CN106085659A - A kind of high skin-moisturizing, skin handmade soap and preparation method thereof - Google Patents
A kind of high skin-moisturizing, skin handmade soap and preparation method thereof Download PDFInfo
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- CN106085659A CN106085659A CN201610395155.9A CN201610395155A CN106085659A CN 106085659 A CN106085659 A CN 106085659A CN 201610395155 A CN201610395155 A CN 201610395155A CN 106085659 A CN106085659 A CN 106085659A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/06—Inorganic compounds
- C11D9/08—Water-soluble compounds
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/44—Perfumes; Colouring materials; Brightening agents ; Bleaching agents
- C11D9/442—Perfumes
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- General Health & Medical Sciences (AREA)
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- Veterinary Medicine (AREA)
- Detergent Compositions (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a kind of high skin-moisturizing, skin handmade soap and preparation method thereof, belonging to handmade soap technical field, it is made up of the raw material of following weight parts: by fresh dendrobium extract 3～12 parts, camellia oil 150～250 parts, palm oil 15～65 parts, coconut oil 35～85 parts, 25～55 parts of NaOH, pure water 80～125 parts and plants essential oil or 0.3～6 part of essence；Its technique includes that (1) gets the raw materials ready；(2) preparation of alkali lye；(3) mix oil plant and heat；(4) saponification；(5) mold forming is entered；(6) demoulding and the soap that dries in the air；(7) packaging preserves；It is desirable to provide a kind of, preparation method is simple, product is neither too hard, nor too soft, gentle and respond well high skin-moisturizing, skin handmade soap and preparation method thereof of filling a prescription；Preparation for handmade soap.
Description
Technical field
The present invention relates to a kind of handmade soap, more specifically, particularly relate to a kind of high skin-moisturizing, skin handmade soap.The present invention is same
When further relate to the preparation method of this handmade soap.
Background technology
Soap and perfumed soap are washing important in people's daily life and cleaning supplies.Commercially available perfumed soap great majority are hot method machines
Soapmaking, because continuous high temperature makes the destroyed loss of the natural active matter in base oil in production process.For improving perfumed soap performance
Or attract the sense of taste of client and vision, can be artificial in soap base, add some chemical substances, such as pigment, essence etc..Hand
Work soap has another name called manual cold process soap, is a kind of ancient low temperature soap manufacturing process coming from Europe, during low-temperature saponification, contained in base oil
Natural active matter will not be destroyed, glycerine is also intactly saved in soap body.Glycerine is natural moisturizing agent.Therefore
Handmade soap is in use than mechanism soap moisturizing, moisturizing and skin care.And perfumed soap is the easily-consumed products in daily life, consumption is big.At note
Heavily health care, emphasizes natural, healthy, organic and environmental protection today, uses colory crude vegetal, and in soap body
The material to skin beneficiating for the interpolation makes handmade soap and necessarily has the wide market space.
Camellia oil has another name called tea-seed oil, is the squeezing of tea seed the vegetable oil obtaining through the process of concise winterization in Property of Tea oil Tree Fruit.Mountain
Aliphatic acid composition in tea oil is extremely similar to olive oil, and contained unrighted acid is up to more than 90%, wherein single insatiable hunger
Exceed 80% with the content of aliphatic acid, possibly together with Tea Polyphenols, Tea Saponin, vitamin E, vitamin D, vitamin K and squalene
Deng the active material to skin beneficiating.Unrighted acid major part in camellia oil is oleic acid and linoleic acid, and oleic acid is easily by skin
Skin absorbs, to skin Yellow Gentian Extract；Tea Saponin has certain bactericidal effect；The Wheat Protein such as Tea Polyphenols, vitamin E.
Making base oil low temperature process with the concise camellia oil of winterization and preparing handmade soap, the major part remaining in camellia oil because of low temperature preparation has
The active material of benefit, also also retains the glycerine that saponification generates simultaneously.Remove with the handmade soap that camellia oil makes and there is cleaning
Outside skin effect, also there is the effects such as deep moisturizing, nourishes rough skin and sterilization.But, with camellia oil as main foundation oil
Handmade soap, during use, soap body is partially soft, uses the time short, and performance of keeping humidity is inadequate.
The stem of noble dendrobium, formal name used at school: Dendrobium nobile Lindl, is famous rare Chinese medicine.Monocot genus plant guiding principle Tianmen
Winter mesh the orchid family Dendrobium, is epiphyte.China there are about 76 kinds, is distributed in the ground such as southwest, south China and Taiwan.The stem of noble dendrobium has enriching yin clear
Effect and the effects such as heat, moistening lung nourishing the stomach, strengthening the muscles and bones." China's pharmacy dictionary " claims it " to be good at nourishing Yin and promoting production of body fluid ", " enriching yin is raw
Blood ".The stem of noble dendrobium is containing the dendrobine such as dendrobine, dendramine, the stem of noble dendrobium time alkali, dendroxine, dendrine, 6-hydroxydendroxine and enriches
Dendrobium polysaccharide.Skim the cream off milk from the fresh stem of noble dendrobium liquid, as the adding ingredient of handmade soap, because it contains abundant dendrobine and stone
Dry measure used in former times polysaccharide, can quick skin care, improve skin quality, keratinization skin can be repaired in time, be effectively improved scaly dry skin, lack of water, tight
Stretch tight.
