CN108904321B - Wet tissue with moisturizing function and manufacturing method thereof - Google Patents
Wet tissue with moisturizing function and manufacturing method thereof Download PDFInfo
- Publication number
- CN108904321B CN108904321B CN201810898933.5A CN201810898933A CN108904321B CN 108904321 B CN108904321 B CN 108904321B CN 201810898933 A CN201810898933 A CN 201810898933A CN 108904321 B CN108904321 B CN 108904321B
- Authority
- CN
- China
- Prior art keywords
- mass
- parts
- chitosan
- oxide
- titanium dioxide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/736—Chitin; Chitosan; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0208—Tissues; Wipes; Patches
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/27—Zinc; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/29—Titanium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
Abstract
The invention relates to the field of tissue manufacturing, and provides a wet tissue with a moisturizing function and a manufacturing method thereof, which are used for improving the moisturizing effect of the wet tissue. The wet tissue with the moisturizing function comprises a base material and a humectant, wherein the humectant comprises 10-20 parts by mass of chitosan, 1-3 parts by mass of trehalose, 1-3 parts by mass of propylene glycol, 10-12 parts by mass of sodium hyaluronate and 60-70 parts by mass of deionized water. The wet tissue containing chitosan has the moisturizing and skin moistening effects, so that the skin can be effectively kept moist, the skin problem caused by the fact that the skin is wiped by the wet tissue for multiple times is avoided, and the skin can be kept moist for a long time.
Description
Technical Field
The invention relates to the field of tissue manufacturing, in particular to a wet tissue with a moisturizing function and a manufacturing method thereof.
Background
With the improvement of the life quality of people, the household paper is widely applied by people, and the functions of the household paper are expanded. The conventional high-grade tissue paper containing a medicinal liquid such as a softener to make the skin soft is not likely to cause skin irritation or red swelling even when frequently applied to the nose, and thus has been sought after by users.
However, conventional toilet paper containing a medicinal liquid has insufficient effects of preventing skin prickling and skin redness, and may cause problems such as skin dryness due to multiple uses in a short time, further skin irritation, skin redness, and skin itching. Therefore, the improvement of the moisturizing effect of the paper towels is a problem to be solved urgently.
Disclosure of Invention
The invention provides a wet tissue with a moisturizing function and a manufacturing method thereof, aiming at improving the moisturizing effect of the moisturizing wet tissue.
In order to solve the technical problems, the technical scheme provided by the invention is as follows:
the wet tissue with the moisturizing function comprises a base material and a humectant, wherein the humectant comprises 10-20 parts by mass of chitosan, 1-3 parts by mass of trehalose, 1-3 parts by mass of propylene glycol, 10-12 parts by mass of sodium hyaluronate and 60-70 parts by mass of deionized water.
The chitosan is compounded with glycerol, propylene glycol and the like, so that a good moisturizing effect can be generated, and after the chitosan is further loaded on a base material, the moisturizing effect of the wet tissue is also improved after the wet tissue is prepared.
The wet tissue containing chitosan can effectively keep the skin moist, avoid the skin problem caused by the repeated wiping of the skin by the wet tissue, and can keep the skin moist for a long time.
Preferably, the humectant comprises 15-20 parts by mass of chitosan, 2-3 parts by mass of trehalose, 2-3 parts by mass of propylene glycol, 11-12 parts by mass of sodium hyaluronate and 65-70 parts by mass of deionized water. .
Preferably, the humectant comprises 15 parts by mass of chitosan, 2 parts by mass of trehalose, 2 parts by mass of propylene glycol, 11 parts by mass of sodium hyaluronate and 65 parts by mass of deionized water. .
Preferably, the chitosan is oxide modified chitosan. The oxide modified chitosan can obviously improve the moisturizing effect of the moisturizing agent.
Preferably, the oxidation modified chitosan comprises 30-40 parts by mass of chitosan and 0.8-3 parts by mass of oxide; dissolving chitosan in 100-150 parts by mass of ethanol, adding 1-2 parts by mass of acetic acid, and uniformly stirring to obtain an alcoholic solution of chitosan; adding the oxide into an alcohol solution of chitosan, performing ultrasonic dispersion, heating in a water bath at 80-100 ℃ for 2 hours, cooling, filtering, taking filter residue, washing the filter residue with absolute ethyl alcohol, and drying to obtain the oxide modified chitosan, wherein the oxide comprises 1-2 parts by mass of nano zinc oxide, 1-3 parts by mass of nano silicon dioxide and 0.2-0.5 part by mass of nano titanium dioxide.
