CN107541365A - Cocoon shells silk camellia handmade soap through desensitization process and preparation method thereof - Google Patents
Cocoon shells silk camellia handmade soap through desensitization process and preparation method thereof Download PDFInfo
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- 239000000344 soap Substances 0.000 title claims abstract description 42
- 238000000034 method Methods 0.000 title claims abstract description 21
- 238000000586 desensitisation Methods 0.000 title claims abstract description 17
- 240000001548 Camellia japonica Species 0.000 title claims description 46
- 238000002360 preparation method Methods 0.000 title claims description 9
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- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 21
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Abstract
The present invention relates to a kind of Cocoon shells silk camellia handmade soap through desensitization process, it is bound up according to mass fraction by following component：12 20 parts of camellia oil, 10 20 parts of Sweet Almond Oil, 8 15 parts of grape-kernel oil, 10 18 parts of coconut oil, 10 18 parts of palm oil, 14 20 parts of deionized water, 8 12 parts of sodium hydroxide, 35 parts of Cocoon shells, 36 parts of tea seed extract solution, 0.1 0.5 parts of essence；Wherein tea seed extract solution is desensitization process.Cocoon shells silk camellia handmade soap addition desensitization tea seed extract solution+fibroin hydrolyzate completely so that handmade soap of the invention has the function that anti-inflammatory, gentle fine and smooth, deep layer Glycerin.
Description
Technical field
The present invention relates to a kind of camellia handmade soap, particularly a kind of Cocoon shells silk camellia through desensitization process is manual
Soap.
Background technology
Since 2014, handmade soap product is a dark horse washing shield product market, and all kinds of vegetable fat collocation plants carry
Thing is taken to apply in handmade soap and more and more common, using tea oil as main glyceride stock collocation fibroin hydrolyzate and tea seed
The handmade soap of extract solution, there is the effects such as extraordinary anti-inflammatory, gentle fine and smooth, deep layer Glycerin, especially suitable for sensitive and
Dry skin；As a kind of natural agents, tea seed powder but has anaphylactogen so that allergy sufferers pruitus, plays erythema so that tea
Seed powder class product can not largely use tea seed powder raw material, so solving the allergen issue of tea seed powder, can just cause tea seed powder class
Product can preferably import market.
The content of the invention
An object of the present invention is to overcome existing tea seed extract solution allergic problem, there is provided a kind of silkworm through desensitization process
Cocoon shell silk camellia handmade soap, there is the effect of anti-inflammatory, anti-acne.
The second object of the present invention is the preparation for providing the above-mentioned Cocoon shells silk camellia handmade soap through desensitization process
Method.
The technical scheme is that：
A kind of Cocoon shells silk camellia handmade soap through desensitization process, it is made up according to mass fraction of following component:Camellia
Oily 12-20 parts, Sweet Almond Oil 10-20 parts, 8-15 parts of grape-kernel oil, coconut oil 10-18 parts, palm oil 10-18 parts, deionization
Water 14-20 parts, sodium hydroxide 8-12 parts, Cocoon shells 3-5 parts, tea seed extract solution 3-6 parts, essence 0.1-0.5 parts.
Preferably, described tea seed extract solution technique is specific as follows：
（1）Squeezing：Tea seed is squeezed and obtains camellia seed slag；
（2）Leach：By step（1）Camellia seed slag is obtained by n-hexane extraction, obtains the camellia seed slag that deoils；
（3）Crush：By step（2）The obtained camellia seed ground-slag that deoils is broken, is sieved through 30-100 eye mesh screens, obtains camellia seed powder；
（4）Heat extraction：Weigh step（3）Obtained tea seed powder and deionized water mixing, are heated, stirring, through 150-200 mesh after cooling
Filter-cloth filtering obtains filtrate 1；
（5）Enzymolysis：By step（4）The PH of gained filtrate 1 is adjusted to 2.5-4, adds acid protease, heating water bath to 50-60
DEG C, after 20-30min, decolorising agent is added, 80-100 DEG C is again heated to, persistently stirs 30min, cold filtration obtains filtrate 2；
（6）It is refined：By step（5）The filtrate 2 of acquisition adds filter aid, filtering, adjusts tea seed extract solution pH to 5-6, obtains clear
Clear camellia seed extract solution.
Step（4）Middle camellia seed powder and deionization mixed proportion are 1:（3-10）, 60-100 DEG C is heated to, mixing speed is
20-60 revs/min, stir 40-60 minutes.
