CN115068381A - Natural mild makeup removing lotion and preparation method thereof - Google Patents

Natural mild makeup removing lotion and preparation method thereof Download PDF

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Publication number
CN115068381A
CN115068381A CN202210764823.6A CN202210764823A CN115068381A CN 115068381 A CN115068381 A CN 115068381A CN 202210764823 A CN202210764823 A CN 202210764823A CN 115068381 A CN115068381 A CN 115068381A
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skin
makeup removing
parts
emollient
humectant
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CN115068381B (en
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魏泽新
陈国祥
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Hangzhou Xinyue Cosmetic Co ltd
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Hangzhou Xinyue Cosmetic Co ltd
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
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    • A61K8/34Alcohols
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    • A61K8/36Carboxylic acids; Salts or anhydrides thereof
    • A61K8/365Hydroxycarboxylic acids; Ketocarboxylic acids
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    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/42Amides
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    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/60Sugars; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/63Steroids; Derivatives thereof
    • AHUMAN NECESSITIES
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    • A61K8/67Vitamins
    • A61K8/678Tocopherol, i.e. vitamin E
    • AHUMAN NECESSITIES
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    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/735Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8147Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
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    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/14Preparations for removing make-up
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/005Antimicrobial preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
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    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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Abstract

The application relates to the field of makeup removing lotion, in particular to natural mild makeup removing lotion and a preparation method thereof. A natural mild makeup removing lotion is prepared from the following raw materials in parts by weight: 60-80 parts of solvent, 5.1001-20.1 parts of emollient, 0.3-19 parts of humectant, 0.11-1.5 parts of chelating agent, 0.1-1 part of pH regulator, 0.1-1 part of thickener, 0.01-1 part of hair conditioner, 0.01-1 part of antioxidant and 0.009-0.5 part of skin conditioner. The skin care cream has the advantages of good makeup removing capability, mild makeup removing, small skin irritation, capability of balancing cutin, skin moistening, no-washing, full-face massage and use as skin care cream, and effects of water and oil balance and smooth skin feel.

Description

Natural mild makeup removing lotion and preparation method thereof
Technical Field
The application relates to the field of makeup removing lotion, in particular to natural mild makeup removing lotion and a preparation method thereof.
Background
The beauty is good for all people, and one beautiful face can add different colors to the individual, thereby bringing different senses to people. From ancient times to present, face care and makeup are all necessary things for people. People can certainly not take off the makeup removing process, but if the makeup is not completely removed, the residual cosmetic components can cause the pore blockage of the facial skin, so that the water and oil secretion of skin oil is disordered, and then the puzzling skin problems of acne, comedo, blackhead and the like are caused.
Currently, the makeup removing products on the market are roughly divided into three types, namely makeup removing water, makeup removing oil/cream and makeup removing cream. Among them, makeup remover is generally composed of aqueous base, and oil phase is little or even absent, resulting in poor makeup remover ability. The makeup removing oil/cream is usually composed of oil and an emulsifier, and can also have makeup removing effect on cosmetics taking oil as a matrix such as lipstick, mascara and the like, but the polymer and the film forming agent which are required to be waterproof and oilproof are difficult to remove. The makeup removing emulsion is an oil phase, a water phase and an emulsifier, can remove grease, film forming agents, macromolecular polymers and the like, and has an increasing advantage in the future makeup removing market. However, the makeup removing capability on the market at present basically meets the makeup removing requirement, but the makeup removing capability has large irritation to skin, needs to be washed by water, has low makeup removing efficiency, and wastes makeup removing raw materials after being removed.
Disclosure of Invention
In order to solve the technical problems, the application provides a natural mild makeup removing lotion and a preparation method thereof.
The application provides a natural mild type makeup removing lotion, can realize through following technical scheme:
a natural mild makeup removing lotion is prepared from the following raw materials in parts by weight: 60-80 parts of solvent, 5.1001-20.1 parts of emollient, 0.3-19 parts of humectant, 0.11-1.5 parts of chelating agent, 0.1-1 part of pH regulator, 0.1-1 part of thickener, 0.01-1 part of hair conditioner, 0.01-1 part of antioxidant and 0.009-0.5 part of skin conditioner.
