CN106309200A - Chitosan derivative based clean makeup-removing wet tissue with effects of bacterial inhibition and moisture preservation and preparation method of chitosan derivative based clean makeup-removing wet tissue - Google Patents
Chitosan derivative based clean makeup-removing wet tissue with effects of bacterial inhibition and moisture preservation and preparation method of chitosan derivative based clean makeup-removing wet tissue Download PDFInfo
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- CN106309200A CN106309200A CN201610788429.0A CN201610788429A CN106309200A CN 106309200 A CN106309200 A CN 106309200A CN 201610788429 A CN201610788429 A CN 201610788429A CN 106309200 A CN106309200 A CN 106309200A
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- wet tissue
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0208—Tissues; Wipes; Patches
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/736—Chitin; Chitosan; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/14—Preparations for removing make-up
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
- D04H1/42—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece
- D04H1/4382—Stretched reticular film fibres; Composite fibres; Mixed fibres; Ultrafine fibres; Fibres for artificial leather
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/28—Rubbing or scrubbing compositions; Peeling or abrasive compositions; Containing exfoliants
Abstract
The invention discloses chitosan derivative based clean makeup-removing wet tissue with effects of bacterial inhibition and moisture preservation. The chitosan derivative based clean makeup-removing wet tissue with the effects of bacterial inhibition and moisture preservation is prepared from raw materials in percentage by weight as follows: 2%-5% of chitosan derivatives, 5%-10% of PEG-8 caprylic/capric glycerides, 3%-8% of butanediol, 2%-5% of glycerin, 1%-3% of trehalose, 1%-5% of olive oil PEG-6 esters, 0.5%-3% of a skin conditioner, 0.15%-0.3% of phenoxyethanol, 0.15%-0.3% of ethylhexylglycerin, 0.1%-0.2% of methylparaben, 0.05%-0.2% of sodium hyaluronate, 0.01%-0.05% of essence and the balance of deionized water. According to the chitosan derivative based clean makeup-removing wet tissue with the effects of bacterial inhibition and moisture preservation and a preparation method, the makeup-removing wet tissue prepared with the preparation method is low in production cost, high in stability and good in cleansing power and realizes deep cleaning, besides, the makeup-removing wet tissue further has the effects of bacterial inhibition and moisture preservation, the facial skin after application of the makeup-removing wet tissue is smooth and tender, and makeup residues on the facial skin are removed.
Description
Technical field
Novel wet tissue material technical field of the present invention, be specifically related to a kind of based on chitosan derivatives antibacterial, moisturizing is clear
Clean makeup-removing wet tissue and preparation method thereof.
Background technology
Along with the development of economic society, modern metropolitan cities women plays the work of irreplaceability in the development of society
With, modern metropolitan cities women the most gradually starts to focus on the appearance instrument of oneself, and on the one hand urban woman is made up can increase women's
Beauty, another aspect is also to respect others on etiquette.Therefore, no matter any occasion does not advocates " vegetarian noodles now
Towards sky ", though not requiring with heavy makeup, but changing upper light adornment, the most still planting basic courtesy, it is possible to promote the confidence of oneself
The heart.Urban woman is made up, it is avoided that every day will be toward be coated with various cosmetics on the face, if makeup removing is thorough, cosmetics remain
On the face, blocked pore, the seriousness of consequence is well imagined, therefore, thorough cleaning skin, remove ornaments and formal dress up hill and dale, be definitely beauty treatment
Basic, on the one hand, although makeup removing uncomplicated, but after this process always can terminate at one day, that time to be had a rest enters
OK, during this time a lot of people are through daylong hardworking, often the most out of patience make a return journey at the bottom of dry linting with energy, eye shadow, lip pomade
And the mascara solution of stubbornness, going to bed with residual adornment, it is big to embrace head sleep；On the other hand, urban woman is in long-distance travel, often
On the vehicles such as train, motor-car, steamer, aircraft overnight, it has not been convenient to makeup removing, if things go on like this, skin there will be flavescence, pore
The phenomenon such as thick.