Content of the invention
The previous purpose of the present invention is for above-mentioned the deficiencies in the prior art, provides a kind of neither too hard, nor too soft, formula gentleness
And respond well high skin-moisturizing, skin handmade soap.
The latter purpose of the present invention is to provide a kind of preparation method simply to prepare above-mentioned high skin-moisturizing, skin handmade soap
Method.
The previous technical scheme of the present invention is achieved in that a kind of high skin-moisturizing, skin handmade soap, and it is by following weight
Part raw material make: by fresh dendrobium extract 3～12 parts, camellia oil 150～250 parts, palm oil 15～65 parts, coconut oil 35～
85 parts, 25～55 parts of NaOH, pure water 80～125 parts and plants essential oil or 0.3～6 part of essence.
In above-mentioned one high skin-moisturizing, skin handmade soap, it is that the raw material of following weight parts is made: by fresh dendrobium extract 5
～10 parts, camellia oil 160～220 parts, palm oil 20～60 parts, coconut oil 40～80 parts, 30～50 parts of NaOH, pure water
85～120 parts and plants essential oil or 0.5～5 part of essence.
In above-mentioned one high skin-moisturizing, skin handmade soap, described plants essential oil is wormwood essential oil, Rosa Damascana, sweet osmanthus essence
Any one in oil, Rosemary Oil or Lavender.
The latter technique scheme of the present invention is achieved in that a kind of method preparing high skin-moisturizing, skin handmade soap, the party
Method comprises the steps:
(1) get the raw materials ready: weigh each material by formula ratio, standby；
(2) preparation of alkali lye: add water NaOH, stirring, to being completely dissolved, forms alkali lye, standby；
(3) mix oil plant and heat: camellia oil, palm oil and coconut oil are mixed formation miscella, then will be mixed
Close oil and be heated to same or like with alkali liquid temperature, standby；
(4) saponification: add alkali lye in miscella and stir, carrying out saponification and obtain saponification liquor, then proceed to stir to
It when saponification liquor thickens, is sequentially added into fresh dendrobium extract and plants essential oil or essence, continue stirring saponification liquor and reach viscous
Thick shape；
(5) enter mold forming: soap lye is poured in silica gel mould, rap up and down after entering mould and drive bubble away, then 30～35
Place 20～36h under DEG C environment, complete the shaping of handmade soap；
(6) handmade soap is taken out together with mould and carries out the demoulding, after the demoulding dries in the air handmade soap by the demoulding and the soap that dries in the air: after 20～36h
Dry, the soap time of drying in the air is 25～35d；
(7) packaging preserves: after handmade soap dries, and with preservative film parcel, deposits in the place that shady and cool ventilation is dried.
In the method for above-mentioned a kind of high skin-moisturizing, skin handmade soap, step (2) is particularly as follows: the preparation of alkali lye: by hydroxide
Sodium is slowly added in pure water in three times, and limit edged is gently mixed to being completely dissolved, and forms alkali lye, treats that alkali lye is cooled to 45 DEG C
When, it is placed in constant temperature in the water-bath of 40～45 DEG C and deposit, standby；
In the method for above-mentioned a kind of high skin-moisturizing, skin handmade soap, step (4) is particularly as follows: check miscella and alkali liquid temperature
When close, miscella is continuously stirred, and add alkali lye to miscella in three times, it is stirred until homogeneous after adding every time and add again
Next group, until all adding；Alkali lye mix with miscella whole during all keep continuously stirred, mixing speed is
150-250rpm；After 20min, suspend stirring 5min, observe the color of oil simultaneously and check temperature, then proceed to stirring, slowly
Regulation mixing speed, to 1000rpm continuously stirred, when soap lye density starts to thicken, is sequentially added into fresh dendrobium extract
With plants essential oil or essence, continue stirring soap lye and reach thick.
In the method for above-mentioned a kind of high skin-moisturizing, skin handmade soap, it is characterised in that in step (4), the described fresh stem of noble dendrobium carries
Take the preparation technology of liquid particularly as follows: with pure water by fresh stem of noble dendrobium washes clean, drain surface moisture, be cut into 0.8-1.5cm
Segment length, adds the pure water of 10 times of quality, with electric squeezer, stirs into muddy, constant temperature oscillation extraction under 25 DEG C of environment
24 hours；Suction filtration, is concentrated in vacuo to half volume and obtains concentrate, standby.
In the method for above-mentioned a kind of high skin-moisturizing, skin handmade soap, step (6) is particularly as follows: after 20～36h, connect handmade soap
Take out with mould, check between soap and mould, whether there is space, whether the soft durometer of soap is moderate determines demoulding opportunity；If soap body
Cross and bond between soft, overly moist or soap dye, the demoulding again after a period of time can be placed again；After the demoulding, soap is placed on cool place, drying, ventilation
Natural air drying, the soap time of drying in the air is 25～35d；Dry in the air during soap, detect pH value and hard with LX-C type hardness tester meter detection soap body every day
Degree, when pH value is not less than 60HW less than the 8th, hardness, soap is ripe, it is possible to use or packaging preservation.