The makeup removing device has good makeup removing capability, good and mild makeup removing effect and small skin irritation. The massage can balance cutin and moisten skin. The skin care cream can be free of washing, can be used for full-face massage of the skin care cream better due to the compound use of the grease and the emulsifier, and has the effect of the cream carried by the makeup removal cream without wiping the cream after makeup removal. In addition, the skin-care cream can be balanced by water and oil, and has the effect of smoothing skin.
Preferably, the skin conditioning agents comprise 0.005-0.1 parts of the first skin conditioning agent, 0.001-0.1 parts of the second skin conditioning agent, 0.001-0.1 parts of the third skin conditioning agent, 0.001-0.1 parts of the fourth skin conditioning agent and 0.001-0.1 parts of the fifth skin conditioning agent; the first skin conditioner is mainly prepared from deionized water, butanediol and a citrus junos extract; the second skin conditioner is mainly prepared from water, an extract of the rhizome/root of Taraxacum officinale, and 1, 2-pentanediol; the third skin conditioner is mainly prepared from deionized water, glycerol, moringa oleifera seed extract, phenoxyethanol, disodium hydrogen phosphate and citric acid; the fourth skin conditioner is dipotassium glycyrrhizinate; the fifth skin conditioning agent is sodium hyaluronate.
The first skin conditioner comprises an extract of Citrus aurantium fruit having cell proliferation activity, and is effective in inhibiting uricase, reducing ammonia-containing substances produced by uricase activity, and inhibiting body odor.
The second skin conditioner contains extract of rhizome/root of Taraxacum officinale Kitag which has antiinflammatory, antibacterial and skin conditioning effects.
The moringa oleifera seed extract in the third skin conditioner has the effects of resisting oxidation, resisting aging, preserving moisture and supplementing water, can eliminate free radicals, and has good oxidation and aging resisting functions. The phenoxyethanol has antibacterial effect and antiseptic effect, the disodium hydrogen phosphate is used as an acid-base blending agent, and the citric acid is used as a pH regulator, so that the pH value of a system can be regulated, and the cutin can be removed to play an antibacterial effect.
The fourth skin conditioner, dipotassium glycyrrhizinate, has antibacterial, antiinflammatory, toxic materials clearing away, antiallergic, and deodorant effects.
The fifth skin conditioner, sodium hyaluronate, has the effects of moisturizing, gelling and resisting wrinkles.
The components and the proportion of the first skin conditioner, the second skin conditioner, the third skin conditioner, the fourth skin conditioner and the fifth skin conditioner are regulated, optimized, so that the skin care cream has the advantages of better moisture retention and moisturizing, oxidation resistance, aging resistance, wrinkle resistance, cutin removal, bacteria resistance and inflammation diminishing, mild makeup removal, small skin irritation, capability of balancing cutin and skin moistening effect.
Preferably, the mass ratio of the deionized water to the butanediol to the citrus junos extract is 29.98: 69.96: 0.06; the mass ratio of the water to the extract of the rhizome/root of the dandelion and the 1, 2-pentanediol is 85.7:4.3: 10; the mass ratio of the deionized water to the glycerin to the moringa oleifera seed extract to the phenoxyethanol to the disodium hydrogen phosphate to the citric acid is 28.1:67:1.6:2:0.7: 0.6.
By optimizing the proportion of the components, the moisture retention and water supplement, oxidation resistance, aging resistance, wrinkle resistance, cutin removal, bacteria resistance and inflammation elimination performances of the water-based paint can be improved, the production cost is reduced, and the water-based paint has market competitiveness.
Preferably, the humectant is mainly prepared from the following raw materials in parts by weight: 0.1-8 parts of first humectant, 0.1-8 parts of second humectant and 0.1-3 parts of third humectant; the first humectant is dipropylene glycol DPG; the second humectant is butanediol; the third humectant is trehalose.
