CN107603782A - A kind of light speckles, beautification and white Mo Luohai buds camellia grinding soap and preparation method thereof - Google Patents
A kind of light speckles, beautification and white Mo Luohai buds camellia grinding soap and preparation method thereof Download PDFInfo
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- CN107603782A CN107603782A CN201710973001.8A CN201710973001A CN107603782A CN 107603782 A CN107603782 A CN 107603782A CN 201710973001 A CN201710973001 A CN 201710973001A CN 107603782 A CN107603782 A CN 107603782A
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Abstract
The present invention relates to a kind of light speckles, beautification and white Mo Luohai buds camellia grinding soap, it is made up according to mass fraction meter of following raw material：60 85 parts of camellia oil cold process soap soap powder, 15 parts of Mo Luohai bean sprouts powder, 15 parts of camellia flower extract, 0.5 3 parts of pearl powder, 5 10 parts of deionized water, 0.1 0.5 parts of essence.Its manufacture craft is：Ripe camellia oil cold process soap soap blank is dug into soap silk；Soap silk is placed between the foster soap of placement to hang to drying and breaks into soap powder；Stirring rubbing sticks together into soap after soap powder is added into Mo Luohai bean sprouts powder, camellia flower extract, pearl powder, essence, deionized water, is finally molded.Meaning of the present invention is to develop a Mo Luohai buds camellia grinding soap for having and moistening moisturizing, light speckles, beautification and white, the effect of anti-inflammatory anti-acne.
Description
Technical field
The present invention relates to a kind of camellia to grind soap, particularly a kind of light speckles, beautification and white Mo Luohai buds camellia grinding soap.
Background technology
The production of soap product has a long history, and about with regard to useful grease and contains carbonic acid at B.C. 2500
The plant ass of potassium produces potash soap, and the record of wool is washed with this soap, since 19th century, due to Leblanc soda ash production method
Development, makes the production of soap enter industrialized stage, now, as the improvement of people's living standards, people are for thing
The requirement also more and more higher of matter life, soap products at present on the market are different, but wherein most all containing substantial amounts of chemistry
Product, there is side effect and injury to skin, and people use rear dry skin, and easy allergy.
The content of the invention
An object of the present invention is to provide a kind of light speckles, beautification and white Mo Luohai buds camellia grinding soap, is that solution cold process soap pH is inclined
Alkali, there are certain stimulation sex chromosome mosaicism, characteristic component Mo Luohai bud powder Mineral Elements therein and vitamin content pole to skin
Height, the juice in Mo Luohai bud-leafs have to skin gently releive, lubricate, anti-aging and other effects, add energy after later stage curing
Its nutritional ingredient is sufficiently reserved, is not destroyed.
The second object of the present invention is the preparation method for providing above-mentioned light speckles, beautification and white Mo Luohai buds camellia grinding soap.
A kind of light speckles, beautification and white Mo Luohai buds camellia grinding soap, according to mass fraction meter, is made up of following raw material：Camellia oil cooling
Soapmaking 60-85 parts, Mo Luohai bean sprout powder 1-5 parts, camellia flower extract 1-5 parts, pearl powder 0.5-3 parts, deionized water 5-10 parts,
Essence 0.1-0.5 parts.
Described light speckles, beautification and white Mo Luohai buds camellia grinding soap manufacture craft comprises the following steps：
（1）Scraping：Ripe camellia oil cold process soap soap blank is dug into soap silk；
（2）Dry：By step（1）Soap silk be placed in placement and support to hang 5-10 days between soap and can be milled to drying；
（3）Beat powder：By step（2）The soap silk dried is put into pulverizer and is ground into soap powder；
（4）Spice：By step（3）Soap powder add Mo Luohai bean sprouts powder, camellia flower extract, pearl powder, perfume (or spice) by a certain percentage
Stirring rubbing sticks together into soap after essence, deionized water；
（5）Shaping：By step（4）Soap stick together input billet cutter in be squeezed into cylindrical soap body；
（6）Packaging：By step（5）Cylindrical soap body be fitted into spiral soap pipe.
Preferably, described camellia oil cold process soap, it is made up according to mass fraction of following component：Camellia oil 15-25 parts,
Grape-kernel oil 6-12 parts, maize germ oil 15-20 parts, coconut oil 15-20 parts, palm oil 15-20 parts, deionized water 14-20 parts,
Sodium hydroxide 8-12 parts, tea seed extract solution 3-6 parts.
