodiment 2-7: a kind of mild clean micella makeup remover, the difference from embodiment 1 is that, included component and Its corresponding parts by weight is as shown in table 1.
Component and its parts by weight included by 1. embodiment 1-7 of table
Embodiment 8: a kind of mild clean micella makeup remover, the difference from embodiment 1 is that, the first skin conditioning agent by Bermuda lily bulb extract that weight percent is 99.4%: 0.5%: 0.1%, sodium formate, citric acid composition;Second Skin Conditioner is made of 15%: 30%: 55% calendula extract, propylene glycol, Second Skin conditioner with water.
Embodiment 9: a kind of mild clean micella makeup remover, the difference from embodiment 1 is that, the first skin conditioning agent by Bermuda lily bulb extract that weight percent is 99.2%: 0.5%: 0.3%, sodium formate, citric acid composition;Second Skin Conditioner is made of 15%: 22%: 63% calendula extract, propylene glycol, Second Skin conditioner with water.
Embodiment 10: a kind of mild clean micella makeup remover, the difference from embodiment 1 is that, in step 1, when constant temperature Between be 20min;In step 2,85 DEG C are heated to, is cooled to 50 DEG C;In step 5, adjusting pH is 5.8;In step 6, it is cooled to 30 ℃。
Embodiment 11: a kind of mild clean micella makeup remover, the difference from embodiment 1 is that, in step 5, essence is added When propylhomoserin, the speed of stirring is 110rpm, and adding arginic speed is 0.00118 part/15s.
Embodiment 12: a kind of mild clean micella makeup remover, the difference from embodiment 1 is that, in step 5, essence is added When propylhomoserin, the speed of stirring is 120rpm, and adding arginic speed is 0.0002 part/15s.
Comparative example 1-5: a kind of makeup remover, the difference with embodiment 3 be, included component and its corresponding parts by weight Number is as shown in table 2.
Component and its parts by weight included by 2. comparative example 1-5 of table
Comparative example 6: a kind of makeup remover, the difference with embodiment 3 are, by water, PEG-8 caprylic/capric glyceride type, fourth Glycol, glycerol, bermuda lily bulb extract, sodium benzoate, citric acid, calendula extract, propylene glycol, Second Skin conditioning It is agent water, decoyl hydroximic acid, Sensiva SC50,1,2- hexylene glycol, antibacterial agent butanediol, antibacterial agent water, arginine mixed It closes uniformly, obtains makeup remover.
Comparative example 7: a kind of makeup remover, the difference with embodiment 3 be, the component including following parts by weight: lecithin 11 parts, 8 parts of camomile extract, 7 parts of disodium ethylene diamine tetraacetate, 10 parts of glycerol, 3 parts of cocinic acid sucrose ester, lanolin 6 Part, 12 parts of polyvinyl alcohol, 4- parts of olive oil, 1 part of methyl isopropyl thiazolinone, 2 parts of zinc gluconate, 2 parts of tea tree ethereal oil, polyoxy second 9 parts of alkene sorbitan monolaurate, 25 parts of deionized water.
Test: makeup removing effect evaluation test
Test specimen: using embodiment 1-12 and comparative example 1-7 as test specimen.
Subjects: choose areal, age bracket 25-35 year old, facial skin health, without acne, inflammation, sensitivity The women white collar of type skin quality 190 is equally divided into 19 groups, every group 10, is respectively labeled as 1-19 group.Wherein 1-12 group volunteer Embodiment 1-12 is used respectively, and 13-19 group aspiration uses comparative example 1-7 respectively.
Test method: every volunteer uses respectively with a BB white (w/o type), with a eye shadow, with a informer, same A lipstick is made up, and is then removed ornaments and formal dress respectively using corresponding test specimen.Every volunteer according to makeup removing effect and Skin sense after makeup removing is evaluated.