Step（5）Middle decolorising agent and the weight ratio of filtrate 1 are（1-2）：100；Described decolorising agent is activated carbon and activity
Carclazyte, adsorption specific surface area 1000m2/g-1500m2/ g or adsorption capacity reach 80%-100%, are calculated with part by weight, activity
Charcoal：Atlapulgite=1：（3-10）.
Preferably, step（5）Described acid protease and the weight ratio of filtrate 1 are（0.1-4）：1000.
Step（5）Described acid protease is that the excellent Aspergillus usamii depth fermentation of seed selection is made.
Step（6）Diatomaceous addition is the 1-6% of the weight of filtrate 2, is filtered by leaf-type filter, obtains clarification mountain
Tea seed extract solution.
The preparation method of Cocoon shells silk camellia handmade soap of the invention through desensitization process, in turn includes the following steps：
（1）Coconut oil, palm oil, grape-kernel oil are dissolved by heating, then add camellia oil, Sweet Almond Oil, stirring and dissolving；
（2）Sodium hydroxide is dissolved in deionized water, Cocoon shells is added, after stirring, to being completely dissolved, is slowly added to walk
Suddenly（1）In obtained grease, lasting stirring, through saponification in it is thread when, add tea seed extract solution, essence, after stirring,
Reverse mould, it is stripped after shaping, handmade soap is obtained after supporting soap curing.
The beneficial effects of the present invention are：
The fibroin hydrolyzate extracted by being hydrolyzed in Cocoon shells, contain 18 kinds of amino acid and human body cell structure extremely phase
Seemingly, skin-friendly is splendid, the EGF in fibroin（EGF）And moisturizing ingredient, it can activate and Glycerin, silk
Albumen is applied to have in handmade soap the effect of gentle fine and smooth, deep layer Glycerin.
Primary raw material used in the present invention is described as follows：
Camellia seed：It is the fruit of tea oil tree.Tea oil tree is the main woody oleiferous plants tree in China, is described as " east tree ", belongs to camellia
Section's Camellia evergreen dungarunga, it is the distinctive woody vegetable oil resource in China；3-6 meters of the height of tree, the diameter of a cross-section of a tree trunk 1.3 meters above the ground is up to 24-30 lis
Rice, smooth bark is taupe；Tea oil tree list leaf alternate, flower are both sexes white, and October, Post flowering was until fruit between October next year
Can be ripe, therefore, tea oil tree has rare flowers and fruits homophyletic phenomenon；Fruit is capsule, is mostly ellipse, has fine, soft fur.Seed
Mostly yellowish-brown, glossy, triangular shape.Tea oil tree is grown in remote mountains, inhales natural nutrient to the greatest extent, evergreen longevity, the age of tree was up to 200 years
More than.
Camellia oil：Camellia seed kernel is through cleaning, air-drying（Temperature is less than 100 DEG C）, shelling, seed selection sterilization after, at 20-50 DEG C
Obtained by being squeezed, active material enriches, generally about containing vitamin E 200mg/Kg, sterol 30mg/Kg, squalene
100mg/Kg。
Sweet Almond Oil：Squeezed by apricot fruit, be a germplasm rich in mineral matter, candy thing and vitamin and protein
Ground is soft, the natural moisture preserving agent of high osmosis, has protective effect to pimples, rich and honour hand and sensitiveness skin, gentle to have again
Good skin-friendly, various skin quality are all suitable for, and can be improved dry skin and be itched phenomenon, and mitigation is ached, and anti-inflammatory, quality is softly slided
Profit；The sagging gland of brain, thymus gland and the adrenal gland of internal system can be more balanced, promotes cell turnover；Sweet Almond Oil is very salubrious, grows
Moisten skin and softening skin quality effect is good, be adapted to do whole body massage；And contain rich nutrient, can be with any vegetable oil phase intermodulation
Be good miscella；It is well suited for the sensitiveness skin that dryness, wrinkle, acne, pimples and easy allergy are itched, quality temperature
All it can be used with baby skin；The soap durable lather and moistening effect worked it out with Sweet Almond Oil are very good.
Grape-kernel oil：Grape-kernel oil has two kinds of very important elements, linolenic acid and proanthocyanidin.Linolenic acid can be with
Free radical is resisted, anti-aging, help absorbs vitamin C and E, strengthens the elasticity of the circulatory system, reduces the injury of ultraviolet, protects
Collagen in skin, improve venous engorgement and oedema, prevent melanin deposition.Proanthocyanidin has protection blood vessel elasticity, protects
Skin afflicting with great suffering torment from ultraviolet is protected, prevents the destruction of collagenous fibres and elastomer, skin is kept due elasticity and is opened
Power, skin sagging and wrinkle is avoided to produce；Grape-kernel oil penetration is strong, salubrious non-greasy, is easily absorbed by the skin, any skin quality
It is applicable.