Preferably, described camellia oil cold process soap manufacture craft comprises the following steps：
（1）Under normal temperature, NaOH solids are dissolved with low temperature deionized water in a reservoir, it is in clear or white solution to make it, is controlled
Temperature processed is 30-50 DEG C；
（2）In another container, camellia oil, grape-kernel oil, maize germ oil, coconut oil, palm fibre are put into the greases such as oil and mixed in proportion
Close, heating stirring is transparent to whole fat clarifications；
（3）Will（1）It is slowly added to（2）Keeping temperature be less than 35-45 DEG C mixing, be sufficiently stirred, up to soap lye close to or up
It is slight sticky；
（4）The additives such as tea seed extract solution, essence are separately added into, are again stirring for uniformly；
（5）When soap lye sticky hanging wire, mould is poured into, is incubated, after standing 24-48h, the demoulding；
（6）Hung in shady and cool, ventilation, the place dried, continue to cure 6 weeks to handmade soap.
Wherein described preferred 2-5 parts of Mo Luohai bean sprout powder.
The preferred 2-5 parts of wherein described camellia flower extract.
Preferably, the tea seed extract solution described in camellia oil cold process soap will pass through desensitization, and technique is：
（1）Squeezing：Tea seed is squeezed and obtains camellia seed slag；
（2）Leach：By step（1）Camellia seed slag is obtained by n-hexane extraction, obtains the camellia seed slag that deoils；
（3）Crush：By step（2）The obtained camellia seed ground-slag that deoils is broken, is sieved through the eye mesh screen of 30 mesh -100, obtains camellia seed
Powder；
（4）Heat extraction：Weigh step（3）Obtained tea seed powder and deionized water mixing, are heated, stirring, through 150-200 mesh after cooling
Filter-cloth filtering obtains filtrate 1；
（5）Enzymolysis：By step（4）The pH value of gained filtrate 1 is adjusted to 2.5-4, adds acid protease, heating water bath to 50-
60 DEG C, decolorising agent is added, is again heated to 80-100 DEG C, lasting stirring, cold filtration obtains filtrate 2；
（6）It is refined：By step（5）The filtrate 2 of acquisition adds filter aid diatomite, adjustment tea seed extracting liquid pH value to 5-6, mistake
Filter, obtain clarification camellia seed extract solution.
Step（4）Middle camellia seed powder and deionization mixed proportion are 1:（3-10）, 60 DEG C -100 DEG C are heated to, mixing speed
For 20-60 revs/min, 40-60 minutes are stirred.
Preferably, step（5）Described acid protease and the weight ratio of filtrate 1 are（0.1-4）：1000.
Step（5）Described acid protease is that the excellent Aspergillus usamii of seed selection is made through depth fermentation.
Step（5）Middle decolorising agent and the weight ratio of filtrate 1 are（1-2）：100；Described decolorising agent is activated carbon and activity
Carclazyte, adsorption specific surface area 1000m2/g-1500m2/ g or adsorption capacity reach 80%-100%, are calculated with part by weight, activity
Charcoal：Atlapulgite=1：（3-10）.
Step（6）Diatomaceous addition is the 1-6% of the weight of filtrate 2, is filtered by leaf-type filter, obtains clarification mountain
Tea seed extract solution.
Natural plants and essential oil of the addition with skin care effect are being rubbed after the present invention crushes the tea oil cold process soap cured
The camellia grinding soap of type is twisted into, there is the effect such as extraordinary cleaning, reparation, nourishing, anti-acne, be adapted to the crowd of all kinds of skin quality to make
With.
Primary raw material used in the present invention is described as follows：
Camellia seed：It is the fruit of tea oil tree；Tea oil tree is the main woody oleiferous plants tree in China, is described as " east tree ", belongs to camellia
Section's Camellia evergreen dungarunga, it is the distinctive woody vegetable oil resource in China；3-6 meters of the height of tree, the diameter of a cross-section of a tree trunk 1.3 meters above the ground is up to 24-30 lis
Rice, smooth bark is taupe；Tea oil tree list leaf alternate, flower are both sexes white, and October, Post flowering was until fruit between October next year
Can be ripe, therefore, tea oil tree has rare flowers and fruits homophyletic phenomenon；Fruit is capsule, is mostly ellipse, has fine, soft fur；Seed
Mostly yellowish-brown, glossy, triangular shape.Tea oil tree is grown in remote mountains, inhales natural nutrient to the greatest extent, evergreen longevity, the age of tree was up to 200 years
More than.