The chitosan compounded with the nano oxide has obvious moisturizing effect, and the oxide can promote the chitosan to be uniformly distributed on the base material.
Preferably, the oxidation modified chitosan comprises 35-40 parts by mass of chitosan and 1.5-3 parts by mass of oxide; dissolving the chitosan in 120-150 parts by mass of ethanol, adding 1.5-2 parts by mass of acetic acid, and uniformly stirring to obtain an alcoholic solution of the chitosan; adding the oxide into an alcohol solution of chitosan, performing ultrasonic dispersion, heating in a water bath at 90-100 ℃ for 2 hours, cooling, filtering, taking filter residue, washing the filter residue with absolute ethyl alcohol, and drying to obtain the oxide modified chitosan, wherein the oxide comprises 1.5-2 parts by mass of nano zinc oxide, 2-3 parts by mass of nano silicon dioxide and 0.3-0.5 part by mass of nano titanium dioxide. .
Preferably, the oxidation modified chitosan comprises 35 parts by mass of chitosan and 1.5 parts by mass of oxide; dissolving the chitosan in 120 parts by mass of ethanol, adding 1.5 parts by mass of acetic acid, and uniformly stirring to obtain an alcoholic solution of the chitosan; adding the oxide into an alcohol solution of chitosan, performing ultrasonic dispersion, heating in a water bath at 90 ℃ for 2 hours, cooling, filtering, taking filter residue, washing with absolute ethyl alcohol, and drying to obtain the oxide modified chitosan, wherein the oxide comprises 1.5 parts by mass of nano zinc oxide, 2 parts by mass of nano silicon dioxide and 0.3 part by mass of nano titanium dioxide. .
Preferably, the nano titanium dioxide is modified nano titanium dioxide; the modification method of the modified nano titanium dioxide comprises the following steps: taking 20-25 parts by mass of TiCl4Dissolving the modified nano titanium dioxide in 80-100 parts by mass of deionized water, stirring in an ice water bath, adding 16-20 parts by mass of 25% ammonia water, adding 20-24 parts by mass of hydroxymethyl cellulose, fully stirring, carrying out hydrothermal reaction at 110-120 ℃, washing a product after the reaction is finished by the deionized water, and drying at 90 ℃ to obtain the modified nano titanium dioxide.
After the modified nano titanium dioxide is compounded with nano zinc oxide and nano silicon dioxide, the moisturizing effect of the chitosan can be obviously improved, and meanwhile, the modified titanium dioxide can adsorb certain pollutants, remove grease on the skin and improve the moisturizing effect.
Preferably, the nano titanium dioxide is modified nano titanium dioxide; the modification method of the modified nano titanium dioxide comprises the following steps: taking 24 parts by mass of TiCl4Dissolving the modified nano titanium dioxide in 95 parts by mass of deionized water, stirring the mixture in an ice-water bath, adding 18 parts by mass of 25% ammonia water, adding 22 parts by mass of hydroxymethyl cellulose, fully stirring the mixture, carrying out hydrothermal reaction at 112 ℃, washing a product after the reaction is finished by the deionized water, and drying the product at 90 ℃ to obtain the modified nano titanium dioxide. .
A method for manufacturing wet tissues with moisturizing functions comprises the following steps: preparing a humectant, mixing chitosan, trehalose, propylene glycol, sodium hyaluronate and deionized water, and fully stirring to obtain the humectant; and spraying the humectant on the base cloth to obtain the wet tissue with the moisturizing function, wherein the mass ratio of the non-woven cloth to the humectant is 1: 1.8.
The humectant is sprayed on the base material, so that the humectant can be effectively prevented from being wasted, and the wet tissue prepared by spraying has small change of chemical properties, so that the moisturizing effect of the humectant is kept to the maximum extent.
