CN108977290A - A kind of handmade soap of niacinamide-containing and preparation method thereof - Google Patents
A kind of handmade soap of niacinamide-containing and preparation method thereof Download PDFInfo
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- CN108977290A CN108977290A CN201710404859.2A CN201710404859A CN108977290A CN 108977290 A CN108977290 A CN 108977290A CN 201710404859 A CN201710404859 A CN 201710404859A CN 108977290 A CN108977290 A CN 108977290A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/06—Preparations for care of the skin for countering cellulitis
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
- C11D9/265—Organic compounds, e.g. vitamins containing oxygen containing glycerol
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/30—Organic compounds, e.g. vitamins containing nitrogen
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Dermatology (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Emergency Medicine (AREA)
- Cosmetics (AREA)
- Detergent Compositions (AREA)
Abstract
The present invention relates to articles for washing fields, disclose a kind of handmade soap of niacinamide-containing, in terms of the grease weight in raw material, containing 0.05%~10% niacinamide.Preparation methods steps include: that (1) grease is mixed at 25~50 DEG C of aqueous slkali, and stirs saponification 2~16 hours；(2) it is enclosed at 15~45 DEG C and keeps the temperature to pH=8~9；(3) soap blank is ground into pureed, and niacinamide or nicotinoyl amine composition is added, is fully ground uniformly mixed；The additive amount of niacinamide is the 0.05%~10% of grease weight；(4) it forms and places to maturation.Above method handmade soap obtained, while cleaning and is moist, also with the skin-care effect of niacinamide；And niacinamide can be stabilized wherein, can long-term preservation is non-discolouring never degenerates.
Description
Technical field
The present invention relates to articles for washing field, specially a kind of handmade soap and preparation method are especially added to niacinamide
Or the handmade soap and preparation method of nicotinoyl amine composition.
Background technique
Soaps preparation is common cleaning products, and commercially available perfumed soap in saponification, will be saponified generated glycerol and take out mostly
From as cosmetic use.Without the perfumed soap of glycerol, it is easy to make dry skin after washing.The primary raw material of handmade soap be grease,
Alkali and water do not remove the glycerol generated when saponification, are capable of forming protective film while cleaning, moisturize the skin.
Niacinamide is also known as niacinamide, belongs to vitamin B complex, in addition to can also make for medicine and nutrient additive for food
For the nutritive additive of cosmetics, there are a variety of skin-care effects, mainly have:
1, whitening: the melanosome transhipment from melanocyte to keratinocyte is lowered, cutaneous pigmentation is reduced；Interference angle
Change the cell signal channel between cell and melanocyte, reduces melanin production；It may act on the melanin generated, subtract
Few its is shifted to cells of superficial layer.
2, improve skin barrier function, anti-aging, moisturizing: improving the water of the free fatty acid and ceramide in skin
It is flat, skin corium microcirculation is stimulated, skin water loss is prevented.It can also promote protein synthesis (such as keratin), improve cell
Interior NADPH is horizontal, and accelerates the differentiation of angle albuminous cell.
3, oil-control and convergence pore, treat acne.
Due to the skin-care effect that niacinamide is excellent, by worlds such as Olay, SK II, Paris L'Oreal, reason skin spring, Ponds
Big shot is used in skin-protection product, and product forms have cream, frost, cream, water.
Currently, few reports that niacinamide is used for cleaning product, especially soap product.
Patent CN101475884A relates to a kind of perfumed soap composition containing vitamin active additive, wherein vitamin
Class additive kind includes niacinamide.This kind of perfumed soap also contains perfumed soap soap base, antioxidant, fungicide, titanium dioxide, fluorescent brightening
Agent, sodium silicate and essence belong to the perfumed soap of soap base preparation.Soap base is that salt is added after the saponification of soapmaking, is separated
It is prepared in addition to the lye and moisture content of glycerol, excess in system.
Patent CN1886116A discloses a kind of personal cleansing soap composition containing the skin lightenings agent such as niacin, niacinamide.