Evaluation criterion:
Makeup removing degree: it is poor, poor, general, substantially clean, very clean that number 1,2,3,4,5 respectively represents;
Skin sense is evaluated after makeup removing: the soft and moist degree that number 1,2,3,4,5 respectively represents skin is poor, poor, medium, preferable, good;
Whether had acne or acne phenomenon: "Yes" selects " 1 ", and "No" selects " 0 ";
Ocular irritation: number 1,2,3 respectively represent Ocular irritation without, slightly stimulation, obviously feel to stimulate.
Every tested volunteer evaluates according to above-mentioned standard, and then as unit of group, statistical test result is simultaneously asked Average value records and analyzes.
Test result: the makeup removing effect evaluation result using embodiment 1-12, comparative example 1-7 is as shown in table 3.
Table 3 uses the makeup removing effect evaluation result of embodiment 1-12, comparative example 1-7
From table 3 it can be seen that the makeup removing degree of comparative example 1-12 and comparative example 1-7, the makeup removing journey of embodiment 1-10 Degree is apparently higher than comparative example 1-6, and the degree of removing ornaments and formal dress of comparative example 7 is suitable with embodiment 1-12, and wherein the makeup removing effect of embodiment 3 is most It is good.According to the composition analysis of the raw material components of makeup remover it can be concluded that, butanediol, glycerol, the first skin conditioning agent, Second Skin The mutual cooperation of conditioner can largely influence the makeup removing effect of makeup remover.And butanediol therein, glycerol, the second skin Propylene glycol in skin conditioner has the function of solvent, can cooperate with PEG-8 caprylic/capric glyceride type and improve makeup remover The performance of dirt is dissolved, to be conducive to improve the makeup removing degree of makeup remover.
The makeup removing effect evaluation of comparative example 3, embodiment 10-12 and comparative example 6 can be seen that the production work of makeup remover Heating temperature, time in skill, the pH of mixing speed, time and mixture can influence the makeup removing effect of makeup remover, especially It is the skin sense after makeup removing degree, makeup removing.
After comparison can be seen that the makeup removing of embodiment 1-12 using the skin sense after embodiment 1-12 and comparative example 1-7 makeup removing Skin sense evaluation be apparently higher than comparative example 1-7, wherein embodiment 3,4 remove ornaments and formal dress after skin sense evaluate highest.According to the original of makeup remover Expect component composition it can be concluded that, butanediol, glycerol, the first skin conditioning agent, Second Skin conditioner will affect makeup remover Makeup removing degree.Butanediol, glycerol are small molecule moisturizing ingredient, have preferable moistening effect to skin;First skin tune Bermuda lily bulb extract and citric acid in reason agent have effects that moisturizing, oxidation resistant, Second Skin conditioner to skin In calendula extract have the function of anti-inflammatory, antibacterial and anti-aging to skin.Thus said components are conducive to improve Mildness, the moisture retention of makeup remover, so that volunteer is after using embodiment 1-9, skin sense is preferable.
Volunteer is compared in can be seen that the phenomenon that whether playing acne or acne using embodiment 1-12 and comparative example 1-7 Using not had the phenomenon that acne or acne after embodiment 1-12, and volunteer after comparative example 1-3,6-7 using occurring The phenomenon that acne or acne, wherein has there is acne in comparative example 1 or acne phenomenon is most.Comparative example embodiment 1-12 and comparative example 1-3 Test case, according to the composition of the raw material components of makeup remover it can be concluded that, the first skin conditioning agent, Second Skin conditioner pair Skin has preferable anti-inflammatory, bacteriostasis efficacy, so as to effectively inhibit the generation of acne or acne phenomenon.
Comparison volunteer can be seen that implementation the case where Ocular irritation after using embodiment 1-12 and comparative example 1-7 Example 1-12 and comparative example 1-6 without irritation, illustrates raw material components used in this application and dosage to eye part skin eye It is mild non-stimulated.And comparative example 7 has irritation to eye part skin, without mild feature, this illustrates addition Component has large effect to the irritation of test specimen.
