CN110339108A - A kind of moisturizing efficiently adjusts the facial mask liquid and preparation method thereof of sebum secretion amount - Google Patents
A kind of moisturizing efficiently adjusts the facial mask liquid and preparation method thereof of sebum secretion amount Download PDFInfo
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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Abstract
The present invention relates to cosmetic technical fields, disclose the facial mask liquid that a kind of moisturizing efficiently adjusts sebum secretion amount, composition, the 1-5% pale flag root extracting solution, 0.5-0.6% parahydroxyacet-ophenone, 0.4-0.5%1 of sebum secretion amount, 2- hexylene glycol, 73.8-87.07% deionized water are adjusted including 3-5% glycerol, 3-5% butanediol, 0.03-0.1% hydroxyethyl cellulose, 5-10%；Wherein, the group for adjusting the composition of sebum secretion amount becomes isoflavones, Barosma betulina leaf extract, radix bardanae extracting solution, Spiraea ulmaria extract.The invention also discloses the preparation methods that a kind of moisturizing efficiently adjusts the facial mask liquid of sebum secretion amount.For the present invention, not only safety is mild, can effective moisturizing, and sebum secretion amount can be adjusted, have the effect of pore refining.
Description
Technical field
The present invention relates to cosmetic technical field, specially a kind of moisturizing efficiently adjust sebum secretion amount facial mask liquid and its
Preparation method.
Background technique
Facial mask is the important content in skin nursing, for the regular application facial mask of all kinds of skin characteristics, can make oiliness skin
Skin degreasing, coarse pore are restrained, and the skin for the gauffer that dries up restores gloss, and the inflammation of dark sore skin is inhibited.Facial mask
Skin is set to seem salubrious, smooth and pure white delicacy after use, this is because facial mask and skin generate when facial mask is coated on skin
Affinity, gradual drying with facial mask, skin temperature increases, and blood circulation is accelerated, skin-tightening and tension is reinforced, skin secretion
Sebum and moisture reverse osmosis unfold epidermis softness in cuticula, and pore instinct is opened, and the effective component in facial mask liquid penetrates into skin
It is absorbed, while facial mask is tightly connected with skin, when removing facial mask, deep layer dirt in the aging cutin, pore on skin
Also by leukorrhagia simultaneously, keep skin pure and fresh clean.
The principle of facial mask is temporarily isolating extraneous air and pollution, improves exactly using the of short duration time for being covered on face
Skin temperature, the pore expansion of skin, promotes sweat gland secretion and metabolism, increase the oxygen content of skin, be conducive to skin
The product of epidermal cell metabolism and the oil substances of accumulation are excluded, the moisture in facial mask penetrates into the cutin of skin epidermis
Layer, skin become soft, and skin is naturally bright flexible.
Pursuit with the raising and people of people's quality of the life to beauty, the requirement for facial mask is also higher and higher, though
The facial mask of right commercial type is many kinds of, but for moisturizing effect, pore refining effect and the effect for adjusting water and oil balance
Fruit is all less desirable, is not able to satisfy the needs of people.
Summary of the invention
In order to overcome above-mentioned technical problem of the existing technology, there is provided a kind of moisturizing height for the first object of the present invention
Effect adjusts the facial mask liquid of sebum secretion amount, and not only safety is mild, can effective moisturizing, and sebum secretion amount can be adjusted, had
There is the effect of pore refining.
To solve the above-mentioned problems, the present invention is achieved by following technical scheme:
A kind of moisturizing efficiently adjusts the facial mask liquid of sebum secretion amount, is made of the raw material of following mass percent:
Wherein, the composition for adjusting sebum secretion amount is mentioned comprising isoflavones, Barosma betulina leaf extract, radix bardanae
Take liquid, Spiraea ulmaria extract.
Glycerol can as the moisturizer in cosmetics, contain in glycerol molecule there are three-OH can form hydrogen with hydrone
Key can firmly lock hydrone, play moistening effect, and glycerol has apparent moisten to imitate the skin tissue of human body
Fruit can increase the dissolubility of cosmetics, it is easier to permeate；Glycerol can also repair skin barrier as moisturizer, and protect
Sheath skin adjusts the hydration function of skin, can not only increase the water content of skin, improves dry skin, for outer
The stimulation on boundary also has certain protective effect, can promote the self-regeneration of damaged cell.
Butanediol makees moisturizer and solvent in cosmetics, is the polyalcohols being gentle, is commonly used in skin care item
Moisture can be stayed in cuticula by small molecule moisturizing ingredient, have good hygroscopicity, absorbable to be equivalent to quality itself
The moisture of 12.5% (relative humidity 50%) and 38.5% (relative humidity 80%), also has certain bacteriostasis, and addition exists
In skin care item moisturizing safety it is good, it is salubrious, without stick soapy feeling.Butanediol and hydroxyethyl cellulose are combined, there is brilliant water suction
Property, it rests on skin surface after absorbing moisture and plays moisture-keeping function.