By adopting the technical scheme, the dipropylene glycol DPG, the butanediol and the trehalose have a good moisturizing effect, and the trehalose can form a unique protective film on the cell surface, so that the biomolecular structure is effectively protected from being damaged, and the skin-care lotion has a good skin-protecting effect and a skin-moistening effect.
Preferably, the emollient comprises 5-15 parts of a first emollient, 0.1-5 parts of a second emollient, and 0.0001-0.1 parts of a third emollient, the first emollient being PEG-7 glyceryl cocoate; the second emollient is composed of avocado oil PEG-11 esters and water, and the mass ratio of the avocado oil PEG-11 esters to the water is 99: 1.
The PEG-7 glyceryl cocoate has the advantages of excellent emulsifying, solubilizing and dispersing capabilities, and relatively good makeup removing effect is ensured; the avocado oil PEG-11 ester has excellent emulsifying, solubilizing, dispersing and lubricating capabilities, and is small in makeup removal stimulation and mild in makeup removal. Through adopting above-mentioned emollient formula for this application has better skin moisturizing effect and emulsification, solubilization, dispersibility are better, and this application has better makeup removing ability, and it is gentle to make up removing, and is amazing little to the skin, and guarantees the stability of quality and the production stability of this application.
In addition, based on the formula of the application, PEG-7 glyceryl cocoate and avocado oil PEG-11 ester are combined and compounded for use, so that the makeup removing capability of the application can be ensured, and meanwhile, when the application is used for removing makeup, the makeup removing stimulation is small, the makeup removing is mild, and the user experience is better.
Preferably, the third emollient is hydrogenated soybean oil, sweet almond oil, daily essence, coconut oil, tassel gardenia extract, tocopherol; the mass ratio of the hydrogenated soybean oil to the sweet almond oil to the daily essence to the coconut oil to the gardenia extract to the tocopherol is 48.485:48.5: 1.255: 0.85: 0.69: 0.22.
hydrogenated soybean oil is used herein as a lubricant. The sweet almond oil has the advantages of relieving, anti-allergy, moisturizing and low risk coefficient. Coconut oil has moistening and moisturizing effects, and coconut extract has good inhibitory effect on metalloprotease, and has antiaging and antiaging effects. The extract of the gardenia has the advantages of antibiosis, relieving and anti-allergy, low risk coefficient, and has the functions of calming, reducing blood pressure, bacteriostasis, diarrhea, easing pain, resisting inflammation, relieving and accelerating the healing of soft tissues. The tocopherol can increase the antioxidation of cells, maintain and promote the reproductive function, has certain anti-aging effect, can improve lipid metabolism, prevent arteriosclerosis and reduce blood fat, and is preferably prepared from 0.1-1 part of a first chelating agent and 0.01-0.5 part of a second chelating agent, wherein the first chelating agent is mainly prepared from 1, 3-propylene glycol, caprylyl hydroximic acid and 1, 2-hexanediol; the mass ratio of the 1, 3-propylene glycol, the caprylyl hydroximic acid and the 1, 2-hexanediol is 65:5: 30; the second chelating agent is mainly prepared from EDTA disodium and deionized water; the mass ratio of the EDTA disodium to the deionized water is 9: 1.
By adopting the technical scheme, the chelating agent is used in the skin care product and is mainly complexed with harmful metal ions in the raw materials, so that the harmful metal ions are prevented from causing adverse effects (such as fading, rancidity, inactivation and the like) on the product.
Preferably, the solvent is deionized water; the pH regulator is arginine; the thickening agent is carbomer; the antioxidant is p-hydroxyacetophenone; the hair conditioner is a daily essence.
Arginine is used as a pH regulator in the application, and also has the functions of detoxifying and diminishing inflammation. Carbomers act as thickening agents and are used as rheology modifiers. P-hydroxyacetophenone has better oxidation resistance.
