CN107653107A - A kind of preparation method of cape jasmine whitening and skin-protecting type craft cold process soap - Google Patents
A kind of preparation method of cape jasmine whitening and skin-protecting type craft cold process soap Download PDFInfo
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- CN107653107A CN107653107A CN201710887142.8A CN201710887142A CN107653107A CN 107653107 A CN107653107 A CN 107653107A CN 201710887142 A CN201710887142 A CN 201710887142A CN 107653107 A CN107653107 A CN 107653107A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/005—Synthetic soaps
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/44—Perfumes; Colouring materials; Brightening agents ; Bleaching agents
- C11D9/442—Perfumes
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/44—Perfumes; Colouring materials; Brightening agents ; Bleaching agents
- C11D9/444—Dyes; Pigments
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/48—Superfatting agents
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- Oil, Petroleum & Natural Gas (AREA)
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Abstract
The invention discloses a kind of preparation method of cape jasmine whitening and skin-protecting type craft cold process soap.Weigh a certain amount of coconut oil, palm oil, rice bran oil, plant white oil, wheat-germ oil, cocoa butter, grape-kernel oil, whitish honey wax to be placed in beaker, heating water bath.A certain amount of NaOH and water are weighed respectively simultaneously, sodium hydroxide is poured slowly into water, stirring becomes clear to solution and is completely dissolved, it is essentially identical with grease temperature to treat that it is cooled to, slowly pour into grease, quick stirring, treat that soap lye starts to become sticky, other additives such as cape jasmine oil, cape jasmine shell extract, gardenia pollen, cape jasmine flower essential oil, ginseng extract can be added, 8 words can be drawn to soap lye surface by, which stirring, terminates, and pours into immediately in mould, it is stripped after isothermal solidifying, it is placed at shady and cool ventilation and preserves, treats that it is ripe, packed for standby use.
Description
Technical field
The present invention relates to articles for daily use technical field, is related to a kind of preparation side of cape jasmine whitening and skin-protecting type craft cold process soap
Method.
Background technology
Cape jasmine (Garadenia jasminoides), also known as Yellow Fructus Gardeniae, mountain Cape jasmine, Fructus Gardeniae etc., are rubiaceous one
Kind evergreen shrubs, main product is in Jiangxi, Zhejiang, Hunan and other places.Cape jasmine fruit system traditional Chinese medicine, also fall within Ministry of Public Health's promulgation first
Medicine-food two-purpose resource, effect are clearing heat and promoting diuresis, and purging intense heat dehumidifies, removing pattogenic heat from the blood and toxic material from the body, externally used detumescence analgesic.Modern pharmacological research shows Cape jasmine
Son has the effect such as anti-oxidant, anti-inflammatory and antalgic, antimicrobial, hepatic cholagogic, hypoglycemic.Cape jasmine is mainly Cape jasmine using part
Sub- fruit and gardenia, the complex chemical composition of cape jasmine fruit, mainly include crocin class, glucoside and polyatomic phenol, additionally
Contain 20 various trace elements such as pectin, mannitol and Fe, Mn, Zn, Cu；Gardenia essential oil containing cape jasmine, it is to refine Cape jasmine
The primary raw material of sub- essence.
Cold process soap refers to handmade soap in the narrow sense, refers to and is obtained at 45 DEG C using grease with saponification that alkali lye is carried out
Handmade soap.Formula is：Oil+alkali（It is dissolved in the sodium hydroxide or potassium hydroxide of water）=soap+natural glycerin.Due to soapmaking process
In avoid high temperature, therefore contain natural complex and nutritional ingredient in remaining vegetable oil and other additives to greatest extent,
Therefore it is the best skin care products of skin.There are a large amount of nutriments for being not involved in saponification in vegetable oil, these preciousnesses exist into branch
In being penetrated to the skin during use through pore, so as to reach cleaning, maintenance while the effect carried out.Cold process soap can be directed to certainly
Oneself skin quality makes, therefore oneself understands and what material is with the addition of in perfumed soap, strange into branch's injury skin without worrying, can pacify
The heart uses；Handmade soap is not only gently non-stimulated to skin, and also helps environmental protection；Handmade soap is " natural face cleaning activating agent ",
Grease can be effectively cleaned, and will not at all destroy the cuticula of skin；Add olive oil in handmade soap, and with other oil with
Different proportion mixes, and the handmade soap for making to make washes sense and function with unique.