After the present invention uses such scheme, compared with prior art, there is following advantage:
(1) handmade soap accounts for 70%～80% for main with oil with the natural camellia seed oil of low melting point, remainings and 20%～30% is
Dystectic other plant oil, such as palm oil etc..The handmade soap hardness made by the various feedstock oils of rational proportion is moderate, makes
With conveniently.
(2) prepared by low temperature, and the natural active matter in camellia oil, the fresh stem of noble dendrobium is retained, and can be absorbed by the skin, can be quick
Skin care, exfoliating improves skin quality.Glycerine after camellia oil saponification is retained in handmade soap, the abundant stem of noble dendrobium in the fresh stem of noble dendrobium
Polysaccharide, forms one layer of natural moisture film on skin, has comparison high skin under glycerine and dendrobium polysaccharide double action
Moisturizing effect.The present invention, with the material of natural origin as key component, does not contains preservative, synthetic surfactant, not only
Can be with cleaning skin, can be gentle to skin with skin care, experience nourishing, the soft effect that natural material brings to skin.
(3) dendrobine and dendrobium polysaccharide, the quick skin care of energy, improves skin quality, can repair keratinization skin in time, effectively
Improve scaly dry skin, lack of water, tight etc..Dendrobine in the stem of noble dendrobium participates in saponification, can reduce the consumption of NaOH, be to meet
The mild of environmental requirement, the green product of naturalization.
(4) production process equipment needed thereby of the present invention is simple, and production site is little, and method is also simple and practical, easily operates.Throw
Enter few, be suitable for miniaturization or family production.Have stronger practicality and higher economic benefit.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is described in further detail, but be not intended that to the present invention any
Limit.
The one high skin-moisturizing, skin handmade soap of the present invention, it is made up of the raw material of following weight parts: extracted by the fresh stem of noble dendrobium
Liquid 3～12 parts, camellia oil 150～250 parts, palm oil 15～65 parts, coconut oil 35～85 parts, 25～55 parts of NaOH, pure
Water purification 80～125 parts and plants essential oil or 0.3～6 part of essence.Above-mentioned formula, it is preferable that be that the raw material of following weight parts is made:
By fresh dendrobium extract 5～10 parts, camellia oil 160～220 parts, palm oil 20～60 parts, coconut oil 40～80 parts, NaOH
30～50 parts, pure water 85～120 parts and plants essential oil or 0.5～5 part of essence.
Camellia oil is cosmetic rank camellia oil.To squeeze crude oil, impurity is removed by filtration, alkali is practiced and depickling degumming, decolouring
Deodorization, drying winterization processes the cosmetics-stage camellia oil that acid number is low, peroxide value is little obtaining.
In above-mentioned formula, described plants essential oil is wormwood essential oil, Rosa Damascana, osmanthus essential oil, Rosemary Oil or smokes
Clothing grass essential oil in any one.
A kind of method preparing high skin-moisturizing, skin handmade soap of the present invention, the method comprises the steps:
(1) get the raw materials ready: weigh each material by formula ratio, standby；
(2) preparation of alkali lye: be slowly added into NaOH in pure water in three times, limit edged is gently mixed to completely
Dissolve, form alkali lye, when alkali lye is cooled to 45 DEG C, is placed in constant temperature in the water-bath of 40～45 DEG C and deposits, standby；
(3) mix oil plant and heat: camellia oil, palm oil and coconut oil are mixed, existing with increasing electric blender
Stir under the rotating speed of 200-250rpm formation miscella, is then heated to miscella same or like with alkali liquid temperature,
Standby；
(4) saponification: when checking that miscella and alkali liquid temperature are close, miscella is continuously stirred, and in three times alkali lye is added
Enter to miscella, be stirred until homogeneous after adding every time and add next group again, until all adding；Mix with miscella at alkali lye
All keeping continuously stirred during Zheng Ge, mixing speed is 150-250rpm；After 20min, suspend stirring 5min, observe oil simultaneously
Color and check temperature, then proceed to stirring, slowly regulation mixing speed is simultaneously continuously stirred to 1000rpm, slowly regulates, i.e.
Gather way until 1000rpm with the speed of 100-200r/s；It when soap lye density starts to thicken, is sequentially added into the fresh stem of noble dendrobium
Extract and plants essential oil or essence, continue stirring soap lye and reach thick.
The preparation technology of described fresh dendrobium extract is particularly as follows: with pure water by fresh stem of noble dendrobium washes clean, drain table
Face moisture, is cut into 0.8-1.5cm segment length, adds the pure water of 10 times of quality, with electric squeezer, stirs into muddy, 25
Under DEG C environment, constant temperature oscillation extracts 24 hours；Suction filtration, is concentrated in vacuo to half volume and obtains concentrate, standby.
