CN110693789A - Natural plant grapefruit essence shampoo and preparation method thereof - Google Patents
Natural plant grapefruit essence shampoo and preparation method thereof Download PDFInfo
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- CN110693789A CN110693789A CN201911138732.6A CN201911138732A CN110693789A CN 110693789 A CN110693789 A CN 110693789A CN 201911138732 A CN201911138732 A CN 201911138732A CN 110693789 A CN110693789 A CN 110693789A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/70—Biological properties of the composition as a whole
- A61K2800/72—Hypo-allergenic
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
Abstract
The invention relates to the technical field of deep processing of pomelos, in particular to natural plant pomelo essence shampoo and a preparation method thereof, wherein the formula of the natural plant pomelo essence shampoo comprises 15-25% of sodium laureth sulfate, 5-10% of disodium cocoyl amphodiacetate, 3-8% of sodium lauroyl sarcosinate, 3-8% of sodium laureth sulfate, 1-4% of coconut diethanolamide, 231-4% of laureth, 1-3% of allantoin, 0.1-0.3% of citric acid, 8-15% of natural plant extracts, deionized water and the like, wherein the natural plant extracts comprise 2-4% of pomelo flower pure dew, 2-4% of pomelo peel powder, 1-3% of pomelo essential oil, 2-4% of pomelo fruit extracts and 1-3% of tea seed extracts. The grapefruit flower hydrolat, the grapefruit peel powder and the grapefruit essential oil which are prepared by taking the grapefruit peel as the raw material are added into the formula, and the prepared shampoo has the unique effects of nourishing, moistening, protecting hair and the like, is easy to absorb, cannot cause irritant damage to hair and scalp, is easy to process, and can realize industrial application of the grapefruit peel.
Description
Technical Field
The invention relates to the technical field of deep processing of pomelos, and in particular relates to natural plant pomelo essence shampoo and a preparation method thereof.
Background
Shampoo is also called shampoo, and is a cosmetic product for basic hair and scalp care in daily use. The shampoo contains various components, and the combined action of the components can play a role in cleaning scalp and hair. With the increasing emphasis on the safety, health and effectiveness of cosmetics, especially natural plant cosmetics taking extracts from natural plants as raw materials, the natural plant cosmetics not only can clean and protect human hair and scalp, but also can not cause irritant damage to hair and scalp. Therefore, on the premise of ensuring the product functionality, consumers are more willing to buy shampoos which are added with natural materials to replace artificially synthesized chemical components, and are more scientific and environment-friendly.
The pomelo is a mature fruit of the grapefruit which is a rutaceae plant, is produced in the southern area of China, is sour, sweet, cool and moist, and is rich in nutrition; both pericarp and pomelo flower can be used as medicine. Wherein, the soil temperature, the soil moisture and the soil pH of Meizhou Yuedong are suitable for the growth and development of the pomelo, so the golden pomelo produced in Meizhou has large fruit and beautiful appearance; the peel is smooth, even and clean; the pulp is sweet and tasty, and has a honey taste, so it is known as "the king of shaddock". The pomelo is rich in nutrient substances and high in medicinal value, particularly the pomelo peel is rich in various active polysaccharides, flavones, pectins, natural pigments and other active ingredients beneficial to health, and the content of the active ingredients is higher than that of the pomelo fruit, and the pomelo peel contains more pomelo oil, and the purely natural pomelo essential oil can be obtained by extraction. However, after the grapefruits are eaten and processed by people, the grapefruits still have 20 to 30 percent of fresh weight of the grapefruits, which cannot be utilized. Most of the shaddock peels are dried in the sun, burned or directly thrown away as wastes, which not only causes serious pollution to the ecological environment, but also greatly wastes abundant resources in the shaddock peels. Therefore, how to fully utilize a large amount of shaddock peel to develop a novel shampoo which is natural in raw materials, capable of moistening and protecting hair and simple in process is a development direction for really realizing large-scale and industrial application of shaddock peel.
Disclosure of Invention
The invention aims to provide a natural plant pomelo essence shampoo and a preparation method thereof, aiming at the defects in the prior art, the method takes pomelo peel as raw material to prepare the pomelo flower pure shampoo, the pomelo peel powder and the pomelo essential oil which are added into a formula, and the prepared shampoo not only has unique efficacies of nourishing, moistening, protecting hair and the like, but also can not cause irritant damage to hair and scalp, and is easy to process and realizes the industrial application of the pomelo peel.