Soap base therein is the saponification resultant for eliminating glycerol.Niacinamide is incompatible with this soaps, is easy to lose stability and cause
Soaps preparation discoloration, especially under conditions of damp and hot.By the way that diethylene-triamine pentaacetic acid (DTPA) is added to solve containing cigarette
The problems such as soaps stability and discoloration of amide active constituent.
Accordingly, it is desirable to provide a kind of strong cleaning force, have moisturizing effect niacinamide-containing handmade soap, with cleaning,
The multi-efficiency of skin care.
Summary of the invention
The present invention is intended to provide the handmade soap and preparation side of a kind of niacinamide-containing or niacinamide and other compositions of additives
Method.
The technical solution of the present invention is as follows: a kind of handmade soap of niacinamide-containing contains 0.05% in terms of the grease weight in raw material
~10% niacinamide.Preferably, in terms of the grease weight in raw material, the content of niacinamide is 2%~8%.
Also contain fragrance, essential oil, at least one of whitening, moisturizing and/or active constituent of anti-aging in handmade soap.
Above-mentioned handmade soap preparation method includes the following steps:
(1) grease is mixed at 25~50 DEG C of aqueous slkali, and stirs saponification 2~16 hours；
Preferably, aqueous slkali is poured into stir in grease and is saponified；Preferably, grease and aqueous slkali mix at 35~45 DEG C
It closes, and stirs saponification 4~8 hours；Alkali is NaOH or KOH；
(2) then at 15~45 DEG C sealed thermal insulating to pH=8~9；
(3) soap blank is ground into pureed, and niacinamide or nicotinoyl amine composition is added, is fully ground uniformly mixed；Niacinamide
Additive amount be grease weight 0.05%~10%；
(4) it forms and places to maturation；Usually place 20~70 days.
In step (1), the aqueous slkali is using deionized water as solvent, conductivity≤5 μ s/cm of deionized water, alkali with
The weight ratio of deionized water is 1.5~3；It is furthermore preferred that the conductivity of deionized water≤1 μ s/cm, the weight of alkali and deionized water
Than being 2~2.8, more preferably 2.2~2.4.
In step (1), the dosage of alkali is the 93%~99% of the fully saponified amount of grease, preferably 94%~98%.
Fully saponified amount (alkali required for fully saponified)=oil quality × saponification value of grease；When grease is miscella
When, fully saponified amount is the sum of products of all kinds of oil qualities and corresponding saponification number, it may be assumed that 1 mass of grease × grease, 1 saponification value+
2 mass of grease × grease, 2 saponification value+...+grease n mass × grease n saponification value.In order to ensure that there is no free NaOH, with
Exempt to injure skin, the dosage of alkali can be generally reduced according to calculated value.
Preferably, alkali NaOH.
Grease is vegetable fat, animal fat, mineral oil, beeswax or its any mixture.
Vegetable fat includes coconut oil, palm oil, palmin, palm kernel oil, palm stearin acid, corn oil, soybean oil, olive
Olive oil, peanut oil, wheat-germ oil, tea oil, hazelnut oil, canola oil, mustard oil, sunflower oil, rice bran oil, shea butter, castor
Sesame oil, cocoa butter, Sweet Almond Oil, apricot persic oil, honey peach nucleolus oil, caffeol, aloe, evening primrose oil, avocado oil, Xia Wei
Smooth fruit oil, sesame oil, borage oil, cedar oil, rose-seed oil, rose hip oil, safflower oil, pumpkin seed oil, mango oil, linseed
Oil, linseed oil, grape seed oil, cottonseed oil, camellia caul-fat, SIMMONDSIA CHINENSIS SEED OIL, sesame oil, nut oil, hemp oil, cardamom rouge, small-mouthed jar
Grain seed oil, tung oil etc..
Animal fat include lanolin, house oil, ermine oil, butter, sheep oil, deer oil, lard, goose oil, ostrich oil, fat of Oromaius norvaehollandeae,
Chicken fat.
Mineral oil includes white oil, vaseline, paraffin etc..
Preferably, grease includes at least one of palm oil and coconut oil, accounts for the 20%~60% of grease total amount.