Coconut oil：Coconut oil is the indispensable glyceride stock of perfumed soap, and produces natural acid, fatty alcohol and surface
The raw material of activating agent；It can increase the rich of foam with coconut oil soapmaking, strengthen cleaning effect.
Palm oil：Palm oil is also known as brown oily, brown skin oil, and the grease extracted by pericarp in oil palm fruit, is non-drying oil.In right amount
Collocation can increase finished product hardness in the formula of handmade soap, be that handmade soap is more stable, effectively extend the resting period.
Sodium hydroxide：As the alkali reacted with fat saponification.
Deionized water：Refer to eliminate the pure water in after ionic species impurity, International Organization for standardization ISO/TC 147 is advised
Fixed " deionization " is defined as：" deionized water is complete or incompletely removes ionic species." using the method system of RO counter-infiltrations
Take, the anion and cation gone using ion exchange resin in water removal.
Cocoon shells：Fibroin is fibrous proteins, and its molecular structure is similar to the collagenous fibres for forming skin, can
Naturally strengthen the elasticity of skin, be referred to as fiber queen, contained amino acid is a large amount of Tom Clancy Splinter Cells propagation in fibroin
Institute is required, and then can accelerate skin metabolism, prevents that wrinkle from forming, and compact skin, smooth fine and smooth；Fibroin can be strong in addition
Effect suppresses the formation of skin splash arch-criminal's tyrosinase, and skin and muscles are fair for holding, fine and smooth；And have the ability for absorbing UV light, it is average anti-
UVB abilities have 90%, and uva-resistant ability then has more than 50%；The structure of mulberry silk is extremely similar to human skin, therefore someone again
The laudatory title of body " Second Skin ".Early in the Ming Dynasty of China, silk is using the beautifying secret recipe as imperial palace highest-ranking imperial concubine, and Li Shizhen (1518-1593 A.D.) is his
Medical science monumental work《Compendium of Materia Medica》In just it is on the books, natural silk can make skin beautify, eliminate it is black dim, moreover it is possible to treat suppurative skin
Skin；Modern medicine further confirms that silk protein content is much higher than pearl, and wherein nitrogen content is higher than pearl 37 times, mainly
Amino acid content is high more than 10 times；These amino acid can directly be human hair, and skin absorbs and absorption；I.e. in human epidermal
Outer layer is easier to permeate, and accelerates the metabolism of skin.
Essence：The smell of finished product is adjusted, is allowed to pleasant comfortable.
Embodiment
Tea seed extract solution used, is made up of following processing step in embodiment：
（1）Squeezing：Tea seed is squeezed and obtains camellia seed slag；
（2）Leach：By step（1）Camellia seed slag is obtained by n-hexane extraction, obtains the camellia seed slag that deoils；
（3）Crush：By step（2）The obtained camellia seed ground-slag that deoils is broken, is sieved through 50 eye mesh screens, obtains camellia seed powder；
（4）Heat extraction：Weigh step（3）Obtained tea seed powder and deionized water mixing, camellia seed powder and deionization mixed proportion are
1:4, heat, stirring, filtrate 1 is obtained through 150-200 mesh filter-cloth filterings after cooling；
（5）Enzymolysis：By step（4）The PH of gained filtrate 1 is adjusted to 3, adds acid protease（Acid protease is that seed selection is excellent
Aspergillus usamii is made through depth fermentation, and the weight ratio with filtrate 1 is 0.5：1000）, heating water bath is to 55 DEG C, addition decolorising agent
Activated carbon and atlapulgite, average adsorption specific surface area are respectively 1200m2/ g and 1300m2/ g, is calculated with part by weight, activity
Charcoal：Atlapulgite=1：（3-10）, the weight ratio of decolorising agent and filtrate 1 is 2：100；80 DEG C are again heated to, lasting stirring, cooling
Filter to get filtrate 2；
（6）It is refined：By step（5）The filter aid diatomite of the addition of filtrate 2 3% of acquisition, adjusts tea seed extract solution pH to 5.5, mistake
Filter, obtain clarification camellia seed extract solution.
