CN104974866A - Tea seed essence soap and preparation method - Google Patents
Tea seed essence soap and preparation method Download PDFInfo
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- CN104974866A CN104974866A CN201510428492.9A CN201510428492A CN104974866A CN 104974866 A CN104974866 A CN 104974866A CN 201510428492 A CN201510428492 A CN 201510428492A CN 104974866 A CN104974866 A CN 104974866A
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Abstract
The invention discloses a tea seed essence soap which is prepared from the following raw materials in percentage by weight: 50.7-69.7% of camellia oil, 8-12% of coconut oil, 6-10% of palm oil, 1-4% of lavender essential oil, 6-10% of deionized water and 9.3-13.3% of sodium hydroxide, wherein the camellia oil is prepared by the following steps: fetching fresh camellia seeds, and selecting the camellia seeds, cleaning and drying in the sun; crushing the dried camellia seeds into powder, and cooking; pouring the cooked camellia seed powder into a tea oil machine for squeezing original camellia oil; adding dried chamomile flowers into the original camellia oil for 30 days and filtering; and fetching the filtrate a to obtain the camellia oil. By adopting the tea seed essence soap prepared by the proportion, the problem in cleaning the skin of people with sensitive skin can be solved, the allergen and stimulation are reduced, and an auxiliary effect of relieving is realized.
Description
Technical field
The invention belongs to tea oil processing technique field, particularly a kind of tea seed elite soap and preparation method.
Background technology
Perfumed soap product is in the market many containing chemical added ingredients, for child, responsive skin crowd and pregnant woman, all has hormesis.Tea oil perfumed soap is natural cleaning and nourishing product, unlike industrial production synthesis soap how many Diazolidinyl Ureas out mostly sold on the market.Along with improving constantly of people's living standard, the demand of people to daily living article quality also improves constantly, and people like green, natural product more.And in daily washing product, tea oil perfumed soap is a hair soap containing camellia seed oil at high proportion, the blood circulation of scalp can be promoted, anti-loss, make hair moist, glossy; Lotus fragrant plant oil seepage force is good, can safeguard skin moisture, softening skin, is also a kind of well hair conditioner.
Camellia oil (having another name called Oleum camelliae, tea-seed oil, camellia seed oil) takes from the seed of tea oil tree.The making processes of Camellia oil can be divided into: shell, dry, and pulverizes, oil expression, and filter, whole process is physical method, and therefore it is real fully natural green edible oil.Not containing erucic acid in tea oil, cholesterol, flavacin and other additive.After tested: in tea oil, unsaturated fatty acids is up to more than 90%, oleic acid reaches 80-83%, and linolic acid reaches 7-13%, and rich in proteins and vitamin A, B, D, E etc., the abundant linolenic acid especially contained by it is needed by human and can not synthesizes.Through scientific verification, the oleic acid of Camellia oil and linoleic acid content are all higher than sweet oil.Research uses Camellia oil as the perfumed soap of raw oil material, can reduce the pungency of perfumed soap to skin, have certain nursing role simultaneously to skin.
Summary of the invention
For the skin solving responsive skin crowd uses easily irritated, stimulate large, the invention provides a kind of tea seed elite soap and preparation method, prior art problem can be solved.
Concrete technical scheme of the present invention is as follows:
A kind of tea seed elite soap, described elite soap following proportioning raw material is by weight percentage made: Camellia oil 50.7%-69.7%, Oleum Cocois 8%-12%, plam oil 6%-10%, Herba Lysimachiae foenumgraeci quintessence oil 1%-4%, deionized water 6%-10%, sodium hydroxide 9.3%-13.3%
Described Camellia oil obtains as follows: get fresh camellia seed, tea seed is carried out selecting seed, clean, dry, the tea seed shone shatters to Powdered, carry out boiling, the vegetable seed powder boiled pours tea oil machine into, squeeze out original Camellia oil, add in original Camellia oil after Flos Matricariae chamomillae dried flower soaks 30 days and filter, get filtrate a and be Camellia oil.
