CN110747075A - Chitosan oligosaccharide handmade soap and preparation method thereof - Google Patents
Chitosan oligosaccharide handmade soap and preparation method thereof Download PDFInfo
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- CN110747075A CN110747075A CN201911073645.7A CN201911073645A CN110747075A CN 110747075 A CN110747075 A CN 110747075A CN 201911073645 A CN201911073645 A CN 201911073645A CN 110747075 A CN110747075 A CN 110747075A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
- C11D9/262—Organic compounds, e.g. vitamins containing oxygen containing carbohydrates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Dermatology (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Molecular Biology (AREA)
- Emergency Medicine (AREA)
- Cosmetics (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses a chitosan oligosaccharide handmade soap and a preparation method thereof, and relates to the technical field of preparation of handmade soaps. The composite material comprises the following raw materials in parts by weight: 40-60 parts of soap base, 5-15 parts of chitosan oligosaccharide and 10-20 parts of plant essential oil. The plant essential oil is selected from one or more of oleum Olivarum, oleum Cocois, avocado oil, oleum Armeniacae amarum, shea butter, oleum Camelliae Japonicae, cacao butter, grapeseed oil, oleum Lini, macadamia nut oil or oleum Rosae Davuricae. In the raw materials selected by the invention, the chitosan oligosaccharide can obviously eliminate the oxygen anion free radicals of the human body, activate the cells of the organism, delay senility, inhibit the breeding of harmful bacteria on the surface of the skin and have beneficial moisturizing performance, thus being the basic raw material in the field of daily chemicals. The chitosan oligosaccharide has water solubility, is convenient to use, has remarkable effect of inhibiting putrefying bacteria, and has multiple functions. The handmade soap prepared by the invention can meet the daily skin care requirements of people, and can also effectively inhibit bacteria and preserve moisture.
Description
Technical Field
The invention relates to the technical field of preparation of handmade soaps, and particularly relates to a chitosan oligosaccharide handmade soap and a preparation method thereof.
Background
The handmade soap is made up by using natural oil and alkali liquor and adopting manual process. Basically as a result of saponification of the oil and fat with the alkaline solution. The handmade soap can be used as a face wash and also as a bath soap. The hand soap has fine and rich foam, can thoroughly remove oil stains in the deep pores, and enables the skin to be moist, glossy and elastic.
With the pursuit of high-quality life, various handmade soaps with functionality are researched in the market. The main research reports are:
CN 108485851 a discloses a tea seed handmade soap and a process for making the same, the composition formula of which is: 18-25 parts of camellia oil, 18-20 parts of coconut oil, 10-15 parts of olive oil, 10-18 parts of hydrogenated palm oil, 0.00032-0.00036 part of orange flower essential oil, 15-20 parts of cocoyl glutamic acid, 10-20 parts of sodium lauroyl glutamate, 10-25 parts of tea seed powder, 10-18 parts of grape seed oil, 15-25 parts of jojoba seed oil, 10-15 parts of propylene glycol, 10-15 parts of betaine, 10-15 parts of cane sugar, 10-18 parts of sodium hyaluronate, 10-15 parts of tocopheryl acetate, 2-3 parts of essence, 5-8 parts of beeswax and 3-5 parts of jasmine pollen.
CN 108531321A discloses a preparation method of a tea fruit handmade soap, which comprises the following steps: (1) preparing raw materials, (2) pretreating tea fruits, (3) preparing soap liquid, and (4) preparing handmade soap.
CN 109456862A discloses a folium artemisiae argyi handmade soap and a preparation method thereof, wherein the added folium artemisiae argyi extract has the effects of diminishing inflammation and resisting allergy, can prevent skin from being invaded by bacteria, effectively prolongs the quality guarantee period of the handmade soap, has the effects of diminishing inflammation and swelling, and can relieve skin pruritus and skin inflammation.
The prior art gives the handmade soap multiple functions, but after the handmade soap is used, the problems of skin chapping, tight skin and the like still exist, so the antibacterial and moisturizing effects of the handmade soap in the prior art need to be further improved.
Disclosure of Invention
The invention aims to provide a chitosan oligosaccharide handmade soap and a preparation method thereof, which can meet the daily skin care requirements of people and can also effectively inhibit bacteria and preserve moisture.