Makeup removal products the most in the market is when the dressing that the role's adornment etc. for color make-up, opera performer is thick and heavy, clear by it
Reason totally seems particularly difficult, it is necessary to remove coloured silk by oil-soluble product or by fat power is strong and the most irritating makeup removing liquid etc.
Adornment, role's adornment of opera performer, but, the said goods is easy to damage face skin than more sensitive women, unfavorable
In life-time service.The most modal makeup removing liquid and makeup removing breast are mostly canned, going on business or during out on tours, carry not
Delivery conveniently and can only be selected when airplane, it is impossible to take with oneself, in long-distance and needs women the most overnight, nothing
Method is removed ornaments and formal dress, and brings inconvenience.Therefore, a kind of easy to carry, makeup removal products thoroughly of removing ornaments and formal dress becomes cosmetic technical field
Fresh target.
Summary of the invention
The deficiency existed for prior art, novelty of the present invention provide a kind of based on chitosan derivatives press down
Bacterium, moisturizing cleaning makeup-removing wet tissue and preparation method thereof, makeup-removing wet tissue production cost prepared by this preparation method is low, has stability
By force, deep clean, good dirt-removing power, additionally, also have antibacterial, effect of moisturizing, the face skin after using is smooth, water
Tender, without color make-up residual.
The technical scheme is that and be achieved in that:
Antibacterial, moisturizing cleaning makeup-removing wet tissue based on chitosan derivatives, is made up of the raw material of following weight proportioning: chitosan spreads out
Biological 2-5%, PEG-8 caprylic/capric glyceride type 5-10%, butanediol 3-8%, glycerol 2-5%, trehalose 1-3%, olive oil
PEG-6 esters 1-5%, skin conditioning agent 0.5-3%, phenoxyethanol 0.15-0.3%, Sensiva SC50 0.15-0.3%, oxybenzene
Methyl ester 0.1-0.2%, hyaluronate sodium 0.05-0.2%, essence 0.01-0.05%, surplus are deionized water.
Preferably, it is made up of the raw material of following weight proportioning: chitosan derivatives 3%, PEG-8 caprylic/capric glyceride
Class 8%, butanediol 5%, glycerol 3%, trehalose 2%, olive oil PEG-6 esters 2%, skin conditioning agent 1.5%, phenoxyethanol
0.2%, Sensiva SC50 0.2%, methyl hydroxybenzoate 0.15%, hyaluronate sodium 1%, essence 0.03%, surplus are deionized water.
Preferably, described skin conditioning agent is that butanediol, Radix Astragali root extract, opoponax extract, Flos Inulae carry
Take thing, Flos Albiziae extract, Rhizoma Gastrodiae root extract and deionized water, mix with arbitrary proportion.
Preferably, described chitosan derivatives is any one in chitosan, oligochitosan and carboxymethyl chitosan, or two
Mix with arbitrary proportion more than kind.
The invention also discloses a kind of antibacterial, preparation method of moisturizing cleaning makeup-removing wet tissue based on chitosan derivatives,
Described preparation method comprises the following steps:
(1), weigh: check various raw material as requested, standby after weighing various raw materials according to formula proportion；
(2), successively by PEG-8 caprylic/capric glyceride type, butanediol, glycerol, trehalose, olive oil PEG-6 esters, hydroxyl
Benzene methyl, hyaluronate sodium and deionized water add in water preparation pot, open homogenizing, and frequency is 35Hz, and the time is 3-5min, open
Stirring, stirring is warming up to 90 DEG C, and rotating speed is that 30-40 turns/min, and mixing time is 10-20min, makes each raw material be completely dissolved to all
One water preparation shape；
(3), mixing liquid obtained in step (2) is cooled to 28-42 DEG C, then by water preparation pot is sequentially added into butanediol,
Radix Astragali root extract, opoponax extract, Flos Inulae extract, Flos Albiziae extract, Rhizoma Gastrodiae root extract and deionization
Water, open stirring, rotating speed is that 35-45 turns/min, and mixing time is 5-10min, after mixing time arrives, then by water preparation pot successively
Adding chitosan derivatives, phenoxyethanol, Sensiva SC50 and essence, be then turned on stirring, rotating speed is that 35-45 turns/min, stirs
The time of mixing is 10-15min, and stirring makes each raw material be completely dissolved to homogeneous water preparation shape；
(4), inspection: sample self-inspection, do the inspection of the PH before discharging, appearance test, filter discharging under qualified rear stirring at low speed；Discharging
After carry out microbial bacterial sum mycete inspection；
(5) after mixing time arrives, the filtrate that will prepare in step (4), after being cooled to room temperature, import full-automatic facial tissues machine, and
In full-automatic facial tissues machine, put into the non-woven fabrics folded after cutting, non-woven fabrics is immersed in filtrate 2-3 hour, after unlatching, entirely
Automatically facial tissues machine produces makeup-removing wet tissue, after makeup-removing wet tissue is put into packaging bag and seal.