The purpose of the invention is realized by the following technical scheme:
the natural plant grapefruit essence shampoo is provided and is prepared from the following raw materials in percentage by mass:
15-25% of sodium lauryl ether sulfate, 5-10% of disodium cocoyl amphoteric diacetate, 3-8% of sodium lauroyl sarcosinate, 3-8% of sodium lauryl ether sulfate, 3-8% of cocamidopropyl betaine, 1-4% of coconut diethanolamide, 231-4% of laureth, 1-3% of allantoin, 1-3% of guar hydroxypropyl trimethyl ammonium chloride, 1-3% of polydimethylsiloxane, 1-3% of dodecyl benzene sulfonic acid TEA salt, 1-3% of acrylic acid (ester)/C10-30 alkyl acrylate cross-linked polymer, 0.1-0.3% of essence, 0.1-0.3% of citric acid, 100.2-0.4% of polyquaternium, 60.2-0.4% of polyquaternium, and 0.2-0.4% of DMDM hydantoin, 0.2 to 0.4 percent of methyl chloro isothiazolinone, 0.1 to 0.3 percent of methyl isothiazolinone, 0.1 to 0.3 percent of magnesium chloride, 0.1 to 0.3 percent of magnesium nitrate, 8 to 15 percent of natural plant extract and the balance of deionized water; wherein:
the natural plant extract is composed of 2-4% of shaddock flower hydrosol, 2-4% of shaddock peel powder, 1-3% of shaddock essential oil, 2-4% of shaddock fruit extract and 1-3% of tea seed extract.
In the technical scheme, the natural plant grapefruit essence shampoo is prepared from the following raw materials in percentage by mass:
20% of sodium lauryl polyether sulfate, 8% of disodium cocoyl amphodiacetate, 6% of sodium lauroyl sarcosinate, 5% of sodium lauryl sulfate, 5% of cocamidopropyl betaine, 2% of coconut diethanolamide, 232% of laureth, 2% of allantoin, 2% of guar hydroxypropyl trimonium chloride, 2% of polydimethylsiloxane, 2% of dodecylbenzene sulfonic acid TEA salt, 2% of acrylic acid (ester)/C10-30 alkanol acrylate crosspolymer, 0.2% of essence, 0.2% of citric acid, 100.3% of polyquaternium, 60.3% of polyquaternium, 0.3% of DMDM hydantoin, 0.3% of methyl chloro isothiazolinone, 0.2% of methyl isothiazolinone, 0.1% of magnesium chloride, 0.1% of magnesium nitrate, 10% of natural plant extract and 30% of deionized water;
the natural plant extract is composed of 2% of shaddock flower hydrolat, 2% of shaddock peel powder, 2% of shaddock fruit extract, 2% of shaddock essential oil and 2% of tea seed extract.
In the technical scheme, the shaddock flower hydrolat is prepared by distilling 3-8 parts of shaddock flower, 3-8 parts of Meizhou golden shaddock peel and 80-120 parts of purified water.
In the technical scheme, the grapefruit essential oil is prepared by distilling and extracting fresh grapefruit peel of Meizhou.
In the technical scheme, the shaddock peel powder is prepared by soaking, drying and grinding fresh Meizhou golden shaddock peel.
The invention also provides a preparation method of the natural plant grapefruit essence shampoo, which comprises the following steps:
step a, picking fresh pomelo fruits of Meizhou gold pomelo for 3-5 months, cleaning the outer peel of the pomelo fruits, and then cutting the outer peel of the pomelo from outside to inside to obtain the Meizhou gold pomelo peel for later use;
step b, preparing grapefruit ferment:
taking 15-25 parts of brown sugar, 8-12 parts of brown sugar, 2-4 parts of brown sugar or honey, 75-85 parts of Meizhou golden pomelo peel, 8-12 parts of orange peel, 3-8 parts of orange peel, 2-4 parts of tea seeds, 0.5-1.5 parts of pomelo flower, 0.1-0.3 part of pomelo leaf, 0.1-0.3 part of rose and 8-12 parts of purified water, uniformly mixing, filling the pomelo into a sealed container, naturally fermenting for 1-3 years, and filtering to obtain the ferment;
step c, preparing the shaddock flower hydrolat:
taking 3-8 parts of shaddock flower and 3-8 parts of Meizhou golden shaddock peel, adding 80-120 parts of purified water, and distilling at 95-100 ℃ for 2-3h to obtain shaddock flower hydrolat;
step d, preparing the grapefruit essential oil:
d1) shredding the gold pomelo peels of the Meizhou in the step a1, and then soaking the shredded gold pomelo peels in the pomelo enzyme for a period of time (20-40 min);
d2) drying the soaked pomelo peel, grinding into powder, and placing into an extraction kettle for supercritical CO2Extracting, and collecting the grapefruit essential oil after extraction is finished;
step e, preparing pomelo peel powder:
e1) taking the Meizhou golden pomelo peels obtained in the step a1, cutting the pomelo peels with the thickness of 2-4mm from outside to inside, removing black spots on the pomelo peels, then cutting the pomelo peels into slices, putting the slices into the pomelo ferment, soaking for a period of time, rinsing with clear water, and drying in the air;