The application provides a preparation method of a natural mild makeup removing lotion, which is realized by the following technical scheme: a preparation method of natural mild makeup removing lotion comprises the following steps:
firstly, accurately metering raw materials according to a ratio, and re-weighing the raw materials before manufacturing; 1% of volatile water needs to be supplemented in advance for standby;
adding deionized water with accurate measurement into a high-speed dispersion kettle, starting stirring, dispersing carbomer with accurate measurement into the high-speed dispersion kettle at the adding speed of 0.2-3g/min, after the raw materials are completely dispersed, adding dipropylene glycol, butanediol, trehalose, an antioxidant p-hydroxyacetophenone, a second chelating agent, a fourth skin conditioner dipotassium glycyrrhizinate and a fifth skin conditioner sodium hyaluronate into a humectant in the high-speed dispersion kettle, starting heating to 70 +/-2 ℃, and continuously stirring until the material body is uniform and free of agglomerated particles;
step three, after the material in the high-speed dispersion kettle is uniformly stirred and does not have agglomerated particles, cooling to 50-55 ℃; mixing and dissolving arginine and deionized water in a mass ratio of 1:3 to obtain a transparent solution, adding the prepared arginine aqueous solution, adjusting the pH value to 4.5-7.5, starting homogenizing at 2000 +/-200 rpm, ultrasonically stirring for 3-5min at an ultrasonic frequency of 20-25kHZ, and then continuously stirring and cooling;
step four, when the temperature of the materials in the high-speed dispersion kettle is reduced to 50 +/-2 ℃, adding a first emollient, a second emollient, a first skin conditioner, a second skin conditioner and a third skin conditioner into the high-speed dispersion kettle, starting homogenization at 2000 +/-200 rpm, ultrasonically stirring for 3-5min at the ultrasonic frequency of 20-25kHZ, and then continuously stirring and reducing the temperature;
fifthly, when the temperature of the materials in the high-speed dispersion kettle is reduced to 40 +/-2 ℃, adding a first chelating agent, a hair conditioner and a third emollient, starting homogenizing at 2500 +/-50 rpm, and carrying out ultrasonic stirring for 2min at an ultrasonic frequency of 20 kHZ;
and sixthly, stirring and cooling to 37 +/-0.5 ℃, sampling and conveying to a product pipe for detection, and discharging to obtain a finished product after the product pipe is qualified.
By adopting the technical scheme, the preparation method is relatively simple and mature, can be used for batch production, and the quality of finished products in the same batch is relatively stable.
In summary, the present application has the following advantages:
1. the cleansing cream has good cleansing capability, mild cleansing, small stimulation to skin, capability of balancing cutin and moisturizing skin,
2. the skin care cream can be used as a skin care cream for full-face massage, and achieves the effects of water-oil balance and smooth skin feel.
3. The preparation method is relatively simple and mature, can be used for batch production, and the quality of finished products in the same batch is relatively stable.
Detailed Description
The present application will be described in further detail with reference to examples and comparative examples.