Further, described deionized water adopts deionization apparatus to carry out filtration to tap water to obtain.
Further, the weight ratio of described original Camellia oil and Flos Matricariae chamomillae dried flower is 50: 1.
Further, described elite soap following proportioning raw material is by weight percentage made: Camellia oil 60.7%, Oleum Cocois 10%, plam oil 8%, Herba Lysimachiae foenumgraeci quintessence oil 2%, deionized water 8%, sodium hydroxide 11.3%.
A preparation method for tea seed elite soap, described tea seed elite soap is obtained as follows by the raw material weighed described in 1:
The first step, divides sodium hydroxide equivalent and adds for 3-5 time in deionized water, stirs and melts to sodium hydroxide for 3-5 minute, be then cooled to 40-50 DEG C with stirrer;
Second step, raw material Camellia oil, Oleum Cocois, plam oil are added mixing in Stainless Steel Kettle and stir with stirrer, this raw mixture produces saponification reaction, color becomes milk yellow by transparent oil colours, 40 DEG C are heated to again with electromagnetic oven, sodium hydroxide liquid in step one is poured in the raw mixture of stirring, does not stop stirring 30 minutes with stirrer;
3rd step, gets with dropper the mixing solutions that several step 2 obtain and puts into clean test tube, add 2-5 and drip distilled water, heating constantly jolting, if do not have oil droplet to dissociate, then represents that saponification is complete; If there is oil droplet to dissociate, represent that saponification is not yet complete, then need the mixing solutions in step 2 to continue to stir, until do not have oil droplet to dissociate;
4th step, in step 3 inspection saponification completely mixing solutions, add Herba Lysimachiae foenumgraeci quintessence oil, stir, then soap dye mould is poured in cooling into, air-dry in the aseptic room ventilated, temperature controls in 14-15 degree, the then demoulding, quietly put 40 days, solidify that rear depanning prints, packaging, sampling observation shipment.
Further, dissociate without oil droplet in described step 2, represent saponification completely, namely represent that in without sodium hydroxide, total free alkali and free caustic alkali content are 0.
The Advantageous Effects that the present invention brings is: the cleaning product that the skin for responsive skin crowd provides, and can be good at reducing allergen, reduces and stimulates, have the auxiliary effect of releiving; Meanwhile, all quote plant constituent and add in this formula, adopt not plant and the good ratio allotment of plants essential oil, to improving, skin is obscure obvious effect to tea seed elite soap of the present invention.
Specific embodiment
In order to make object of the present invention, technical scheme and advantage clearly understand, below in conjunction with embodiment, the present invention is further elaborated.Should be appreciated that specific embodiment described herein only in order to explain the present invention, be not intended to limit the present invention.
Saponification reaction is the ester hydrolysis reaction under base catalysis, espespecially the hydrolysis of grease.Saying of narrow sense, saponification reaction is only limitted to grease and mixes with sodium hydroxide, obtains the sodium salt of higher fatty acid and the reaction (also having part water) of glycerine.This reaction manufactures the step in soap flow process, therefore gains the name.Saponification reaction is except common grease and sodium hydroxide react, and also have the reaction fat of grease and strong aqua and plant main body of oil to be triglyceride level, the equation that they are hydrolyzed in the basic conditions is:
R base may be different, but the R-COONa generated can make soap.Common R-has: CH-:8-heptadecene base.R-COOH is oleic acid.CH-: Pentadecane base.R-COOH is Palmiticacid.CH-: n-heptadecane base.R-COOH is stearic acid.Oleic acid is monounsaturated fatty acids, is solved by profit; Soft, stearic acid is all saturated fatty acid, is obtained by fat splitting.If use KOH hydrolysis, the soap obtained is soft.The present invention uses NaOH to be hydrolyzed, and obtains the soap of certain degree of hardness.