Compared with the prior art, the invention has the beneficial effects that: the wet tissue containing chitosan has the moisturizing and skin moistening effects, so that the skin can be effectively kept moist, the skin problem caused by the fact that the skin is wiped by the wet tissue for multiple times is avoided, and the skin can be kept moist for a long time; the chitosan compounded with the nano oxide has obvious moisturizing effect, and the oxide can promote the chitosan to be uniformly distributed on the base material.
Detailed Description
The following examples are further illustrative of the present invention and are not intended to be limiting thereof.
Example 1
The wet tissue with the moisturizing function comprises a base material and a humectant, wherein the humectant comprises 15 parts by mass of chitosan, 2 parts by mass of trehalose, 2 parts by mass of propylene glycol, 11 parts by mass of sodium hyaluronate and 65 parts by mass of deionized water. The chitosan is oxide modified chitosan. The oxidation modified chitosan comprises 35 parts by mass of chitosan and 1.5 parts by mass of oxide; dissolving the chitosan in 120 parts by mass of ethanol, adding 1.5 parts by mass of acetic acid, and uniformly stirring to obtain an alcoholic solution of the chitosan; adding the oxide into an alcohol solution of chitosan, performing ultrasonic dispersion, heating in a water bath at 90 ℃ for 2 hours, cooling, filtering, taking filter residue, washing with absolute ethyl alcohol, and drying to obtain the oxide modified chitosan, wherein the oxide comprises 1.5 parts by mass of nano zinc oxide, 2 parts by mass of nano silicon dioxide and 0.3 part by mass of nano titanium dioxide.The nano titanium dioxide is modified nano titanium dioxide; the modification method of the modified nano titanium dioxide comprises the following steps: taking 24 parts by mass of TiCl4Dissolving the modified nano titanium dioxide in 95 parts by mass of deionized water, stirring the mixture in an ice-water bath, adding 18 parts by mass of 25% ammonia water, adding 22 parts by mass of hydroxymethyl cellulose, fully stirring the mixture, carrying out hydrothermal reaction at 112 ℃, washing a product after the reaction is finished by the deionized water, and drying the product at 90 ℃ to obtain the modified nano titanium dioxide.
The chitosan is compounded with glycerol, propylene glycol and the like, so that a good moisturizing effect can be generated, and after the chitosan is further loaded on a base material, the moisturizing effect of the wet tissue is also improved after the wet tissue is prepared. The moisturizing and skin moistening effect of the wet tissue containing chitosan can effectively keep the skin moist, avoid the skin problem caused by the repeated wiping of the skin by the wet tissue, and can keep the moisturizing effect of the moisturizing agent remarkably improved by the chitosan modified by the skin moistening oxide for a long time.
The chitosan compounded with the nano oxide has obvious moisturizing effect, and the oxide can promote the chitosan to be uniformly distributed on the base material.
After the modified nano titanium dioxide is compounded with nano zinc oxide and nano silicon dioxide, the moisturizing effect of the chitosan can be obviously improved, and meanwhile, the modified titanium dioxide can adsorb certain pollutants, remove grease on the skin and improve the moisturizing effect.
A method for manufacturing wet tissues with moisturizing functions comprises the following steps: preparing a humectant, mixing chitosan, trehalose, propylene glycol, sodium hyaluronate and deionized water, and fully stirring to obtain the humectant; and spraying the humectant on the base cloth to obtain the wet tissue with the moisturizing function, wherein the mass ratio of the non-woven cloth to the humectant is 1: 1.8.
The humectant is sprayed on the base material, so that the humectant can be effectively prevented from being wasted, and the wet tissue prepared by spraying has small change of chemical properties, so that the moisturizing effect of the humectant is kept to the maximum extent.
Example 2
The embodiment 2 is different from the embodiment 1 in that the moisture-retaining agent comprises a base material and a moisture-retaining agent, wherein the moisture-retaining agent comprises 10 parts by mass of chitosan, 1 part by mass of trehalose, 1 part by mass of propylene glycol, 10 parts by mass of sodium hyaluronate and 60 parts by mass of deionized water.