This specific embodiment is only explanation of the invention, is not limitation of the present invention, those skilled in the art Member can according to need the modification that not creative contribution is made to the present embodiment after reading this specification, but as long as at this All by the protection of Patent Law in the scope of the claims of invention.

Claims (9)

1. a kind of mild clean micella makeup remover, which is characterized in that the component including following parts by weight:
1.0-10 parts of PEG-8 caprylic/capric glyceride type;
0.5-5 parts of butanediol;
0.5-5 parts of glycerol;
0.002-2 parts of skin conditioning agent;
0.5-5 parts of antibacterial agent;
0.0011-0.0015 parts of pH adjusting agent;
85-95 parts of water;
The skin conditioning agent includes at least one of the first skin conditioning agent, Second Skin conditioner;First skin Conditioner is made of bermuda lily bulb extract, sodium benzoate, citric acid;The Second Skin conditioner is by propylene glycol, gold Small cup flower extract, Second Skin conditioner are formed with water.
2. a kind of mild clean micella makeup remover according to claim 1, which is characterized in that the skin conditioning agent by The group of following parts by weight is grouped as:
First 0.001-1 parts of skin conditioning agent;0.001-1 parts of Second Skin conditioner.
3. a kind of mild clean micella makeup remover according to claim 1, which is characterized in that first skin condition Agent is bermuda lily bulb extract, the sodium formate, lemon of (99-99.4) %:0.5%:(0.1-0.5) % by following weight percent Lemon acid composition.
4. a kind of mild clean micella makeup remover according to claim 1, which is characterized in that the Second Skin conditioning Agent by following weight percent be 15%:(15-30) %:(55-70) and % calendula extract, propylene glycol, Second Skin conditioner It is formed with water.
5. a kind of mild clean micella makeup remover according to claim 1, which is characterized in that the antibacterial agent is by decoyl Hydroximic acid, Sensiva SC50,1,2- hexylene glycol, antibacterial agent butanediol, antibacterial agent are formed with water.
6. a kind of mild clean micella makeup remover according to claim 5, which is characterized in that pungent in the antibacterial agent Acyl hydroximic acid, Sensiva SC50,1,2- hexylene glycol, antibacterial agent butanediol, antibacterial agent water weight fraction ratio be 1.8: 1:1.2:13:3。
7. a kind of mild clean micella makeup remover according to claim 1, which is characterized in that the pH adjusting agent is essence Propylhomoserin.
8. a kind of production technology of mild clean micella makeup remover, feature described in any one of claim 1-7 exist In including the following steps:
Step 1, according to parts by weight, water is weighed, is heated to 100 DEG C, constant temperature 10-20min is cooled to room temperature;
Step 2, according to parts by weight, weigh PEG-8 caprylic/capric glyceride type, antibacterial agent butanediol, glycerol be added to by It is cooled in step 1 in the water of room temperature, is heated to 80-85 DEG C, sufficiently dissolve and mixed to transparent, obtain mixture A;
Step 3, mixture A obtained in step 2 is cooled to 40-50 DEG C, according to parts by weight, weighs the first skin condition Agent, Second Skin conditioner, and be added sequentially in mixture A are sufficiently dissolved and are mixed to transparent, obtain mixture A1;
Step 4, according to parts by weight, weigh antibacterial agent and be added in the mixture A1 obtained by step 3, sufficiently dissolve and mix It is even to transparent, obtain mixture A2;
Step 5, according to parts by weight, arginine is weighed, is added in the mixture A2 obtained by step 4, is sufficiently dissolved and mix It is even, the pH of mixture is adjusted between 5.5-5.8, obtains mixture A3;
Step 6, the mixture A3 obtained by step 5 is cooled to 25-30 DEG C, discharging obtains the micella makeup remover of mild moisturizing.
9. a kind of production technology of mild clean micella makeup remover according to claim 8, which is characterized in that the step In rapid 5, when arginine is added, arginine is added while stirring, the speed of stirring is 100-120rpm, adds arginic speed For 0.00115-0.0002 parts/15s.
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