Raw material sources details of the present invention are as follows:
Camellia oil: province (district) village co op's purchase camellia seed such as from China Hunan, Jiangxi, Guangxi, Fujian; Oleum Cocois: this daily use chemicals development in science and technology company limited of the Guangzhou Chinese one hundred, country of origin: Philippines, specification: 180KG/ bucket, oily; Plam oil: this daily use chemicals development in science and technology company limited of the Guangzhou Chinese one hundred, country of origin: Malaysian 180KG/ bucket, oily; Herba Lysimachiae foenumgraeci quintessence oil: five colours river valley agricultural development company limited of Huocheng County, aluminium pot is filling, 10KG/ bucket, the place of production: Xinjiang, liquid; Deionized water: Jingjiang City Heng Xin environmental protection equipment company limited 100KG/ bucket, liquid; Sodium hydroxide: continent, Tianjin chemical reagent factory, 500g/ bottle, particle (beans half shape) pearl.Deionized water adopts deionization apparatus to carry out filtration to tap water and obtains.
Embodiment one:
A kind of tea seed elite soap, described elite soap following proportioning raw material is by weight percentage made: Camellia oil 50.7%, Oleum Cocois 12%, plam oil 10%, Herba Lysimachiae foenumgraeci quintessence oil 4%, deionized water 10%, sodium hydroxide 13.3%.
Wherein, Camellia oil obtains as follows: get fresh camellia seed, tea seed is carried out selecting seed, clean, dry, the tea seed shone shatters to Powdered, carry out boiling, the vegetable seed powder boiled pours tea oil machine into, squeezes out original Camellia oil, add in original Camellia oil after Flos Matricariae chamomillae dried flower soaks 30 days and filter, get filtrate a and be Camellia oil.The weight ratio of original Camellia oil and Flos Matricariae chamomillae dried flower is 50: 1.
This tea seed elite soap obtains as follows according to above raw material:
The first step, divides sodium hydroxide equivalent and adds for 3-5 time in deionized water, stirs and melts to sodium hydroxide for 3-5 minute, be then cooled to 4050 DEG C with stirrer;
Second step, raw material Camellia oil, Oleum Cocois, plam oil are added mixing in Stainless Steel Kettle and stir with stirrer, this raw mixture produces saponification reaction, color becomes milk yellow by transparent oil colours, 40 DEG C are heated to again with electromagnetic oven, sodium hydroxide liquid in step one is poured in the raw mixture of stirring, does not stop stirring 30 minutes with stirrer;
3rd step, gets with dropper the mixing solutions that several step 2 obtain and puts into clean test tube, add 2-5 and drip distilled water, heating is constantly jolting also, if do not have oil droplet to dissociate, then represents that saponification is complete, namely represent that in without sodium hydroxide, total free alkali and free caustic alkali content are 0; If there is oil droplet to dissociate, represent that saponification is not yet complete, then need the mixing solutions in step 2 to continue to stir, until do not have oil droplet to dissociate;
4th step, in step 3 inspection saponification completely mixing solutions, add Herba Lysimachiae foenumgraeci quintessence oil, stir, then soap dye mould is poured in cooling into, air-dry in the aseptic room ventilated, temperature controls in 14-15 degree, the then demoulding, quietly put 40 days, solidify that rear depanning prints, packaging, sampling observation shipment.
Embodiment two
A kind of tea seed elite soap, described elite soap following proportioning raw material is by weight percentage made: Camellia oil 69.7%, Oleum Cocois 8%, plam oil 6%, Herba Lysimachiae foenumgraeci quintessence oil 1%, deionized water 6%, sodium hydroxide 9.3%.
Wherein, Camellia oil obtains as follows: get fresh camellia seed, tea seed is carried out selecting seed, clean, dry, the tea seed shone shatters to Powdered, carry out boiling, the vegetable seed powder boiled pours tea oil machine into, squeezes out original Camellia oil, add in original Camellia oil after Flos Matricariae chamomillae dried flower soaks 30 days and filter, get filtrate a and be Camellia oil.The weight ratio of original Camellia oil and Flos Matricariae chamomillae dried flower is 50: 1.