Above-mentioned tea seed extract solution is subjected to patch test, patch test results are without allergic reaction；Method of testing is as follows:
Step 1：The gauze of four thickness is cut into a diameter of 1cm circle with scissors, totally 8, draws 25uL's respectively with liquid-transfering gun
Tea seed extract solution, is dropped on circular gauze, and blank is done with deionized water；
Step 2：The gripping of gauze tweezers is placed on subject（To tea seed extract solution allergy sufferers）At anteflexion arm, adhesive tape is used
Fix, start timing；
Step 3：Torn after 48h adhesive tape, and observe the reaction of skin at gauze covering immediately.
Embodiment 1
Handmade soap preparation method is as follows：
170 grams of coconut oil is weighed, 150 grams of palm oil, 90 grams of grape-kernel oil, is dissolved by heating, adds 200 grams of camellia oil, dessert almond
There are 170 grams, stirring and dissolving, weigh 90 grams of sodium hydroxide, be dissolved in 175 grams of deionized waters, add 4 grams of Cocoon shells, stirring is equal
After even, to being completely dissolved, be slowly added in grease, lasting stirring, through saponification in it is thread when, add above-mentioned tea seed extract solution
40 grams, 2 grams of essence, after stirring, reverse mould, it is stripped after shaping, 994 grams of handmade soap solid is obtained after supporting soap curing.
Embodiment 2-5
Embodiment 2-5, comparative example 1-2 handmade soap, its preparation process condition simply reaction raw materials and are matched somebody with somebody substantially with embodiment 1
The conditions such as material ratio are slightly different, specifically as listed in table 1.
The embodiment 1-5 of table 1, comparative example 1-2 Cocoon shells silk camellia handmade soap preparation method
。
Comparative example 3
Comparative example 3 eliminates Cocoon shells on the basis of embodiment 1, and tea seed extract solution dosage is 44 grams, other and embodiment 1
It is identical.
Comparative example 4
Comparative example 4 eliminates tea seed extract solution on the basis of embodiment 1, and Cocoon shells dosage is 44 grams, other and embodiment 1
It is identical.
Comparative example 5
Comparative example 5 is only in that tea seed extraction liquid and preparation method thereof is different from the difference of embodiment 1.
Tea seed extract solution used in comparative example 5, is made up of following processing step：
（1）Squeezing：Tea seed is squeezed and obtains camellia seed slag；
（2）Leach：By step（1）Camellia seed slag is obtained by n-hexane extraction, obtains the camellia seed slag that deoils；
（3）Crush：By step（2）The obtained camellia seed ground-slag that deoils is broken, is sieved through 50 eye mesh screens, obtains camellia seed powder；
（4）Heat extraction：Weigh step（3）Obtained tea seed powder and deionized water mixing, are heated, stirring, through 150-200 mesh after cooling
Filter-cloth filtering obtains filtrate；
（5）It is refined：By step（4）The filter aid diatomite of the filtrate addition 3% of acquisition, filtering, adjustment tea seed extract solution pH are arrived
5.5, obtain clarification camellia seed extract solution.
After handmade soap obtained by embodiment 1-5, comparative example 1-5 is stood into 48 hours, depanning, it is placed at shady and cool ventilation,
Its pH value is tested every a couple of days, when pH is reduced to below 10.5, it is tested and moistens moisturizing, anti-inflammatory anti-itch effect；Specifically it is shown in Table
2。
Its functional attributes test result of handmade soap obtained by the embodiment 1-5 of table 2, comparative example 1-5
。
The method of testing of the moist performance of keeping humidity of handmade soap is tested for hand skin obtained by embodiment 1-5, comparative example 1-5,
Specific method：By the camellia handmade soap obtained by embodiment 1-5, comparative example 1-5, got blisters with the net of getting blisters drenched, treat that foam has filled
Point abundant to observe depth of foam, then rinse hand with clear water when be further added by, record was rinsed to the clean time, to not having
Untill having glutinous soapy feeling, with clean towel water purification beads, the back of the hand portion moisture is detected with digital skin moisture detector after half an hour
Value（Note：The back of the hand portion moisture value is detected before being washed one's hands using handmade soap, and is recorded）；Statistical result such as table 3.
The embodiment 1-5 of table 3, comparative example 1-5 handmade soap trial effects
。
From table 3, it can be seen that moisture retention comes from the addition of silk cocoon albumen and tea oil, and moistness is more preferable.
Embodiment 1-5, comparative example 1-5 Cocoon shells silk camellia craft saponaria vaccaria anti-acne effect method of testing are as follows：
Embodiment 1-5, comparative example 1-5 Cocoon shells silk camellia handmade soap are chosen into 20 respectively the on probation of whelk
Person, try out two months, count rehabilitation situation quantity, statistical conditions such as table 4.