Preferably, described non-woven fabrics is by the ES fiber preparation of carboxymethyl chitosan fiber, chitin fiber and low melting point
Become.
Preferably, the percentage by weight of described four kinds of fibers is: carboxymethyl chitosan fiber 1%-5%, chitin fiber 10-
25%, ES fiber 70%-80%.
Preferably, described non-woven fabrics is combined and is added with granule for massage, a diameter of 1-1.5mm of described granule for massage.
Compared with prior art, the beneficial effects of the present invention is:
The invention discloses a kind of antibacterial, moisturizing cleaning makeup-removing wet tissue based on chitosan derivatives and preparation method thereof, add
Chitosan and carboxymethyl chitosan, belong to natural antimicrobial substance, raw material is extensive, with low cost, is a kind of natural polysaccharide, has
Unique molecular structure, is unique a large amount of basic amine group polysaccharide existed in natural polysaccharide, has antibacterial, effect of sterilization；Add
Entering the makeup-removing wet tissue after oligochitosan, have raising skin immunity, stingless excitation, the female friend being suitable for face skin sensitive makes
With.
The makeup-removing wet tissue of the present invention, for water solublity makeup-removing wet tissue, its production cost is low, and the stability of product is strong, the degree of depth
Cleaning, dirt-removing power are strong, are effectively increased the makeup removing ability of makeup-removing wet tissue；Additionally, add Sensiva SC50, glycerol and
The compositions such as hyaluronate sodium also have antibacterial, effect of moisturizing, make that the face skin after makeup removing is smooth, water is tender, without tight sense, and
There is no color make-up residual face；The base material of makeup-removing wet tissue of the present invention is non-woven fabrics, the carboxymethyl chitosan fiber added in non-woven fabrics
And chitin fiber, add the antibiotic property of makeup-removing wet tissue, water solublity and improve the immunity of face skin, the ES of interpolation is fine
Dimension, fluffy performance is good, adds the flexibility of makeup-removing wet tissue, breathability and then water absorption, and wet tissue intensity is big, not easy fracture；Nothing
Spin the compound granule for massage added in cloth, make wet tissue in use play the effect to facial massage, there is alleviation face
Fatigue, promotes effect of facial blood circulation.
In the preparation method of makeup-removing wet tissue of the present invention, between the chitosan derivatives of interpolation and wetting agent, skin conditioning agent
Interaction, add the stability of product, there is antibacterial, moisturizing, effect of deep clean；This makeup-removing wet tissue is water-soluble
Property, the production equipment after using, to clean simple and convenient, production process is time saving and energy saving.
A kind of based on chitosan derivatives antibacterial, the moisturizing cleaning makeup-removing wet tissue of the present invention, preparation method is simple, cost
Cheap, durable antibacterial effect is effective, excitation stingless to human body face skin, and wet tissue is packed, light, be easy to carry, and is suitable for big
Area promotion and application.
Detailed description of the invention
Below in conjunction with detailed description of the invention, technical scheme is clearly and completely described, it is clear that retouched
The embodiment stated is only a part of embodiment of the present invention rather than whole embodiments.Based on the embodiment in the present invention, this
The every other embodiment that field those of ordinary skill is obtained under not making creative work premise, broadly falls into the present invention
The scope of protection.