This tea seed elite soap obtains as follows according to above raw material:
The first step, divides sodium hydroxide equivalent and adds for 3-5 time in deionized water, stirs and melts to sodium hydroxide for 3-5 minute, be then cooled to 40-50 DEG C with stirrer;
Second step, raw material Camellia oil, Oleum Cocois, plam oil are added mixing in Stainless Steel Kettle and stir with stirrer, this raw mixture produces saponification reaction, color becomes milk yellow by transparent oil colours, 40 DEG C are heated to again with electromagnetic oven, sodium hydroxide liquid in step one is poured in the raw mixture of stirring, does not stop stirring 30 minutes with stirrer;
3rd step, gets with dropper the mixing solutions that several step 2 obtain and puts into clean test tube, add 2-5 and drip distilled water, heating is constantly jolting also, if do not have oil droplet to dissociate, then represents that saponification is complete, namely represent that in without sodium hydroxide, total free alkali and free caustic alkali content are 0; If there is oil droplet to dissociate, represent that saponification is not yet complete, then need the mixing solutions in step 2 to continue to stir, until do not have oil droplet to dissociate;
4th step, in step 3 inspection saponification completely mixing solutions, add Herba Lysimachiae foenumgraeci quintessence oil, stir, then soap dye mould is poured in cooling into, air-dry in the aseptic room ventilated, temperature controls in 14-15 degree, the then demoulding, quietly put 40 days, solidify that rear depanning prints, packaging, sampling observation shipment.
Embodiment three
A kind of tea seed elite soap, this elite soap following proportioning raw material is by weight percentage made: Camellia oil 60.7%, Oleum Cocois 10%, plam oil 8%, Herba Lysimachiae foenumgraeci quintessence oil 2%, deionized water 8%, sodium hydroxide 11.3%.
Wherein, Camellia oil obtains as follows: get fresh camellia seed, tea seed is carried out selecting seed, clean, dry, the tea seed shone shatters to Powdered, carry out boiling, the vegetable seed powder boiled pours tea oil machine into, squeezes out original Camellia oil, add in original Camellia oil after Flos Matricariae chamomillae dried flower soaks 30 days and filter, get filtrate a and be Camellia oil.The weight ratio of original Camellia oil and Flos Matricariae chamomillae dried flower is 50: 1.
This tea seed elite soap obtains as follows according to above raw material:
The first step, divides sodium hydroxide equivalent and adds for 3-5 time in deionized water, stirs and melts to sodium hydroxide for 3-5 minute, be then cooled to 40-50 DEG C with stirrer;
Second step, by raw material Camellia oil, Oleum Cocois, plam oil, add mixing in Stainless Steel Kettle and stir with stirrer, this raw mixture produces saponification reaction, color becomes milk yellow by transparent oil colours, 40 DEG C are heated to again with electromagnetic oven, sodium hydroxide liquid in step one is poured in the raw mixture of stirring, does not stop stirring 30 minutes with stirrer;
3rd step, gets with dropper the mixing solutions that several step 2 obtain and puts into clean test tube, add 2-5 and drip distilled water, heating is constantly jolting also, if do not have oil droplet to dissociate, then represents that saponification is complete, namely represent that in without sodium hydroxide, total free alkali and free caustic alkali content are 0; If there is oil droplet to dissociate, represent that saponification is not yet complete, then need the mixing solutions in step 2 to continue to stir, until do not have oil droplet to dissociate;
4th step, in step 3 inspection saponification completely mixing solutions, add Herba Lysimachiae foenumgraeci quintessence oil, stir, then soap dye mould is poured in cooling into, air-dry in the aseptic room ventilated, temperature controls in 14-15 degree, the then demoulding, quietly put 40 days, solidify that rear depanning prints, packaging, sampling observation shipment.