Example 3
The difference of the embodiment 3 from the embodiment 1 is that the moisturizing agent comprises 20 parts by mass of chitosan, 3 parts by mass of trehalose, 3 parts by mass of propylene glycol, 12 parts by mass of sodium hyaluronate and 70 parts by mass of deionized water.
Example 4
Real-time example 4 is different from example 1 in that the oxidized modified chitosan comprises 30 parts by mass of chitosan and 0.8 part by mass of an oxide; dissolving chitosan in 100 parts by mass of ethanol, adding 1 part by mass of acetic acid, and uniformly stirring to obtain an alcoholic solution of chitosan; adding the oxide into an alcoholic solution of chitosan, carrying out ultrasonic dispersion, heating in a water bath at 80 ℃ for 2h, cooling, filtering, taking filter residue, washing with absolute ethyl alcohol, and drying to obtain the oxide modified chitosan, wherein the oxide comprises 1 part by mass of nano zinc oxide, 1 part by mass of nano silicon dioxide and 0.2 part by mass of nano titanium dioxide.
Example 5
Real-time example 5 is different from example 1 in that the oxidized modified chitosan includes 40 parts by mass of chitosan and 3 parts by mass of an oxide; dissolving the chitosan in 150 parts by mass of ethanol, adding 2 parts by mass of acetic acid, and uniformly stirring to obtain an alcoholic solution of the chitosan; adding the oxide into an alcohol solution of chitosan, performing ultrasonic dispersion, heating in a water bath at 100 ℃ for 2 hours, cooling, filtering, taking filter residue, washing with absolute ethyl alcohol, and drying to obtain the oxide modified chitosan, wherein the oxide comprises 2 parts by mass of nano zinc oxide, 3 parts by mass of nano silicon dioxide and 0.5 part by mass of nano titanium dioxide.
Example 6
Real-time example 6 is different from example 1 in that the nano titanium dioxide is modified nano titanium dioxide; the modification method of the modified nano titanium dioxide comprises the following steps: taking 20 parts by mass of TiCl4Dissolving in 80 deg.CStirring 16 parts by mass of 25% ammonia water and 20 parts by mass of hydroxymethyl cellulose in deionized water in an ice-water bath, fully stirring, carrying out hydrothermal reaction at 110 ℃, washing a product after the reaction is finished by the deionized water, and drying at 90 ℃ to obtain the modified nano titanium dioxide.
Example 7
Example 7 is the same as example 1 except that the nano titanium dioxide is modified nano titanium dioxide; the modification method of the modified nano titanium dioxide comprises the following steps: taking 25 parts by mass of TiCl4Dissolving the modified nano titanium dioxide in 100 parts by mass of deionized water, stirring the mixture in an ice-water bath, adding 20 parts by mass of 25% ammonia water, adding 24 parts by mass of hydroxymethyl cellulose, fully stirring the mixture, carrying out hydrothermal reaction at 120 ℃, washing a product after the reaction is finished by the deionized water, and drying the product at 90 ℃ to obtain the modified nano titanium dioxide.
Comparative example 1
Comparative example 1 is different from example 1 in that the chitosan does not contain an oxide.
Comparative example 2
Comparative example 2 is the same as example 1 except that the moisture retention agent in the tissue is propylene glycol.
Examples of the experiments
Randomly selecting 30 healthy people of 18-50 years old as volunteers, providing the paper towels of examples 1-7 and comparative examples 1-3, wiping the nose according to a specified number of times, evaluating whether the nose is not easy to feel pain in 5 grades, recording and counting the use experience of each volunteer, and taking an average value, wherein the table 1 is an experimental result.
Table 1 Wet wipes use experience
| The nose is not easy to prick | Sense of wetness | Skin moisture rising ratio (%) | Comprehensive evaluation | |
| Example 1 | 4.96 | 4.92 | 35.2 | 4.94 |
| Example 2 | 4.62 | 4.72 | 23.1 | 4.67 |
| Example 3 | 4.75 | 4.83 | 26.3 | 4.79 |
| Example 4 | 4.42 | 4.47 | 29.3 | 4.45 |
| Example 5 | 4.78 | 4.77 | 25.2 | 4.78 |
| Example 6 | 4.32 | 4.26 | 22.1 | 4.29 |
| Example 7 | 4.76 | 4.79 | 26.4 | 4.78 |
| Comparative example 1 | 3.62 | 3.76 | 14.2 | 3.69 |
| Comparative example 2 | 2.88 | 3.12 | 10 | 3.00 |
As can be seen from table 1, examples 1 to 7 all have certain moisturizing and skin-moistening effects, and compared with comparative examples, the skin-moistening and skin-moistening cosmetic has small irritation, which indicates that the oxide-containing chitosan used in the examples has a better moisturizing function and a significant moisturizing effect.
