CN106635525B - A kind of seaweed cold process soap and preparation method thereof - Google Patents
A kind of seaweed cold process soap and preparation method thereof Download PDFInfo
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- CN106635525B CN106635525B CN201610861185.4A CN201610861185A CN106635525B CN 106635525 B CN106635525 B CN 106635525B CN 201610861185 A CN201610861185 A CN 201610861185A CN 106635525 B CN106635525 B CN 106635525B
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/24—Hydrocarbons
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
- C11D9/262—Organic compounds, e.g. vitamins containing oxygen containing carbohydrates
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/30—Organic compounds, e.g. vitamins containing nitrogen
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
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Abstract
The present invention relates to daily cosmetics fields, more particularly to a kind of seaweed cold process soap.It is formed including following components in percentage by weight: seaweed extracted liquor 5-20%, celery alcohol extract 1-10%.For the present invention using the alcohol extract of the extracting solution of tangleweed and celery as main active, other active materials such as algal oil, saualane, niacinamide and natural complex E oil are added in cooperation, under cryogenic manufactured cold process soap.The present invention has the advantages that safe mild, anti-inflammatory moisturizing, natural no stimulation, it can be at low temperature than more completely saving flavones and natural pigment isoreactivity nutritional ingredient in polysaccharide in seaweed extracted liquor, phenols, protein, vitamin, amino acid and celery alcohol extract, it is one kind safely and effectively skin cleaning and beauty product, the crowd suitable for different sexes, age and skin quality.
Description
Technical field
The present invention relates to daily cosmetics field fields, more particularly to a kind of seaweed cold process soap and preparation method thereof.
Background technique
Manual cold process soap is a kind of soap of rising in recent years, basic preparation principle be by vegetable fat at low temperature with
Saponification occurs for alkali, generates the natural glycerin and fatty acid salt surfactant of high-content, adds other auxiliary material systems
?.Presently commercially available industrial perfumed soap is mostly hot soapmaking, is quickly obtained finished product by lasting high temperature when production, has irritation
Greatly, alkalinity is strong, destroys pH value and the urea retained, uric acid, salinity, lactic acid, amino acid, free fatty acid of human body surface etc.
Acidic materials, and the glycerol generated is extracted, and adds a large amount of chemical agents, keeps product skin-care effect poor, to skin irritatin
Greatly.
With the development of society, people increasingly advocate health, natural, environmental protection Green Lifestyle, thus to perfumed soap
The requirement of the washing product of itself body surface of this kind of close contact is more and more.The cold process soap for not needing high-temperature heating, due to can be with
Retain the nutritional ingredient in vegetable oil and other additives to greatest extent, obtains the favor of people.
The production of cold process soap is mainly using pure natural cold press vegetable fat as raw material, at low temperature with sodium hydroxide by stirring
The process soapmaking base mix, being saponified further according to the different effect of product or meets the diversified demand of product, be added it is a variety of effectively at
Point, then enter mould, forming, demoulding, curing are made.The marine biomaterials such as collagen, phenols, oligosaccharide have succeeded
All kinds of cosmetics are developed into, but the cold process soap containing seaweed extracted liquor still belongs to blank.And Flavonoid substances contain in celery alcohol extract
Amount is abundant, can treat various inflammation, is good antioxidant, has the effect of calm, to calm the nerves, be depressured, cooperates seaweed extracted liquor
The effect of enhancing cold process soap.
The present invention in view of the shortcomings of the prior art, adds the active material containing seaweed extracted liquor and celery alcohol extract, cooperation
Other active materials such as algal oil, saualane, niacinamide, vitamin E oil, sodium alginate make in cold process soap nutritional ingredient more
It is comprehensive available, reach that skin whitening, moisturizing, anti-inflammatory be crease-resistant, mild clean effect.