(5) enter mold forming: soap lye is poured in silica gel mould, rap up and down after entering mould and drive bubble away, then mould is put down
Put into foamed plastics incubator, outside case, cover one layer of woollen blanket insulation 20～36h；If it is cold, foamed plastics can be incubated
Case is placed in water proof insulating box, keeps temperature 30～35 DEG C, is incubated 20～36h, completes the shaping of handmade soap；
(6) handmade soap is taken out by the demoulding and the soap that dries in the air: after 20～36h together with mould, checks whether have time between soap and mould
Gap, the soft durometer of soap whether moderate determine demoulding opportunity；If soap body is excessively soft, bonding between overly moist or soap dye, one can be placed again
The demoulding again after the section time；Soap is placed on after the demoulding cool place, drying, ventilation natural air drying, and the soap time of drying in the air is 25～35d；Dry in the air soap
During, detect pH value every day and detect soap body hardness with LX-C type hardness tester meter, when pH value is not less than 60HW less than the 8th, hardness, soap
Ripe, it is possible to use or packaging preservation；
(7) packaging preserves: after handmade soap is ripe, modifies soap body surface and surrounding corner with electrician's knife, makes good looking appearance.With
Preservative film wraps up, and film and soap are close to do not have space, are then deposited in the place that shady and cool ventilation is dried.
Embodiment 1
1st, fill a prescription: fresh dendrobium extract 5g, camellia oil 160g, palm oil 20g, coconut oil 40g, NaOH 30g, pure
Water 85g, plants essential oil or essence 0.5g.
2nd, making step:
(1) each material quality number is weighed out with electronic balance (precision 0.01g).
(2) pure water 85g in 500mL beaker, 30g NaOH is slowly added in three times, and limit edged is gently mixed to complete
CL obtains alkali lye.It when being cooled to 45 DEG C, is placed in constant temperature in 40～45 DEG C of water-baths.
(3) 160g camellia oil, 20g palm oil, 40g coconut oil are mixed in the stainless steel cup of 1000mL, with reinforcement electricity
Dynamic mixer stirring, rotating speed 200rpm, stirring is subsequently placed in water-bath and is heated to same or like with alkali liquid temperature.
(4) when checking that miscella and alkali liquid temperature are close, miscella is continuously stirred, and in three times alkali lye is added extremely mixed
Close in oil, be stirred until homogeneous after adding every time and add next group again, until all adding；The whole mistake mixing with miscella at alkali lye
All keeping continuously stirred in journey, mixing speed is 150rpm；After 20min, suspend stirring 5min, observe the color of oil simultaneously and examine
Looking into temperature, then proceeding to stirring, slow regulation mixing speed to 1000rpm is simultaneously continuously stirred；Start to thicken at soap lye density
It when thick, is sequentially added into the fresh dendrobium extract of 5g and 0.5g plants essential oil or essence, continue stirring soap lye and reach thick.
(5) soap lye is poured in six silica gel moulds connecting square moulding, rap up and down after entering mould and drive bubble away.Mould is put down
Put into foamed plastics incubator, outside case, cover one layer of woollen blanket insulation 20h.If it is cold, foamed plastics incubator can be put
In water proof insulating box, keep temperature 35 DEG C, 20h.
(6), after being incubated 20h, soap gang mould is taken out from foamed plastics incubator.Reach to carry out the demoulding during demoulding requirement.The demoulding
After soap is placed on cool place, drying, ventilation natural air drying, the soap time of drying in the air is 25～35d.Dry in the air during soap, detect every day pH value,
Measurement soap body quality and observation soap body hardness.PH value is harder less than the 8th, hardness, soap body constant weight when, soap is maturation.
(7), after handmade soap is ripe, modifies soap body surface and surrounding corner with electrician's knife, make good looking appearance.Every piece of finished product is about
70g.With preservative film parcel, film and soap are close to do not have space.Deposit shady and cool ventilation and be dried local preservation.
By total free alkali of the handmade soap to preparation for the national standard (QB/T2485 2008 perfumed soap quality standard), free severe
Property alkali, moisture content and volatile matter, total chloride content detect, and indices all meets national standard.
Table 1 handmade soap Quality Detection result
Embodiment 2
1st, fill a prescription: fresh dendrobium extract 10g, camellia oil 220g, palm oil 60g, coconut oil 80g, NaOH 50g, pure
Water purification 120g, plants essential oil or essence 5g.
2nd, making step:
(1) each material quality number is weighed out with electronic balance (precision 0.01g).
(2) pure water 120g in 500mL beaker, 50g NaOH is slowly added in three times, and limit edged is gently mixed to complete
CL obtains alkali lye.It when being cooled to 45 DEG C, is placed in constant temperature in 40～45 DEG C of water-baths.
(3) 220g camellia oil, 60g palm oil, 80g coconut oil are mixed in the stainless steel cup of 1000mL, with reinforcement electricity
Dynamic mixer stirring, rotating speed 250rpm, stirring is subsequently placed in water-bath and is heated to same or like with alkali liquid temperature.
(4) when checking that miscella and alkali liquid temperature are close, miscella is continuously stirred, and in three times alkali lye is added extremely mixed
Close in oil, be stirred until homogeneous after adding every time and add next group again, until all adding；The whole mistake mixing with miscella at alkali lye
All keeping continuously stirred in journey, mixing speed is 250rpm；After 20min, suspend stirring 5min, observe the color of oil simultaneously and examine
Looking into temperature, then proceeding to stirring, slow regulation mixing speed to 1000rpm is simultaneously continuously stirred；Start to thicken at soap lye density
It when thick, is sequentially added into the fresh dendrobium extract of 10g and 5g plants essential oil or essence, continue stirring soap lye and reach thick.