Example 1 is a preferred embodiment, and the comprehensive evaluation is higher (average of two evaluation indexes), but the addition amount of each raw material in example 3 is larger, and the cost is higher, so example 1 is a more preferred embodiment, and the addition amount of example 2 is smaller, and the moisturizing effect is still remarkable compared with the comparative example, which indicates that the effect of oxide-containing chitosan on skin protection is more important; the chitosan adopted in the comparative example 1 does not contain oxides, so that the user response is poor, but the comprehensive evaluation of the user is still more than 3, and the chitosan has a considerable moisturizing function; the liquid medicine in the comparative example 2 is propylene glycol, and the effect is remarkably lower than those of the liquid medicines in the examples 1-7 and the comparative example 1 compared with the traditional moisturizing agent.
In examples 4 and 5, the chitosan is added in different amounts, and the effect is obviously different; wherein the moisturizing effect of example 4 is weaker than that of example 2, indicating that the effect of the change of the content of each component in the chitosan on the moisturizing effect of the paper towel is larger than the effect of the change of the addition amount of the chitosan on the moisturizing effect of the paper towel.
In examples 6 and 7, the content of each substance in the oxide is different, wherein the moisturizing effect of example 6 is weaker than that of example 4, indicating that the effect of the change of the content of each component in the oxide on the moisturizing effect of the tissue is larger than the effect of the change of the addition amount of the oxide on the moisturizing effect of the tissue.
As can be seen from the rising proportion of the skin moisture, the content of each component in the chitosan has more important influence on changing the moisturizing effect of the paper towel.
The above detailed description is specific to possible embodiments of the present invention, and the above embodiments are not intended to limit the scope of the present invention, and all equivalent implementations or modifications that do not depart from the scope of the present invention should be included in the present claims.
Claims (7)
1. The wet tissue with the moisturizing function is characterized by comprising a base material and a humectant, wherein the humectant comprises 10-20 parts by mass of chitosan, 1-3 parts by mass of trehalose, 1-3 parts by mass of propylene glycol, 10-12 parts by mass of sodium hyaluronate and 60-70 parts by mass of deionized water;
the chitosan is oxide modified chitosan;
the oxide modified chitosan comprises 30-40 parts by mass of chitosan and 0.8-3 parts by mass of oxide;
dissolving chitosan in 100-150 parts by mass of ethanol, adding 1-2 parts by mass of acetic acid, and uniformly stirring to obtain an alcoholic solution of chitosan;
adding the oxide into an alcohol solution of chitosan, performing ultrasonic dispersion, heating in a water bath at 80-100 ℃ for 2h, cooling, filtering, taking filter residue, washing with absolute ethyl alcohol, and drying to obtain oxide modified chitosan;
the oxide comprises 1-2 parts by mass of nano zinc oxide, 1-3 parts by mass of nano silicon dioxide and 0.2-0.5 part by mass of nano titanium dioxide;
the nano titanium dioxide is modified nano titanium dioxide;
the modification method of the modified nano titanium dioxide comprises the following steps:
taking 20-25 parts by mass of TiCl4Dissolving the modified nano titanium dioxide in 80-100 parts by mass of deionized water, stirring in an ice water bath, adding 16-20 parts by mass of 25% ammonia water, adding 20-24 parts by mass of hydroxymethyl cellulose, fully stirring, carrying out hydrothermal reaction at 110-120 ℃, washing a product after the reaction is finished by the deionized water, and drying at 90 ℃ to obtain the modified nano titanium dioxide.