Wheat-germ oil is also added into the present invention, containing protein, mineral matter, vitamin, pantothenic acid, niacin and insatiable hunger
And aliphatic acid, eczema, chronic eczema, aged skin can be improved, promote skin regeneration, have nourishes effect to blackspot, striae of pregnancy and scar；
Grape-kernel oil, containing vitamin, mineral matter, chlorophyll, fructose, glucose, vine polyphenol and protein, it is adapted to dark sore, acne oil
Property skin, prevention melanin deposition etc. adds cape jasmine in manual cold process soap, soap can also be made to have anti-oxidant, anti-inflammatory in addition
Analgesic acts on.
Extracted in addition, also adding such as ginseng of the natural plant extracts thing with whitening function in this money handmade soap simultaneously
Thing Rhizoma Chuanxiong extract, Angelica Dahurica extract and rose extract and pearl powder.Wherein, ginseng can be with sun-proof nti-freckle, for face
Portion's color spot, chloasma, ginseng extract can absorb ultraviolet, reduce skin injury, and ginsenoside can remove free radical, suppress black
Pigment, make skin pure white smooth.Ligusticum wallichii can be with freckle removing and whitening, and for chloasma, color spot, ligustrazine can suppress the work of tyrosinase
Property, understand oxygen radical, expand blood vessel, suppress platelet aggregation, improve microcirculation so as to effectively prevent chloasma, freckle, black
Spot etc..The root of Dahurain angelica also can freckle removing and whitening, for chloasma, color spot, blackhead, acne, the root of Dahurain angelica can improve local blood circulation, eliminate color
Element deposits in excessive tissue, promotes the metabolism of Skin Cell, and then the effect of beauty, in content in freckle cream external used medicine
In, the root of Dahurain angelica is conventional medicine.Rose has the function that nti-freckle of invigorating blood circulation, and for chloasma, color spot, eliminates endocrine disturbance and draws
The facial dark sore that rises, pigmentation, the disease such as chloasma.Pearl powder has whitening wrinkle-removing nti-freckle, precious for facial lines, color spot
Pearl contains the growth that a variety of protein hydrolysate promote cell, adsorbable in forming the preferable film of water-retaining property on dry skin, has
There are good nutrition and protection skin, local blood circulation can be promoted again, effective pre- anti-wrinkle and color spot.Therefore,
Not only the effect such as the anti-inflammatory with cape jasmine series of elements, antibacterial also has superior white-skinned face function to this money handmade soap, plus pure craft
Prepare, make the performance of this money handmade soap more prominent.
The content of the invention
It is an object of the invention to provide a kind of preparation method of cape jasmine whitening and skin-protecting type craft cold process soap, by cape jasmine series member
Element is applied in handmade soap, and adds pure natural plant extract and pearl powder with white-skinned face function, while carries out pure craft
Prepare.
It is a further object to provide the preparation scheme of above-mentioned cape jasmine whitening and skin-protecting type craft cold process soap.
The present invention is implemented according to following scheme：
The base oil of handmade soap of the present invention has：Coconut oil, palm oil, rice bran oil, plant white oil, wheat-germ oil, cocoa butter, Portugal
Grape seed oil and whitish honey wax, its sodium hydroxide saponification valency is respectively 0.19,0.141,0.128,0.136,0.131,0.137,
0.1265th, 0.069, INS values are respectively 258,145,70,115,58,157,66,84.
The alkali lye of handmade soap of the present invention is analysis level sodium hydroxide solution.
The INS values 125 ~ 150 of the handmade soap of the present invention are appropriate.