Camellia oil：Camellia seed kernel is through cleaning, air-drying（Temperature is less than 100 DEG C）, shelling, seed selection sterilization after, at 20-50 DEG C
Obtained by being squeezed, active material enriches, and contains vitamin E 200mg/Kg, sterol 30mg/Kg, squalene 100mg/Kg.
Grape-kernel oil：Grape-kernel oil has two kinds of very important elements, linolenic acid and proanthocyanidin；Linolenic acid can be with
Free radical is resisted, anti-aging, help absorbs vitamin C and E, strengthens the elasticity of the circulatory system, reduces the injury of ultraviolet, protects
Collagen in skin, improve venous engorgement and oedema, prevent melanin deposition；Proanthocyanidin has protection blood vessel elasticity, protects
Skin afflicting with great suffering torment from ultraviolet is protected, prevents the destruction of collagenous fibres and elastomer, skin is kept due elasticity and is opened
Power, skin sagging and wrinkle is avoided to produce.Grape-kernel oil penetration is strong, salubrious non-greasy, is easily absorbed by the skin, any skin quality
It is applicable.
Maize germ oil：Maize germ oil is the vegetable oil refined from the plumule of corn, contains abundant unsaturated lipid
Fat acid（Based on oleic acid and linoleic acid）, vitamin E and polyphenols, it is higher containing trans-fat levels；Corn germ fatty
Content constitutes about more than the 80% of corn total fats content between 17%~45%.Aliphatic acid feature in corn oil is insatiable hunger
80%~85% is up to content of fatty acid.
Coconut oil：Coconut oil is the indispensable glyceride stock of perfumed soap, and produces natural acid, fatty alcohol and surface
The raw material of activating agent；It can increase the rich of foam with coconut oil soapmaking, strengthen cleaning effect.
Palm oil：Palm oil is also known as brown oily, brown skin oil, and the grease extracted by pericarp in oil palm fruit, is non-drying oil.In right amount
Collocation can increase finished product hardness in the formula of handmade soap, be that handmade soap is more stable, effectively extend the resting period.
Mo Luohai bud powder：Mo Luohai buds are also known as emperor's dish, scientific name corchorus olitorius；In the famous pharmacopeia in China《Dictionary of medicinal plant》
Deng the medicinal description for having jute and false jute in ancient books and records, but not yet take in the medicinal record of corchorus olitorius；Jute enters in China
The history of medicine at least also has more than thousand, early in the Song Dynasty《Bencao Tujing》In have been described " for example weak and narrow point of roundpod jute leaf, stem side,
High four or five chi, chrysanthemum are raw sub small into room such as flax angle；Tender leaf is edible, very sweet cunning, profit large intestine "；China's traditional medicine is recognized
For roundpod jute leaf is bitter in taste, temperature；Enter the heart, liver two passes through；There are regulating qi-flowing for relieving pain, the function such as removing toxic substances apocenosis and hemostasis；Mineral in Mo Luohai buds
Element and vitamin content are high, the juice in Mo Luohai bud-leafs have to skin gently releive, lubricate, anti-aging and other effects.
Sodium hydroxide：As the alkali reacted with fat saponification.
Deionized water：Refer to eliminate the pure water in after ionic species impurity, International Organization for standardization ISO/TC 147 is advised
Fixed " deionization " is defined as：" deionized water is complete or incompletely removes ionic species；" using the method system of RO counter-infiltrations
Take, the anion and cation gone using ion exchange resin in water removal.
Essence：The smell of finished product is adjusted, is allowed to pleasant comfortable.
Camellia flower extract：Contain abundant multivitamin, protein, fat, starch and various micro mineral matters
, can be with spleen benefiting and stimulating the appetite after eating Deng nutriment, moreover it is possible to treat the illnesss such as dysentery, be a kind of natural food, have very deep
Health effect；The Tea Polyphenols being rich in camellia can remove free radical, have anti-aging, sliding tender skin, remove the work(such as color spot
Effect.