Examples
The formula of a natural mild cleansing milk disclosed in examples 1-3 is shown in table 1:
table 1 shows the formulation of the natural mild makeup remover in examples 1 to 3
Figure BDA0003721783350000041
Figure BDA0003721783350000051
A preparation method of natural mild makeup removing lotion comprises the following steps:
firstly, accurately metering raw materials according to a ratio, and re-weighing the raw materials before manufacturing; 1% of volatile water needs to be supplemented in advance for standby; preparing a chelating agent for later use by using 1, 3-propylene glycol, caprylyl hydroximic acid and 1, 2-hexanediol according to the mass ratio of 65:5: 30; preparing a second chelating agent for later use according to the mass ratio of the EDTA disodium to the deionized water of 9: 1;
hydrogenated soybean oil, sweet almond oil, daily essence, coconut oil, the extract of the gardenia jasminoides, and tocopherol are mixed according to the mass ratio of 48.485:48.5: 1.255: 0.85: 0.69: 0.22 preparing a third emollient for standby;
preparing a second emollient for later use by using avocado oil PEG-11 esters and water in a mass ratio of 99: 1;
deionized water, butanediol and orange fruit extract are mixed according to the mass ratio of 29.98: 69.96, 0.06 preparing a first skin conditioner for standby;
preparing a second skin conditioner for later use by using water, the extract of the rhizome/root of the dandelion and the 1, 2-pentanediol, wherein the mass ratio of the water to the extract of the rhizome/root of the dandelion is 85.7:4.3: 10; preparing a third skin conditioner for later use by using deionized water, glycerol, a moringa oleifera seed extract, phenoxyethanol, disodium hydrogen phosphate and citric acid in a mass ratio of 28.1:67:1.6:2:0.7: 0.6;
adding deionized water with accurate measurement into a high-speed dispersion kettle, starting stirring, dispersing carbomer with accurate measurement into the high-speed dispersion kettle at the adding speed of 0.8g/min, after the raw materials are completely dispersed, adding dipropylene glycol, butanediol, trehalose, an antioxidant p-hydroxyacetophenone, a second chelating agent, a fourth skin conditioner dipotassium glycyrrhizinate and a fifth skin conditioner sodium hyaluronate into a humectant, starting heating to 70 +/-2 ℃, and continuously stirring until the material is uniform and free of agglomerated particles;
step three, after the material in the high-speed dispersion kettle is uniformly stirred and does not contain agglomerated particles, cooling to 50-55 ℃; mixing and dissolving accurately-measured arginine and deionized water in a mass ratio of 1:3 to obtain a transparent solution, adding the prepared arginine aqueous solution, adjusting the pH value to 6-7, starting homogenizing at 2000rpm, carrying out ultrasonic stirring for 5min at an ultrasonic frequency of 20kHz, and then continuing stirring and cooling;
step four, when the temperature of the materials in the high-speed dispersion kettle is reduced to 50 +/-2 ℃, adding a first emollient, a second emollient, a first skin conditioner, a second skin conditioner and a third skin conditioner into the high-speed dispersion kettle, starting homogenizing at 2000rpm, carrying out ultrasonic stirring for 3min at the ultrasonic frequency of 20kHz, and then continuing stirring and reducing the temperature;
fifthly, when the temperature of the materials in the high-speed dispersion kettle is reduced to 40 +/-2 ℃, adding a first chelating agent, a hair conditioner and a third emollient, starting homogenizing at 2500rpm, and ultrasonically stirring for 2min at the ultrasonic frequency of 25 kHz;
and sixthly, stirring and cooling to 37 +/-0.5 ℃, sampling and conveying to a product pipe for detection, and discharging to obtain a finished product after the product pipe is qualified. The sample in the application meets the standards of technical specifications of cosmetics (2015 edition) and GB/T35914-.
Comparative example
Comparative example 1 is a commercially available makeup remover water-ni yan culvert oxygen deep moisturizing remover 22941 water.
Comparative example 2 is a commercially available makeup removing milk-Keke dry sensitive muscle makeup removing honey.
The formula of one of the natural mild makeup removers disclosed in comparative examples 3 to 4 is shown in table 2:
table 2 shows the formulation of the natural mild makeup remover in example 1 and comparative examples 3 to 4
Figure BDA0003721783350000061
Figure BDA0003721783350000071
Performance test
Detection method/test method
One, usage evaluation-consumer experience:
(1) evaluating the object: the test group used the cleansing cream of examples 1-3, code A/B/C; the control group is the cleansing water in comparative example 1, number D; the makeup remover cream in comparative example 2, No. E; the cleansing milk in comparative examples 3 to 4, No. F/G.
(2) Test objects: 5 females of 16-24 years old, 5 females of 25-36 years old, 5 females of 37-45 years old and 5 females above 45 years old, wherein the skin sensitivity index of a tester is 0, and the skin is healthy.