2. The wet tissue with the moisturizing function as claimed in claim 1, wherein the moisturizing agent comprises 15 to 20 parts by mass of chitosan, 2 to 3 parts by mass of trehalose, 2 to 3 parts by mass of propylene glycol, 11 to 12 parts by mass of sodium hyaluronate, and 65 to 70 parts by mass of deionized water.
3. The wet wipe with moisturizing function according to claim 2, wherein the moisturizing agent comprises 15 parts by mass of chitosan, 2 parts by mass of trehalose, 2 parts by mass of propylene glycol, 11 parts by mass of sodium hyaluronate, and 65 parts by mass of deionized water.
4. The wet wipe with moisturizing function as claimed in claim 1, wherein the oxide-modified chitosan comprises 35 to 40 parts by mass of chitosan, 1.5 to 3 parts by mass of oxide;
dissolving the chitosan in 120-150 parts by mass of ethanol, adding 1.5-2 parts by mass of acetic acid, and uniformly stirring to obtain an alcoholic solution of the chitosan;
the oxide is added into an alcohol solution of chitosan, the mixture is subjected to ultrasonic dispersion, then is heated in a water bath at 90-100 ℃ for 2 hours, is cooled and filtered, filter residue is taken, is washed by absolute ethyl alcohol and is dried, and the oxide modified chitosan is obtained, wherein the oxide comprises 1.5-2 parts by mass of nano zinc oxide, 2-3 parts by mass of nano silicon dioxide and 0.3-0.5 part by mass of nano titanium dioxide.
5. The wet wipe with a moisturizing function according to claim 1, wherein the oxide-modified chitosan comprises 35 parts by mass of chitosan, 1.5 parts by mass of an oxide;
dissolving the chitosan in 120 parts by mass of ethanol, adding 1.5 parts by mass of acetic acid, and uniformly stirring to obtain an alcoholic solution of the chitosan;
adding the oxide into an alcohol solution of chitosan, performing ultrasonic dispersion, heating in a water bath at 90 ℃ for 2h, cooling, filtering, taking filter residue, washing with absolute ethyl alcohol, and drying to obtain oxide modified chitosan;
the oxide comprises 1.5 parts by mass of nano zinc oxide, 2 parts by mass of nano silicon dioxide and 0.3 part by mass of nano titanium dioxide.
6. The wet wipe with moisturizing function as claimed in claim 1, wherein the nano titanium dioxide is modified nano titanium dioxide; the modification method of the modified nano titanium dioxide comprises the following steps: taking 24 parts by mass of TiCl4Dissolving the modified nano titanium dioxide in 95 parts by mass of deionized water, stirring the mixture in an ice-water bath, adding 18 parts by mass of 25% ammonia water, adding 22 parts by mass of hydroxymethyl cellulose, fully stirring the mixture, carrying out hydrothermal reaction at 112 ℃, washing a product after the reaction is finished by the deionized water, and drying the product at 90 ℃ to obtain the modified nano titanium dioxide.
7. The method for manufacturing a wet wipe having a moisturizing function according to any one of claims 1 to 6, comprising the steps of: preparing a humectant, mixing chitosan, trehalose, propylene glycol, sodium hyaluronate and deionized water, and then fully stirring to obtain the humectant; and spraying the humectant on a base material to obtain the wet tissue with the moisturizing function, wherein the mass ratio of the base material to the humectant is 1: 1.8.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810898933.5A CN108904321B (en) | 2018-08-08 | 2018-08-08 | Wet tissue with moisturizing function and manufacturing method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810898933.5A CN108904321B (en) | 2018-08-08 | 2018-08-08 | Wet tissue with moisturizing function and manufacturing method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN108904321A CN108904321A (en) | 2018-11-30 |
| CN108904321B true CN108904321B (en) | 2021-11-26 |
Family
ID=64397264
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810898933.5A Active CN108904321B (en) | 2018-08-08 | 2018-08-08 | Wet tissue with moisturizing function and manufacturing method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108904321B (en) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111058189A (en) * | 2019-12-12 | 2020-04-24 | 杭州诚品实业有限公司 | Hyaluronic acid-loaded high-moisture-retention degradable bamboo fiber non-woven fabric and preparation method thereof |