(5) soap lye is poured in six silica gel moulds connecting square moulding, rap up and down after entering mould and drive bubble away.Mould is put down
Put into foamed plastics incubator, outside case, cover one layer of woollen blanket insulation 36h.If it is cold, foamed plastics incubator can be put
In water proof insulating box, keep temperature 30 DEG C, 36h.
(6), after being incubated 36h, soap gang mould is taken out from foamed plastics incubator.Reach to carry out the demoulding during demoulding requirement.The demoulding
After soap is placed on cool place, drying, ventilation natural air drying, the soap time of drying in the air is 25～35d.Dry in the air during soap, detect every day pH value,
Measurement soap body quality and observation soap body hardness.PH value is harder less than the 8th, hardness, soap body constant weight when, soap is maturation.
(7), after handmade soap is ripe, modifies soap body surface and surrounding corner with electrician's knife, make good looking appearance.Every piece of finished product is about
70g.With preservative film parcel, film and soap are close to do not have space.Deposit shady and cool ventilation and be dried local preservation.
By total free alkali of the handmade soap to preparation for the national standard (QB/T2485 2008 perfumed soap quality standard), free severe
Property alkali, moisture content and volatile matter, total chloride content detect, and indices all meets national standard.
Table 2 handmade soap Quality Detection result
Embodiment 3
1st, fill a prescription: fresh dendrobium extract 3g, camellia oil 150g, palm oil 15g, coconut oil 35g, NaOH 25g, pure
Water 80g, plants essential oil or essence 0.3g.
2nd, making step:
(1) each material quality number is weighed out with electronic balance (precision 0.01g).
(2) pure water 80g in 500mL beaker, 25g NaOH is slowly added in three times, and limit edged is gently mixed to complete
CL obtains alkali lye.It when being cooled to 45 DEG C, is placed in constant temperature in 40～45 DEG C of water-baths.
(3) 150g camellia oil, 15g palm oil, 35g coconut oil are mixed in the stainless steel cup of 1000mL, with reinforcement electricity
Dynamic mixer stirring, rotating speed 220rpm, stirring is subsequently placed in water-bath and is heated to identical with alkali liquid temperature.
(4) when checking that miscella and alkali liquid temperature are close, miscella is continuously stirred, and in three times alkali lye is added extremely mixed
Close in oil, be stirred until homogeneous after adding every time and add next group again, until all adding；The whole mistake mixing with miscella at alkali lye
All keeping continuously stirred in journey, rotating speed controls at 200rpm.After 20min, suspend stirring 5min, observe the color of oil simultaneously and examine
Look into temperature.Slowly regulation mixing speed is continuously stirred to 1000rpm, when soap lye density nearly thickens slightly, is sequentially added into
The fresh dendrobium extract of 3g and 0.3g plants essential oil or essence.Continue stirring soap lye to reach and thick can enter next step.
(5) pour soap lye in hexagonal silica gel mould into, rap up and down after entering mould and drive bubble away, then mould is kept flat
Enter in foamed plastics incubator, outside case, cover one layer of woollen blanket insulation 24h；If it is cold, foamed plastics incubator can be placed in
In water proof insulating box, keep temperature 35 DEG C, be incubated 24h, complete the shaping of handmade soap；
(6), after being incubated 24h, soap gang mould is taken out from foamed plastics incubator.Reach to carry out the demoulding during demoulding requirement.The demoulding
After soap is placed on cool place, drying, ventilation natural air drying, the soap time of drying in the air is 25～35d.Dry in the air during soap, detect every day pH value,
Measurement soap body quality and observation soap body hardness.PH value is harder less than the 8th, hardness, soap body constant weight when, soap is maturation.
(7), after handmade soap is ripe, modifies soap body surface and surrounding corner with electrician's knife, make good looking appearance.Every piece of finished product is about
70g.With preservative film parcel, film and soap are close to do not have space.Deposit shady and cool ventilation and be dried local preservation.
By total free alkali of the handmade soap to preparation for the national standard (QB/T2485 2008 perfumed soap quality standard), free severe
Property alkali, moisture content and volatile matter, total chloride content detect, and indices all meets national standard.
Table 3 handmade soap Quality Detection result
Embodiment 4
1st, the raw material of fresh stem of noble dendrobium camellia oil handmade soap and composition
Fresh dendrobium extract 12g, camellia oil 250g, palm oil 65g, coconut oil 85g, NaOH 55g, pure water
125g, plants essential oil or essence 6g.
2nd, the making step of fresh stem of noble dendrobium camellia oil handmade soap
(1) each material quality number is weighed out with electronic balance (precision 0.01g).
(2) pure water 125g in 500mL beaker, 55g NaOH is slowly added in three times, and limit edged is gently mixed to complete
CL obtains alkali lye.It when being cooled to 40 DEG C, is placed in constant temperature in 40 DEG C of water-baths.