(3) The test method comprises the following steps: the makeup removing cream in the examples 1 to 3 and the makeup removing products in the comparative examples 1 to 4 are selected as a test group, and corresponding labels are attached to the bottoms of the makeup removing products, such as label A attached to the bottoms of the makeup removing products containing the makeup removing cream in the example 1. Each test subject needs to evaluate a test set. Before the test subjects used, the makeup removal products in one test group were evaluated after being disorganized in sequence. And (4) arranging the makeup removing products to be tested in sequence from the best to the next according to personal judgment by the evaluation object, recording marks of the arrangement sequence of the makeup removing products, and collecting statistics, ranking and forming a table. The judgment standard is divided into four parts, specifically, makeup removing effect, moisturizing effect, anti-allergic and anti-inflammatory irritation and smearing feeling.
Table 3 is an evaluation of the use of the make-up removal products of examples 1 to 3 and examples 1 to 4
Figure BDA0003721783350000081
As can be seen by combining examples 1-3 and comparative examples 1-4 with Table 3, the makeup remover creams of examples 1-3 in this application are better in popularity than comparative examples 1-2 than comparative examples 3-4. Wherein, after the content of PEG-7 glyceryl cocoate is too low, the makeup removing capability is reduced, so that the use evaluation ranking is lower, and the PEG-7 glyceryl cocoate is controlled to be 10-15% more suitably. Example 1 is the best formulation in this application and is best accepted by the market.
As can be seen by combining examples 1-3 and comparative examples 1-4 with Table 3, the cleansing milk in example 4 was the least evaluated in terms of use, mainly because of irritation in cleansing, poor application feeling, and high skin-friendliness during the consumption of the cleansing product by the consumer.
Second, use evaluation-sensory rating of consumer:
(1) evaluating the object: the test groups were prepared using the make-up remover in example 1, comparative example 1 and the make-up remover in comparative example 2, example 1 No. a, comparative example 2 No. b.
(2) Test objects: 10 women aged 16 to 35 and 10 women aged 35 and older, the skin sensitivity index of the test person was 0, the skin was healthy, 20 evaluation groups were formed, and the use ratings were made for the makeup removal products in example 1 and comparative examples 1 to 2. The test subjects applied the same amount of mascara (karaya mascara, product number: 262705) to the eyelashes and removed makeup after 1 hour.
(3) The test method comprises the following steps: the test person evaluated A, a and b test makeup removal products for makeup removal effect, moisturizing effect, anti-allergic anti-inflammatory irritation, and spreading sensation, respectively. The rating scoring criteria were as follows:
Figure BDA0003721783350000082
table 4 is an evaluation of the cleansing milks in example 1 and comparative example 2
Figure BDA0003721783350000091
By combining the example 1 and the comparative examples 1-2 and the table 4, the total score of the cleansing milk in the example 1 is 144, the total score of the cleansing milk in the comparative example 2 is 128, and the total score of the cleansing water in the comparative example 1 is 126, so that the cleansing milk in the example 1 has better cleansing effect, moisturizing effect, anti-allergic and anti-inflammatory irritation property and smearing feeling than market products, has better cleansing capability, is mild in cleansing, has less irritation to skin, can balance cutin and has the function of moistening skin.
Thirdly, testing the makeup removing capability: the test group used the make-up remover of example 1; the control group was the makeup remover cream of comparative example 2. Test object(s): 3 females aged 16-24, 3 females aged 25-36, 3 females aged 37-45, and 3 females over 45.
Test method 1, the test subjects applied the same dose of sunscreen (yulan Oil (OLAY) skin lightening sunscreen, trade designation: 216110) to the half face and removed makeup after 1 hour.
The test method 2: the test subjects applied the same amount of lip glaze (YSL small black bar 302 of holy land) to the lips and removed makeup after 1 hour.
Test method 3: the test subjects applied the same amount of mascara (karaya mascara, product number: 262705) to the eyelashes and removed makeup after 1 hour.
And recording the evaluation and scoring of the makeup removing capability of the test object.
Evaluation criteria: well: 3 minutes, preferably: 1 minute, general: 0 min, difference: -1 point.