Step 1, weigh the g of coconut oil 20 ~ 100 on balance, palm oil 10 ~ 50 g, 15 ~ 65g of rice bran oil, plant white oil
15 ~ 75 g, the g of wheat-germ oil 10 ~ 50, the g of cocoa butter 15 ~ 75, the g of grape-kernel oil 20 ~ 100, the g of whitish honey wax 5 ~ 25 are placed in 1000
In mL beaker；Weigh the g of NaOH 15 ~ 75 respectively to be placed in 100 mL beaker, the g of water 30 ~ 150 is placed in 1000 mL beaker
In.
Step 2, the sodium hydroxide weighed up is slowly poured into water, while slowly stirs and become clear to solution and be
Only, that is, it is completely dissolved, stands, treat that its temperature is down to 45 ~ 50 DEG C.
Step 3, grease is placed in water-bath and heated, and with its temperature of thermometer measure, when temperature rises to 40 ~ 50 DEG C
Beaker is taken out from water-bath.
Step 4, the sodium hydroxide solution after cooling slowly poured into grease, side edged quickly stirs, at 40 ~ 50 DEG C
Under water bath condition, continue the h of stirring 0.5 ~ 1.0.
Step 5, stirring start to become sticky to solution, then add 5 ~ 25 mL cape jasmine oil, 5 ~ 25mL cape jasmine shell
Extract, 5 ~ 25 g gardenia pollen, 5 ~ 25 mL cape jasmine flower essential oil, 5 ~ 25 g Rhizoma Chuanxiong extracts, 5 ~ 25 g are white
Root of Dahurian angelica extract, can write after stirring on soap lye and 20 ~ 30 s do not disappear to stir and terminated, and pour into immediately in mould,
Rest in 30 ~ 35 DEG C of incubators, be stripped after 2 ~ 5 days.
Step 6, preservation at shady and cool ventilation is placed on, 25 ~ 35 DEG C of temperature, humidity is below 60, after 30 ~ 45 days, surveys its pH value 7
It is ripe when ~ 8, can packed for standby use.
The preparation method of the cape jasmine whitening and skin-protecting type craft cold process soap of the present invention also resides in：
The wet concentration used of the cape jasmine whitening and skin-protecting type craft cold process soap of the present invention selects rose extract.
The cape jasmine added before soap lye enters mould the oil of the cape jasmine whitening and skin-protecting type craft cold process soap of the present invention, by fresh cape jasmine fruit
Extract and obtain through ultrasonic assistant, condition is solid-liquid ratio 5:1~15:1, the min of extraction time 30 ~ 60,30 ~ 50 DEG C of Extracting temperature,
Extraction time 2 ~ 5 times, Extraction solvent are the one or several kinds such as petroleum ether, ethyl acetate, ethanol.
The cape jasmine shell extract added before soap lye enters mould of the cape jasmine whitening and skin-protecting type craft cold process soap of the present invention, by doing
Cape jasmine shell after dry is extracted and obtained through soxhlet extraction, and condition is solid-liquid ratio 5:1~15:1, the min of extraction time 45 ~ 60, extraction
60 ~ 80 DEG C of temperature, extraction time 2 ~ 4 times, Extraction solvent are the one or several kinds such as petroleum ether, ethyl acetate, ethanol.
The gardenia pollen added before soap lye enters mould of the cape jasmine whitening and skin-protecting type craft cold process soap of the present invention, it is to have newly
It is pollen that particle diameter is 200 ~ 300 mesh that fresh gardenia is crushed after drying in the shade naturally with pulverizer, sieving for standby.
The cape jasmine flower essential oil added before soap lye enters mould of the cape jasmine whitening and skin-protecting type craft cold process soap of the present invention, it is to utilize
Fresh gardenia utilizes Microwave Extraction, and condition is plus 5 ~ 10 times of water is measured, and the W of microwave power 100 ~ 300, extracts 0.5 ~ 1.5 h,
Then extracted with the one or more of petroleum ether, ether, ethyl acetate, then dry, concentrate, obtained light yellow with virtue
The cape jasmine flower essential oil of fragrance taste.
Also lemon, clove oil, jasmine essence can be separately added in the cape jasmine whitening and skin-protecting type craft cold process soap of the present invention
Oil, Rosa Damascana, Lavender are one or several kinds of.