e2) soaking sliced pericarpium Citri Grandis in 75-85 deg.C hot water for 11-13h, and further soaking in clear water for 11-13h for debitterizing treatment;
e3) dehydrating the debitterized shaddock peel, and then drying;
e4) grinding the dried shaddock peel, and sieving to obtain shaddock peel powder;
step f, preparing the shampoo:
f1) according to the formula amount, uniformly mixing the shaddock flower hydrosol, the shaddock peel powder, the shaddock essential oil, the shaddock fruit extract and the tea seed extract to obtain a natural plant extract;
f2) according to the formula, sodium laureth sulfate, disodium cocoyl amphodiacetate, sodium lauroyl sarcosinate, sodium laureth sulfate, cocamidopropyl betaine, cocoanut oil diethanolamide, laureth-23, allantoin, guar hydroxypropyl trimethyl ammonium chloride, polydimethylsiloxane, dodecyl benzene sulfonic acid TEA salt, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer and deionized water are stirred and mixed, heating to 65-75 deg.C, slowly adding natural plant extract while stirring, adding essence, citric acid, polyquaternium-10, polyquaternium-6, DMDM hydantoin, methylchloroisothiazolinone, methylisothiazolinone, magnesium chloride and magnesium nitrate, stirring, bottling, and sterilizing to obtain natural plant fructus Citri Grandis essence shampoo.
In the technical scheme, in the steps d1 and e1, the soaking time is 20-40 min.
In the above technical scheme, in the step d2, the extraction temperature is 35-40 ℃, the extraction pressure is 9-15MPa, the extraction time is 30-45min, and CO is added2The flow rate is 30-38L/h.
In the technical scheme, in the step e3, the dehydration time is 4-6 min; the drying temperature is 60-90 ℃ and the drying time is 14-16 h.
In the above technical solution, in the step e4, the mesh number of the sieve is 200-400 meshes.
The invention has the beneficial effects that:
the invention relates to a natural plant grapefruit essence shampoo and a preparation method thereof, wherein the formula comprises 15-25% of sodium laureth sulfate, 5-10% of disodium cocoyl amphodiacetate, 3-8% of sodium lauroyl sarcosinate, 3-8% of sodium lauryl sulfate, 3-8% of cocamidopropyl betaine, 1-4% of coconut diethanolamide, 231-4% of laureth, 1-3% of allantoin, 1-3% of guar hydroxypropyl trimethyl ammonium chloride, 1-3% of polydimethylsiloxane, 1-3% of dodecyl benzene sulfonate TEA, 1-3% of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.1-0.3% of essence, 0.1-0.3% of citric acid, 100.2-0.4% of polyquaternium, and, 60.2 to 0.4 percent of polyquaternium, 0.2 to 0.4 percent of DMDM hydantoin, 0.2 to 0.4 percent of methylchloroisothiazolinone, 0.1 to 0.3 percent of methylisothiazolinone, 0.1 to 0.3 percent of magnesium chloride, 0.1 to 0.3 percent of magnesium nitrate, 8 to 15 percent of natural plant extract and the balance of deionized water; wherein the natural plant extract comprises 2-4% of shaddock flower hydrosol, 2-4% of shaddock peel powder, 1-3% of shaddock essential oil, 2-4% of shaddock fruit extract and 1-3% of tea seed extract. Compared with the prior art, the invention has the following advantages: (1) the formula is added with the grapefruit flower hydrolat, the grapefruit peel powder and the grapefruit essential oil in scientific proportions, the three components are all prepared by taking the grapefruit peel of a Meizhou gold grapefruit picked for 3-5 months as a raw material, a large amount of physiologically active substances such as naringin contained in the grapefruit peel are extracted through special process treatment on the grapefruit peel, particularly the grapefruit essential oil extracted through supercritical extraction, the active substances have strong permeability and can permeate 3 microns on the surface layer of skin, and multiple unique effects such as moistening, moisture-preserving and oil-regulating, anti-inflammatory and antibacterial, anti-allergy, antioxidation and the like are realized through the synergistic effect of the grapefruit essential oil and other components; (2) the shaddock peel is soaked and cleaned by the specially-made shaddock enzyme, the shaddock enzyme is prepared by naturally fermenting shaddock peel pomace and the like, and can generate a large amount of active enzyme and thoroughly remove pesticide residues, bacteria, worm eggs, viruses and the like on the shaddock peel, so that the active ingredients extracted from the shaddock peel have natural, pollution-free and non-irritant qualities; (3) the preparation method disclosed by the invention is simple in preparation process, good in stability, low in equipment requirement, short in production period and high in yield, so that large-scale and industrial application of the shaddock peel is realized.