(3) 250g camellia oil, 65g palm oil, 85g coconut oil are mixed in the stainless steel cup of 1000mL, with reinforcement electricity
Dynamic mixer rotating speed 250rpm, stirs, is subsequently placed in water-bath and is heated to identical with alkali liquid temperature.
(4) when checking that miscella and alkali liquid temperature are close, miscella is continuously stirred, and in three times alkali lye is added extremely mixed
Close in oil, be stirred until homogeneous after adding every time and add next group again, until all adding；The whole mistake mixing with miscella at alkali lye
All keeping continuously stirred in journey, mixing speed is 250rpm；After 20min, suspend stirring 5min, observe the color of oil simultaneously and examine
Looking into temperature, then proceeding to stirring, slow regulation mixing speed to 1000rpm is simultaneously continuously stirred；Start to thicken at soap lye density
It when thick, is sequentially added into the fresh dendrobium extract of 12g and 6g plants essential oil or essence, continue stirring soap lye and reach thick.
(5) soap lye is poured in six silica gel moulds connecting square moulding, rap up and down after entering mould and drive bubble away.Keep flat into bubble
In foam Plastic Foam Box, outside case, cover one layer of woollen blanket insulation 30h.If it is cold, foamed plastics incubator can be placed in water proof
In insulating box, keep temperature 35 DEG C, 30h.
(6), after being incubated 30h, soap gang mould is taken out from foamed plastics incubator.Reach to carry out the demoulding during demoulding requirement.The demoulding
After soap is placed on cool place, drying, ventilation natural air drying, dry in the air soap time about 25～35d.Dry in the air during soap, detect every day pH value,
Measurement soap body quality and observation soap body hardness.PH value is harder less than the 8th, hardness, soap body constant weight when, soap is maturation.
(7), after handmade soap is ripe, modifies soap body surface and surrounding corner with electrician's knife, make good looking appearance.Every piece of finished product is about
70g.With preservative film parcel, film and soap are close to do not have space.Deposit shady and cool ventilation and be dried local preservation.
By total free alkali of the handmade soap to preparation for the national standard (QB/T2485 2008 perfumed soap quality standard), free severe
Property alkali, moisture content and volatile matter, total chloride content detect, and indices all meets national standard.
Table 4 handmade soap Quality Detection result
Embodiment 5
1st, fill a prescription: fresh dendrobium extract 8g, camellia oil 180g, palm oil 40g, coconut oil 60g, NaOH 40g, pure
Water the 100th, plants essential oil or essence 2g.
2nd, making step:
(1) each material quality number is weighed out with electronic balance (precision 0.01g).
(2) pure water 100g in 500mL beaker, 40g NaOH is slowly added in three times, and limit edged is gently mixed to complete
CL obtains alkali lye.It when being cooled to 45 DEG C, is placed in constant temperature in 40～45 DEG C of water-baths.
(3) 180g camellia oil, 40g palm oil, 60g coconut oil are mixed in the stainless steel cup of 1000mL, with reinforcement electricity
Dynamic mixer stirring, rotating speed 200rpm, stirring is subsequently placed in water-bath and is heated to same or like with alkali liquid temperature.
(4) when checking that miscella and alkali liquid temperature are close, miscella is continuously stirred, and in three times alkali lye is added extremely mixed
Close in oil, be stirred until homogeneous after adding every time and add next group again, until all adding；The whole mistake mixing with miscella at alkali lye
All keeping continuously stirred in journey, mixing speed is 200rpm；After 20min, suspend stirring 5min, observe the color of oil simultaneously and examine
Looking into temperature, then proceeding to stirring, slow regulation mixing speed to 1000rpm is simultaneously continuously stirred；Start to thicken at soap lye density
It when thick, is sequentially added into the fresh dendrobium extract of 8g and 2g plants essential oil or essence, continue stirring soap lye and reach thick.
(5) soap lye is poured in six silica gel moulds connecting square moulding, rap up and down after entering mould and drive bubble away.Mould is put down
Put into foamed plastics incubator, outside case, cover one layer of woollen blanket insulation 36h.If it is cold, foamed plastics incubator can be put
In water proof insulating box, keep temperature 30 DEG C, 36h.
(6), after being incubated 36h, soap gang mould is taken out from foamed plastics incubator.Reach to carry out the demoulding during demoulding requirement.The demoulding
After soap is placed on cool place, drying, ventilation natural air drying, the soap time of drying in the air is 25～35d.Dry in the air during soap, detect every day pH value,
Measurement soap body quality and observation soap body hardness.PH value is harder less than the 8th, hardness, soap body constant weight when, soap is maturation.
(7), after handmade soap is ripe, modifies soap body surface and surrounding corner with electrician's knife, make good looking appearance.Every piece of finished product is about
70g.With preservative film parcel, film and soap are close to do not have space.Deposit shady and cool ventilation and be dried local preservation.
By total free alkali of the handmade soap to preparation for the national standard (QB/T2485 2008 perfumed soap quality standard), free severe
Property alkali, moisture content and volatile matter, total chloride content detect, and indices all meets national standard.
Table 5 handmade soap Quality Detection result
Embodiment 6
1st, fill a prescription: fresh dendrobium extract 10g, camellia oil 200g, palm oil 50g, coconut oil 50g, NaOH 35g, pure
Water purification the 100th, plants essential oil or essence 2.5g.