Pearl powder：Three kinds of trace elements such as manganese that pearl powder contains in itself, copper, zinc are the compositions for forming SOD, use pearl powder
Painting face, human skin superoxide dismutase can be promoted（SOD）Activity, suppress the synthesis of melanin, keep whitening skin；This
Outside, because SOD has the function that to remove free radical, therefore skin senescence, corrugation can be prevented by applying face with pearl powder.
Embodiment
Tea seed extract solution used, is made up of following processing step in embodiment：
（1）Squeezing：Tea seed is squeezed and obtains camellia seed slag；
（2）Leach：By step（1）Camellia seed slag is obtained by n-hexane extraction, obtains the camellia seed slag that deoils；
（3）Crush：By step（2）The obtained camellia seed ground-slag that deoils is broken, is sieved through 50 eye mesh screens, obtains camellia seed powder；
（4）Heat extraction：Weigh step（3）Obtained tea seed powder and deionized water mixing, camellia seed powder and deionization mixed proportion are
1:4, heat, stirring, filtrate 1 is obtained through 150-200 mesh filter-cloth filterings after cooling；
（5）Enzymolysis：By step（4）The PH of gained filtrate 1 is adjusted to 3, adds acid protease（Acid protease is that seed selection is excellent
The fermentation of Aspergillus usamii depth is made, and the weight ratio with filtrate 1 is 0.5：1000）, heating water bath to 55 DEG C, live by addition decolorising agent
Property charcoal and atlapulgite, average adsorption specific surface area are respectively 1200m2/ g and 1300m2/ g, is calculated with part by weight, activated carbon：
Atlapulgite=1：4, the weight ratio of decolorising agent and filtrate 1 is 2：100；80 DEG C are again heated to, lasting stirring, cold filtration must be filtered
Liquid 2；
（6）It is refined：By step（5）The filtrate 2 of acquisition adds 3% filter aid diatomite of the weight of filtrate 2, adjusts tea seed extract solution
PH to 5.5, filtering, obtain clarification camellia seed extract solution.
Above-mentioned tea seed extract solution is subjected to patch test, patch test results are without allergic reaction；Method of testing is as follows, real
Test step：
Step 1：The gauze of four thickness is cut into a diameter of 1cm circle with scissors, totally 8, draws 25uL's respectively with liquid-transfering gun
Tea seed extract solution, is dropped on circular gauze, and blank is done with deionized water；
Step 2：The gripping of gauze tweezers is placed on subject（To tea seed extract solution allergy sufferers）At anteflexion arm, adhesive tape is used
Fix, start timing；
Step 3：Torn after 48h adhesive tape, and observe the reaction of skin at gauze covering immediately.
Embodiment 1
170 grams of coconut oil is weighed, 170 grams of palm oil, after heating for dissolving, adds 200 grams of tea oil, 60 grams of grape-kernel oil, maize
160 grams of bud oil, after stirring, weighs 100 grams of sodium hydroxides and is dissolved in 180 grams of deionized waters, after stirring, be slowly added to
In grease, lasting stirring, treat that saponification is abundant, when material body is in thread, adds 50 grams of tea seed extract solutions, be stirring evenly and then adding into soap lye
In, reverse mould after stirring, depanning after shaping, after supporting soap to complete curing, scraping is carried out, dries, be ground into soap powder.
Weigh soap powder 600g, after heating for dissolving, Jia Moluohai buds powder 30g, pearl powder 20g, camellia flower extract 40g, go
Ionized water 60g, essence 0.2g, reverse mould after stirring, depanning after shaping, dry.
Embodiment 2-5
Embodiment 2-5 handmade soap, its preparation process condition is substantially with embodiment 1, the simply bar such as reaction raw materials and proportion scale
Part is slightly different, specifically as listed in table 1.
The light speckles, beautification and white Mo Luohai buds camellia grinding soap formula of the embodiment of table 1, comparative example
。
Comparative example 3
Comparative example 3 eliminates Mo Luohai bud powder on the basis of embodiment 1, and camellia flower extract dosage is 70 grams, it is other with it is real
It is identical to apply example 1.
Comparative example 4
Comparative example 4 eliminates camellia flower extract on the basis of embodiment 1, and Mo Luohai bud powder dosage is 70 grams, it is other with it is real
It is identical to apply example 1.