Isoflavones, Barosma betulina leaf extract, radix bardanae extracting solution, Spiraea ulmaria extract, pale flag root are mentioned
Liquid is taken to carry out scientific compatibility, coordinative role, the flavonoids being rich in by said extracted object (predominantly flavones, isoflavones, petroselinum
Glucoside), phenols and saccharide compound work, sebum secretion amount can not only be adjusted, also there is moisture-keeping function；Flavonoid
Object is able to suppress the activity of androgen, Aminopeptidase N and 5 alpha-reductases, adjusts sebum secretion amount, and have inhibition to make oxygen radical
With, free radical can be inhibited to the injury of Skin Cell, avoid skin moisture caused by due to radical damage cell be lost, have guarantor
Wet effect；Phenolic compound has obvious inhibiting effect to bacterium, and pore can be excited to shrink, and phenolic hydroxyl group has water imbibition, energy
Moisture in adsorption solvent or environment has moisture-keeping function to skin；The pale flag root extracting solution of extraction contains carbohydrate and phenols
Compound has castering action to the fungistatic effect of other components, and pore can be excited to shrink, and keeps moisture of skin.
Further, the composition for adjusting sebum secretion amount is made of the raw material of following mass percent: 20-30%
Isoflavones, the Barosma betulina leaf extract of 25-40%, the radix bardanae extracting solution of 30-45%, 3-4% Spiraea ulmaria mention
Take object；The each component content setting of the composition for adjusting sebum secretion amount, so that its effect for adjusting sebum secretion amount is more
It is good.
Further, the extracting method of the pale flag root extracting solution includes the following steps:
1) after the cleaning of pale flag root, drying, crushing, powder and 60-80% ethanol solution is normal by solid-to-liquid ratio 1: 20
Temperature is impregnated 12-24 hours, and mixed liquor is obtained；
2) the resulting mixed liquor of step 1) is heated to reflux 3-6 hours, is cooled to room temperature, filtered, ethyl alcohol is evaporated off to no alcohol
Taste obtains concentrated extracting solution；
3) the resulting concentrated extracting solution of step 2) and propylene glycol are mixed with the ratio of 1:4, the as described pale flag root
Extracting solution.
Pale flag root extracting solution isoflavones containing iris has albumen enzyme inhibition, can protect extracellular matrix
Protein (collagen and pancreatopeptidase E) can stimulate the synthesis of fixed member, keep the endoplasm and skin of dermal-epidermal binder course
Internal coagulability protects skin corium and enhances the barrier effect of skin, reduces water loss, prevent dry skin, have and protect
Wet and anti-aging function, and it is able to ascend the antiphlogistic effects of other components.
Further, the extracting method of the radix bardanae extracting solution includes the following steps:
1) it crushes drying: taking radix bardanae pulverizing medicinal materials at 8 mesh, and kept dry；
2) ethyl alcohol extracts: by the resulting radix bardanae of step 1) and ethanol solution with the solid-liquid ratio of 1g:12-24mL, in 50-70
Refluxing extraction is three times, 3.5-4.5 hours each at a temperature of DEG C, obtains extracting solution；
3) filtering and concentrating: by the filtering of step 2) resulting extracting solution and merging filtrate, using rotary evaporator to filtrate into
Row is concentrated by evaporation, and obtains concentrate；
4) petroleum ether extraction: using petroleum ether to the resulting concentrate ungrease treatment of step 3), with temperature after degreasing concentrate
The baking oven forced air drying that degree is 75-85 DEG C, obtains crude extract；
5) it isolates and purifies: the resulting crude extract of step 4) is prepared into the Burdok root P.E aqueous solution of 0.01g/mL, it will
Macroreticular resin is placed in the Burdok root P.E aqueous solution, and is put into constant temperature oscillator, and 20-30 DEG C of constant temperature is kept, static
Absorption 1-4 hours, obtains the Burdok root P.E of preliminary purification；Into the macroreticular resin for being adsorbed with Burdok root P.E, it is added
The ethanol solution of concentration 15-60% elutes, and elution speed 1.25-2.75BV/h collects eluent after elution, is concentrated and dried and is
Powdery Burdok root P.E；
6) by powdery Burdok root P.E obtained by upper step, butanediol aqueous solution with 75% is mixed with the ratio of 1:4,
The as described radix bardanae extracting solution.
Radix bardanae extracting solution also has inhibiting effect to androgen levels, cooperates with isoflavones, and antibacterial action can rise
To antiphlogistic effects.