Preferably, grease includes: the palm oil and coconut oil that (1) weight ratio is 0.1~10:1, and the two accounts for grease total amount
20%~60%, more excellent is 30%~50%；And (2) palmin, palm kernel oil, palm stearin acid, corn oil, soybean oil,
Olive oil, peanut oil, wheat-germ oil, tea oil, hazelnut oil, canola oil, mustard oil, sunflower oil, rice bran oil, shea butter,
Castor oil, cocoa butter, Sweet Almond Oil, apricot persic oil, honey peach nucleolus oil, caffeol, aloe, evening primrose oil, avocado oil, summer
Prestige razes fruit oil, sesame oil, borage oil, cedar oil, rose-seed oil, rose hip oil, safflower oil, pumpkin seed oil, mango oil, flax
Seed oil, linseed oil, grape seed oil, cottonseed oil, camellia caul-fat, SIMMONDSIA CHINENSIS SEED OIL, sesame oil, nut oil, hemp oil, cardamom rouge,
It is poppy seed oil, tung oil, lanolin, house oil, ermine oil, butter, sheep oil, deer oil, lard, goose oil, ostrich oil, fat of Oromaius norvaehollandeae, chicken fat, white
At least one of oil, vaseline, paraffin, beeswax.
In step (2), sealed thermal insulating 4~10 days at 20~40 DEG C are taken out when pH=8~9.
In step (3), the nicotinoyl amine composition includes: a. niacinamide, b. fragrance, essential oil, with whitening, moisturizing
And/or at least one of activity of fighting against senium nutriment.
Preferably, in terms of the weight of grease, the additive amount of niacinamide is 2%~8%.
Essential oil is Peppermint essential oil, Lavender, chamomile essential oil, Geranium Essential, refined jasmine oil, flores aurantii essential oil, meat
Osmanthus essential oil, Rosa Damascana, sandalwood essential oil, Rosemary Oil, grapefruit essential oil, lemon etc., additive amount are grease total amount
0.01%~5%, preferably 0.05%~0.2%.
Moisturizing active nutrients include glycerol, honey, hyaluronic acid, Sodium Hyaluronate, aloe extract etc..
Whitening active nutriment includes arbutin, VC, VE etc..
In a preferred embodiment of the invention, the preparation method comprises the following steps: the deionized water solution of (1) grease and NaOH are 35~45
It is mixed at DEG C, keep the temperature and stirs 4~6hr of saponification；The dosage of NaOH is the 95%~98% of the fully saponified amount of grease；
Preferably, grease are as follows: the palm oil and coconut oil of 0.1~10:1 of a. weight ratio, the two account for grease total amount 30~
50%, more preferably 40%；And b. palmin, palm kernel oil, palm stearin acid, corn oil, soybean oil, olive oil, peanut
Oil, wheat-germ oil, tea oil, hazelnut oil, canola oil, mustard oil, sunflower oil, rice bran oil, shea butter, castor oil, cocoa
Rouge, Sweet Almond Oil, apricot persic oil, honey peach nucleolus oil, caffeol, aloe, evening primrose oil, avocado oil, Macadamia nut oil, sesame
Sesame oil, borage oil, cedar oil, rose-seed oil, rose hip oil, safflower oil, pumpkin seed oil, mango oil, linseed oil, flaxseed
Oil, grape seed oil, cottonseed oil, camellia caul-fat, SIMMONDSIA CHINENSIS SEED OIL, sesame oil, nut oil, hemp oil, cardamom rouge, poppy seed oil, paulownia
Oil, lanolin, house oil, ermine oil, butter, sheep oil, deer oil, lard, goose oil, ostrich oil, fat of Oromaius norvaehollandeae, chicken fat, white oil, vaseline,
At least one of paraffin, beeswax；
It is furthermore preferred that palm oil and coconut oil weight ratio are 0.5~2, in an embodiment of the invention, the two weight
Amount is than being 1:1；The two accounts for grease total amount 40%.