After grinding soap shaping obtained by embodiment 1-5, comparative example 1-4 is made, its foam, rinsability, moist is tested
Moisturizing, light speckles, beautification and white, the test result of anti-inflammatory anti-acne are as shown in table 2：
Its functional attributes test result of grinding soap obtained by the embodiment of table 2, comparative example
。
Its functional attributes of grinding soap obtained by embodiment, comparative example and the method for testing used in physical and chemical index test have：
(1) foam, method of testing that is rinsability, moistening performance of keeping humidity are tested for hand skin, and specific method is as follows：
By the grinding soap obtained by embodiment 1-5, comparative example 1-4, got blisters with the net of getting blisters drenched, treating that foam is fully abundant can not
When being further added by, depth of foam is observed, and record（- represent almost without foam ,+represent a small amount of foam, ++ represent more foam,
+++ represent very more foams）, hand then is rinsed with clear water, record was rinsed to the clean time, untill not glutinous soapy feeling,
With clean towel water purification beads, the back of the hand portion moisture value is detected with digital skin moisture detector after half an hour（Note：Using hand
Work, which is soaped, will detect the back of the hand portion moisture value before hand, and record）；Statistical result such as table 3：
The embodiment of table 3, comparative example camellia grinding soap trial effect mean scores table
。
From table 3, it can be seen that foaming abundancy degree and coconut oil of the present invention, camellia oil, grape-kernel oil, maize germ oil add
Added with pass, addition correlation of the moisture retention with Mo Luohai buds powder, tea seed extract solution is moistened, addition is more, and effect is better.
Example 1-5, comparative example 1-4 grinding soap carry out light speckles, beautification and white measure of merit, and subjects are to have spot on the face
（Sunburn, freckle, chloasma etc.）Young woman, 20 people be one group, experimental group uses light speckles, beautification and white Mo Luohai bud camellias every night
Face of soaping is ground, control group is washed one's face using pearl whitening handmade soap on the market every night, and service life is 45 days, is used every 15 days
Melanin content in dermal melanin tester checkout facility subject's skin, and melanin inhibiting rate is calculated according to the following formula
Average value --- melanin inhibiting rate=（Control group dermal melanin content average value-experimental group dermal melanin content is averaged
Value）/ control group dermal melanin content average value * 100%.Draw the result of the test of table 4.
Table 4
。
Through experimental observation, light speckles, beautification and white Mo Luohai buds camellia of the invention grinds soap to skin speckle（Sunburn, freckle, Huang
Foxiness etc.）There is obvious desalination effect, skin colourity is decreased obviously, and illustrates the light speckles, beautification and white Mo Luohai buds camellia grinding of the present invention
Soap has the function that suppression melanin, can reach whitening effect.
Embodiment 1-5, comparative example 1-4 grinding saponaria vaccaria anti-acne effect method of testing are as follows：
Embodiment 1-5, comparative example 1-4 grinding soap are chosen into 20 triers for having long acne skin respectively, tried out three months, system
Count rehabilitation situation quantity, statistical conditions such as table 5.
The camellia of table 5 grinds the number of effects statistical form of saponaria vaccaria anti-acne
。
From table 5, it can be seen that the addition of Mo Luohai buds powder, camellia flower extract and tea seed extract solution has extraordinary disappear
Scorching anti-acne effect.
Claims (10)
1. the present invention relates to a kind of light speckles, beautification and white Mo Luohai buds camellia grinding soap, according to mass fraction meter, by following raw material system
Into：Camellia oil cold process soap 60-85 parts, Mo Luohai bean sprout powder 1-5 parts, camellia flower extract 1-5 parts, pearl powder 0.5-3 parts, go from
Sub- water 5-10 parts, essence 0.1-0.5 parts.
2. light speckles, beautification and white Mo Luohai buds camellia grinding soap according to claim 1, it is characterised in that described Mo Luohai buds
Vegetable powder dosage is 2-5 parts.
3. light speckles, beautification and white Mo Luohai buds camellia grinding soap according to claim 1, it is characterised in that described camellia carries
It is 2-5 parts to take thing dosage.