The cape jasmine whitening and skin-protecting type craft cold process soap of the present invention carries out adding micro food coloring, dimension before soap lye enters mould
The one or several kinds of the additives such as raw plain E, pearl powder, long carbon dust.
Total free alkali of the cape jasmine whitening and skin-protecting type craft cold process soap of the present invention is 0.07 ~ 0.10%（In terms of NaOH）.
The free causticity alkali content of the cape jasmine whitening and skin-protecting type craft cold process soap of the present invention is 0.06 ~ 0.10%（With NaOH
Meter）.
The moisture and volatile matter of the cape jasmine whitening and skin-protecting type craft cold process soap of the present invention are 20 ~ 24%（Temperature is 60 DEG C ± 2 DEG C）.
The content of the chloride of the cape jasmine whitening and skin-protecting type craft cold process soap of the present invention is 0.5 ~ 0.9%（In terms of NaCl）.
The phosphatic content of the cape jasmine whitening and skin-protecting type craft cold process soap of the present invention is 0.005 ~ 0.009%（With P2O5
Meter）.
Experimental implementation of the present invention is easy, and Lipid use rate is high, and can be changed according to the hobby of oneself and the requirement to function
The species of the ratio of grease, essential oil and pigment.
Embodiment
Following examples are some citings of the present invention, should not be seen as limitation of the invention.
Embodiment 1
The g of coconut oil 20, the g of palm oil 10, the g of rice bran oil 15, plant white oil 15g, the g of wheat-germ oil 10 are weighed on balance,
The g of cocoa butter 15, the g of grape-kernel oil 20, the g of whitish honey wax 5, it is placed in 500 mL beaker；Weigh the g of NaOH 15.42, water 30.84
G is placed in 250 mL beaker.
The sodium hydroxide weighed up is slowly poured into water, while slowly stirred untill solution becomes clear, i.e., it is complete
Fully dissolved, stand, treat that its temperature is down to 45 DEG C, grease is placed in water-bath and heated, and with its temperature of thermometer measure, work as temperature
Degree takes out beaker when rising to 45 DEG C from water-bath.
Sodium hydroxide solution is slowly poured into grease, side edged quickly stirs, and under 45 DEG C of water-baths and continues stirring 0.5
H is until soap lye starts to become cape jasmine oil that is thick and then adding 10 mL, 10 mL cape jasmine shell extract, 10 g gardenia
Powder, 10 mL cape jasmine flower essential oil, 5 g Rhizoma Chuanxiong extracts, 5 g Angelica Dahurica extracts, it can be write after stirring on soap lye
And 20 ~ 30 s do not disappear i.e. stirring terminate, pour into immediately in mould, rest in 30 ~ 35 DEG C of incubators, be stripped after 2 ~ 5 days.
The cape jasmine added before soap lye enters mould the oil of cape jasmine whitening and skin-protecting type craft cold process soap, by fresh cape jasmine fruit through ultrasonic wave
Assisted extraction and obtain, condition is solid-liquid ratio 5:1, extraction time 30min, 30 DEG C of Extracting temperature, extraction time 2 times, Extraction solvent
For petroleum ether.
The cape jasmine shell extract added before soap lye enters mould of cape jasmine whitening and skin-protecting type craft cold process soap, by dried Cape jasmine
Sub- shell is extracted and obtained through soxhlet extraction, and condition is solid-liquid ratio 5:1, the min of extraction time 45,80 DEG C of Extracting temperature, extraction time
2 times, Extraction solvent is petroleum ether.
The gardenia pollen added before soap lye enters mould of cape jasmine whitening and skin-protecting type craft cold process soap, is to have fresh cape jasmine
It is pollen that particle diameter is 300 mesh to spend nature to be crushed after drying in the shade with pulverizer.
The cape jasmine flower essential oil added before soap lye enters mould of cape jasmine whitening and skin-protecting type craft cold process soap, it is to utilize fresh Cape jasmine
Son flower utilizes Microwave Extraction, and condition is plus 10 times of water is measured, and the W of microwave power 150, extracts 1 h, is then extracted with petroleum ether,
Then dry, concentrate, obtain the light yellow cape jasmine flower essential oil with aromatic odor.