The base material of the makeup-removing wet tissue of the present invention is non-woven fabrics, described non-woven fabrics by the carboxymethyl chitosan fiber of 1%-5%,
The chitin fiber of 10-25%, the ES fiber of 70%-80% are prepared from, and the filtrate prepared with this preparation method following is automatically
Output in facial tissues machine.Non-woven fabrics can be combined and be added with small granule for massage, and granule for massage is made up of eiastomeric silicone glue, diameter
1-1.5mm, makes wet tissue in use play the effect to facial massage, alleviates face tired, promote facial blood circulation.
Embodiment one:
Antibacterial, moisturizing cleaning makeup-removing wet tissue based on chitosan derivatives, is made up of the raw material of following weight proportioning: chitosan spreads out
Biology 2%, PEG-8 caprylic/capric glyceride type 5%, butanediol 3%, glycerol 2%, trehalose 1%, olive oil PEG-6 esters
1%, skin conditioning agent 0.5%, phenoxyethanol 0.15%, Sensiva SC50 0.15%, methyl hydroxybenzoate 0.1%, hyaluronate sodium
0.05%, essence 0.01%, surplus are deionized water.
Further, described skin conditioning agent is that butanediol 0.07%, Radix Astragali root extract 0.075%, opoponax carry
Take thing 0.08%, Flos Inulae extract 0.075%, Flos Albiziae extract 0.05%, Rhizoma Gastrodiae root extract 0.06% and deionized water
0.09% mixes.
Further, described chitosan derivatives is any one in chitosan, oligochitosan and carboxymethyl chitosan, or
Two or more mix with arbitrary proportion.
The preparation method of antibacterial, moisturizing cleaning makeup-removing wet tissue based on chitosan derivatives, described preparation method include with
Lower step:
(1), weigh: check various raw material as requested, standby after weighing various raw materials according to formula proportion；
(2), successively by PEG-8 caprylic/capric glyceride type 5%, butanediol 3%, glycerol 2%, trehalose 1%, olive oil PEG-6
Esters 1%, methyl hydroxybenzoate 0.1%, hyaluronate sodium 0.05% and deionized water add in water preparation pot, open homogenizing, and frequency is
35Hz, the time is 3min, opens stirring, and stirring is warming up to 90 DEG C, and rotating speed is 30 turns/min, and mixing time is 10min, makes each former
Material is completely dissolved to homogeneous water preparation shape；
(3), mixing liquid obtained in step (2) is cooled to 28 DEG C, then water preparation pot will be sequentially added into butanediol
0.07%, Radix Astragali root extract 0.075%, opoponax extract 0.08%, Flos Inulae extract 0.075%, Flos Albiziae are extracted
Thing 0.05%, Rhizoma Gastrodiae root extract 0.06% and deionized water 0.09%, open stirring, and rotating speed is 35 turns/min, and mixing time is
5min, after mixing time arrives, then will be sequentially added into chitosan 2%, phenoxyethanol 0.15%, Sensiva SC50 in water preparation pot
0.15% and essence 0.01%, it is then turned on stirring, rotating speed is 35 turns/min, and mixing time is 10min, and stirring makes each raw material the most molten
Solve to homogeneous water preparation shape；
(4), inspection: sample self-inspection, do the inspection of the PH before discharging, appearance test, filter discharging under qualified rear stirring at low speed；Discharging
After carry out microbial bacterial sum mycete inspection；
(5) after mixing time arrives, the filtrate that will prepare in step (4), after being cooled to room temperature, import full-automatic facial tissues machine, and
In full-automatic facial tissues machine, put into the non-woven fabrics folded after cutting, non-woven fabrics is immersed in filtrate 2-3 hour, after unlatching, entirely
Automatically facial tissues machine produces makeup-removing wet tissue, after makeup-removing wet tissue is put into packaging bag and seal.