The conductivity of deionized water≤1 μ s/cm, and the weight ratio of NaOH and deionized water is 1.5~3, more preferably 2
~2.8；In an embodiment of the invention, weight ratio 2.3；
(2) 25~35 DEG C sealed thermal insulating 5~7 days, taken out when pH=8~9；
(3) soap blank is ground into pureed, and addition niacinamide or nicotinoyl amine composition are fully ground uniformly mixed；Niacinamide
Additive amount is the 2%~8% of grease weight, more preferably 4%~5%；Nicotinoyl amine composition are as follows: a. niacinamide；B. fragrance, essence
Oil, at least one of whitening, moisturizing and/or active constituent of anti-aging, preferably essential oil and/or fragrance；
(4) it is placed 30~65 days after forming, keeps saponification complete.
Handmade soap of the invention is the handmade soap of a kind of niacinamide-containing or niacinamide and other compositions of additives, is had clear
Clean, moist, skin care multi-efficiency.This handmade soap is not prepared by perfumed soap soap base, by grease and sodium hydroxide saponification
Molding obtains after reaction, contains sodium soap and glycerol that reaction generates, and add nicotinoyl in handmade soap forming process
Amine or nicotinoyl amine composition (additive includes but are not limited to nutriment, fragrance, essential oil etc.) containing other additives, and
And niacinamide can be stabilized in handmade soap.
In the above-mentioned obtained handmade soap finished product of preparation method, the content of niacinamide can achieve 3%~5% even more
Height, and stability can be kept.The foam exquisiteness of handmade soap is abundant, and cleaning force is high, and very mild to skin, non-stimulated, silk
The cuticula of skin can not be destroyed.It is different from soap base perfumed soap, after handmade soap is reacted by grease and alkali (not excessive) are fully saponified
Molding directly obtains, and contains the glycerol generated in reaction.Glycerol has moisture-keeping function, can in many skin care products and cosmetics
The moisturizing ingredient of addition, therefore this handmade soap can form layer protecting film while cleaning dirt, reach protection skin
Effect.This handmade soap washes sense better than soap base perfumed soap, not will cause and excessively tight after washing washes sense.
This handmade soap is while cleaning and is moist, also with the skin-care effect of niacinamide, including whitening, improvement skin
Barrier, anti-aging, moisturizing, oil-control and convergence pore, treatment acne etc., with the application value in industry.Meanwhile it is of the invention
In handmade soap, niacinamide can be stabilized, and not need that the additives such as stabilizer, chelating agent are added.By long-time storage,
Handmade soap is non-discolouring to never degenerate, and effective component niacinamide invariance or loss contained therein.After placing 6~8 months, hand
Work soap does not change colour, and the content of niacinamide does not change substantially, is conducive to the long-term preservation of handmade soap and keeps effectively living
The stability of property ingredient.
Specific embodiment
It is exemplified below two niacinamide handmade soap product and preparation method is illustrated the present invention program.It should be understood that this hair
Bright protection scope is not limited only to this.Those skilled in the art are as needed, the type and proportion of adjustable used grease,
And add essential oil, fragrance or other nutritional ingredients.
Embodiment 1
By 200g palm oil (saponification value 0.142gNaOH/g), 66.2 He of 200g coconut oil (saponification value 0.19gNaOH/g)
600g soybean oil (saponification value 0.135gNaOH/g) keeps the temperature at 40 DEG C and is persistently stirred, total saponification amount (147.2g of grease
NaOH)；It weighs 144g sodium hydroxide (about 98% saponification amount), 331ml deionized water (conductivity≤1 μ s/cm) is added and is configured to
NaOH solution is down to 40 DEG C to NaOH solution temperature, is poured slowly into miscella, and 40 DEG C of heat preservations, lasting stirring be saponified anti-
It answers.
After reacting 5hr, enter mould, above covers film in order to avoid moisture evaporates, 5-7 days are kept the temperature in 30 DEG C of incubators, during heat preservation
PH is monitored, pH takes out demoulding at 8~9, and soap blank is worn into pureed, 99.32% niacinamide crystal 50g of content is added, sufficiently rubs
Be uniformly mixed, press-in die molding, demoulding, handmade soap after demoulding it is shady and cool, be protected from light, the place of drying dries in the air and puts one to two moon,
It is packed after detection is qualified.Final finished weight 1378g, is creamy white, pH=8~9.