2nd, making step:
(1) each material quality number is weighed out with electronic balance (precision 0.01g).
(2) pure water 100g in 500mL beaker, 35g NaOH is slowly added in three times, and limit edged is gently mixed to complete
CL obtains alkali lye.It when being cooled to 45 DEG C, is placed in constant temperature in 40～45 DEG C of water-baths.
(3) 00g camellia oil, 50g palm oil, 50g coconut oil are mixed in the stainless steel cup of 1000mL, electronic with reinforcement
Mixer stirs, rotating speed 200rpm, and stirring is subsequently placed in water-bath and is heated to same or like with alkali liquid temperature.
(4) when checking that miscella and alkali liquid temperature are close, miscella is continuously stirred, and in three times alkali lye is added extremely mixed
Close in oil, be stirred until homogeneous after adding every time and add next group again, until all adding；The whole mistake mixing with miscella at alkali lye
All keeping continuously stirred in journey, mixing speed is 200rpm；After 20min, suspend stirring 5min, observe the color of oil simultaneously and examine
Looking into temperature, then proceeding to stirring, slow regulation mixing speed to 1000rpm is simultaneously continuously stirred；Start to thicken at soap lye density
It when thick, is sequentially added into the fresh dendrobium extract of 10g and 2.5g plants essential oil or essence, continue stirring soap lye and reach thick.
(5) soap lye is poured in six silica gel moulds connecting square moulding, rap up and down after entering mould and drive bubble away.Mould is put down
Put into foamed plastics incubator, outside case, cover one layer of woollen blanket insulation 26h.If it is cold, foamed plastics incubator can be put
In water proof insulating box, keep temperature 30 DEG C, 36h.
(6), after being incubated 36h, soap gang mould is taken out from foamed plastics incubator.Reach to carry out the demoulding during demoulding requirement.The demoulding
After soap is placed on cool place, drying, ventilation natural air drying, the soap time of drying in the air is 25～35d.Dry in the air during soap, detect every day pH value,
Measurement soap body quality and observation soap body hardness.PH value is harder less than the 8th, hardness, soap body constant weight when, soap is maturation.
(7), after handmade soap is ripe, modifies soap body surface and surrounding corner with electrician's knife, make good looking appearance.Every piece of finished product is about
70g.With preservative film parcel, film and soap are close to do not have space.Deposit shady and cool ventilation and be dried local preservation.
By total free alkali of the handmade soap to preparation for the national standard (QB/T2485 2008 perfumed soap quality standard), free severe
Property alkali, moisture content and volatile matter, total chloride content detect, and indices all meets national standard.
Table 6 handmade soap Quality Detection result
Embodiment provided above is the better embodiment of the present invention, is only used for the convenient explanation present invention, not to this
Bright make any pro forma restriction, any art has usually intellectual, if without departing from the carried skill of the present invention
In the range of art feature, utilize the Equivalent embodiments that the done local of disclosed technology contents is changed or modified, and
Without departing from the technical characteristic content of the present invention, in the range of all still falling within the technology of the present invention feature.
Claims (8)
1. one kind high skin-moisturizing, skin handmade soap, it is characterised in that it is made up of the raw material of following weight parts: extracted by the fresh stem of noble dendrobium
Liquid 3～12 parts, camellia oil 150～250 parts, palm oil 15～65 parts, coconut oil 35～85 parts, 25～55 parts of NaOH, pure
Water purification 80～125 parts and plants essential oil or 0.3～6 part of essence.
2. one according to claim 1 high skin-moisturizing, skin handmade soap, it is characterised in that it is the raw material of following weight parts
Make: by fresh dendrobium extract 5～10 parts, camellia oil 160～220 parts, palm oil 20～60 parts, coconut oil 40～80 parts, hydrogen
Sodium oxide molybdena 30～50 parts, pure water 85～120 parts and plants essential oil or 0.5～5 part of essence.
3. one according to claim 1 and 2 high skin-moisturizing, skin handmade soap, it is characterised in that described plants essential oil is Chinese mugwort
Grass essential oil, Rosa Damascana, osmanthus essential oil, any one in Rosemary Oil or Lavender.
4. the method preparing high skin-moisturizing, skin handmade soap described in any of the above-described claim, it is characterised in that the method bag
Include following step:
(1) get the raw materials ready: weigh each material by formula ratio, standby；
(2) preparation of alkali lye: add water NaOH, stirring, to being completely dissolved, forms alkali lye, standby；
(3) mix oil plant and heat: camellia oil, palm oil and coconut oil being mixed formation miscella, then by miscella
It is heated to same or like with alkali liquid temperature, standby；
(4) saponification: add alkali lye in miscella and stir, carrying out saponification and obtain saponification liquor, then proceedes to stirring to saponification
It when liquid thickens, is sequentially added into fresh dendrobium extract and plants essential oil or essence, continue stirring saponification liquor and reach thick；
(5) enter mold forming: soap lye is poured in silica gel mould, rap up and down after entering mould and drive bubble away, then at 30～35 DEG C of rings
Place 20～36h under border, complete the shaping of handmade soap；
(6) handmade soap is taken out together with mould and carries out the demoulding, after the demoulding dries handmade soap by the demoulding and the soap that dries in the air: after 20～36h,
Soap time of drying in the air is 25～35d；
(7) packaging preserves: after handmade soap dries, and with preservative film parcel, deposits in the place that shady and cool ventilation is dried.