One of the tasks of the invention is to provide a chitosan oligosaccharide handmade soap, which adopts the following technical scheme:
the chitosan oligosaccharide handmade soap comprises the following raw materials in parts by weight:
40-60 parts of soap base, 5-15 parts of chitosan oligosaccharide and 10-20 parts of plant essential oil.
As a preferable scheme of the invention, the weight parts of the raw materials are as follows: 50 parts of soap base, 10 parts of chitosan oligosaccharide and 15 parts of plant essential oil.
As another preferred embodiment of the present invention, the above-mentioned plant essential oil is selected from one or more of olive oil, coconut oil, avocado oil, sweet almond oil, shea oil, camellia oil, cocoa butter, grape seed oil, linseed oil, macadamia nut oil or rose hip seed oil.
Further, the plant essential oil is selected from olive oil, sweet almond oil and macadamia nut oil.
The invention also aims to provide a preparation method of the chitosan oligosaccharide handmade soap, which sequentially comprises the following steps:
s1, heating the soap base at the temperature of 55-65 ℃ to melt the soap base into a liquid state;
s2, adding the chitosan oligosaccharide and the plant essential oil into the liquid soap base obtained in the step S1, and stirring at the temperature of 60-65 ℃ for 3-5 min to obtain a mixed liquid;
and S3, pouring the mixed liquid into a mould, and demoulding after the mixed liquid in the mould is completely solidified to obtain the chitosan oligosaccharide handmade soap.
Further, step S1, the soap base is heated at a temperature of 60 ℃.
In the raw materials selected by the invention, the chitosan oligosaccharide can obviously eliminate the oxygen anion free radicals of the human body, activate the cells of the organism, delay senility, inhibit the breeding of harmful bacteria on the surface of the skin and have beneficial moisturizing performance, thus being the basic raw material in the field of daily chemicals. The chitosan oligosaccharide has water solubility, is convenient to use, has remarkable effect of inhibiting putrefying bacteria, and has multiple functions.
The handmade soap is prepared by using any one or a mixture of several of pure plant essential oils, such as olive oil, coconut oil, avocado oil, sweet almond oil, shea butter, camellia oil, cocoa butter, grape seed oil, linseed oil, macadamia nut oil, rose hip seed oil and other natural plant essential oils, chitosan oligosaccharide and soap base together, and has the functions of resisting bacteria and cleaning skin.
The above preferred plant essential oil is a mixture of olive oil, sweet almond oil and macadamia nut oil.
The olive oil, the sweet almond oil and the macadamia nut oil have a synergistic effect with the chitosan oligosaccharide and the soap base, and the good water solubility of the chitosan oligosaccharide can obviously improve the moisture of the sweet almond oil and the skin, so that the effects of moistening the skin and resisting bacteria are achieved together.
Compared with the prior art, the invention has the following beneficial technical effects:
the invention adopts pure natural vegetable oil, the vegetable oil contains a large amount of nutrient substances which do not participate in saponification, and the components can permeate into skin through pores when in use, thereby achieving the effect of cleaning and maintaining simultaneously.
The handmade soap does not contain irritant substances and has the effects of moisturizing and resisting bacteria; the skin-care product can achieve the effects of whitening, resisting wrinkles and inhibiting bacteria while cleaning the skin, and is a natural skin-care product.
Detailed Description
The invention provides a chitosan oligosaccharide handmade soap and a preparation method thereof, and in order to make the advantages and technical scheme of the invention clearer and clearer, the invention is described in detail with reference to specific embodiments.
The "soap base" as referred to in the present invention, wherein the PH is between 6.5 and 8, except that the effective laundry will contain a large amount of glycerin and moisture.
The plant essential oil can be obtained from plants by a conventional process.
Example 1:
40 parts of soap base, 15 parts of chitosan oligosaccharide, 3 parts of olive oil, 3 parts of coconut oil and 4 parts of avocado oil.
Example 2:
60 parts of soap base, 5 parts of chitosan oligosaccharide, 5 parts of coconut oil, 3 parts of avocado oil and 12 parts of sweet almond oil.