Further, the extracting method of the Spiraea ulmaria extract includes the following steps:
1) Hua Heye for choosing Spiraea ulmaria, uses concentration 55-65% ethanol solution as solvent, Extracting temperature 65-75
DEG C, extraction time is 2 times, and each extraction time is 1.5-2.5 hours, and each solvent usage is 10 times of Spiraea ulmaria weight,
Filtering, obtains the first extracting solution and first dregs of a decoction；First extracting solution recycles ethyl alcohol, is concentrated into relative density d=1.12, mistake
Filter, obtains the first medical fluid；
2) resulting first medical fluid of step 1) is first eluted with water by ADS-3 macroporous absorbent resin, then with concentration 75-
85% ethanol solution elution, collects 75-85% concentration ethanol eluent, is concentrated and dried to get the first Spiraea ulmaria extract；
3) by resulting first dregs of a decoction of step 1), use concentration 2-3% hydrochloric acid solution as solvent, 65-75 DEG C of Extracting temperature,
Extraction time is 2 times, and each extraction time is 1.5-2.5 hours, and each solvent usage is 12 times of Spiraea ulmaria weight, mistake
Filter, combined extract are concentrated into relative density d=1.16, with ammonium hydroxide tune pH to 9-10, are extracted with ethyl acetate 4 times, acetic acid second
After ester extract liquor is washed with water 3 times, ethyl acetate is recycled, is concentrated, it is dry, obtain the second Spiraea ulmaria extract；
4) the resulting first Spiraea ulmaria extract of step 2) and the resulting second Spiraea ulmaria extract of step 3) is mixed
The even Spiraea ulmaria extract to get powdery.
Spiraea ulmaria extract can inhibit the generation of inflammation, cooperate with isoflavones, have inhibiting effect, and energy to androgen
Keep skin moisture, pore refining.
Further, the extracting method of the isoflavones includes the following steps:
1) feedstock processing: being crushed to partial size in 0.5-0.8mm for soybean meal, spare；
2) solvent extraction: the resulting soybean meal of step 1) is extracted with the ethanol water that concentration is 40-80%, raw material
Solid-liquid ratio with solvent is 1g:8-16mL, and Extracting temperature is 60-80 DEG C, extraction time 5-8h, and extraction time is 1-3 times, is obtained
To extracting solution；
3) it separates: after using centrifuge separation to the resulting extracting solution of step 2), by the dry 5- of obtained extraction object
10h；
4) it refines: being combined using ultrafiltration membrane with absorption resin, remove partial impurities, the cutting point of ultrafiltration membrane with ultrafiltration membrane
Son amount is 600-100000, by the leaching liquor temperature of ultrafiltration membrane at 80-90 DEG C, then it is big in resin adsorption leaching liquor with adsorbing
Beans isoflavones；
5) it desorbs, is dry: after absorption resin adsorption, being desorbed with stripping liquid, be dried after desorption, obtain powdery soybean
Isoflavones；
6) dissolve: by powdery soybean isoflavones obtained by upper step, butanediol aqueous solution with 70% is mixed with the ratio of 1:99
It closes, the as described isoflavones.
The molecular structure of isoflavones and human endogenous's property estrogen estradiol are very much like, therefore have estrogen living
Property, have estrogen-like action, skin is one of the target tissue that estrogen plays a role, estrogen by on Skin Cell
Estrogen receptor, which combines, plays biological effect, it has the function of promoting collagen and hyaluronic acid synthesis, keeps skin fine and smooth, clean
White, high resilience and gloss, and it is inhibited to androgen, to inhibit androgen to sebocyte cell sebum secreted
It influences；Isoflavones can also inhibit free radical to the injury of Skin Cell, avoid flesh caused by due to radical damage cell
Skin water loss.
Further, the Barosma betulina leaf extract is made through the method for microwave abstracting；Wherein, the Barosma betulina leaf extracts
Extractant used in liquid is butanediol aqueous solution, microwave frequency 400-250000MHz；Preferably, microwave frequency is
2450MHz。
Barosma betulina leaf extract is rich in flavonoids, and chief active molecule is diosmin, can inhibit precursor sebocyte cell
Differentiation, and secretion of the mature sebocyte cell to grease have fine and smooth pore, control fat secretion, restore skin natural light
The effect in pool.
To solve the above-mentioned problems, there is provided a kind of moisturizings efficiently to adjust sebum secretion amount for the second object of the present invention
The preparation method of facial mask liquid, step is simple, easy to make.
To solve the above-mentioned problems, the present invention is achieved by following technical scheme:
A kind of moisturizing efficiently adjusts the preparation method of the facial mask liquid of sebum secretion amount, includes the following steps:
S1, ingredient: it is equipped with following raw material: the glycerol of 3-5%, the butanediol of 3-5%, 0.03-0.1% by mass percentage
Hydroxyethyl cellulose, the adjusting composition of sebum secretion amount of 5-10%, 1-5% pale flag root extracting solution, 0.5-
0.6% parahydroxyacet-ophenone, the 1,2- hexylene glycol of 0.4-0.5%, 73.8-87.07% deionized water；Wherein, the adjusting
The group of the composition of sebum secretion amount becomes isoflavones, Barosma betulina leaf extract, radix bardanae extracting solution, Spiraea ulmaria and extracts
Object；
S2, it sequentially adds the glycerol, is the butanediol, the hydroxyethyl cellulose, the parahydroxyacet-ophenone, described
1,2- hexylene glycol, the deionized water open blender stirring, and are heated to 80-85 DEG C, stop heating after keeping the temperature 3-5min；
S3, when temperature is down to 40-45 DEG C, sequentially add and described adjust the composition of sebum secretion amount, the cus-cus kite
Root of the tail extracting solution, is evenly stirred until room temperature, and the facial mask liquid that the moisturizing efficiently adjusts sebum secretion amount is made.