Cape jasmine whitening and skin-protecting type craft cold process soap can also be separately added into 2 mL lemons, cloves essence before soap lye enters mould
Oil, refined jasmine oil, Rosa Damascana.
Cape jasmine whitening and skin-protecting type craft cold process soap can add micro food coloring, appropriate vitamin before soap lye enters mould
E, the additive such as pearl powder, long carbon dust.
INS values calculate
INS values are used for representing the hardness of soap.The ratio of soap base shared by the INS value * greases of grease=after the completion of soap hardness.INS
Value is lower, and the perfumed soap after the completion of representative is softer；On the contrary, INS values are higher, the perfumed soap after the completion of expression is harder.INS values between 125 ~
150 be all to belong to appropriate hardness.
The measure of total free alkali
Dissolve soap in ethanol solution, with known excessive concentration be 0.5 mol/L sulfuric acid solution in and free alkali, then
With the excessive acid of the potassium hydroxide-ethanol solution residual titration that concentration is 0.5 mol/L.Specific method refers to QB/T 2623.2-2003.
The measure of free causticity alkali content
Soap is dissolved in neutral alcohol, then titrates trip with the acidic alcohol standard titration solution that concentration is 0.5 mol/L
From caustic alkali.Specific method refers to QB/T 2623.1-2003.
The measure of moisture and volatile matter
At an established temperature, by a certain amount of sample drying to constant weight, weigh and reduce.Specific method refers to QB-T 2623.4-
2003。
The measure of chloride content
Decomposition experiment part and after being separated by filtration aliphatic acid, silver consuming amount method determines the content of chloride.Specific method refers to QB/T
2623.6-2003。
The measure of phosphate content
After sample is acidified, with petroleum ether extraction aliphatic acid not soluble in water, certain raffinate solution is taken to add ammonium molybdate-sulfuric acid molten
Liquid and ascorbic acid solution, 45min is heated in boiling water bath, Quadrafos is hydrolyzed into phosphate and generates P-Mo blue, with light splitting
Photometer determines absorbance A under wavelength 650nm, by the phosphorus pentoxide that corresponding absorbance is obtained on standard curve（P2O5）Amount,
Calculate the content of relative sample.Specific method refers to QB-T 2623.8-2003.
There is soap powder generation on the soap surface that this scheme is worked it out, partially firmly；Possible cause saponification is incomplete, and the few water of alkali is more.
Embodiment 2
The g of coconut oil 25, the g of palm oil 10, the g of rice bran oil 10, plant white oil 10g, the g of wheat-germ oil 10 are weighed on balance,
The g of cocoa butter 15, the g of grape-kernel oil 15, the g of whitish honey wax 5, it is placed in 500 mL beaker；Weigh the g of NaOH 14.41, water 28.82
G is placed in 250 mL beaker.
Operating process such as embodiment 1.
The soap body that this scheme is worked it out is softer, and there is soap powder on soap surface, and water outlet is fuel-displaced, occurs oil mark in maturation, easily by air
Oxidation.
Embodiment 3
Coconut oil 25g, the g of palm oil 15, the g of rice bran oil 10, plant white oil 10g, the g of wheat-germ oil 10 are weighed on balance, can
Can the g of fat 15, the g of grape-kernel oil 10, the g of whitish honey wax 5, be placed in 500 mL beaker；Weigh the g of NaOH 14.484, water 28.968
G is placed in 250 mL beaker.
Operating process such as embodiment 1.
There is soap powder on the soap surface that this scheme is worked it out, easily fuel-displaced, and possible cause stirring is insufficient, and soap body is harder.
Embodiment 4
The g of coconut oil 25, the g of palm oil 15, the g of rice bran oil 15, plant white oil 10g, the g of wheat-germ oil 10 are weighed on balance,
The g of cocoa butter 10, the g of grape-kernel oil 10, the g of whitish honey wax 5, it is placed in 500 mL beaker；Weigh the g of NaOH 14.438, water
28.876 g are placed in 250 mL beaker.