Example 3:
50 parts of soap base, 15 parts of chitosan oligosaccharide, 5 parts of avocado oil, 5 parts of sweet almond oil and 5 parts of shea butter.
Example 4:
50 parts of soap base, 10 parts of chitosan oligosaccharide, 5 parts of olive oil, 5 parts of sweet almond oil and 5 parts of macadamia nut oil.
Example 5:
50 parts of soap base, 10 parts of chitosan oligosaccharide, 5 parts of olive oil, 5 parts of sweet almond oil and 5 parts of rose hip seed oil.
Example 6:
40 parts of soap base, 10 parts of chitosan oligosaccharide, 5 parts of olive oil, 5 parts of sweet almond oil and 5 parts of macadamia nut oil.
The preparation methods of the above examples 1 to 6 are all as follows:
step one, heating the soap base at the temperature of 55-65 ℃ to melt the soap base into a liquid state;
step two, adding chitosan oligosaccharide and plant essential oil into the liquid soap base obtained in the step one, and stirring at the temperature of 60-65 ℃ for 3-5 min to obtain mixed liquid;
and step three, pouring the mixed liquid into a mold, and demolding after the mixed liquid in the mold is completely solidified to obtain the chitosan oligosaccharide handmade soap.
Comparative example 1:
50 parts of soap base, 5 parts of olive oil, 5 parts of sweet almond oil and 5 parts of rose hip seed oil.
The preparation method comprises the following steps:
step one, heating the soap base at the temperature of 55-65 ℃ to melt the soap base into a liquid state;
step two, adding plant essential oil into the liquid soap base obtained in the step one, and stirring at 60-65 ℃ for 3-5 min to obtain mixed liquid;
and step three, pouring the mixed liquid into a mold, and demolding after the mixed liquid in the mold is completely solidified to obtain the chitosan oligosaccharide handmade soap.
Comparative example 2:
50 parts of soap base and 10 parts of chitosan oligosaccharide.
The preparation method comprises the following steps:
step one, heating the soap base at the temperature of 55-65 ℃ to melt the soap base into a liquid state;
step two, adding chitosan oligosaccharide into the liquid soap base obtained in the step one, and stirring at 60-65 ℃ for 3-5 min to obtain a mixed liquid;
and step three, pouring the mixed liquid into a mold, and demolding after the mixed liquid in the mold is completely solidified to obtain the chitosan oligosaccharide handmade soap.
The handmade soaps prepared in examples 1-6 and comparative examples 1 and 2 were tested.
Test example I, user experience testing
Test subjects: 80 healthy volunteers (40 each for men and women) aged between 20-25 years.
Test materials: handmade soaps prepared according to examples 1-6 of the present invention and comparative examples 1-2.
The test method comprises the following steps:
80 subjects were randomly divided into 8 groups, and each group was washed on the inner side of the arm to which the BB cream was applied using the handmade soaps prepared in examples 1 to 6 and comparative examples 1 to 2, every 8 hours, 2 times per day, and continuously used for 2 weeks. The subjects scored the cleanliness and irritation of the skin after use and the foam properties (0-10 points, higher score indicates good cleaning effect)
And (3) test results: the test results are shown in table 1.
TABLE 1 user experience test results
| Group of | Example 1 | Example 2 | Example 3 | Example 4 | Example 5 | Example 6 | Comparative example 1 | Comparative example 2 |
| Cleanliness | 9.1 | 8.8 | 9.2 | 9.8 | 9.4 | 9.5 | 8.6 | 8.4 |
As can be seen from Table 1, the handmade soap of the present invention has high cleanliness to skin and no adverse reactions such as allergy.
Test example 2 moisture retention Performance test
Test subjects: 80 healthy women aged 20-35 years, dry skin, and those with allergic constitution were excluded from the test subjects.
Test materials: handmade soaps prepared according to examples 1-6 of the present invention and comparative examples 1-2.
The test method comprises the following steps:
the skin moisture content was measured using a skin moisture meter. The higher the value, the higher the skin moisture content.
The subjects were divided into 8 groups at random, and the test sites on the backs of the hands of the subjects were selected. The test sites were washed with handmade soap and the skin moisture content was measured after 2, 4, 6, 8 hours using a skin moisture meter.
