CN106635525A - Algae cold soap and preparation method thereof - Google Patents

Algae cold soap and preparation method thereof Download PDF

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Publication number
CN106635525A
CN106635525A CN201610861185.4A CN201610861185A CN106635525A CN 106635525 A CN106635525 A CN 106635525A CN 201610861185 A CN201610861185 A CN 201610861185A CN 106635525 A CN106635525 A CN 106635525A
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algae
oil
sargassum
herba apii
apii graveolentis
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CN106635525B (en
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付晓婷
刘楠楠
许加超
高昕
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Ocean University of China
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Ocean University of China
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/02Compositions of detergents based essentially on soap on alkali or ammonium soaps
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/005Antimicrobial preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/48Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22Organic compounds, e.g. vitamins
    • C11D9/24Hydrocarbons
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22Organic compounds, e.g. vitamins
    • C11D9/26Organic compounds, e.g. vitamins containing oxygen
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22Organic compounds, e.g. vitamins
    • C11D9/26Organic compounds, e.g. vitamins containing oxygen
    • C11D9/262Organic compounds, e.g. vitamins containing oxygen containing carbohydrates
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22Organic compounds, e.g. vitamins
    • C11D9/30Organic compounds, e.g. vitamins containing nitrogen
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22Organic compounds, e.g. vitamins
    • C11D9/38Products in which the composition is not well defined

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Dermatology (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Emergency Medicine (AREA)
  • Molecular Biology (AREA)
  • Gerontology & Geriatric Medicine (AREA)
  • Detergent Compositions (AREA)
  • Cosmetics (AREA)

Abstract

The invention relates to the field of daily cosmetics, particularly to an algae cold soap. The algae cold soap is composed of, by weight percentage, 5-20% of algae extracts and 1-10% of celery alcohol extracts. According to the algae cold soap, the macroalgae extracts and the celery alcohol extracts serve as major active ingredients and are matched with other active materials such as algal oil, squalane, nicotinamide and natural vitamin E oil to produce the algae cold soap at low temperatures. The algae cold soap has the advantages of being safe, mild, natural, non-stimulative and capable of achieving diminishing inflammation and achieving moisturizing; polysaccharides, phenols, proteins, vitamins and amino acids contained in the algae extracts as well as active nutrient ingredients contained in the celery alcohol extracts can be relatively completely reserved at low temperatures. Therefore, the algae cold soap is a safe and effective skin cleaning and cosmetic product and is applicable users of different genders and ages and with different skin types.