Table 5 shows the makeup removing ability test parameters of the makeup removing cream of example 1
Figure BDA0003721783350000092
Figure BDA0003721783350000101
As can be seen by combining example 1 and comparative example 2 with table 5, the makeup removing effect of example 1 in the present application is better.
Fourthly, moisture retention test: the test group used the make-up remover of example 1; the control group was moisturizing bath oil. Test objects: 3 females aged 16-24, 3 females aged 25-36, 3 females aged 37-45, and 3 females aged over 45.
The test method comprises the following steps: the pixel color was tested, and after washing off the cream in example 1 with clean water, the cream was wiped on one half of the face and the moisturizing bath oil was wiped on the other half of the face.
And recording the evaluation and the scoring of the moisturizing capability of the test object. Evaluation criteria: well: 3 minutes, preferably: 1 minute, general: 0 min, difference: -1 point.
Table 6 shows the moisturizing ability test parameters
Figure BDA0003721783350000102
As can be seen from the combination of example 1 and comparative example 2 and table 6, the moisturizing effect of example 1 in the present application is better.
In conclusion, the makeup remover has better makeup removing capability, good and mild makeup removing effect and small skin irritation. The massage can balance cutin and moisten skin. The skin care cream can be free of washing, can be used for full-face massage of the skin care cream better due to the compound use of the grease and the emulsifier, and has the effect of the cream carried by the makeup removal cream without wiping the cream after makeup removal. In addition, the skin-care cream can be balanced by water and oil, and has the effect of smoothing skin.
The present embodiment is only for explaining the present application, and it is not limited to the present application, and those skilled in the art can make modifications of the present embodiment without inventive contribution as needed after reading the present specification, but all of them are protected by patent law within the scope of the claims of the present application.

Claims (9)

1. A natural mild makeup removing lotion is characterized in that: the feed is prepared from the following raw materials in parts by weight: 60-80 parts of solvent, 5.1001-20.1 parts of emollient, 0.3-19 parts of humectant, 0.11-1.5 parts of chelating agent, 0.1-1 part of pH regulator, 0.1-1 part of thickener, 0.01-1 part of hair conditioner, 0.01-1 part of antioxidant and 0.009-0.5 part of skin conditioner.
2. The natural mild makeup removing cream according to claim 1, characterized in that: the skin conditioning agent comprises 0.005-0.1 part of first skin conditioning agent, 0.001-0.1 part of second skin conditioning agent, 0.001-0.1 part of third skin conditioning agent, 0.001-0.1 part of fourth skin conditioning agent and 0.001-0.1 part of fifth skin conditioning agent; the first skin conditioner is mainly prepared from deionized water, butanediol and a citrus junos extract; the second skin conditioner is mainly prepared from water, an extract of the rhizome/root of Taraxacum officinale, and 1, 2-pentanediol; the third skin conditioner is mainly prepared from deionized water, glycerol, moringa oleifera seed extract, phenoxyethanol, disodium hydrogen phosphate and citric acid; the fourth skin conditioner is dipotassium glycyrrhizinate; the fifth skin conditioning agent is sodium hyaluronate.
3. The natural mild makeup removing cream according to claim 1, characterized in that: the mass ratio of the deionized water to the butanediol to the citrus junos extract is 29.98: 69.96: 0.06; the mass ratio of the water, the dandelion rhizome/root extract and the 1, 2-pentanediol is 85.7:4.3: 10; the mass ratio of the deionized water to the glycerin to the moringa oleifera seed extract to the phenoxyethanol to the disodium hydrogen phosphate to the citric acid is 28.1:67:1.6:2:0.7: 0.6.
4. The natural mild makeup removing cream according to claim 2, characterized in that: the humectant is mainly prepared from the following raw materials in parts by weight: 0.1-8 parts of first humectant, 0.1-8 parts of second humectant and 0.1-3 parts of third humectant; the first humectant is dipropylene glycol DPG; the second humectant is butanediol; the third humectant is trehalose.