Detailed Description
The present invention will be described in further detail with reference to the following examples, but the present invention is not limited thereto.
Example 1:
the preparation method of the natural plant grapefruit essence shampoo comprises the following steps:
step a, picking fresh pomelo fruits of Meizhou gold pomelo for 3-5 months, cleaning the outer peel of the pomelo fruits, and then cutting the outer peel of the pomelo from outside to inside to obtain the Meizhou gold pomelo peel for later use;
step b, preparing grapefruit ferment:
taking 15 parts by weight of brown sugar, 8 parts by weight of brown sugar, 2 parts by weight of yellow sugar, 75 parts by weight of golden pomelo peel, 8 parts by weight of orange peel, 3 parts by weight of orange peel, 2 parts by weight of tea seeds, 1 part by weight of pomelo flower, 0.5 part by weight of pomelo leaf, 0.3 part by weight of rose and 8 parts by weight of purified water, uniformly mixing, putting into a sealed container, naturally fermenting for 1 year, and then filtering to obtain pomelo ferment;
step c, preparing the shaddock flower hydrolat:
taking 3 parts of shaddock flower and 3 parts of Meizhou golden shaddock peel, adding 80 parts of purified water, and then distilling 2 at 100 ℃ to obtain shaddock flower hydrolat;
step d, preparing the grapefruit essential oil:
d1) shredding the preserved golden pomelo peels obtained in the step a1, and then soaking the shredded golden pomelo peels in pomelo enzyme for 20 min;
d2) drying the soaked pomelo peel, grinding into powder, and placing into an extraction kettle for supercritical CO2Extracting at 35 deg.C under 9MPa for 30min with CO2The flow rate is 30L/h, and after extraction is finished, the grapefruit essential oil is collected;
step e, preparing pomelo peel powder:
e1) taking the Meizhou golden pomelo peels in the step a1, cutting the pomelo peels with the thickness of 2-4mm from outside to inside, removing black spots on the pomelo peels, then cutting the pomelo peels into slices, soaking the slices in pomelo enzymes for 20min, rinsing with clear water, and drying in the air;
e2) soaking sliced pericarpium Citri Grandis in 75 deg.C hot water for 13h, and further soaking in clear water for 13h for debittering;
e3) dehydrating the debitterized shaddock peel for 4 min; then drying is carried out, the drying temperature is 60 ℃, and the drying time is 16 h;
e4) grinding the dried shaddock peel, and sieving with a 200-mesh and 400-mesh sieve to obtain shaddock peel powder;
step f, preparing the shampoo:
f1) uniformly mixing 4% of shaddock flower hydrolat, 3% of shaddock peel powder, 3% of shaddock essential oil, 4% of shaddock extract and 1% of tea seed extract by mass percent to obtain a natural plant extract;
f2) according to mass percentage, 25 percent of sodium laureth sulfate, 5 percent of disodium cocoyl amphoteric diacetate, 3 percent of sodium lauroyl sarcosinate, 6 percent of sodium laureth sulfate, 3 percent of cocamidopropyl betaine, 4 percent of coconut diethanolamide, 231 percent of laureth, 3 percent of allantoin, 1 percent of guar hydroxypropyltrimonium chloride, 1 percent of polydimethylsiloxane, 1 percent of dodecylbenzene sulfonate TEA salt, 3 percent of acrylic acid (ester) type/C10-30 alkanol acrylate cross-linked polymer and 26.5 percent of deionized water are stirred and mixed, then the temperature is increased to 65 ℃, the natural plant extract is slowly added while stirring, and finally 0.1 percent of essence, 0.3 percent of citric acid, 100.4 percent of polyquaternium salt, 60.2 percent of polyquaternium salt, 0.4 percent of DMDM hydantoin, 0.4 percent of methyl chloro isothiazolinone and 0.3 percent of methyl isothiazolinone are added, 0.2 percent of magnesium chloride and 0.2 percent of magnesium nitrate, and after being uniformly stirred, the natural plant grapefruit essence shampoo is prepared by filling and sterilization.