Embodiment 2
(1) by 200g palm oil, 200g coconut oil and 600g corn oil (saponification value 0.136gNaOH/g), (total saponification amount is about
147.8g NaOH) it is kept the temperature at 40 DEG C, it is persistently stirred, weighs 140g sodium hydroxide (about 95% saponification amount), be added
322ml deionized water (conductivity≤1 μ s/cm) is configured to NaOH solution, is down to 40 DEG C to NaOH solution temperature, is poured slowly into mixed
It closes in oil, 40 DEG C of heat preservations, lasting stirring carries out saponification, reacts 5hr；
(2) enter mould, above cover film in order to avoid moisture evaporates, keep the temperature 5-7 days in 30 DEG C of incubators, monitor pH during heat preservation,
PH takes out demoulding in 8-9；
(3) soap blank is worn into pureed, addition content is 99.32% niacinamide crystal 50g, and Lavender 20 is added and drips
(about 1~1.2mL) is sufficiently rubbed up uniformly mixed；
(4) press-in die forms, demoulding, handmade soap after demoulding it is shady and cool, be protected from light, the place of drying dries in the air and puts one to two moon,
It is packed after detection is qualified.Final finished is creamy white, weight 1370g, pH about 8~9.
Handmade soap made from Examples 1 and 2 is detected, wherein concentration for nicotinamide is respectively 3.62% and 3.64%.By QB/
II standard of T2485-2008 executes other detection projects, as a result such as table 1:
Table 1
The amount of niacinamide substance is accounted as follows:
Input amount: 50 × 99.32%=49.66g
Finished product: 1378 × 3.61%=49.74g；1370 × 3.64%=49.87g；
The amount of niacinamide substance before and after finished product reaches balance, it can be seen that there is no damage in preparation process niacinamide
It loses.Above-mentioned handmade soap continues at room temperature after placing storage 6 months, and there is no variations for color；Through detecting, wherein niacinamide
Content is still above 3.4%.
The handmade soap of above method preparation, when washing, generates a large amount of foams, and foam is fine and smooth, and detergency is strong, after use
Skin is not dried, and cleaning and moisturizing effect are good.And niacinamide can steadily be present in product, there is the effect of whitening.
Claims (10)
1. a kind of handmade soap of niacinamide-containing, which is characterized in that in terms of the grease weight in raw material, contain 0.05%~10%
Niacinamide.
2. the handmade soap of niacinamide-containing described in claim 1, which is characterized in that in terms of the grease weight in raw material, containing 2%~
8% niacinamide.
3. the handmade soap of niacinamide-containing as claimed in claim 1 or 2, which is characterized in that also contain fragrance, essential oil, whitening, moisturizing
And/or at least one of active constituent of anti-aging.
4. the preparation method of the handmade soap of any one of claims 1 to 3 niacinamide-containing, which is characterized in that step includes:
(1) grease is mixed at 25~50 DEG C of aqueous slkali, and stirs saponification 2~16 hours；The alkali is KOH or NaOH；
(2) then at 15~45 DEG C sealed thermal insulating to pH=8~9；
(3) soap blank is ground into pureed, and niacinamide or nicotinoyl amine composition is added, and it is equal to be fully ground mixing；The niacinamide
Composition includes: a. niacinamide, b. fragrance, essential oil, at least one of whitening, moisturizing and/or active constituent of anti-aging；
(4) it forms and places to maturation.
5. preparation method as claimed in claim 4, which is characterized in that the dosage of alkali be the fully saponified amount of grease 93%~
99%.
6. preparation method as claimed in claim 4, which is characterized in that the grease is vegetable fat, animal fat, mineral
Oil, beeswax or its any mixture.
7. preparation method as claimed in claim 4, which is characterized in that aqueous slkali is using deionized water as solvent, the electricity of deionized water
Conductance≤5 μ s/cm, and the weight ratio of alkali and deionized water is 1.5~3.
8. preparation method as claimed in claim 4, which is characterized in that the conductivity of deionized water≤1 μ s/cm, and alkali with go
The weight ratio of ionized water is 2~2.8.