Summary of the invention
The present invention is destroyed for nutritional ingredient existing for the hot soapmaking on the market using continuous high temperature heating, rejects generation
Natural glycerin, and the problems such as a large amount of chemicals of addition, preservative, artificial essence, pigment, it is mild to provide a kind of safety, has
Anti-inflammatory moisturizing, natural no stimulation advantage cold process soap.
The present invention using the alcohol extract of the extracting solution of tangleweed and celery as main active, cooperation be added algal oil,
Other active materials such as saualane, niacinamide and natural complex E oil, under cryogenic made of cold process soap.It can be low
Temperature is lower than more completely saving in seaweed extracted liquor in polysaccharide, phenols, protein, vitamin, amino acid and celery alcohol extract
Flavones and natural pigment isoreactivity nutritional ingredient solve existing perfumed soap and wash rear tight, and anti-inflammatory moisture retention is poor, and irritation is big, chemistry
The problems such as preparation is mostly few with functional component.It has many advantages, such as moisturizing, whitening anti-wrinkling, mild non-stimulated, is a kind of safety
Effective skin cleaning and beauty product, the crowd suitable for different sexes, age and skin quality.
The technical solution adopted by the invention is as follows: a kind of seaweed cold process soap, including following components in percentage by weight composition:
Seaweed extracted liquor 5-20%, celery alcohol extract 1-10%.
Further, the preparation method of above-mentioned seaweed extracted liquor include the following:
(1) after rinsing seaweed well, drying crushes to obtain algae powder, 1g algae powder is uniformly mixed with the water of 10-100mL, protects
Temperature is held at 20-60 DEG C, extracts 6-48h under oscillating condition, the seaweed refer to one of brown alga, red algae, green alga or
Several combinations；
(2) it is centrifuged 15min under the conditions of revolving speed 4000r/min, then obtains seaweed extracted liquor after filtering.
Further, the preparation method of above-mentioned celery alcohol extract:
Dries pulverizing after fresh celery is cleaned is mentioned by the 70%-100% EtOH Sonicate that 20-100ml is added in 1g powder
It after taking 0.5-3h, filters, removing ethyl alcohol is concentrated under reduced pressure, obtain alcohol extract.
Further, the present invention also provides a kind of preparation methods of seaweed cold process soap, comprising the following steps:
(1) it by basic grease 60-80%, remaining grease 0-10%, is heated at 20-50 DEG C, is allowed to be completely dissolved, obtains A
Phase, the basic grease refer to olive oil, palm oil, coconut oil, Sweet Almond Oil, in evening primrose oil two or more
Combination, remaining described grease refer to SIMMONDSIA CHINENSIS SEED OIL, sesame oil, natural complex E oil, avocado oil, one or two kinds of in algal oil
Above combination；
(2) sodium hydroxide 2-20% is weighed, 2-20% deionized water dissolving is added, stirring condition is cooled to 20-50 DEG C, obtains
B phase；
(3) claim saualane 0.1-5%, niacinamide 0.1-5%, sodium alginate 0.1-5%, seaweed extracted liquor 5-20%, celery
Dish alcohol extract 1-10% is dissolved in 1-20% deionized water, is dissolved by heating at 20-50 DEG C, is obtained C phase；
(4) above-mentioned ABC tri- is mixed, accelerates to be saponified with blender high-speed stirred, to sticky after stirring 20-120min
State pours into mold；
(5) above-mentioned steps (4) demould after 1-5 days, be placed under shady and cool dry environment place 10-50 days to its completely at
It is ripe, obtain product.
Cold process soap produced by the invention contains seaweed extracted liquor and celery alcohol extract, trehalose, polyphenol and the Huang contained
Ketone isoreactivity component content is abundant, has the characteristics that moisture-keeping crease-shedding, natural whiting, mild cleaning.Cold process soap produced by the invention
It is nontoxic non-stimulated without adding chemical preservative and artificial color containing natural antibacterial agent and natural pigment, it is a kind of safety
Effective skin cleaning and beauty product, the crowd suitable for different sexes, age and skin quality.The preparation side of cold process soap of the present invention
Forensic science, simple process, manufacturing process pollution-free, environmentally protective are suitble to industrialized production.