Compared with prior art, the beneficial effects of the present invention are:
(1) moisturizing that the present invention is prepared efficiently adjusts the facial mask liquid of sebum secretion amount, by isoflavones, mountain cloth
Dead leaf extracting solution, radix bardanae extracting solution, Spiraea ulmaria extract, pale flag root extracting solution progress scientific compatibility, coordinative role,
Flavonoids (predominantly flavones, isoflavones, diosmin), phenols and the saccharide compound being rich in by said extracted object act as
With, sebum secretion amount can not only be adjusted, also have moisture-keeping function；Flavone compound is able to suppress androgen, Aminopeptidase N
With the activity of 5 alpha-reductases, sebum secretion amount is adjusted, and has inhibiting effect to oxygen radical, free radical can be inhibited to Skin Cell
Injury, avoid skin moisture caused by due to radical damage cell be lost, have moistening effect；Phenolic compound has bacterium
Obvious inhibiting effect, and pore can be excited to shrink, and phenolic hydroxyl group has water imbibition, the moisture in energy adsorption solvent or environment is right
Skin has moisture-keeping function；The pale flag root extracting solution of extraction contains carbohydrate and phenolic compound, to the antibacterial effect of other components
Fruit has castering action, and pore can be excited to shrink, and keeps moisture of skin.
(2) moisturizing of the present invention efficiently adjusts the preparation method of the facial mask liquid of sebum secretion amount, and step is simple, preparation
It is convenient.
Detailed description of the invention
In order to more clearly explain the embodiment of the invention or the technical proposal in the existing technology, to embodiment or will show below
There is attached drawing needed in technical description to be briefly described, it should be apparent that, the accompanying drawings in the following description is only this
Some embodiments of invention for those of ordinary skill in the art without creative efforts, can be with
It obtains other drawings based on these drawings.
Fig. 1 is the preparation technology flow chart for the facial mask liquid that a kind of moisturizing of the present invention efficiently adjusts sebum secretion amount.
Specific embodiment
The technical scheme in the embodiments of the invention will be clearly and completely described below, it is clear that described implementation
Example is only a part of the embodiments of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, this field is common
Technical staff's all other embodiment obtained without making creative work belongs to the model that the present invention protects
It encloses.
As shown in Figure 1, the invention discloses the facial mask liquid that a kind of moisturizing efficiently adjusts sebum secretion amount, by following quality hundred
Divide the raw material composition of ratio:
Wherein, the group for adjusting the composition of sebum secretion amount becomes isoflavones, Barosma betulina leaf extract, radix bardanae and mentions
Take liquid, Spiraea ulmaria extract.
Pale flag root comes from Mediterranean basin, buys in French GATTEFOSSE company；Barosma betulina leaf comes from South America
With South Africa crop growing spots, buy in Provital Group company, Spain；Radix bardanae comes from domestic shop of Chinese medicines；Spiraea ulmaria
For the native country Spiraea ulmaria of country's plantation, there is cultivation on Liaoning, the Inner Mongol, Hebei, Shandong, Shanxi and other places, buy in the country
Shop of Chinese medicines；Other raw materials and reagent are commercial product.
Embodiment 1
One, the preparation of raw material:
(1) extracting method of pale flag root extracting solution includes the following steps:
1) after the cleaning of pale flag root, drying, crushing, powder and 70% ethanol solution are soaked by 1: 20 room temperature of solid-to-liquid ratio
Bubble 20 hours, obtains mixed liquor；
2) the resulting mixed liquor of step 1) is heated to reflux 5 hours, is cooled to room temperature, filtered, ethyl alcohol be evaporated off to no alcohol taste,
Obtain concentrated extracting solution；
3) the resulting concentrated extracting solution of step 2) and propylene glycol are mixed with the ratio of 1:4, the as described pale flag root
Extracting solution.
(2) extracting method of radix bardanae extracting solution includes the following steps:
1) it crushes drying: taking radix bardanae pulverizing medicinal materials at 8 mesh, and kept dry；
2) ethyl alcohol extracts: by the resulting radix bardanae of step 1) and ethanol solution with the solid-liquid ratio of 1g:20mL, in 60 DEG C of temperature
It spends lower refluxing extraction three times, 4 hours every time, obtains extracting solution；
3) filtering and concentrating: by the filtering of step 2) resulting extracting solution and merging filtrate, using rotary evaporator to filtrate into
Row is concentrated by evaporation, and obtains concentrate；
4) petroleum ether extraction: using petroleum ether to the resulting concentrate ungrease treatment of step 3), with temperature after degreasing concentrate
The baking oven forced air drying that degree is 80 DEG C, obtains crude extract；
5) it isolates and purifies: the resulting crude extract of step 4) is prepared into the Burdok root P.E aqueous solution of 0.01g/mL, it will
Macroreticular resin is placed in the Burdok root P.E aqueous solution, and is put into constant temperature oscillator, and 25 DEG C of constant temperature, Static Adsorption are kept
3 hours, obtain the Burdok root P.E of preliminary purification；Into the macroreticular resin for being adsorbed with Burdok root P.E, concentration is added
45% ethanol solution elution, elution speed 2.75BV/h collect eluent after elution, are concentrated and dried and mention for powdery radix bardanae
Take object；
6) by powdery Burdok root P.E obtained by upper step, butanediol aqueous solution with 75% is mixed with the ratio of 1:4,
The as described radix bardanae extracting solution.