Description

A kind of Sargassum cold process soap and preparation method thereof
Technical field
The present invention relates to daily cosmetics FIELD OF THE INVENTIONThe, more particularly to a kind of Sargassum cold process soap and preparation method thereof.
Background technology
Manual cold process soap is a kind of soap of rising in recent years, its basic preparation principle be by Vegetable oil lipoprotein at low temperature with There is saponification in alkali, generate the natural glycerin and soap surfactant of high-load, add other auxiliary material systems .Presently commercially available industrial fancy soap mostly is hot soapmaking, quickly obtains finished product by lasting high temperature, with zest during making Greatly, alkalescence is strong, the pH value for destroying human body surface and the carbamide for retaining, uric acid, salinity, lactic acid, aminoacid, free fatty etc. Acidic materials, and the glycerol for producing is extracted, and adds a large amount of chemical agents again, makes product skin-care effect poor, to skin irritation Greatly.
With the development of society, people increasingly advocate healthy, natural, environmentally friendly Green Lifestyle, thus to fancy soap The requirement of the washing product of this kind of close contact itself body surface is more and more.The cold process soap of high-temperature heating is not needed, due to can be with Retain vegetable oil and the nutritional labeling in other additives to greatest extent, obtain the favor of people.
The making of cold process soap is mainly with pure natural cold pressing Vegetable oil lipoprotein as raw material, at low temperature with sodium hydroxide through stirring Mix, the process soapmaking base of saponification, further according to the different effect of product or meet the diversified demand of product, add it is various effectively into Point, then enter mould, shaping, the demoulding, ripening and make.The success of the marine biomaterials such as collagen protein, phenols, oligosaccharide All kinds of cosmetics are developed into, but the cold process soap containing seaweed extracted liquor still belongs to blank.And Flavonoid substances contain in Herba Apii graveolentis ethanol extract Amount is abundant, can treat various inflammation, be good antioxidant, have functions that calmness, calm the nerves, blood pressure lowering, coordinate seaweed extracted liquor Strengthen effect of cold process soap.
Shortcoming of the present invention for prior art, active substance of the addition containing seaweed extracted liquor and Herba Apii graveolentis ethanol extract, coordinates Other active substances such as algal oil, squalane, nicotiamide, vitamin E oil, sodium alginate, in making cold process soap, nutritional labeling is more It is comprehensive available, reach that whitening skin and preserving moisture, antiinflammatory be crease-resistant, the effect of gentle cleaning.
The content of the invention
The present invention rejects what is produced for the nutritional labeling destruction for existing using the hot soapmaking of continuous high temperature heating on the market Natural glycerin, and the problems such as a large amount of chemicals of addition, preservative, artificial essence, pigment, there is provided a kind of safety is gentle, has Antiinflammatory moisturizing, the cold process soap of natural no stimulation advantage.
The present invention with the ethanol extract of the extracting solution and Herba Apii graveolentis of tangleweed as main active, coordinate add algal oil, Other active substances such as squalane, nicotiamide and natural complex E oil, under cryogenic made by cold process soap.Can be low Temperature is lower than in polysaccharide, phenols, protein, vitamin, aminoacid and Herba Apii graveolentis ethanol extract in more completely preservation seaweed extracted liquor Flavone and natural pigment isoreactivity nutritional labeling, solve existing fancy soap and wash rear tight, and antiinflammatory moisture retention is poor, and zest is big, chemistry The problems such as preparation is more and functional component is few.Which has the advantages that moisturizing, whitening anti-wrinkling, gentle non-stimulated, is a kind of safety Effective skin clean and cosmetics, it is adaptable to the crowd of different sexes, age and skin quality.
The technical solution used in the present invention is as follows:A kind of Sargassum cold process soap, including following components in percentage by weight composition: Seaweed extracted liquor 5-20%, Herba Apii graveolentis ethanol extract 1-10%.
Further, the preparation method of above-mentioned seaweed extracted liquor includes following:
(1), after rinse well Sargassum, drying is crushed to obtain algae powder, 1g algaes powder is mixed homogeneously with the water of 10-100mL, protects Temperature is held at 20-60 DEG C, 6-48h is extracted under oscillating condition, described Sargassum refer to the one kind in Brown algae, red algae, chlorella or Several combinations;
(2) seaweed extracted liquor is obtained after 15min, then sucking filtration being centrifuged under the conditions of rotating speed 4000r/min.
Further, the preparation method of above-mentioned Herba Apii graveolentis ethanol extract:
Fresh Herba Apii graveolentis are cleaned into after bake dry grinding, adds by 1g powder the 70%-100% EtOH Sonicates of 20-100ml to carry After taking 0.5-3h, sucking filtration, concentrating under reduced pressure remove ethanol, obtain ethanol extract.
Further, present invention also offers a kind of preparation method of Sargassum cold process soap, comprises the following steps:
(1) by basic grease 60-80%, remaining oils and fats 0-10%, heat at 20-50 DEG C, be allowed to be completely dissolved, obtain A Phase, the basic grease refer to two or more in olive oil, Petiolus Trachycarpi oil, Oleum Cocois, Semen pruni armeniacae oil, Radix Oenotherae erythrosepalae oil Combination, described remaining oils and fats refer in Jojoba oil, Oleum sesami, natural complex E oil, American Avocado Tree oil, algal oil one or two Combination above;
(2) sodium hydroxide 2-20%, plus 2-20% deionized water dissolving are weighed, stirring condition is cooled to 20-50 DEG C, obtains B phases;
(3) squalane 0.1-5%, nicotiamide 0.1-5%, sodium alginate 0.1-5%, seaweed extracted liquor 5-20%, celery are claimed Dish ethanol extract 1-10% is dissolved in 1-20% deionized waters, in 20-50 DEG C of heating for dissolving, obtains C phases;
(4) above-mentioned ABC tri- is mixed, accelerates saponification with agitator high-speed stirred, it is extremely sticky after stirring 20-120min State, pours mould into;
(5) above-mentioned steps (4) demoulding after 1-5 days, be placed under shady and cool dry environment place treat within 10-50 days its completely into It is ripe, obtain product.
The cold process soap of present invention production contains seaweed extracted liquor and Herba Apii graveolentis ethanol extract, trehalose, polyphenol and Huang which contains Ketone isoreactivity component content enrich, with moisture-keeping crease-shedding, natural whiting, gently clean the features such as.The cold process soap of present invention production Containing natural antibacterial and natural pigment, chemical preservative and artificial color need not be added, it is nontoxic non-stimulated, it is a kind of safety Effective skin clean and cosmetics, it is adaptable to the crowd of different sexes, age and skin quality.The preparation side of cold process soap of the present invention Forensic science, process is simple, manufacturing process are pollution-free, environmental protection, are adapted to industrialized production.
Specific embodiment
The present invention obtains seaweed extracted liquor by the way of water extraction from the tangleweed of pure natural, and extraction cost is low, and Coordinate Herba Apii graveolentis ethanol extract, with its abundant flavone active component, the present invention is there is cleaning reparation, whitening skin and preserving moisture, crease-resistant is disappeared Inflammation and other effects.Furthermore, containing natural antibacterial in Sargassum zymolyte, antibacterial effect is good, need not add chemical preservative.More Further, artificial color need not be added, it is ensured that product containing abundant natural pigment in the Herba Apii graveolentis ethanol extract in the present invention It is nontoxic non-stimulated, it is adaptable to the crowd of different sexes, age and skin quality, cost performance are high, environmental protection.
The present invention is described in further detail below by way of concrete preferred embodiment, but the present invention be not limited in it is following Embodiment.
Embodiment 1:
1.1 constitute composition and its percentage by weight of the present invention containing seaweed extracted liquor and the cold process soap of Herba Apii graveolentis ethanol extract is:
A phases:It is olive oil 12%, Petiolus Trachycarpi oil 18%, Oleum Cocois 18%, Semen pruni armeniacae oil 12%, Jojoba oil 1.5%, natural Vitamin E oil 1.5%, algal oil 0.5%;
B phases:Sodium hydroxide 5%, deionized water 10%;
C phases:Squalane 2%, nicotiamide 0.5%, sodium alginate 1%, seaweed extracted liquor 8%, Herba Apii graveolentis ethanol extract 2%, go Ionized water 8%;
1.2 technical process:
The preparation method of above-mentioned seaweed extracted liquor:After Sargassum fusiforme (Harv.) Setch is rinsed well, drying crushes to obtain algae powder, by 1g algaes Powder is mixed homogeneously with the water of 100mL, maintains the temperature at 60 DEG C, extracts 10 hours under oscillating condition.Then, after taking-up 15min is centrifuged under the conditions of 4000r/min, Sargassum fusiforme (Harv.) Setch extracting solution after sucking filtration, is obtained.
The preparation method of above-mentioned Herba Apii graveolentis ethanol extract:Fresh Herba Apii graveolentis are cleaned into after bake dry grinding, adds 20ml by 1g dry powder 70% ethanol ultrasonic extraction 1h after, then sucking filtration, concentrating under reduced pressure remove ethanol after obtain ethanol extract.
At 20 DEG C, will mix after above-mentioned tri- phased solns of ABC, accelerate saponification with agitator high-speed stirred, stir 30min To viscous pasty state, mould is poured into.The demoulding after 1 day, is put into placement after ripening in 10 days under shady and cool dry environment, obtains carrying containing Sargassum Take the cold process soap of liquid and Herba Apii graveolentis ethanol extract.
Embodiment 2:
2.1. constituting composition and its percentage by weight of the present invention containing seaweed extracted liquor and the cold process soap of Herba Apii graveolentis ethanol extract is:
A phases:Olive oil 30%, Radix Oenotherae erythrosepalae oil 18%, Semen pruni armeniacae oil 18%;
B phases:Sodium hydroxide 4%, deionized water 10%;
C phases:Squalane 1%, nicotiamide 1%, sodium alginate 2%, seaweed extracted liquor 10%, Herba Apii graveolentis ethanol extract 3%, go from Sub- water 3%;
2.2. technical process:
The preparation method of the seaweed extracted liquor:After Yi Guzao is rinsed well, drying crushes to obtain algae powder, by 1g algae powder Mix homogeneously with the water of 50mL, maintain the temperature at 20 DEG C, extract 24 hours under oscillating condition.In 4000r/min bars after taking-up 15min is centrifuged under part, Yi Gu algae extracting solution after sucking filtration, is obtained.