4. light speckles, beautification and white Mo Luohai buds camellia grinding soap according to claim 1, it is characterised in that described camellia oil cooling
Soapmaking, it is made up according to mass fraction of following component：Camellia oil 15-25 parts, grape-kernel oil 6-12 parts, maize germ oil 15-20
Part, coconut oil 15-20 parts, palm oil 15-20 parts, deionized water 14-20 parts, sodium hydroxide 8-12 parts, tea seed extract solution 3-6
Part.
5. light speckles, beautification and white Mo Luohai buds camellia grinding soap according to claim 4, it is characterised in that described camellia oil cooling
Soapmaking preparation method comprises the following steps:
（1）Under normal temperature, NaOH solids are dissolved with low temperature deionized water water in a reservoir, make it be in clear or white solution,
It is 30-50 DEG C to control temperature；
（2）In another container, camellia oil, grape-kernel oil, maize germ oil, coconut oil, palm fibre are put into oil and mixed in proportion, is heated
Stirring is transparent to whole fat clarifications；
（3）Will（1）It is slowly added to（2）Keeping temperature be less than 35-45 DEG C mixing, be sufficiently stirred, up to soap lye close to or up
It is slight sticky；
（4）Then tea seed extract solution is added, is again stirring for uniformly；
（5）When soap lye sticky hanging wire, mould is poured into, is incubated, after standing 24-48 h, the demoulding；
（6）Hung in shady and cool, ventilation, the place dried, continue curing 6 weeks.
6. light speckles, beautification and white Mo Luohai buds camellia grinding soap according to claim 4, it is characterised in that described tea seed extraction
Liquid and preparation method thereof is as follows：
（1）Squeezing：Tea seed is squeezed and obtains camellia seed slag；
（2）Leach：By step（1）Camellia seed slag is obtained by n-hexane extraction, obtains the camellia seed slag that deoils；
（3）Crush：By step（2）The obtained camellia seed ground-slag that deoils is broken, is sieved through 30-100 eye mesh screens, obtains camellia seed powder；
（4）Heat extraction：Weigh step（3）Obtained tea seed powder and deionized water mixing, are heated, stirring, through 150-200 mesh after cooling
Filter-cloth filtering obtains filtrate 1；
（5）Enzymolysis：By step（4）The pH value of gained filtrate 1 is adjusted to 2.5-4, adds acid protease, heating water bath to 50-
60 DEG C, decolorising agent is added, is again heated to 80-100 DEG C, lasting stirring, cold filtration obtains filtrate 2；
（6）It is refined：By step（5）The filtrate 2 of acquisition adds filter aid, adjustment tea seed extracting liquid pH value to 5-6, filters, and obtains
Tea seed extract solution.
7. light speckles, beautification and white Mo Luohai buds camellia grinding soap according to claim 6, it is characterised in that step（4）Middle camellia
Seed powder and deionization mixed proportion are 1:（3-10）, 60 DEG C -100 DEG C are heated to, mixing speed is 20-60 revs/min, stirring
40-60 minutes.
8. light speckles, beautification and white Mo Luohai buds camellia grinding soap according to claim 6, it is characterised in that step（5）Middle decolouring
Agent and the weight ratio of filtrate 1 are（1-2）：100；Described decolorising agent is activated carbon and atlapulgite, is calculated with part by weight,
Activated carbon：Atlapulgite=1：（3-10）.
9. light speckles, beautification and white Mo Luohai buds camellia grinding soap according to claim 6, it is characterised in that step（5）Described
Acid protease is that the excellent Aspergillus usamii of seed selection is made through depth fermentation, and the weight ratio with filtrate 1 is（0.1-4）：1000.
10. the preparation method of light speckles, beautification and white Mo Luohai buds camellia grinding soap according to claim 1, it is characterised in that wrap successively
Include following steps：
Scraping：Camellia oil cold process soap is dug into soap silk；
Dry：By step（1）Soap silk be placed in placement and support to hang 5-10 days between soap and can be milled to drying；
Beat powder：By step（2）The soap silk dried is put into pulverizer and is ground into soap powder；
（4）Spice：By step（3）Soap powder add Mo Luohai bean sprouts powder, camellia flower extract, pearl powder, perfume (or spice) by a certain percentage
Stirring rubbing sticks together into soap after essence, deionized water；
（5）Shaping：By step（4）Soap stick together input billet cutter in be squeezed into cylindrical soap body.
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