Specific embodiment
The present invention selects pure natural tangleweed, and seaweed extracted liquor is obtained in such a way that water mentions, and extraction cost is low, and
Cooperate celery alcohol extract, with its flavones active component abundant, makes the present invention that there is cleaning reparation, skin whitening, moisturizing, crease-resistant disappear
Inflammation and other effects.Furthermore contain natural antibacterial agent in seaweed zymolyte, antibacterial effect is good, without adding chemical preservative.More
Further, natural pigment rich in without adding artificial color ensure that product in the celery alcohol extract in the present invention
It is nontoxic non-stimulated, suitable for the crowd of different sexes, age and skin quality, cost performance is high, environmentally protective.
Below by way of specific preferred embodiment, invention is further described in detail, but the present invention be not limited in it is following
Embodiment.
Embodiment 1:
1.1 form the ingredient of the cold process soap containing seaweed extracted liquor and celery alcohol extract of the invention and its weight percent is:
A phase: olive oil 12%, palm oil 18%, coconut oil 18%, Sweet Almond Oil 12%, SIMMONDSIA CHINENSIS SEED OIL 1.5%, natural
Vitamin E oil 1.5%, algal oil 0.5%；
B phase: sodium hydroxide 5%, deionized water 10%；
C phase: saualane 2%, sodium alginate 1%, seaweed extracted liquor 8%, celery alcohol extract 2%, is gone niacinamide 0.5%
Ionized water 8%；
1.2 technical process:
The preparation method of above-mentioned seaweed extracted liquor: after sargassum fusifome is rinsed well, drying crushes to obtain algae powder, by 1g algae
Powder is uniformly mixed with the water of 100mL, maintains the temperature at 60 DEG C, is extracted 10 hours under oscillating condition.Then, after taking-up
It is centrifuged 15min under the conditions of 4000r/min, sargassum fusifome extracting solution is obtained after suction filtration.
The preparation method of above-mentioned celery alcohol extract: dries pulverizing after fresh celery is cleaned adds 20ml by 1g dry powder
70% EtOH Sonicate extract 1h after, then filter, is concentrated under reduced pressure removing ethyl alcohol after obtain alcohol extract.
It at 20 DEG C, will be mixed after above-mentioned tri- phased soln of ABC, accelerate to be saponified with blender high-speed stirred, stir 30min
To viscous pasty state, mold is poured into.It is demoulded after 1 day, is put under shady and cool dry environment and places after ripening in 10 days, obtain mentioning containing seaweed
Take the cold process soap of liquid and celery alcohol extract.
Embodiment 2:
2.1. the ingredient and its weight percent for forming the cold process soap of the invention containing seaweed extracted liquor and celery alcohol extract are:
A phase: olive oil 30%, evening primrose oil 18%, Sweet Almond Oil 18%；
B phase: sodium hydroxide 4%, deionized water 10%；
C phase: saualane 1%, niacinamide 1%, sodium alginate 2%, seaweed extracted liquor 10%, celery alcohol extract 3%, go from
Sub- water 3%；
2.2. technical process:
The preparation method of the seaweed extracted liquor: after Yi Guzao is rinsed well, drying crushes to obtain algae powder, by 1g algae powder
It is uniformly mixed with the water of 50mL, maintains the temperature at 20 DEG C, extracted 24 hours under oscillating condition.In 4000r/min item after taking-up
It is centrifuged 15min under part, Yi Guzao extracting solution is obtained after suction filtration.
The preparation method of celery alcohol extract: dries pulverizing after fresh celery is cleaned adds the 80% of 100ml by 1g dry powder
EtOH Sonicate extract 3h after, then filter, is concentrated under reduced pressure removing ethyl alcohol after obtain alcohol extract.