(3) extracting method of Spiraea ulmaria extract includes the following steps:
1) Hua Heye for choosing Spiraea ulmaria uses 60% ethanol solution of concentration as solvent, and Extracting temperature is 70 DEG C, extracts
Number is 2 times, and each extraction time is 2 hours, and each solvent usage is 10 times of Spiraea ulmaria weight, and filtering obtains first and mentions
Take liquid and first dregs of a decoction；First extracting solution recycles ethyl alcohol, is concentrated into relative density d=1.12, filters, obtains the first medicine
Liquid；
2) resulting first medical fluid of step 1) is first eluted with water by ADS-3 macroporous absorbent resin, then uses concentration
80% ethanol solution elution, collects 80% concentration ethanol eluent, is concentrated and dried to get the first Spiraea ulmaria extract；
3) it by resulting first dregs of a decoction of step 1), uses 2% hydrochloric acid solution of concentration as solvent, 70 DEG C of Extracting temperature, extracts
Number is 2 times, and each extraction time is 2 hours, and each solvent usage is 12 times of Spiraea ulmaria weight, and filtering merges and extracts
Liquid is concentrated into relative density d=1.16, with ammonium hydroxide tune pH to 9, is extracted with ethyl acetate 4 times, acetic acid ethyl acetate extract is washed with water
After 3 times, ethyl acetate is recycled, is concentrated, it is dry, obtain the second Spiraea ulmaria extract；
4) the resulting first Spiraea ulmaria extract of step 2) and the resulting second Spiraea ulmaria extract of step 3) is mixed
The even Spiraea ulmaria extract to get powdery.
(4) extracting method of isoflavones includes the following steps:
1) feedstock processing: being crushed to partial size in 0.8mm for soybean meal, spare；
2) solvent extraction: by the resulting soybean meal concentration of step 1) be 70% ethanol water extract, raw material with
The solid-liquid ratio of solvent is 1g:12mL, and Extracting temperature is 70 DEG C, extraction time 6h, and extraction time is 3 times, obtains extracting solution；
3) it separates: after using centrifuge separation to the resulting extracting solution of step 2), by the dry 8h of obtained extraction object；
4) it refines: being combined using ultrafiltration membrane with absorption resin, remove partial impurities, the cutting point of ultrafiltration membrane with ultrafiltration membrane
Son amount be 100000, by the leaching liquor temperature of ultrafiltration membrane at 80 DEG C, then with adsorb resin adsorption leaching liquor in the different Huang of soybean
Ketone；
5) it desorbs, is dry: after absorption resin adsorption, being desorbed with stripping liquid, be dried after desorption, obtain powdery soybean
Isoflavones；
6) dissolve: by powdery soybean isoflavones obtained by upper step, butanediol aqueous solution with 70% is mixed with the ratio of 1:99
It closes, the as described isoflavones.
(5) Barosma betulina leaf extract is made through the method for microwave abstracting, and extractant used is butanediol aqueous solution, micro-
Wave frequency rate is 2450MHz.
(6) preparation of the composition of sebum secretion amount is adjusted:
25g isoflavones, 35g Barosma betulina leaf extract, 36g radix bardanae extracting solution, 4g Spiraea ulmaria is sequentially added to mention
Object is taken, is uniformly mixed to get the composition for adjusting sebum secretion amount.
Two, a kind of moisturizing efficiently adjusts the facial mask liquid of sebum secretion amount, is made of the raw material of following quality:
Three, a kind of moisturizing efficiently adjusts the preparation method of the facial mask liquid of sebum secretion amount, includes the following steps:
S1, ingredient: with following raw material: 3g glycerol, 3g butanediol, 0.03g hydroxyethyl cellulose, 5g adjust sebum secretion
Composition, 1g pale flag root extracting solution, the 0.5g parahydroxyacet-ophenone, 0.4g 1,2- hexylene glycol, 87.07g deionization of amount
Water；
S2, glycerol, butanediol, hydroxyethyl cellulose, parahydroxyacet-ophenone, 1,2- hexylene glycol, deionized water are sequentially added,
Blender stirring is opened, and is heated to 80 DEG C, stops heating after keeping the temperature 3min；
S3, when temperature is down to 40 DEG C, sequentially add adjust sebum secretion amount composition, pale flag root extracting solution,
It is evenly stirred until room temperature, the facial mask liquid that the moisturizing efficiently adjusts sebum secretion amount is made.
Embodiment 2
One, the preparation of raw material: same as Example 1.