The skin effect of Camellia oil, the particularly antiinflammation of Laoshan tea oil, we adopt not high temperature soapmaking method, remain the nutritive ingredient in former Camellia oil.A large amount of greases of tea seed elite soap of the present invention skin secretion when cleaning skin; while effectively cleaning grease; a large amount of vegetable glycerides is produced more than grease acid-reaction with on skin; stop skin surface protection skin; therefore to have cleaned skin moist for tea seed elite soap; and nourish, lubrication, more use the more smooth health of skin.By originally sampling tea, seed elite soap cuts 10 grams, convert 50ml clear water, shake to foaming, 5 grams of acid (light-coloured vinegar or citric acid) are poured in the liquid shaken, bubble completely dissolve, the remaining material of reaction is vegetable glycerides and water, and contained in the tea oil just monounsaturated fatty acids (abbreviation oleic acid) of this vegetable glycerides is similar to skin surface oleic acid 70%.Reason is: alkalescence and the skin oil and fat pH value acidity of soap react.
Tea seed elite soap of the present invention meets QB/T 2485-2008 standard (II type) requirement, and details are as shown in the table.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, all any amendments done within the spirit and principles in the present invention, equivalent replacement and improvement etc., all should be included within protection scope of the present invention.
The present invention does not address part and is applicable to prior art.
Claims (6)
1. a tea seed elite soap, is characterized in that: described elite soap following proportioning raw material is by weight percentage made: Camellia oil 50.7%-69.7%, Oleum Cocois 8%-12%, plam oil 6%-10%, Herba Lysimachiae foenumgraeci quintessence oil 1%-4%, deionized water 6%-10%, sodium hydroxide 9.3%-13.3%
Described Camellia oil obtains as follows: get fresh camellia seed, tea seed is carried out selecting seed, clean, dry, the tea seed shone shatters to Powdered, carry out boiling, the vegetable seed powder boiled pours tea oil machine into, squeeze out original Camellia oil, add in original Camellia oil after Flos Matricariae chamomillae dried flower soaks 30 days and filter, get filtrate a and be Camellia oil.
2. tea seed elite soap according to claim 1, is characterized in that: described deionized water adopts deionization apparatus to carry out filtration to tap water and obtains.
3. tea seed elite soap according to claim 1, is characterized in that: the weight ratio of described original Camellia oil and Flos Matricariae chamomillae dried flower is 50: 1.
4. tea seed elite soap according to claim 1, is characterized in that: described elite soap following proportioning raw material is by weight percentage made: Camellia oil 60.7%, Oleum Cocois 10%, plam oil 8%, Herba Lysimachiae foenumgraeci quintessence oil 2%, deionized water 8%, sodium hydroxide 11.3%.
5. a preparation method for tea seed elite soap, is characterized in that: described tea seed elite soap is obtained as follows by the raw material weighed described in 1:
The first step, divides sodium hydroxide equivalent and adds for 3-5 time in deionized water, stirs and melts to sodium hydroxide for 3-5 minute, be then cooled to 40-50 DEG C with stirrer;
Second step, raw material Camellia oil, Oleum Cocois, plam oil are added mixing in Stainless Steel Kettle and stir with stirrer, this raw mixture produces saponification reaction, color becomes milk yellow by transparent oil colours, 40 DEG C are heated to again with electromagnetic oven, sodium hydroxide liquid in step one is poured in the raw mixture of stirring, does not stop stirring 30 minutes with stirrer;
3rd step, gets with dropper the mixing solutions that several step 2 obtain and puts into clean test tube, add 2-5 and drip distilled water, heating constantly jolting, if do not have oil droplet to dissociate, then represents that saponification is complete; If there is oil droplet to dissociate, represent that saponification is not yet complete, then need the mixing solutions in step 2 to continue to stir, until do not have oil droplet to dissociate;
4th step, in step 3 inspection saponification completely mixing solutions, add Herba Lysimachiae foenumgraeci quintessence oil, stir, then soap dye mould is poured in cooling into, air-dry in the aseptic room ventilated, temperature controls in 14-15 degree, the then demoulding, quietly put 40 days, solidify that rear depanning prints, packaging, sampling observation shipment.