Operating process such as embodiment 1.
The soap hardness that this scheme is worked it out is moderate, the smooth no soap powder in surface.
The INS values of four kinds of embodiments, the determining of total free alkali, the measure of free causticity alkali content, moisture and volatile matter
It is as shown in table 2 below.
The index determining result of the experimental program of table 1
Claims (14)
1. a kind of preparation method of cape jasmine whitening and skin-protecting type craft cold process soap, its step are as follows：
The first step, weighs the g of coconut oil 20 ~ 100 on balance, palm oil 10 ~ 50 g, 15 ~ 65g of rice bran oil, and plant white oil 15 ~
75 g, the g of wheat-germ oil 10 ~ 50, the g of cocoa butter 15 ~ 75, the g of grape-kernel oil 20 ~ 100, the g of whitish honey wax 5 ~ 25 are placed in 1000 mL
Beaker in；Weigh the g of NaOH 15 ~ 75 respectively to be placed in 100 mL beaker, the g of water 30 ~ 150 is placed in 1000 mL beaker
In；
Second step, the sodium hydroxide weighed up is slowly poured into water, while slowly stirred untill solution becomes clear, i.e.,
It is completely dissolved, stands, treat that its temperature is down to 45 ~ 50 DEG C；
3rd step, grease is placed in water-bath and heated, and with its temperature of thermometer measure, the general when temperature rises to 40 ~ 50 DEG C
Beaker is taken out from water-bath；
4th step, the sodium hydroxide solution after cooling is slowly poured into grease, side edged quickly stirs, in 40 ~ 50 DEG C of water
Under the conditions of bath, continue the h of stirring 0.5 ~ 1.0；
5th step, stir to solution and start to become sticky, then add 5 ~ 25 mL cape jasmine oil, 5 ~ 25mL cape jasmine shell carries
Take thing, 5 ~ 25 g gardenia pollen, 5 ~ 25 mL cape jasmine flower essential oil, 5 ~ 25 g Rhizoma Chuanxiong extracts, 5 ~ 25 g roots of Dahurain angelica
Extract, can write after stirring on soap lye and 20 ~ 30 s do not disappear to stir and terminated, and pour into immediately in mould, quiet
Put in 30 ~ 35 DEG C of incubators, be stripped after 2 ~ 5 days；
6th step, it is placed at shady and cool ventilation and preserves, 25 ~ 35 DEG C of temperature, humidity is below 60, after 30 ~ 45 days, surveys its pH value 7 ~ 8
When it is ripe, can packed for standby use.
2. the preparation method of cape jasmine whitening and skin-protecting type craft cold process soap according to claim 1, it is characterised in that the first step
Rose extract is selected with wet concentration used in second step.
3. the preparation method of cape jasmine whitening and skin-protecting type craft cold process soap according to claim 1, it is characterised in that the first step
The appropriate INS values of middle grease are 125 ~ 150.
4. the preparation method of cape jasmine whitening and skin-protecting type craft cold process soap according to claim 1, it is characterised in that the 5th step
The cape jasmine oil added before soap lye enters mould, is extracted by fresh cape jasmine fruit and is obtained through ultrasonic assistant, condition is solid-liquid ratio 5:1~15:1,
The min of extraction time 30 ~ 60,30 ~ 50 DEG C of Extracting temperature, extraction time 2 ~ 5 times, Extraction solvent are petroleum ether, ethyl acetate, second
The one or several kinds such as alcohol.
5. the preparation method of cape jasmine whitening and skin-protecting type craft cold process soap according to claim 1, it is characterised in that the 5th step
The cape jasmine shell extract added before soap lye enters mould, extracted by dried cape jasmine shell and obtained through soxhlet extraction, condition is material
Liquor ratio 5:1~15:1, the min of extraction time 45 ~ 60,60 ~ 80 DEG C of Extracting temperature, extraction time 2 ~ 4 times, Extraction solvent is oil
The one or several kinds such as ether, ethyl acetate, ethanol.