Two, a kind of moisturizing efficiently adjusts the facial mask liquid of sebum secretion amount, is made of the raw material of following quality:
Three, a kind of moisturizing efficiently adjusts the preparation method of the facial mask liquid of sebum secretion amount, includes the following steps:
S1, ingredient: with following raw material: 3g glycerol, 3g butanediol, 0.03g hydroxyethyl cellulose, 5g adjust sebum secretion
Composition, 1g pale flag root extracting solution, the 0.55g parahydroxyacet-ophenone, 0.45g 1,2- hexylene glycol, 80.94g deionization of amount
Water；
S2, glycerol, butanediol, hydroxyethyl cellulose, parahydroxyacet-ophenone, 1,2- hexylene glycol, deionized water are sequentially added,
Blender stirring is opened, and is heated to 80 DEG C, stops heating after keeping the temperature 3min；
S3, when temperature is down to 40 DEG C, sequentially add adjust sebum secretion amount composition, pale flag root extracting solution,
It is evenly stirred until room temperature, the facial mask liquid that the moisturizing efficiently adjusts sebum secretion amount is made.
Embodiment 3
One, the preparation of raw material: same as Example 1.
Two, a kind of moisturizing efficiently adjusts the facial mask liquid of sebum secretion amount, is made of the raw material of following quality:
Three, a kind of moisturizing efficiently adjusts the preparation method of the facial mask liquid of sebum secretion amount, includes the following steps:
S1, ingredient: with following raw material: 3g glycerol, 3g butanediol, 0.03g hydroxyethyl cellulose, 5g adjust sebum secretion
Composition, 1g pale flag root extracting solution, the 0.6g parahydroxyacet-ophenone, 0.5g 1,2- hexylene glycol, 73.8g deionized water of amount；
S2, glycerol, butanediol, hydroxyethyl cellulose, parahydroxyacet-ophenone, 1,2- hexylene glycol, deionized water are sequentially added,
Blender stirring is opened, and is heated to 80 DEG C, stops heating after keeping the temperature 3min；
S3, when temperature is down to 40 DEG C, sequentially add adjust sebum secretion amount composition, pale flag root extracting solution,
It is evenly stirred until room temperature, the facial mask liquid that the moisturizing efficiently adjusts sebum secretion amount is made.
Reference examples 1
A kind of facial mask liquid, component is substantially the same manner as Example 1, and difference is: not comprising the group for adjusting sebum secretion amount
Close object；Preparation method is same as Example 1.
Reference examples 2
A kind of facial mask liquid, component is substantially the same manner as Example 1, and difference is: not including pale flag root extracting solution；Its
Preparation method is same as Example 1.
Reference examples 3
A kind of facial mask liquid, component is substantially the same manner as Example 1, and difference is: not comprising the group for adjusting sebum secretion amount
Close object and pale flag root extracting solution；Preparation method is same as Example 1.
Comparative example 1
It is commercially available that there is the facial mask liquid for adjusting sebum effect.
Effete test embodiment
1, the moisturizing that embodiment 1-3 is prepared efficiently is adjusted into the facial mask liquid of sebum secretion amount, reference examples 1-3 is prepared into
To facial mask liquid and comparative example 1 it is commercially available have adjust sebum effect facial mask liquid trier is tested respectively, make
The validity of facial mask liquid is proved with the sebum level after preceding and use, moisture content change.
Test method: non-woven fabrics is immersed to the moisturizing that embodiment 1-3 is prepared respectively and efficiently adjusts sebum secretion amount
The facial mask liquid and the commercially available of comparative example 1 that facial mask liquid, reference examples 1-3 are prepared have the facial mask liquid for adjusting sebum effect
In, so that every non-woven fabrics contains 25mL facial mask liquid, to obtain facial mask piece；
Women 7 of selection age 22-25 years old, are oiliness and Combination skin, without any skin disease and skin allergy
History, a kind of test sample of everyone application apply to the identical position of face, cannot use other than test sample during test
Any cosmetics；
Moisture tester is percutaneously lost using the SebumScale sebum measuring instrument and VapoMeter of dilfin company, Finland
It is tested, selects the same position of face as test position；Before use, first testing the sebum level and moisture of trier respectively
Content；In use, 1 unilateral diaphragm is taken to apply in face, after 15 minutes, the facial mask liquid of facial remnants is washed with clear water, then survey
It has a try the sebum level and moisture content of user, test result is as shown in table 1.
1 test result of table
Seen from table 1, the facial mask liquid that the moisturizing that 1-3 of the embodiment of the present invention is prepared efficiently adjusts sebum secretion amount has
Preferable oil-control effect and moistening effect.
2, the moisturizing that embodiment 1-3 is prepared efficiently is adjusted into the facial mask liquid of sebum secretion amount, reference examples 1-3 is prepared into
To facial mask liquid and comparative example 1 it is commercially available have adjust sebum effect facial mask liquid trier is tested respectively, make
The validity of facial mask liquid is proved with the pore varying aperture after preceding and use.