6. the preparation method of tea seed elite soap according to claim 5, is characterized in that: dissociate without oil droplet in described step 2, represents saponification completely, namely represents that in without sodium hydroxide, total free alkali and free caustic alkali content are 0.
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105647701A (en) * | 2016-03-22 | 2016-06-08 | 桂林航天工业学院 | Versatile handmade soap with horse oil and camellia seed oil and production method of versatile handmade soap |
| CN106085659A (en) * | 2016-06-02 | 2016-11-09 | 嘉应学院 | A kind of high skin-moisturizing, skin handmade soap and preparation method thereof |
| CN106281807A (en) * | 2016-08-17 | 2017-01-04 | 宜春元博山茶油科技农业开发有限公司 | Oleum Camelliae handmade soap and preparation method thereof |
| CN106867721A (en) * | 2017-03-31 | 2017-06-20 | 贵州省镇远县古镇米业有限责任公司 | A kind of camellia oil handmade soap and preparation method thereof |
| CN107541365A (en) * | 2017-10-18 | 2018-01-05 | 湖南大三湘茶油电子商务有限公司 | Cocoon shells silk camellia handmade soap through desensitization process and preparation method thereof |
| CN107541364A (en) * | 2017-10-18 | 2018-01-05 | 湖南大三湘茶油电子商务有限公司 | Mo Luohai bud camellia handmade soaps through desensitization process and preparation method thereof |
| CN107603782A (en) * | 2017-10-18 | 2018-01-19 | 湖南大三湘茶油电子商务有限公司 | A kind of light speckles, beautification and white Mo Luohai buds camellia grinding soap and preparation method thereof |
| CN107739669A (en) * | 2017-10-18 | 2018-02-27 | 湖南大三湘茶油电子商务有限公司 | Moist maintenance anti-inflammation and sterilization camellia handmade soap through desensitization process and preparation method thereof |
| CN114288213A (en) * | 2021-12-27 | 2022-04-08 | 伊犁紫苏丽人生物科技有限公司 | Novel natural composite tea oil foot soaking gel bead and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105647701A (en) * | 2016-03-22 | 2016-06-08 | 桂林航天工业学院 | Versatile handmade soap with horse oil and camellia seed oil and production method of versatile handmade soap |
| CN106085659A (en) * | 2016-06-02 | 2016-11-09 | 嘉应学院 | A kind of high skin-moisturizing, skin handmade soap and preparation method thereof |
| CN106281807A (en) * | 2016-08-17 | 2017-01-04 | 宜春元博山茶油科技农业开发有限公司 | Oleum Camelliae handmade soap and preparation method thereof |
| CN106867721A (en) * | 2017-03-31 | 2017-06-20 | 贵州省镇远县古镇米业有限责任公司 | A kind of camellia oil handmade soap and preparation method thereof |
| CN107541365A (en) * | 2017-10-18 | 2018-01-05 | 湖南大三湘茶油电子商务有限公司 | Cocoon shells silk camellia handmade soap through desensitization process and preparation method thereof |
| CN107541364A (en) * | 2017-10-18 | 2018-01-05 | 湖南大三湘茶油电子商务有限公司 | Mo Luohai bud camellia handmade soaps through desensitization process and preparation method thereof |
| CN107603782A (en) * | 2017-10-18 | 2018-01-19 | 湖南大三湘茶油电子商务有限公司 | A kind of light speckles, beautification and white Mo Luohai buds camellia grinding soap and preparation method thereof |
| CN107739669A (en) * | 2017-10-18 | 2018-02-27 | 湖南大三湘茶油电子商务有限公司 | Moist maintenance anti-inflammation and sterilization camellia handmade soap through desensitization process and preparation method thereof |
| CN114288213A (en) * | 2021-12-27 | 2022-04-08 | 伊犁紫苏丽人生物科技有限公司 | Novel natural composite tea oil foot soaking gel bead and preparation method thereof |
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