5. the method for a kind of high skin-moisturizing, skin handmade soap according to claim 4, it is characterised in that step (2) particularly as follows:
The preparation of alkali lye: be slowly added into NaOH in pure water in three times, limit edged is gently mixed to being completely dissolved, forms alkali
Liquid, when alkali lye is cooled to 45 DEG C, is placed in constant temperature in the water-bath of 40～45 DEG C and deposits, standby.
6. the method for a kind of high skin-moisturizing, skin handmade soap according to claim 4, it is characterised in that step (4) particularly as follows:
When checking that miscella and alkali liquid temperature are close, miscella is continuously stirred, and add alkali lye to miscella in three times, every time
It is stirred until homogeneous after addition and adds next group again, until all adding；Alkali lye mix with miscella whole during all keep
Continuously stirred, mixing speed is 150-250rpm；After 20min, suspend stirring 5min, observe the color of oil simultaneously and check temperature
Degree, then proceedes to stirring, and slow regulation mixing speed to 1000rpm is simultaneously continuously stirred, when soap lye density starts to thicken,
It is sequentially added into fresh dendrobium extract and plants essential oil or essence, continue stirring soap lye and reach thick.
7. the method for a kind of high skin-moisturizing, skin handmade soap according to claim 4 or 6, it is characterised in that in step (4),
The preparation technology of described fresh dendrobium extract is particularly as follows: with pure water by fresh stem of noble dendrobium washes clean, drain surface moisture, cut
Become 0.8-1.5cm segment length, add the pure water of 10 times of quality, with electric squeezer, stir into muddy, permanent under 25 DEG C of environment
Temperature vibration extraction 24 hours；Suction filtration, is concentrated in vacuo to half volume and obtains concentrate, standby.
8. the method for a kind of high skin-moisturizing, skin handmade soap according to claim 4, it is characterised in that step (6) particularly as follows:
After 20～36h, taking out handmade soap together with mould, whether the soft durometer whether having space, soap between inspection soap and mould is moderate next
Determine demoulding opportunity；If soap body is excessively soft, bonding between overly moist or soap dye, the demoulding again after a period of time can be placed again；Will after the demoulding
Soap is placed on cool place, drying, ventilation natural air drying, and the soap time of drying in the air is 25～35d；Dry in the air during soap, detect pH value and soap every day
Body hardness, when pH value is not less than 60HW less than the 8th, hardness, soap is ripe, it is possible to use or packaging preservation.
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| CN106675860A (en) * | 2016-12-05 | 2017-05-17 | 钦州市钦南区生产力促进中心 | High-moisture-retention skin-moistening handmade soap and preparation method thereof |
| CN106753921A (en) * | 2017-01-13 | 2017-05-31 | 江西神州通油茶科技有限公司 | Cold handmade soap processed and preparation method thereof |
| CN106906081A (en) * | 2017-03-13 | 2017-06-30 | 广西南宁隆吉维特生物科技有限公司 | A kind of fiery sesame oil cold process soap |
| CN107557188A (en) * | 2017-07-19 | 2018-01-09 | 安徽霍山县草之灵中药材有限公司 | A kind of skin care stem of noble dendrobium handmade soap and preparation method thereof |
| CN112980598A (en) * | 2021-02-07 | 2021-06-18 | 河南郁兰馨生物科技有限公司 | Laundry cream and production process thereof |
| CN113373010A (en) * | 2021-07-19 | 2021-09-10 | 安顺学院 | Natural plant sterilization handmade soap and preparation method thereof |
| CN115873673A (en) * | 2022-11-29 | 2023-03-31 | 深圳市洁依源科技有限公司 | Detergent block and its preparation |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106675860A (en) * | 2016-12-05 | 2017-05-17 | 钦州市钦南区生产力促进中心 | High-moisture-retention skin-moistening handmade soap and preparation method thereof |
| CN106753921A (en) * | 2017-01-13 | 2017-05-31 | 江西神州通油茶科技有限公司 | Cold handmade soap processed and preparation method thereof |
| CN106906081A (en) * | 2017-03-13 | 2017-06-30 | 广西南宁隆吉维特生物科技有限公司 | A kind of fiery sesame oil cold process soap |
| CN107557188A (en) * | 2017-07-19 | 2018-01-09 | 安徽霍山县草之灵中药材有限公司 | A kind of skin care stem of noble dendrobium handmade soap and preparation method thereof |
| CN112980598A (en) * | 2021-02-07 | 2021-06-18 | 河南郁兰馨生物科技有限公司 | Laundry cream and production process thereof |
| CN113373010A (en) * | 2021-07-19 | 2021-09-10 | 安顺学院 | Natural plant sterilization handmade soap and preparation method thereof |
| CN115873673A (en) * | 2022-11-29 | 2023-03-31 | 深圳市洁依源科技有限公司 | Detergent block and its preparation |
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