Test method: non-woven fabrics is immersed to the moisturizing that embodiment 1-3 is prepared respectively and efficiently adjusts sebum secretion amount
The facial mask liquid and the commercially available of comparative example 1 that facial mask liquid, reference examples 1-3 are prepared have the facial mask liquid for adjusting sebum effect
In, so that every non-woven fabrics contains 25mL facial mask liquid, to obtain facial mask piece；
Personnel 70 of selection age 22-35 years old, each half of masculinity femininity, is oiliness and Combination skin, without any
Skin disease and skin allergy history are divided into 7 groups, and a kind of every group of 10 people, every group of test sample of application applies to the identical portion of face
Position cannot use any cosmetics in test first 2 days, any cosmetics other than test sample cannot be used during test, by
After examination person's clear water face cleaning, facial mask piece is spread on into face 15 minutes, application is primary every night, uses two months；
Skin pore aperture is tested using skin image analyzer, selects the same position of face as test position, respectively
Before and using measuring after two months, analysis obtains pore pore size, and test result is as shown in table 2.
Skin pore aperture (μ g/cm before and after 2 use of table2)
| Sample | Before use | After 2 months |
| Embodiment 1 | 191.1±20.5 | 143.7±22.1 |
| Embodiment 2 | 192.3±19.6 | 140.8±20.5 |
| Embodiment 3 | 191.0±20.4 | 145.2±19.5 |
| Reference examples 1 | 192.1±19.2 | 176.1±21.8 |
| Reference examples 2 | 190.6±21.0 | 169.5±20.5 |
| Reference examples 3 | 191.3±20.8 | 192.1±19.9 |
| Comparative example 1 | 190.0±19.6 | 178.5±20.1 |
As can be seen from Table 2, the facial mask liquid that the moisturizing that 1-3 of the embodiment of the present invention is prepared efficiently adjusts sebum secretion amount has
Preferable pore refining effect.
It is to be illustrated to preferable implementation of the invention, but the present invention is not limited to the embodiment above, it is ripe
Various equivalent deformation or replacement can also be made on the premise of without prejudice to spirit of the invention by knowing those skilled in the art, this
Equivalent deformation or replacement are all included in the scope defined by the claims of the present application a bit.
Claims (8)
1. the facial mask liquid that a kind of moisturizing efficiently adjusts sebum secretion amount, it is characterised in that: by the raw material group of following mass percent
At:
Wherein, the group of the composition for adjusting sebum secretion amount becomes isoflavones, Barosma betulina leaf extract, radix bardanae and mentions
Take liquid, Spiraea ulmaria extract.
2. the facial mask liquid that moisturizing according to claim 1 efficiently adjusts sebum secretion amount, it is characterised in that: the adjusting skin
The composition of rouge secretory volume is made of the raw material of following mass percent: the mountain cloth of the isoflavones of 20-30%, 25-40%
Dead leaf extracting solution, the radix bardanae extracting solution of 30-45%, 3-4% Spiraea ulmaria extract.
3. the facial mask liquid that moisturizing according to claim 1 efficiently adjusts sebum secretion amount, it is characterised in that: the cus-cus kite
The extracting method of root of the tail extracting solution includes the following steps:
1) after the cleaning of pale flag root, drying, crushing, powder and 60-80% ethanol solution are soaked by 1: 20 room temperature of solid-to-liquid ratio
Bubble 12-24 hours, obtains mixed liquor；
2) the resulting mixed liquor of step 1) is heated to reflux 3-6 hours, is cooled to room temperature, filtered, ethyl alcohol is evaporated off to no alcohol taste, obtain
To concentrated extracting solution；
3) the resulting concentrated extracting solution of step 2) and propylene glycol are mixed with the ratio of 1:4, the as described pale flag root extracts
Liquid.
4. the facial mask liquid that moisturizing according to claim 1 efficiently adjusts sebum secretion amount, it is characterised in that: the radix bardanae
The extracting method of extracting solution includes the following steps:
1) it crushes drying: taking radix bardanae pulverizing medicinal materials at 8 mesh, and kept dry；
2) ethyl alcohol extracts: by the resulting radix bardanae of step 1) and ethanol solution with the solid-liquid ratio of 1g:12-24mL, at 50-70 DEG C
At a temperature of refluxing extraction three times, it is 3.5-4.5 hours each, obtain extracting solution；
3) filtering and concentrating: the resulting extracting solution filtering of step 2) and merging filtrate steam filtrate using rotary evaporator
Hair concentration, obtains concentrate；
4) petroleum ether extraction: using petroleum ether to the resulting concentrate ungrease treatment of step 3), it is with temperature after degreasing concentrate
75-85 DEG C of baking oven forced air drying, obtains crude extract；
5) it isolates and purifies: the resulting crude extract of step 4) being prepared into the Burdok root P.E aqueous solution of 0.01g/mL, by macropore
Resin is placed in the Burdok root P.E aqueous solution, and is put into constant temperature oscillator, and 20-30 DEG C of constant temperature, Static Adsorption are kept
1-4 hours, obtain the Burdok root P.E of preliminary purification；Into the macroreticular resin for being adsorbed with Burdok root P.E, concentration is added
The ethanol solution of 15-60% elutes, and elution speed 1.25-2.75BV/h collects eluent after elution, is concentrated and dried as powdery
Burdok root P.E；
6) by powdery Burdok root P.E obtained by upper step, butanediol aqueous solution with 75% is mixed, as with the ratio of 1:4
The radix bardanae extracting solution.