Example 2:
the preparation method of the natural plant grapefruit essence shampoo comprises the following steps:
step a, picking fresh pomelo fruits of Meizhou gold pomelo for 3-5 months, cleaning the outer peel of the pomelo fruits, and then cutting the outer peel of the pomelo from outside to inside to obtain the Meizhou gold pomelo peel for later use;
step b, preparing grapefruit ferment:
according to the weight parts, 20 parts of brown sugar, 10 parts of brown sugar, 3 parts of honey, 80 parts of golden pomelo peel in Meizhou, 10 parts of orange peel, 5 parts of orange peel, 3 parts of tea seeds, 0.5 part of pomelo flower, 0.8 part of pomelo leaf, 0.8 part of rose and 10 parts of purified water are uniformly mixed and then are put into a sealed container for natural fermentation for 3 years, and then the mixture is filtered to obtain pomelo ferment;
step c, preparing the shaddock flower hydrolat:
taking 8 parts of shaddock flower and 8 parts of Meizhou golden shaddock peel, adding 120 parts of purified water, and distilling at 95 ℃ for 3 hours to obtain shaddock flower hydrolat;
step d, preparing the grapefruit essential oil:
d1) shredding the preserved golden pomelo peels obtained in the step a1, and then soaking the shredded golden pomelo peels in pomelo enzyme for 40 min;
d2) drying the soaked pomelo peel, grinding into powder, and placing into an extraction kettle for supercritical CO2Extracting at 40 deg.C under 15MPa for 30min with CO2The flow rate is 38L/h, and after extraction is finished, the grapefruit essential oil is collected;
step e, preparing pomelo peel powder:
e1) taking the Meizhou golden pomelo peel in the step a1, cutting the pomelo peel with the thickness of 2-4mm from outside to inside, removing black spots on the pomelo peel, then cutting the pomelo peel into slices, soaking the slices in pomelo ferment for 40min, rinsing with clear water, and drying in the air;
e2) soaking sliced pericarpium Citri Grandis in 85 deg.C hot water for 11h, and further soaking in clear water for 11h for debitterizing treatment;
e3) dehydrating the debitterized shaddock peel for 6 min; then drying is carried out, the drying temperature is 90 ℃, and the drying time is 14 h;
e4) grinding the dried shaddock peel, and sieving with a 200-mesh and 400-mesh sieve to obtain shaddock peel powder;
step f, preparing the shampoo:
f1) uniformly mixing 3% of shaddock flower hydrolat, 4% of shaddock peel powder, 1% of shaddock essential oil, 3% of shaddock fruit extract and 3% of tea seed extract according to mass percentage to obtain a natural plant extract;
f2) according to the mass percentage, 15 percent of sodium laureth sulfate, 7 percent of disodium cocoyl amphoteric diacetate, 8 percent of sodium lauroyl sarcosinate, 3 percent of sodium laureth sulfate, 6 percent of cocamidopropyl betaine, 1 percent of coconut diethanolamide, 233 percent of laureth, 1 percent of allantoin, 3 percent of guar hydroxypropyltrimonium chloride, 3 percent of polydimethylsiloxane, 2 percent of dodecylbenzene sulfonate TEA salt, 1 percent of acrylic acid (ester) type/C10-30 alkanol acrylate cross-linked polymer and 30.9 percent of deionized water are stirred and mixed, then the temperature is raised to 75 ℃, the natural plant extract is slowly added while stirring, and finally 0.3 percent of essence, 0.1 percent of citric acid, 100.2 percent of polyquaternium salt, 60.4 percent of polyquaternium salt, 0.2 percent of DMDM hydantoin, 0.2 percent of methyl chloro isothiazolinone, 0.1 percent of methyl isothiazolinone, 0.1 percent of sodium lauryl sarcosinate, 8 percent of sodium lauryl sarcosinate, 3 percent of, 0.3 percent of magnesium chloride and 0.3 percent of magnesium nitrate, and after being uniformly stirred, the natural plant grapefruit essence shampoo is prepared by filling and sterilization.
Example 3:
the preparation method of the natural plant grapefruit essence shampoo comprises the following steps:
step a, picking fresh pomelo fruits of Meizhou gold pomelo for 3-5 months, cleaning the outer peel of the pomelo fruits, and then cutting the outer peel of the pomelo from outside to inside to obtain the Meizhou gold pomelo peel for later use;
step b, preparing grapefruit ferment:
according to the weight parts, 25 parts of brown sugar, 12 parts of brown sugar, 4 parts of yellow sugar, 85 parts of golden pomelo peel in Meizhou, 12 parts of orange peel, 8 parts of orange peel, 4 parts of tea seeds, 1.5 parts of pomelo flower, 0.8 part of pomelo leaf, 0.8 part of rose and 12 parts of purified water are uniformly mixed, put into a sealed container and naturally fermented for 3 years, and then filtered to obtain pomelo ferment;