The preparation method of Herba Apii graveolentis ethanol extract:Fresh Herba Apii graveolentis are cleaned into after bake dry grinding, adds the 80% of 100ml by 1g dry powder After ethanol ultrasonic extraction 3h, then ethanol extract is obtained after sucking filtration, concentrating under reduced pressure remove ethanol.
At 30 DEG C, will mix after above-mentioned tri- phased solns of ABC, accelerate saponification with agitator high-speed stirred, stir 60min To viscous pasty state, mould is poured into.The demoulding after 3 days, is put into placement after ripening in 20 days under shady and cool dry environment, obtains carrying containing Sargassum Take the cold process soap of liquid and Herba Apii graveolentis ethanol extract.
Embodiment 3:
3.1. constituting composition and its percentage by weight of the present invention containing seaweed extracted liquor and the cold process soap of Herba Apii graveolentis ethanol extract is:
A phases:Olive oil 32%, Semen pruni armeniacae oil 30%, Jojoba oil 1%, Oleum sesami 1%, natural complex E oil 1%, crocodile Pear oil 1%, algal oil 1%;
B phases:Sodium hydroxide 5.5%, deionized water 7.5%;
C phases:Squalane 1%, nicotiamide 1%, sodium alginate 1%, seaweed extracted liquor 4%, Herba Apii graveolentis ethanol extract 10%, go from Sub- water 3%;
3.2. technical process:
The preparation method of the seaweed extracted liquor:After sea grape is rinsed well, drying crushes to obtain algae powder, by 1g algae powder Mix homogeneously with the water of 10mL, maintain the temperature at 30 DEG C, extract 24 hours under oscillating condition.In 4000r/min conditions after taking-up Lower centrifugation 15min, obtains sea grape extracting solution after sucking filtration.
The preparation method of Herba Apii graveolentis ethanol extract:Fresh Herba Apii graveolentis are cleaned into after bake dry grinding, adds the 90% of 50ml by 1g dry powder After ethanol ultrasonic extraction 0.5h, then ethanol extract is obtained after sucking filtration, concentrating under reduced pressure remove ethanol.
At 50 DEG C, will mix after above-mentioned tri- phased solns of ABC, accelerate saponification, stirring with agitator high-speed stirred 120min pours mould into viscous pasty state.The demoulding after 5 days, is put into placement after ripening in 30 days under shady and cool dry environment, is contained The cold process soap of seaweed extracted liquor and Herba Apii graveolentis ethanol extract.
Embodiment 4
Experimental evaluation is carried out to above-described embodiment
The activity rating of 4.1 seaweed extracted liquors:Reference《The chemical composition and its biological activity assay of Scytosiphon lomentarius (Lyngh.)J. Ag.》In to cheese ammonia Sour enzyme inhibition, the detection method of the ability and moisture absorption and performance of keeping humidity for removing DPPH, hydroxy radical and superoxide anion are entered Row detection.
The activity rating of 4.2 Herba Apii graveolentis ethanol extract:Reference《Herba Apii graveolentis different parts determination of total flavonoids and its antioxidation are lived Property》In the antioxidant activity of ethanol extract is detected to the assay method of hydroxy radical and ultra-oxygen anion free radical.
4.3 using effects are tested:The product that will be prepared, is respectively issued to 10 tester's contrasts and uses.Tester makes Cleaned during with sample in the same manner, every kind of sample is respectively used 2 weeks.Tester according to oneself feel commented Point.Standards of grading take ten point system, and 1 point worst, and 10 points best, and fraction more high effect is better.
4.4 foaming powers and foam stability test:With reference to《The preparation and its performance study of gentle foam facial milk cleanser》In Experimental technique, is slightly improved, and adopts preparation weight/mass percentage composition for 10% each product solution 3mL, is put in graduated cylinder, plus distillation Water is diluted to 15mL, after mixing, takes out the scale test tube that 5ml samples add 25ml, acutely concussion 10 times, immediate record after adding a cover Foam volume (mL), records foam volume again after 10min.Replication 3 times, averages.
4.5 organoleptic indicator:According to《QB/T 2485-2008 fancy soaps》Soap body outward appearance and abnormal smells from the patient method of testing test.
4.6 experimental result
4.6.1 the Activity evaluation of Sargassum extract:
4.6.2 the antioxidant activity evaluation result of Herba Apii graveolentis ethanol extract:
4.6.3 using effect evaluation
4.6.4 foaming power and foam stability test:
4.6.5 organoleptic indicator:
Shown by above-mentioned test result, the present invention addition seaweed extracted liquor and Herba Apii graveolentis ethanol extract cold process soap have it is good Good organoleptic attribute, meets national standard, and using effect is good, with multi-efficiencies such as moisture-keeping crease-shedding, natural whiting, gentle cleanings.
The preferred embodiment of the present invention described in detail above, but, the present invention is not limited in above-mentioned embodiment Detail, the present invention range of the technology design in, various simple variants can be carried out to technical scheme, this A little simple variants belong to protection scope of the present invention.
Additionally, combination in any between a variety of embodiments of the present invention, can also be carried out, as long as which is without prejudice to this The thought of invention, which should equally be considered as content disclosed in this invention.