It at 30 DEG C, will be mixed after above-mentioned tri- phased soln of ABC, accelerate to be saponified with blender high-speed stirred, stir 60min
To viscous pasty state, mold is poured into.It is demoulded after 3 days, is put under shady and cool dry environment and places after ripening in 20 days, obtain mentioning containing seaweed
Take the cold process soap of liquid and celery alcohol extract.
Embodiment 3:
3.1. the ingredient and its weight percent for forming the cold process soap of the invention containing seaweed extracted liquor and celery alcohol extract are:
A phase: olive oil 32%, Sweet Almond Oil 30%, SIMMONDSIA CHINENSIS SEED OIL 1%, sesame oil 1%, natural complex E oil 1%, crocodile
Pear oil 1%, algal oil 1%；
B phase: sodium hydroxide 5.5%, deionized water 7.5%；
C phase: saualane 1%, niacinamide 1%, sodium alginate 1%, seaweed extracted liquor 4%, celery alcohol extract 10%, go from
Sub- water 3%；
3.2. technical process:
The preparation method of the seaweed extracted liquor: after sea grape is rinsed well, drying crushes to obtain algae powder, by 1g algae powder
It is uniformly mixed with the water of 10mL, maintains the temperature at 30 DEG C, extracted 24 hours under oscillating condition.In 4000r/min condition after taking-up
Lower centrifugation 15min obtains sea grape extracting solution after suction filtration.
The preparation method of celery alcohol extract: dries pulverizing after fresh celery is cleaned adds the 90% of 50ml by 1g dry powder
EtOH Sonicate extract 0.5h after, then filter, is concentrated under reduced pressure removing ethyl alcohol after obtain alcohol extract.
It at 50 DEG C, will be mixed after above-mentioned tri- phased soln of ABC, accelerate to be saponified with blender high-speed stirred, stirring
120min pours into mold to viscous pasty state.It is demoulded after 5 days, is put under shady and cool dry environment and places after ripening in 30 days, contained
The cold process soap of seaweed extracted liquor and celery alcohol extract.
Embodiment 4
Experimental evaluation is carried out to above-described embodiment
The activity rating of 4.1 seaweed extracted liquors: to junket ammonia in reference " chemical component and its bioactivity of tawny daylily algae detect "
Sour enzyme inhibition, remove the detection method of DPPH, the ability of hydroxy radical and superoxide anion and moisture absorption and performance of keeping humidity into
Row detection.
The activity rating of 4.2 celery alcohol extracts: referring to " celery different parts determination of total flavonoids and its anti-oxidant work
Property " in the antioxidant activity of the measuring method of hydroxy radical and ultra-oxygen anion free radical detection alcohol extract.
The test of 4.3 using effects: by the product of preparation, 10 testers is respectively issued to and compare use.Tester makes
It is cleaned in the same manner with when sample, every kind of sample uses 2 weeks.Tester according to oneself feel comment
Point.Standards of grading take ten point system, and 1 point worst, and 10 points best, and score more high effect is better.
4.4 foaming powers and foam stability test: with reference in " preparation of mild foam mildy wash and its performance study "
Experimental method is slightly improved, and is used and is prepared mass percentage as 10% each product solution 3mL, is put into graduated cylinder, adds distillation
Water is diluted to 15mL, after mixing, takes out the scale test tube that 25ml is added in 5ml sample, acutely shakes after capping 10 times, immediate record
Foam volume (mL) records foam volume after 10min again.It replication 3 times, is averaged.
4.5 organoleptic indicators: it is tested according to the soap body appearance and smell test method of " QB/T 2485-2008 perfumed soap ".
4.6 experimental result
4.6.1 the Activity evaluation of marine algae extract:
4.6.2 the antioxidant activity evaluation result of celery alcohol extract:
4.6.3 using effect is evaluated
4.6.4 foaming power and foam stability test:
4.6.5 organoleptic indicator:
Show that the present invention adds the cold process soap of seaweed extracted liquor and celery alcohol extract with good by above-mentioned test result
Good organoleptic attribute meets national standard, and using effect is good, has the multi-efficiencies such as moisture-keeping crease-shedding, natural whiting, mild cleaning.