step c, preparing the shaddock flower hydrolat:
taking 5 parts of shaddock flower and 6 parts of Meizhou golden shaddock peel, adding 100 parts of purified water, and distilling at the temperature of 98 ℃ for 2.5 hours to obtain shaddock flower hydrolat;
step d, preparing the grapefruit essential oil:
d1) shredding the preserved golden pomelo peels obtained in the step a1, and then soaking the shredded golden pomelo peels in pomelo enzyme for 30 min;
d2) drying the soaked pomelo peel, grinding into powder, and placing into an extraction kettle for supercritical CO2Extracting at 38 deg.C under 12MPa for 35min with CO2The flow rate is 32L/h, and after extraction is finished, the grapefruit essential oil is collected;
step e, preparing pomelo peel powder:
e1) taking the Meizhou golden pomelo peel in the step a1, cutting the pomelo peel with the thickness of 2-4mm from outside to inside, removing black spots on the pomelo peel, then cutting the pomelo peel into slices, soaking the slices in pomelo ferment for 30min, rinsing with clear water, and drying in the air;
e2) soaking sliced pericarpium Citri Grandis in 78 deg.C hot water for 12h, and further soaking in clear water for 12h for debittering;
e3) dehydrating the debitterized shaddock peel for 5 min; then drying is carried out, the drying temperature is 70 ℃, and the drying time is 15 h;
e4) grinding the dried shaddock peel, and sieving with a 200-mesh and 400-mesh sieve to obtain shaddock peel powder;
step f, preparing the shampoo:
f1) uniformly mixing 2% of the shaddock flower hydrolat, 2% of the shaddock peel powder, 2% of the shaddock fruit extract, 2% of the shaddock essential oil and 2% of the tea seed extract according to the mass percentage to obtain a natural plant extract;
f2) according to mass percentage, 20 percent of sodium laureth sulfate, 8 percent of disodium cocoyl amphoteric diacetate, 6 percent of sodium lauroyl sarcosinate, 5 percent of sodium laureth sulfate, 5 percent of cocamidopropyl betaine, 2 percent of coconut diethanolamide, 232 percent of laureth, 2 percent of allantoin, 2 percent of guar gum hydroxypropyl trimethyl ammonium chloride, 2 percent of polydimethylsiloxane, 2 percent of dodecylbenzene sulfonate TEA salt, 2 percent of acrylic acid (ester) type/C10-30 alkanol acrylate cross-linked polymer and 30 percent of deionized water are stirred and mixed, then the temperature is increased to 70 ℃, the natural plant extract is slowly added while stirring, and finally 0.2 percent of essence, 0.2 percent of citric acid, 100.3 percent of polyquaternium, 60.3 percent of polyquaternium, 0.3 percent of DMDM hydantoin, 0.3 percent of methyl chloro isothiazolinone and 0.2 percent of methyl isothiazolinone are added, 0.1 percent of magnesium chloride and 0.1 percent of magnesium nitrate, and after being uniformly stirred, the natural plant grapefruit essence shampoo is prepared by filling and sterilization.
Example 4:
the preparation method of the natural plant grapefruit essence shampoo comprises the following steps:
step a, picking fresh pomelo fruits of Meizhou gold pomelo for 3-5 months, cleaning the outer peel of the pomelo fruits, and then cutting the outer peel of the pomelo from outside to inside to obtain the Meizhou gold pomelo peel for later use;
step b, preparing grapefruit ferment:
according to the weight parts, 22 parts of brown sugar, 11 parts of brown sugar, 3 parts of honey, 82 parts of golden pomelo peel, 11 parts of orange peel, 6 parts of orange peel, 3 parts of tea seeds, 1.2 parts of pomelo flower, 0.6 part of pomelo leaf, 0.3 part of rose and 9 parts of purified water are taken, mixed uniformly and then put into a sealed container for natural fermentation for 1-3 years, and then filtered to obtain pomelo ferment;
step c, preparing the shaddock flower hydrolat:
taking 7 parts of shaddock flower and 5 parts of Meizhou golden shaddock peel, adding 90 parts of purified water, and distilling at 100 ℃ for 2 to obtain shaddock flower hydrolat;
step d, preparing the grapefruit essential oil:
d1) shredding the preserved golden pomelo peels obtained in the step a1, and then soaking the shredded golden pomelo peels in pomelo enzyme for 35 min;
d2) drying the soaked pomelo peel, grinding into powder, and placing into an extraction kettle for supercritical CO2Extracting at 36 deg.C under 11MPa for 40min with CO2The flow rate is 36L/h, and after extraction is finished, the grapefruit essential oil is collected;
step e, preparing pomelo peel powder:
e1) taking the Meizhou golden pomelo peels in the step a1, cutting the pomelo peels with the thickness of 2-4mm from outside to inside, removing black spots on the pomelo peels, then cutting the pomelo peels into slices, soaking the slices in pomelo enzymes for 35min, rinsing with clear water, and drying in the air;