Claims (4)

1. a kind of Sargassum cold process soap, it is characterised in that:Constitute including following components in percentage by weight:Seaweed extracted liquor 5- 20%th, Herba Apii graveolentis ethanol extract 1-10%.
2. a kind of Sargassum cold process soap according to claim 1, it is characterised in that:The preparation method of seaweed extracted liquor include with Under:
(1), after rinse well Sargassum, drying is crushed to obtain algae powder, 1g algaes powder is mixed homogeneously with the water of 10-100mL, keeps temperature Degree extracts 6-48h under oscillating condition at 20-60 DEG C, and described Sargassum refers to one or more in Brown algae, red algae, chlorella Combination;
(2) seaweed extracted liquor is obtained after 15min, then sucking filtration being centrifuged under the conditions of rotating speed 4000r/min.
3. a kind of Sargassum cold process soap according to claim 2, it is characterised in that:The preparation method of the Herba Apii graveolentis ethanol extract:
Fresh Herba Apii graveolentis are cleaned into after bake dry grinding, the 70%-100% ethanol ultrasonic extraction of 20-100ml are added by 1g powder After 0.5-3h, sucking filtration, concentrating under reduced pressure remove ethanol, obtain ethanol extract.
4. the preparation method of a kind of Sargassum cold process soap according to claims 1 to 3, it is characterised in that:Comprise the following steps:
(1) by basic grease 60-80%, remaining oils and fats 0-10%, heat at 20-50 DEG C, be allowed to be completely dissolved, obtain A phases, institute Two or more the combination during basic grease refers to olive oil, Petiolus Trachycarpi oil, Oleum Cocois, Semen pruni armeniacae oil, Radix Oenotherae erythrosepalae oil is stated, Described remaining oils and fats refer in Jojoba oil, Oleum sesami, natural complex E oil, American Avocado Tree oil, algal oil one or more Combination;
(2) sodium hydroxide 2-20%, plus the deionized water dissolving of 2-20% are weighed, stirring condition is cooled to 20-50 DEG C, obtains B Phase;
(3) squalane 0.1-5%, nicotiamide 0.1-5%, sodium alginate 0.1-5%, seaweed extracted liquor 5-20%, Herba Apii graveolentis alcohol are claimed Extract 1-10% is dissolved in 1-20% deionized waters, in 20-50 DEG C of heating for dissolving, obtains C phases;
(4) above-mentioned ABC tri- is mixed, accelerates saponification with agitator high-speed stirred, it is extremely thick after stirring 20-120min State, pours mould into;
(5) above-mentioned steps (4) demoulding after 1-5 days, is placed into place under shady and cool dry environment and treats within 10-50 days its full maturity, obtain To product.
CN201610861185.4A 2016-09-29 2016-09-29 A kind of seaweed cold process soap and preparation method thereof Active CN106635525B (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108977290A (en) * 2017-06-01 2018-12-11 薛建萍 A kind of handmade soap of niacinamide-containing and preparation method thereof

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