The camellia craft saponaria vaccaria anti-acne effect quantity statistics table of table 4
。
From table 4, it can be seen that recovery of the addition of camellia oil and tea seed extract solution to slight dermatitis patients has clearly
Effect, addition is bigger, and effect is better, arrange in pairs or groups tea seed extract solution after effect it is more preferable.
Claims (8)
1. a kind of Cocoon shells silk camellia handmade soap through desensitization process, it is made up according to mass fraction of following component:Mountain
Tea oil 12-20 parts, Sweet Almond Oil 10-20 parts, 8-15 parts of grape-kernel oil, coconut oil 10-18 parts, palm oil 10-18 parts, go from
Sub- water 14-20 parts, sodium hydroxide 8-12 parts, Cocoon shells 3-5 parts, tea seed extract solution 3-6 parts, essence 0.1-0.5 parts.
2. the Cocoon shells silk camellia handmade soap according to claim 1 through desensitization process, it is characterised in that described
Tea seed extraction liquid preparing process is specific as follows：
（1）Squeezing：Tea seed is squeezed and obtains camellia seed slag；
（2）Leach：By step（1）Camellia seed slag is obtained by n-hexane extraction, obtains the camellia seed slag that deoils；
（3）Crush：By step（2）The obtained camellia seed ground-slag that deoils is broken, is sieved through the eye mesh screen of 30 mesh -100, obtains camellia seed
Powder；
（4）Heat extraction：Weigh step（3）Obtained tea seed powder and deionized water mixing, are heated, stirring, through 150-200 mesh after cooling
Filter-cloth filtering obtains filtrate 1；
（5）Enzymolysis：By step（4）The pH value of gained filtrate 1 is adjusted to 2.5-4, adds acid protease, heating water bath to 50-
60 DEG C, after 20-30min, decolorising agent is added, 80-100 DEG C is again heated to, persistently stirs 30min, cold filtration obtains filtrate 2；
（6）It is refined：By step（5）The filtrate 2 of acquisition adds filter aid, filtering, adjustment tea seed extracting liquid pH value to 5-6, obtains
Clarify camellia seed extract solution.
3. the Cocoon shells silk camellia handmade soap according to claim 2 through desensitization process, it is characterised in that step（4）
Middle camellia seed powder and deionization mixed proportion are 1:（3-10）, 60 DEG C -100 DEG C are heated to, mixing speed is 20-60 revs/min,
Stir 40-60 minutes.
4. the Cocoon shells silk camellia handmade soap according to claim 2 through desensitization process, it is characterised in that step（5）
Described acid protease is that the excellent Aspergillus usamii of seed selection is made through depth fermentation, and the weight ratio with filtrate 1 is（0.1-4）：
1000。
5. the Cocoon shells silk camellia handmade soap according to claim 2 through desensitization process, it is characterised in that step（5）
Middle decolorising agent and the weight ratio of filtrate 1 are（1-2）：100；Described decolorising agent is activated carbon and atlapulgite, and surface is compared in absorption
Product 1000-1500m2/ g or adsorption capacity reach 80%-100%, are calculated with part by weight, activated carbon：Atlapulgite=1：（3-
10）.
A kind of 6. Cocoon shells silk camellia handmade soap according to claim 2, it is characterised in that step（5）Described in
The weight ratio of decolorising agent and tea seed powder is（1-2）：10.
7. the Cocoon shells silk camellia handmade soap according to claim 2 through desensitization process, it is characterised in that step（6）
Diatomaceous addition is the 1-6% of the weight of filtrate 2, is filtered by leaf-type filter, obtains clarification camellia seed extract solution.
8. the preparation method of the Cocoon shells silk camellia handmade soap through desensitization process, its feature exist according to claim 1
In in turn including the following steps：
（1）Coconut oil, palm oil, grape-kernel oil are dissolved by heating, then add camellia oil, Sweet Almond Oil, stirring and dissolving；
（2）Sodium hydroxide is dissolved in deionized water, Cocoon shells is added, after stirring, to being completely dissolved, is slowly added to walk
Suddenly（1）In obtained grease, lasting stirring, through saponification in it is thread when, add tea seed extract solution, essence, after stirring,
Reverse mould, it is stripped after shaping, handmade soap is obtained after supporting soap curing.
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| CN111411027A (en) * | 2020-03-24 | 2020-07-14 | 扬州日光生物科技有限公司 | Plant faint scent clothing washing and protecting soap and preparation method and use method thereof |
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