e2) soaking sliced pericarpium Citri Grandis in 82 deg.C hot water for 12h, and further soaking in clear water for 13h for debittering;
e3) dehydrating the debitterized shaddock peel for 6 min; then drying is carried out, the drying temperature is 80 ℃, and the drying time is 15 h;
e4) grinding the dried shaddock peel, and sieving with a 200-mesh and 400-mesh sieve to obtain shaddock peel powder;
step f, preparing the shampoo:
f1) uniformly mixing 2% of the shaddock flower hydrolat, 2% of the shaddock peel powder, 1% of the shaddock essential oil, 2% of the shaddock fruit extract and 1% of the tea seed extract by mass percent to obtain a natural plant extract;
f2) according to the mass percentage, 18 percent of sodium laureth sulfate, 10 percent of disodium cocoyl amphoteric diacetate, 4 percent of sodium lauroyl sarcosinate, 8 percent of sodium laureth sulfate, 8 percent of cocamidopropyl betaine, 3 percent of coconut diethanolamide, 234 percent of laureth, 2 percent of allantoin, 3 percent of guar hydroxypropyltrimonium chloride, 2 percent of polydimethylsiloxane, 2 percent of dodecylbenzene sulfonate TEA salt, 2 percent of acrylic acid (ester) class/C10-30 alkanol acrylate cross-linked polymer and 23.4 percent of deionized water are stirred and mixed, then the temperature is increased to 72 ℃, the natural plant extract is slowly added while stirring, and finally 0.2 percent of essence, 0.1 percent of citric acid, 100.2 percent of polyquaternium salt, 60.3 percent of polyquaternium salt, 0.2 percent of DMDM hydantoin, 0.2 percent of methyl chloro isothiazolinone, 0.1 percent of methyl isothiazolinone, 0.1 percent of sodium lauryl sulfate, 4 percent of sodium lauryl sarcosinate, 8 percent of sodium, 0.2 percent of magnesium chloride and 0.1 percent of magnesium nitrate, and after being uniformly stirred, the natural plant grapefruit essence shampoo is prepared by filling and sterilization.
The above-mentioned embodiments are only for convenience of description, and are not intended to limit the present invention in any way, and those skilled in the art will understand that the technical features of the present invention can be modified or changed by other equivalent embodiments without departing from the scope of the present invention.
Claims (10)
1. A natural plant pomelo essence shampoo is characterized in that: the material is prepared from the following raw materials in percentage by mass:
15-25% of sodium lauryl ether sulfate, 5-10% of disodium cocoyl amphoteric diacetate, 3-8% of sodium lauroyl sarcosinate, 3-8% of sodium lauryl ether sulfate, 3-8% of cocamidopropyl betaine, 1-4% of coconut diethanolamide, 231-4% of laureth, 1-3% of allantoin, 1-3% of guar hydroxypropyl trimethyl ammonium chloride, 1-3% of polydimethylsiloxane, 1-3% of dodecyl benzene sulfonic acid TEA salt, 1-3% of acrylic acid (ester)/C10-30 alkyl acrylate cross-linked polymer, 0.1-0.3% of essence, 0.1-0.3% of citric acid, 100.2-0.4% of polyquaternium, 60.2-0.4% of polyquaternium, and 0.2-0.4% of DMDM hydantoin, 0.2 to 0.4 percent of methyl chloro isothiazolinone, 0.1 to 0.3 percent of methyl isothiazolinone, 0.1 to 0.3 percent of magnesium chloride, 0.1 to 0.3 percent of magnesium nitrate, 8 to 15 percent of natural plant extract and the balance of deionized water; wherein:
the natural plant extract is composed of 2-4% of shaddock flower hydrosol, 2-4% of shaddock peel powder, 1-3% of shaddock essential oil, 2-4% of shaddock fruit extract and 1-3% of tea seed extract.
2. The natural plant grapefruit essence shampoo according to claim 1, characterized in that: the material is prepared from the following raw materials in percentage by mass:
20% of sodium lauryl polyether sulfate, 8% of disodium cocoyl amphodiacetate, 6% of sodium lauroyl sarcosinate, 5% of sodium lauryl sulfate, 5% of cocamidopropyl betaine, 2% of coconut diethanolamide, 232% of laureth, 2% of allantoin, 2% of guar hydroxypropyl trimonium chloride, 2% of polydimethylsiloxane, 2% of dodecylbenzene sulfonic acid TEA salt, 2% of acrylic acid (ester)/C10-30 alkanol acrylate crosspolymer, 0.2% of essence, 0.2% of citric acid, 100.3% of polyquaternium, 60.3% of polyquaternium, 0.3% of DMDM hydantoin, 0.3% of methyl chloro isothiazolinone, 0.2% of methyl isothiazolinone, 0.1% of magnesium chloride, 0.1% of magnesium nitrate, 10% of natural plant extract and 30% of deionized water;
the natural plant extract is composed of 2% of shaddock flower hydrolat, 2% of shaddock peel powder, 2% of shaddock fruit extract, 2% of shaddock essential oil and 2% of tea seed extract.