Embodiment two:
Antibacterial, moisturizing cleaning makeup-removing wet tissue based on chitosan derivatives, is made up of the raw material of following weight proportioning: chitosan spreads out
Biology 3%, PEG-8 caprylic/capric glyceride type 8%, butanediol 5%, glycerol 3%, trehalose 2%, olive oil PEG-6 esters
2%, skin conditioning agent 1.5%, phenoxyethanol 0.2%, Sensiva SC50 0.2%, methyl hydroxybenzoate 0.15%, hyaluronate sodium 1%, perfume
Essence 0.03%, surplus are deionized water.
Further, described skin conditioning agent is butanediol 0.21%, Radix Astragali root extract 0.15%, opoponax extraction
Thing 0.2%, Flos Inulae extract 0.3%, Flos Albiziae extract 0.25%, Rhizoma Gastrodiae root extract 0.14% and deionized water 0.25% mix
Conjunction forms.
Further, described chitosan derivatives is any one in chitosan, oligochitosan and carboxymethyl chitosan, or
Two or more mix with arbitrary proportion.
The preparation method of antibacterial, moisturizing cleaning makeup-removing wet tissue based on chitosan derivatives, described preparation method include with
Lower step:
(1), weigh: check various raw material as requested, standby after weighing various raw materials according to formula proportion；
(2), successively by PEG-8 caprylic/capric glyceride type 8%, butanediol 5%, glycerol 3%, trehalose 2%, olive oil PEG-6
Esters 2%, methyl hydroxybenzoate 0.15%, hyaluronate sodium 0.1% and deionized water add in water preparation pot, open homogenizing, and frequency is
35Hz, the time is 3min, opens stirring, and stirring is warming up to 90 DEG C, and rotating speed is 35 turns/min, and mixing time is 15min, makes each former
Material is completely dissolved to homogeneous water preparation shape；
(3), mixing liquid obtained in step (2) is cooled to 35 DEG C, then water preparation pot will be sequentially added into butanediol
0.21%, Radix Astragali root extract 0.15%, opoponax extract 0.2%, Flos Inulae extract 0.3%, Flos Albiziae extract
0.25%, Rhizoma Gastrodiae root extract 0.14% and deionized water 0.25%, opens stirring, and rotating speed is 40 turns/min, and mixing time is
7min, after mixing time arrives, then will be sequentially added into chitosan 1.5%, oligochitosan 1.5%, phenoxyethanol 0.2%, ethyl in water preparation pot
Hexyl glycerol 0.2% and essence 0.03%, be then turned on stirring, and rotating speed is 40 turns/min, and mixing time is 12min, and stirring makes each former
Material is completely dissolved to homogeneous water preparation shape；
(4), inspection: sample self-inspection, do the inspection of the PH before discharging, appearance test, filter discharging under qualified rear stirring at low speed；Discharging
After carry out microbial bacterial sum mycete inspection；
(5) after mixing time arrives, the filtrate that will prepare in step (4), after being cooled to room temperature, import full-automatic facial tissues machine, and
In full-automatic facial tissues machine, put into the non-woven fabrics folded after cutting, non-woven fabrics is immersed in filtrate 2-3 hour, after unlatching, entirely
Automatically facial tissues machine produces makeup-removing wet tissue, after makeup-removing wet tissue is put into packaging bag and seal.
Embodiment three:
Antibacterial, moisturizing cleaning makeup-removing wet tissue based on chitosan derivatives, is made up of the raw material of following weight proportioning: chitosan spreads out
Biology 5%, PEG-8 caprylic/capric glyceride type 10%, butanediol 8%, glycerol 5%, trehalose 3%, olive oil PEG-6 esters
5%, skin conditioning agent 3%, phenoxyethanol 0.3%, Sensiva SC50 0.3%, methyl hydroxybenzoate 0.2%, hyaluronate sodium 0.2%, perfume
Essence 0.05%, surplus are deionized water.
Further, described skin conditioning agent is butanediol 0.4%, Radix Astragali root extract 0.45%, opoponax extraction
Thing 0.5%, Flos Inulae extract 0.55%, Flos Albiziae extract 0.4%, Rhizoma Gastrodiae root extract 0.25% and deionized water 0.45% mix
Conjunction forms.
Further, described chitosan derivatives is any one in chitosan, oligochitosan and carboxymethyl chitosan, or
Two or more mix with arbitrary proportion.