9. preparation method as claimed in claim 4, which is characterized in that in step (1), grease and aqueous slkali mix at 35~45 DEG C
It closes, and stirs saponification 4~8 hours；In step (2), sealed thermal insulating 4~10 days is to pH=8~9 at 20~40 DEG C.
10. preparation method as claimed in claim 4, which is characterized in that the grease includes: that (1) weight ratio is 0.1~10:1
Palm oil and coconut oil, the two accounts for the 20%~60% of grease total amount；And (2) palmin, palm kernel oil, palm stearin
Acid, corn oil, soybean oil, olive oil, peanut oil, wheat-germ oil, tea oil, hazelnut oil, canola oil, mustard oil, sunflower oil,
Rice bran oil, shea butter, castor oil, cocoa butter, Sweet Almond Oil, apricot persic oil, honey peach nucleolus oil, caffeol, aloe, the moon
See careless oil, avocado oil, Macadamia nut oil, sesame oil, borage oil, cedar oil, rose-seed oil, rose hip oil, safflower oil, pumpkin
Seed oil, mango oil, linseed oil, linseed oil, grape seed oil, cottonseed oil, camellia caul-fat, SIMMONDSIA CHINENSIS SEED OIL, sesame oil, English walnut
Oil, hemp oil, cardamom rouge, poppy seed oil, tung oil, lanolin, house oil, ermine oil, butter, sheep oil, deer oil, lard, goose oil, ostrich
At least one of oil, fat of Oromaius norvaehollandeae, chicken fat, white oil, vaseline, paraffin, beeswax.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110747075A (en) * | 2019-11-06 | 2020-02-04 | 青岛琅琊台集团股份有限公司 | Chitosan oligosaccharide handmade soap and preparation method thereof |
| US20200239816A1 (en) * | 2019-01-30 | 2020-07-30 | Hunsang KANG | Natural fragrance soap |
| CN113493725A (en) * | 2021-06-21 | 2021-10-12 | 广东菁萃生物科技有限公司 | Mild non-irritating nursing handmade soap and preparation method thereof |
| US20220401338A1 (en) * | 2019-12-16 | 2022-12-22 | Colgate-Palmolive Company | Personal Care Compositions and Methods for the Same |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1886116A (en) * | 2003-11-27 | 2006-12-27 | 荷兰联合利华有限公司 | Stable personal wash soap composition and process to prepare the same |
| CN101489522A (en) * | 2006-07-13 | 2009-07-22 | 荷兰联合利华有限公司 | Improved skin lightening cosmetic composition |
| CN103194334A (en) * | 2013-04-02 | 2013-07-10 | 朱海文 | Cold process soap added with fresh fig protoplasm |
| CN106635525A (en) * | 2016-09-29 | 2017-05-10 | 中国海洋大学 | Algae cold soap and preparation method thereof |
-
2017
- 2017-06-01 CN CN201710404859.2A patent/CN108977290A/en not_active Withdrawn
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1886116A (en) * | 2003-11-27 | 2006-12-27 | 荷兰联合利华有限公司 | Stable personal wash soap composition and process to prepare the same |
| CN101489522A (en) * | 2006-07-13 | 2009-07-22 | 荷兰联合利华有限公司 | Improved skin lightening cosmetic composition |
| CN103194334A (en) * | 2013-04-02 | 2013-07-10 | 朱海文 | Cold process soap added with fresh fig protoplasm |
| CN106635525A (en) * | 2016-09-29 | 2017-05-10 | 中国海洋大学 | Algae cold soap and preparation method thereof |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20200239816A1 (en) * | 2019-01-30 | 2020-07-30 | Hunsang KANG | Natural fragrance soap |
| CN110747075A (en) * | 2019-11-06 | 2020-02-04 | 青岛琅琊台集团股份有限公司 | Chitosan oligosaccharide handmade soap and preparation method thereof |
| US20220401338A1 (en) * | 2019-12-16 | 2022-12-22 | Colgate-Palmolive Company | Personal Care Compositions and Methods for the Same |
| CN113493725A (en) * | 2021-06-21 | 2021-10-12 | 广东菁萃生物科技有限公司 | Mild non-irritating nursing handmade soap and preparation method thereof |
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