3. The natural plant grapefruit essence shampoo according to claim 1 or 2, characterized in that: the shaddock flower hydrolat is prepared by distilling 3-8 parts of shaddock flower, 3-8 parts of Meizhou golden shaddock peel and 80-120 parts of purified water.
4. The natural plant grapefruit essence shampoo according to claim 1 or 2, characterized in that: the pomelo essential oil is prepared by distilling and extracting fresh Jinyou peel of Meizhou.
5. The natural plant grapefruit essence shampoo according to claim 1 or 2, characterized in that: the pomelo peel powder is prepared by soaking, drying and grinding fresh Meizhou golden pomelo peel.
6. The method for preparing the natural plant pomelo essence shampoo according to any one of claims 1 to 5, comprising the following steps:
step a, picking fresh pomelo fruits of Meizhou gold pomelo for 3-5 months, cleaning the outer peel of the pomelo fruits, and then cutting the outer peel of the pomelo from outside to inside to obtain the Meizhou gold pomelo peel for later use;
step b, preparing grapefruit ferment:
taking 15-25 parts of brown sugar, 8-12 parts of brown sugar, 2-4 parts of brown sugar or honey, 75-85 parts of Meizhou golden pomelo peel, 8-12 parts of orange peel, 3-8 parts of orange peel, 2-4 parts of tea seeds, 0.5-1.5 parts of pomelo flower, 0.1-0.3 part of pomelo leaf, 0.1-0.3 part of rose and 8-12 parts of purified water, uniformly mixing, filling the pomelo into a sealed container, naturally fermenting for 1-3 years, and filtering to obtain the ferment;
step c, preparing the shaddock flower hydrolat:
taking 3-8 parts of shaddock flower and 3-8 parts of Meizhou golden shaddock peel, adding 80-120 parts of purified water, and distilling at 95-100 ℃ for 2-3h to obtain shaddock flower hydrolat;
step d, preparing the grapefruit essential oil:
d1) shredding the gold pomelo peels of the Meizhou in the step a1, and then soaking the shredded gold pomelo peels in the pomelo enzyme for a period of time (20-40 min);
d2) drying the soaked pomelo peel, grinding into powder, and placing into an extraction kettle for supercritical CO2Extracting, and collecting the grapefruit essential oil after extraction is finished;
step e, preparing pomelo peel powder:
e1) taking the Meizhou golden pomelo peels obtained in the step a1, cutting the pomelo peels with the thickness of 2-4mm from outside to inside, removing black spots on the pomelo peels, then cutting the pomelo peels into slices, putting the slices into the pomelo ferment, soaking for a period of time, rinsing with clear water, and drying in the air;
e2) soaking sliced pericarpium Citri Grandis in 75-85 deg.C hot water for 11-13h, and further soaking in clear water for 11-13h for debitterizing treatment;
e3) dehydrating the debitterized shaddock peel, and then drying;
e4) grinding the dried shaddock peel, and sieving to obtain shaddock peel powder;
step f, preparing the shampoo:
f1) according to the formula amount, uniformly mixing the shaddock flower hydrosol, the shaddock peel powder, the shaddock essential oil, the shaddock fruit extract and the tea seed extract to obtain a natural plant extract;
f2) according to the formula, sodium laureth sulfate, disodium cocoyl amphodiacetate, sodium lauroyl sarcosinate, sodium laureth sulfate, cocamidopropyl betaine, cocoanut oil diethanolamide, laureth-23, allantoin, guar hydroxypropyl trimethyl ammonium chloride, polydimethylsiloxane, dodecyl benzene sulfonic acid TEA salt, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer and deionized water are stirred and mixed, heating to 65-75 deg.C, slowly adding natural plant extract while stirring, adding essence, citric acid, polyquaternium-10, polyquaternium-6, DMDM hydantoin, methylchloroisothiazolinone, methylisothiazolinone, magnesium chloride and magnesium nitrate, stirring, bottling, and sterilizing to obtain natural plant fructus Citri Grandis essence shampoo.
7. The method for preparing the natural plant pomelo essence shampoo according to claim 6, which is characterized in that: in steps d1 and e1, the soaking time is 20-40 min.
8. The method for preparing the natural plant pomelo essence shampoo according to claim 6The method is characterized in that: in step d2, the extraction temperature is 35-40 deg.C, the extraction pressure is 9-15MPa, the extraction time is 30-45min, and CO is added2The flow rate is 30-38L/h.
9. The method for preparing the natural plant pomelo essence shampoo according to claim 6, which is characterized in that: in step e3, the dehydration time is 4-6 min; the drying temperature is 60-90 ℃ and the drying time is 14-16 h.
10. The method for preparing the natural plant pomelo essence shampoo according to claim 6, which is characterized in that: in step e4, the mesh size of the sieve is 200-400 meshes.
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