The preparation method of antibacterial, moisturizing cleaning makeup-removing wet tissue based on chitosan derivatives, described preparation method include with
Lower step:
(1), weigh: check various raw material as requested, standby after weighing various raw materials according to formula proportion；
(2), successively by PEG-8 caprylic/capric glyceride type 10%, butanediol 8%, glycerol 5%, trehalose 3%, olive oil PEG-
6 esters 5%, methyl hydroxybenzoate 0.2%, hyaluronate sodium 0.2% and deionized water add in water preparation pot, open homogenizing, and frequency is
35Hz, the time is 5min, opens stirring, and stirring is warming up to 90 DEG C, and rotating speed is 40 turns/min, and mixing time is 20min, makes each former
Material is completely dissolved to homogeneous water preparation shape；
(3), mixing liquid obtained in step (2) is cooled to 28-42 DEG C, then water preparation pot will be sequentially added into butanediol
0.4%, Radix Astragali root extract 0.45%, opoponax extract 0.45%, Flos Inulae extract 0.55%, Flos Albiziae extract
0.4%, Rhizoma Gastrodiae root extract 0.25% and deionized water 0.45%, opens stirring, and rotating speed is 45 turns/min, and mixing time is
10min, after mixing time arrives, then by water preparation pot is sequentially added into chitosan 1.5&, oligochitosan 2.5%, carboxymethyl chitosan 1%,
Phenoxyethanol 0.3%, Sensiva SC50 0.3% and essence 0.05%, be then turned on stirring, and rotating speed is 45 turns/min, and mixing time is
15min, stirring makes each raw material be completely dissolved to homogeneous water preparation shape；
(4), inspection: sample self-inspection, do the inspection of the PH before discharging, appearance test, filter discharging under qualified rear stirring at low speed；Discharging
After carry out microbial bacterial sum mycete inspection；
(5) after mixing time arrives, the filtrate that will prepare in step (4), after being cooled to room temperature, import full-automatic facial tissues machine, and
In full-automatic facial tissues machine, put into the non-woven fabrics folded after cutting, non-woven fabrics is immersed in filtrate 2-3 hour, after unlatching, entirely
Automatically facial tissues machine produces makeup-removing wet tissue, after makeup-removing wet tissue is put into packaging bag and seal.
Certainly, described above is not limitation of the present invention, and the present invention is also not limited to the example above, the art
Those of ordinary skill, in the essential scope of the present invention, the change made, retrofit, add or replace, all should belong to the present invention
Protection domain.
Claims (8)
1. antibacterial, moisturizing cleaning makeup-removing wet tissue based on chitosan derivatives, it is characterised in that by the raw material of following weight proportioning
Make: chitosan derivatives 2-5%, PEG-8 caprylic/capric glyceride type 5-10%, butanediol 3-8%, glycerol 2-5%, sea
Algae sugar 1-3%, olive oil PEG-6 esters 1-5%, skin conditioning agent 0.5-3%, phenoxyethanol 0.15-0.3%, ethylhexyl
Glycerol 0.15-0.3%, methyl hydroxybenzoate 0.1-0.2%, hyaluronate sodium 0.05-0.2%, essence 0.01-0.05%, surplus are
Deionized water.
Antibacterial, moisturizing cleaning makeup-removing wet tissue based on chitosan derivatives the most according to claim 1, it is characterised in that
Be made up of the raw material of following weight proportioning: chitosan derivatives 3%, PEG-8 caprylic/capric glyceride type 8%, butanediol 5%,
Glycerol 3%, trehalose 2%, olive oil PEG-6 esters 2%, skin conditioning agent 1.5%, phenoxyethanol 0.2%, ethylhexyl are sweet
Oil 0.2%, methyl hydroxybenzoate 0.15%, hyaluronate sodium 1%, essence 0.03%, surplus are deionized water.
Antibacterial, moisturizing cleaning makeup-removing wet tissue based on chitosan derivatives the most according to claim 1, it is characterised in that
Described skin conditioning agent is butanediol, Radix Astragali root extract, opoponax extract, Flos Inulae extract, Flos Albiziae extraction
Thing, Rhizoma Gastrodiae root extract and deionized water, mix with arbitrary proportion.