6. the gardenia added before soap lye enters mould of cape jasmine whitening and skin-protecting type craft cold process soap according to claim 1
Powder, it is that to have fresh gardenia to be crushed after drying in the shade naturally with pulverizer be pollen that particle diameter is 200 ~ 300 mesh, sieving for standby.
7. the preparation method of cape jasmine whitening and skin-protecting type craft cold process soap according to claim 1, it is characterised in that the 5th step
The cape jasmine flower essential oil added before soap lye enters mould, it is to utilize Microwave Extraction using fresh gardenia, condition is to add 5 ~ 10 times of water
Amount, the W of microwave power 100 ~ 300,0.5 ~ 1.5h is extracted, then carried out with the one or more of petroleum ether, ether, ethyl acetate
Extraction, then dry, concentrate, obtain the light yellow cape jasmine flower essential oil with aromatic odor.
8. the preparation method of cape jasmine whitening and skin-protecting type craft cold process soap according to claim 1, it is characterised in that the 5th step
It is a kind of or several that lemon, clove oil, refined jasmine oil, Rosa Damascana, Lavender can be also added before soap lye enters mould
Kind.
9. the preparation method of cape jasmine whitening and skin-protecting type craft cold process soap according to claim 1, it is characterised in that the 5th step
Carry out adding a kind of or several of the additives such as micro food coloring, vitamin E, pearl powder, long carbon dust before soap lye enters mould
Kind.
10. the preparation method of cape jasmine whitening and skin-protecting type craft cold process soap according to claim 1, it is characterised in that the present invention
Cape jasmine whitening and skin-protecting type craft cold process soap total free alkali be 0.05 ~ 0.10%（In terms of NaOH）.
11. the preparation method of cape jasmine whitening and skin-protecting type craft cold process soap according to claim 1, it is characterised in that the present invention
Cape jasmine whitening and skin-protecting type craft cold process soap free causticity alkali content be 0.05 ~ 0.10%（In terms of NaOH）.
12. the preparation method of cape jasmine whitening and skin-protecting type craft cold process soap according to claim 1, it is characterised in that the present invention
Cape jasmine whitening and skin-protecting type craft cold process soap moisture and volatile matter be 21 ~ 24%（Temperature is 60 DEG C ± 2 DEG C）.
13. the content of the chloride of the cape jasmine whitening and skin-protecting type craft cold process soap of the present invention is 0.5 ~ 0.9%（In terms of NaCl）.
14. the phosphatic content of the cape jasmine whitening and skin-protecting type craft cold process soap of the present invention is 0.005 ~ 0.009%（With P2O5
Meter）.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710887142.8A CN107653107A (en) | 2017-09-27 | 2017-09-27 | A kind of preparation method of cape jasmine whitening and skin-protecting type craft cold process soap |
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| CN201710887142.8A CN107653107A (en) | 2017-09-27 | 2017-09-27 | A kind of preparation method of cape jasmine whitening and skin-protecting type craft cold process soap |
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| CN107653107A true CN107653107A (en) | 2018-02-02 |
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| CN201710887142.8A Pending CN107653107A (en) | 2017-09-27 | 2017-09-27 | A kind of preparation method of cape jasmine whitening and skin-protecting type craft cold process soap |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109998965A (en) * | 2019-05-28 | 2019-07-12 | 福建普民生物科技有限公司 | A kind of gardenia skin care moisture saver mask |
| JP7454355B2 (en) | 2018-12-27 | 2024-03-22 | ロート製薬株式会社 | DKK1 production promoter and method for producing the same, cosmetic composition for promoting DKK1 production and method for producing the same, and method for promoting DKK1 production |
-
2017
- 2017-09-27 CN CN201710887142.8A patent/CN107653107A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP7454355B2 (en) | 2018-12-27 | 2024-03-22 | ロート製薬株式会社 | DKK1 production promoter and method for producing the same, cosmetic composition for promoting DKK1 production and method for producing the same, and method for promoting DKK1 production |
| CN109998965A (en) * | 2019-05-28 | 2019-07-12 | 福建普民生物科技有限公司 | A kind of gardenia skin care moisture saver mask |
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Application publication date: 20180202 |