5. the facial mask liquid that moisturizing according to claim 1 efficiently adjusts sebum secretion amount, it is characterised in that: the elm embroider line
The extracting method of chrysanthemum extract includes the following steps:
1) Hua Heye for choosing Spiraea ulmaria uses concentration 55-65% ethanol solution as solvent, and Extracting temperature is 65-75 DEG C, mentions
Taking number is 2 times, and each extraction time is 1.5-2.5 hours, and each solvent usage is 10 times of Spiraea ulmaria weight, is filtered,
Obtain the first extracting solution and first dregs of a decoction；First extracting solution recycles ethyl alcohol, is concentrated into relative density d=1.12, filters, obtains
To the first medical fluid；
2) resulting first medical fluid of step 1) is first eluted with water by ADS-3 macroporous absorbent resin, then with concentration 75-85%
Ethanol solution elution, collect 75-85% concentration ethanol eluent, be concentrated and dried to get the first Spiraea ulmaria extract；
3) it by resulting first dregs of a decoction of step 1), uses concentration 2-3% hydrochloric acid solution as solvent, 65-75 DEG C of Extracting temperature, extracts
Number is 2 times, and each extraction time is 1.5-2.5 hours, and each solvent usage is 12 times of Spiraea ulmaria weight, is filtered, and is closed
And extracting solution, it is concentrated into relative density d=1.16, with ammonium hydroxide tune pH to 9-10, is extracted with ethyl acetate 4 times, ethyl acetate extraction
After taking liquid to be washed with water 3 times, ethyl acetate is recycled, is concentrated, it is dry, obtain the second Spiraea ulmaria extract；
4) the resulting first Spiraea ulmaria extract of step 2) and the resulting second Spiraea ulmaria extract of step 3) are mixed, i.e.,
Obtain the Spiraea ulmaria extract of powdery.
6. the facial mask liquid that moisturizing according to claim 1 efficiently adjusts sebum secretion amount, it is characterised in that: the soybean is different
The extracting method of flavones includes the following steps:
1) feedstock processing: being crushed to partial size in 0.5-0.8mm for soybean meal, spare；
2) solvent extraction: by the resulting soybean meal of step 1) with concentration be 40-80% ethanol water extract, raw material with it is molten
The solid-liquid ratio of agent is 1g:8-16mL, and Extracting temperature is 60-80 DEG C, extraction time 5-8h, and extraction time is 1-3 times, is mentioned
Take liquid；
3) it separates: after using centrifuge separation to the resulting extracting solution of step 2), by the dry 5-10h of obtained extraction object；
4) it refines: being combined using ultrafiltration membrane with absorption resin, remove partial impurities, the molecular weight cut off of ultrafiltration membrane with ultrafiltration membrane
For 600-100000, by the leaching liquor temperature of ultrafiltration membrane at 80-90 DEG C, then it is different with the soybean in absorption resin adsorption leaching liquor
Flavones；
5) it desorbs, is dry: after absorption resin adsorption, being desorbed with stripping liquid, be dried after desorption, obtain the different Huang of powdery soybean
Ketone；
6) dissolve: by powdery soybean isoflavones obtained by upper step, butanediol aqueous solution with 70% is mixed with the ratio of 1:99,
The as described isoflavones.
7. the facial mask liquid that moisturizing according to claim 1 efficiently adjusts sebum secretion amount, it is characterised in that: the Barosma betulina
Leaf extract is made through the method for microwave abstracting；Wherein, extractant used in the Barosma betulina leaf extract is that butanediol is water-soluble
Liquid, microwave frequency 400-250000MHz.
8. moisturizing according to claim 1-7 efficiently adjusts the preparation method of the facial mask liquid of sebum secretion amount,
It is characterized in that: including the following steps:
S1, ingredient: with following raw material by mass percentage: the glycerol of 3-5%, the butanediol of 3-5%, 0.03-0.1% hydroxyl
Ethyl cellulose, 5-10% adjust the composition of sebum secretion amount, the pale flag root extracting solution of 1-5%, 0.5-0.6%
Parahydroxyacet-ophenone, the 1,2- hexylene glycol of 0.4-0.5%, 73.8-87.07% deionized water；Wherein, the adjusting sebum secretion
The group of the composition of amount becomes isoflavones, Barosma betulina leaf extract, radix bardanae extracting solution, Spiraea ulmaria extract；
S2, the glycerol, the butanediol, the hydroxyethyl cellulose, the parahydroxyacet-ophenone, the 1,2- are sequentially added
Hexylene glycol, the deionized water open blender stirring, and are heated to 80-85 DEG C, stop heating after keeping the temperature 3-5min；
S3, when temperature is down to 40-45 DEG C, sequentially add it is described adjust sebum secretion amount composition, the pale flag root
Extracting solution is evenly stirred until room temperature, and the facial mask liquid that the moisturizing efficiently adjusts sebum secretion amount is made.
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Cited By (2)
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