Antibacterial, moisturizing cleaning makeup-removing wet tissue based on chitosan derivatives the most according to claim 1, it is characterised in that
Described chitosan derivatives is any one in chitosan, oligochitosan and carboxymethyl chitosan, or two or more with arbitrarily than
Example mixes.
5. unload according to based on chitosan derivatives antibacterial, the moisturizing cleaning described in claim any one of claim 1-4
The preparation method of adornment wet tissue, it is characterised in that described preparation method comprises the following steps:
(1), weigh: check various raw material as requested, standby after weighing various raw materials according to formula proportion；
(2), successively by PEG-8 caprylic/capric glyceride type, butanediol, glycerol, trehalose, olive oil PEG-6 esters, oxybenzene
Methyl ester, hyaluronate sodium and deionized water add in water preparation pot, open homogenizing, and frequency is 35Hz, and the time is 3-5min, and unlatching is stirred
Mixing, stirring is warming up to 90 DEG C, and rotating speed is that 30-40 turns/min, and mixing time is 10-20min, makes each raw material be completely dissolved to homogeneous
Water preparation shape；
(3), mixing liquid obtained in step (2) is cooled to 28-42 DEG C, then by water preparation pot is sequentially added into butanediol,
Radix Astragali root extract, opoponax extract, Flos Inulae extract, Flos Albiziae extract, Rhizoma Gastrodiae root extract and deionization
Water, open stirring, rotating speed is that 35-45 turns/min, and mixing time is 5-10min, after mixing time arrives, then by water preparation pot successively
Adding chitosan derivatives, phenoxyethanol, Sensiva SC50 and essence, be then turned on stirring, rotating speed is that 35-45 turns/min, stirs
The time of mixing is 10-15min, and stirring makes each raw material be completely dissolved to homogeneous water preparation shape；
(4), inspection: sample self-inspection, do the inspection of the PH before discharging, appearance test, filter discharging under qualified rear stirring at low speed；Discharging
After carry out microbial bacterial sum mycete inspection；
(5) after mixing time arrives, the filtrate that will prepare in step (4), after being cooled to room temperature, import full-automatic facial tissues machine, and
In full-automatic facial tissues machine, put into the non-woven fabrics folded after cutting, non-woven fabrics is immersed in filtrate 2-3 hour, after unlatching, entirely
Automatically facial tissues machine produces makeup-removing wet tissue, after makeup-removing wet tissue is put into packaging bag and seal.
6. according to based on chitosan derivatives antibacterial, the preparation method of moisturizing cleaning makeup-removing wet tissue described in claim 5,
It is characterized in that, described non-woven fabrics is prepared from by the ES fiber of carboxymethyl chitosan fiber, chitin fiber and low melting point.
7. according to based on chitosan derivatives antibacterial, the preparation method of moisturizing cleaning makeup-removing wet tissue described in claim 6,
It is characterized in that, the percentage by weight of described four kinds of fibers is: carboxymethyl chitosan fiber 1%-5%, chitin fiber 10-
25%, ES fiber 70%-80%.
8. according to based on chitosan derivatives antibacterial, the preparation method of moisturizing cleaning makeup-removing wet tissue described in claim 7,
It is characterized in that, described non-woven fabrics is combined and is added with granule for massage, a diameter of 1-1.5mm of described granule for massage.
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| CN201610788429.0A CN106309200A (en) | 2016-08-31 | 2016-08-31 | Chitosan derivative based clean makeup-removing wet tissue with effects of bacterial inhibition and moisture preservation and preparation method of chitosan derivative based clean makeup-removing wet tissue |
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| CN109044935A (en) * | 2018-10-24 | 2018-12-21 | 娇时日化（杭州）股份有限公司 | A kind of mildly clean micella makeup remover and its production technology |
| CN109044935B (en) * | 2018-10-24 | 2021-09-03 | 虞琼斐 | Mild and clean micelle cleansing water and production process thereof |
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