| CN111441172B (en) * | 2020-05-12 | 2022-03-29 | 安徽普尔德无纺科技有限公司 | Medical paper towel capable of keeping moisture for long time and preparation method thereof |
| CN111493722A (en) * | 2020-05-30 | 2020-08-07 | 青岛玉竹叶纸品科技有限责任公司 | Antibacterial wet tissue and preparation method thereof |
| CN114652660A (en) * | 2022-05-20 | 2022-06-24 | 广州优理氏生物科技有限公司 | Peptide composition with antiallergic effect and application thereof in preparation of skin care product |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106309200A (en) * | 2016-08-31 | 2017-01-11 | 湖北立天生物工程有限公司 | Chitosan derivative based clean makeup-removing wet tissue with effects of bacterial inhibition and moisture preservation and preparation method of chitosan derivative based clean makeup-removing wet tissue |
| CN107074983A (en) * | 2014-06-02 | 2017-08-18 | 特西斯公司 | Modified biopolymer and its production and application method |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3439199B2 (en) * | 2001-05-07 | 2003-08-25 | 憲司 中村 | Moisturizing composition |
-
2018
- 2018-08-08 CN CN201810898933.5A patent/CN108904321B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107074983A (en) * | 2014-06-02 | 2017-08-18 | 特西斯公司 | Modified biopolymer and its production and application method |
| CN106309200A (en) * | 2016-08-31 | 2017-01-11 | 湖北立天生物工程有限公司 | Chitosan derivative based clean makeup-removing wet tissue with effects of bacterial inhibition and moisture preservation and preparation method of chitosan derivative based clean makeup-removing wet tissue |
Also Published As
| Publication number | Publication date |
|---|---|
| CN108904321A (en) | 2018-11-30 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN108904321B (en) | Wet tissue with moisturizing function and manufacturing method thereof | |
| CN108420757B (en) | Moisturizing lotion and preparation process thereof | |
| CN104593893A (en) | Peppermint composite cellulose fibers and preparation method thereof | |
| CN111759767A (en) | Graphene nourishing shampoo and preparation method thereof | |
| CN109504558B (en) | Tea dirt cleaning agent and preparation method thereof | |
| CN107174559A (en) | A kind of anti-fog haze facial mask | |
| CN111714436B (en) | Anti-hair loss shampoo and preparation method thereof | |
| CN109589283B (en) | Fat-endowing agent with skin barrier repairing function and application thereof | |
| JP3019325B2 (en) | Wet tissue | |
| KR20040019977A (en) | Wet wiper | |
| CN106675890A (en) | Bath soap and preparation method thereof | |
| CN107375017B (en) | Cleansing composition and its preparation method and application | |
| JPH03232811A (en) | Cosmetic | |
| CN113398025B (en) | Composition for removing blackheads and shrinking pores as well as preparation method and application thereof | |
| CN113633560B (en) | Needle-shaped amino acid crystal face-cleaning gel and preparation method thereof | |
| CN109568216A (en) | A kind of skin barrier maintenance Mu Lu and preparation method thereof | |
| CN109044886A (en) | A kind of micro-nano cleaning whitening mask mud | |
| CN108904381A (en) | A kind of paper handkerchief and its manufacturing method with moisture-keeping functions | |
| CN114028246A (en) | Anti-aging repairing composition containing acetyl zingerone and application thereof | |
| JP3647744B2 (en) | Dye remover | |
| CN114246810B (en) | Cleansing dry towel and preparation method and use method thereof | |
| CN110747075A (en) | Chitosan oligosaccharide handmade soap and preparation method thereof | |
| JP5684011B2 (en) | Eyelash cosmetic | |
| CN109135972A (en) | Perfumed soap and its production technology | |
| CN115227614B (en) | Blackhead-removing facial cleanser and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| TA01 | Transfer of patent application right | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20211108 Address after: 300380 No. 33, Saida third branch road, economic development zone, Xiqing District, Tianjin Applicant after: Tianjin Kangsen Biological Technology Co.,Ltd. Address before: 523000 Wanjiang Guyong Industrial Zone, Dongguan City, Guangdong Province Applicant before: DONGGUAN BAITIANE PAPER Co.,Ltd. |
|
| GR01 | Patent grant | ||
| GR01 | Patent grant |