The preferred embodiment of the present invention has been described above in detail, still, during present invention is not limited to the embodiments described above
Detail within the scope of the technical concept of the present invention can be with various simple variants of the technical solution of the present invention are made, this
A little simple variants all belong to the scope of protection of the present invention.
In addition, various embodiments of the present invention can be combined randomly, as long as it is without prejudice to originally
The thought of invention, it should also be regarded as the disclosure of the present invention.
Claims (1)
1. a kind of seaweed cold process soap, which is characterized in that the preparation method of the seaweed cold process soap, comprising the following steps:
(1) it by basic grease 60-80%, remaining grease 0-10%, is heated at 20-50 DEG C, is allowed to be completely dissolved, obtains A phase, it is described
Basic grease refers to olive oil, palm oil, coconut oil, Sweet Almond Oil, two or more the combination in evening primrose oil, institute
It states remaining grease and refers to SIMMONDSIA CHINENSIS SEED OIL, sesame oil, natural complex E oil, avocado oil, group one or more kinds of in algal oil
It closes；
(2) sodium hydroxide 2-20% is weighed, the deionized water dissolving of 2-20% is added, stirring condition is cooled to 20-50 DEG C, obtains B
Phase；
(3) claim saualane 0.1-5%, niacinamide 0.1-5%, sodium alginate 0.1-5%, seaweed extracted liquor 5-20%, celery alcohol extract
1-10% is dissolved in 1-20% deionized water, is dissolved by heating at 20-50 DEG C, is obtained C phase；
(4) above-mentioned ABC tri- is mixed, accelerates to be saponified with blender high-speed stirred, to thick after stirring 20-120min
State pours into mold；
(5) above-mentioned steps (4) demould after 1-5 days, are placed under shady and cool dry environment and place 10-50 days to its full maturity, obtain
To product；
The content of above-mentioned each component is weight percentage；
The preparation method of the seaweed extracted liquor the following steps are included:
(1) after rinsing seaweed well, drying crushes to obtain algae powder, 1g algae powder is uniformly mixed with the water of 10-100mL, keeps temperature
Degree extracts 6-48h, the seaweed refers to one or more of brown alga, red algae, green alga at 20-60 DEG C under oscillating condition
Combination；
(2) it is centrifuged 15min under the conditions of 4000 r/min of revolving speed, then obtains seaweed extracted liquor after filtering；
The celery alcohol extract the preparation method comprises the following steps:
Dries pulverizing after fresh celery is cleaned extracts 0.5- by the 70%-100% EtOH Sonicate that 20-100ml is added in 1g powder
It after 3h, filters, removing ethyl alcohol is concentrated under reduced pressure, obtain alcohol extract.
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| CN102978048A (en) * | 2012-11-16 | 2013-03-20 | 广州伊凡生物科技有限公司 | Weakly acidic transparent soap and preparation method thereof |
| CN104371861A (en) * | 2013-08-15 | 2015-02-25 | 青岛鹏远康华天然产物有限公司 | Seaweed health soap and making method thereof |
| CN104513733A (en) * | 2013-09-27 | 2015-04-15 | 青岛畅绿生物研究所 | Natural water lily essential oil perfumed soap |
| KR20150049112A (en) * | 2013-10-29 | 2015-05-08 | (주)제주사랑농수산 | A Soap Composition Containing Algae Fabrics |
| CN105062731A (en) * | 2015-08-20 | 2015-11-18 | 广州栋方生物科技股份有限公司 | Fermented-shea-butter amino acid transparent soap |
| CN105733862A (en) * | 2016-03-01 | 2016-07-06 | 苏州市贝克生物科技有限公司 | Facial soap and preparation method thereof |
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