And (3) test results: the test results are shown in table 2.
Table 2 skin moisture test results
| Categories | 2h | 4h | 6h | 8h |
| Example 1 | 46.2 | 40.7 | 38.7 | 32.1 |
| Example 2 | 50.1 | 48.6 | 42.3 | 39.0 |
| Example 3 | 53.4 | 48.2 | 43.9 | 39.7 |
| Example 4 | 68.4 | 62.5 | 58.3 | 52.5 |
| Example 5 | 58.7 | 52.1 | 48.5 | 42.4 |
| Example 6 | 60.4 | 59.3 | 52.1 | 49.6 |
| Comparative example 1 | 40.3 | 35.6 | 30.1 | 28.9 |
| Comparative example 2 | 39.8 | 33.6 | 29.8 | 26.7 |
As is clear from Table 2, the handmade soap prepared in example 4 of the present invention has the best moisture retention.
The parts which are not described in the invention can be realized by taking the prior art as reference.
It should be noted that: any equivalents, or obvious variations thereof, which may occur to those skilled in the art and which are commensurate with the teachings of this disclosure, are intended to be within the scope of this invention.
Claims (6)
1. The chitosan oligosaccharide handmade soap is characterized by comprising the following raw materials in parts by weight:
40-60 parts of soap base, 5-15 parts of chitosan oligosaccharide and 10-20 parts of plant essential oil.
2. The chitosan oligosaccharide handmade soap of claim 1, wherein: the weight parts of the raw materials are as follows: 50 parts of soap base, 10 parts of chitosan oligosaccharide and 15 parts of plant essential oil.
3. The chitosan oligosaccharide handmade soap of claim 2, wherein: the plant essential oil is selected from one or more of olive oil, coconut oil, avocado oil, sweet almond oil, shea butter, camellia oil, cocoa butter, grape seed oil, linseed oil, macadamia nut oil or rose hip seed oil.
4. The chitosan oligosaccharide handmade soap of claim 3, wherein: the plant essential oil is selected from olive oil, sweet almond oil and macadamia nut oil.
5. The preparation method of the chitosan oligosaccharide handmade soap as claimed in any one of claims 1 to 4, which is characterized by sequentially comprising the following steps:
s1, heating the soap base at the temperature of 55-65 ℃ to melt the soap base into a liquid state;
s2, adding the chitosan oligosaccharide and the plant essential oil into the liquid soap base obtained in the step S1, and stirring at the temperature of 60-65 ℃ for 3-5 min to obtain a mixed liquid;
and S3, pouring the mixed liquid into a mould, and demoulding after the mixed liquid in the mould is completely solidified to obtain the chitosan oligosaccharide handmade soap.
6. The method for preparing a chitosan oligosaccharide handmade soap according to claim 5, which is characterized in that: step S1, heating the soap base at a temperature of 60 ℃.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911073645.7A CN110747075A (en) | 2019-11-06 | 2019-11-06 | Chitosan oligosaccharide handmade soap and preparation method thereof |
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| CN201911073645.7A CN110747075A (en) | 2019-11-06 | 2019-11-06 | Chitosan oligosaccharide handmade soap and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113201420A (en) * | 2021-04-02 | 2021-08-03 | 深圳市多微生保健食品有限公司 | Handmade soap added with plant active ingredients |
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2019
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| CN104130888A (en) * | 2014-08-07 | 2014-11-05 | 张萍 | Special formula of cold-process handmade soap as well as preparation method and application thereof |
| CN106010811A (en) * | 2016-05-20 | 2016-10-12 | 康瑞洁 | Sterilizing detergent |
| CN106148040A (en) * | 2016-06-22 | 2016-11-23 | 詹俊英 | A kind of Radix Arnebiae (Radix Lithospermi) handmade soap and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113201420A (en) * | 2021-04-02 | 2021-08-03 | 深圳市多微生保健食品有限公司 | Handmade soap added with plant active ingredients |
| CN113201420B (en) * | 2021-04-02 | 2022-04-08 | 深圳市多微生保健食品有限公司 | Handmade soap added with plant active ingredients |
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