5. The natural mild makeup removing cream according to claim 4, wherein: the emollient comprises 5-15 parts of a first emollient, 0.1-5 parts of a second emollient and 0.0001-0.1 part of a third emollient, wherein the first emollient is PEG-7 glyceryl cocoate; the second emollient is composed of avocado oil PEG-11 esters and water, and the mass ratio of the avocado oil PEG-11 esters to the water is 99: 1.
6. The natural mild makeup removing cream according to claim 5, wherein: the third emollient is hydrogenated soybean oil, sweet almond oil, daily essence, coconut oil, extract of Gardenia jasminoides Ellis, and tocopherol; the mass ratio of the hydrogenated soybean oil to the sweet almond oil to the daily essence to the coconut oil to the gardenia extract to the tocopherol is 48.485:48.5: 1.255: 0.85: 0.69: 0.22.
7. the natural mild makeup removing cream according to claim 5, wherein: the chelating agent comprises 0.1-1 part of first chelating agent and 0.01-0.5 part of second chelating agent, wherein the first chelating agent is mainly prepared from 1, 3-propylene glycol, caprylyl hydroximic acid and 1, 2-hexanediol; the mass ratio of the 1, 3-propylene glycol, the caprylyl hydroximic acid and the 1, 2-hexanediol is 65:5: 30; the second chelating agent is mainly prepared from EDTA disodium and deionized water; the mass ratio of the EDTA disodium to the deionized water is 9: 1.
8. The natural mild makeup removing cream according to claim 7, wherein: the solvent is deionized water; the pH regulator is arginine; the thickening agent is carbomer; the antioxidant is p-hydroxyacetophenone; the hair conditioner is a daily essence.
9. A method for preparing the natural mild makeup removing cream according to any one of claims 1 to 8, characterized in that: the method comprises the following steps:
firstly, accurately metering raw materials according to a ratio, and re-weighing the raw materials before manufacturing; 1% of volatile water needs to be supplemented in advance for standby;
adding deionized water with accurate measurement into a high-speed dispersion kettle, starting stirring, dispersing carbomer with accurate measurement into the high-speed dispersion kettle at the adding speed of 0.2-3g/min, after the raw materials are completely dispersed, adding dipropylene glycol, butanediol, trehalose, an antioxidant p-hydroxyacetophenone, a second chelating agent, a fourth skin conditioner dipotassium glycyrrhizinate and a fifth skin conditioner sodium hyaluronate into a humectant in the high-speed dispersion kettle, starting heating to 70 +/-2 ℃, and continuously stirring until the material body is uniform and free of agglomerated particles;
step three, after the material in the high-speed dispersion kettle is uniformly stirred and does not contain agglomerated particles, cooling to 50-55 ℃; mixing and dissolving arginine and deionized water in a mass ratio of 1:3 to obtain a transparent solution, adding the prepared arginine aqueous solution, adjusting the pH value to 4.5-7.5, starting homogenizing at 2000 +/-200 rpm, ultrasonically stirring for 3-5min at an ultrasonic frequency of 20-25kHZ, and then continuously stirring and cooling;
step four, when the temperature of the materials in the high-speed dispersion kettle is reduced to 50 +/-2 ℃, adding a first emollient, a second emollient, a first skin conditioner, a second skin conditioner and a third skin conditioner into the high-speed dispersion kettle, starting homogenization at 2000 +/-200 rpm, ultrasonically stirring for 3-5min at the ultrasonic frequency of 20-25kHZ, and then continuously stirring and reducing the temperature;
fifthly, when the temperature of the materials in the high-speed dispersion kettle is reduced to 40 +/-2 ℃, adding a first chelating agent, a hair conditioner and a third emollient, starting homogenizing at 2500 +/-50 rpm, and carrying out ultrasonic stirring for 2min at an ultrasonic frequency of 20 kHZ;
and sixthly, stirring and cooling to 37 +/-0.5 ℃, sampling and conveying to a product pipe for detection, and discharging to obtain a finished product after the product pipe is qualified.
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