CN107126399A - A kind of tencel facial mask of the composition containing dendrobium candidum and preparation method thereof - Google Patents
A kind of tencel facial mask of the composition containing dendrobium candidum and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a kind of tencel facial mask of composition containing dendrobium candidum, it is formulated by tetra- kinds of component raw materials of A, B, C and D.The present invention is used as main active component using dendrobium candidum extract, it is equipped with Tremella fructification extract, saccharomycete lysis thing extract and Gotu Kola P.E, four kinds of component collaborations work, go deep into skin bottom to keep the skin wet, strengthen skin moisture-retaining capacity, moisture content in skin can be made to keep appropriate, improve skin cell metabolism, nurse one's health skin microcirculation, and while moisturizing water lock, skin is promoted to recover good barrier function, effectively reduce water loss, pin moisture, keep 24 hours long-acting water profits, so as to strengthen skin moisturizing degree, elasticity and suppleness, careful nourishing skin, scaly dry skin of releiving and itch, so that the natural regulating power of skin is recovered.
Description
Technical field
The present invention relates to cosmetic field, the more particularly to a kind of tencel facial mask of composition containing dendrobium candidum and its preparation
Method.
Background technology
With the improvement of living standards, the demand of people's material and culture is changed stepwise, a kind of fashion is turned into beautiful pursuit
With it is required.Beauty and skin care turns into most basic life requirement, and various cosmetics, skin care item flood market, and beauty industry prospect is wide
It is wealthy.Facial mask is common cosmetics, good with its effect, reasonable price, is favored by the vast Ms that likes to be beautiful.Face on the market
Film product is a feast for the eyes, various informative.When three seasons of winter in spring and autumn are all dry, skin needs moisture to nourish, because
This moisturizer turns into the hot topic in market.
The principle of facial mask, exactly using the of short duration time for being covered in face, is temporarily isolating air and the pollution in the external world, improves
Skin temperature, the pore expansion of skin, promotes sweat gland secretion and metabolism, the oxygen content of skin is increased, be conducive to skin
Exclude the cutin that the moisture content in the product of epidermal cell metabolism and the oil substances of accumulation, facial mask penetrates into skin epidermis
Layer, skin becomes soft.Light is flexible naturally for skin.
At present, the life stress and operating pressure that people face are all very big, so that the skin of people is not very
Ideal, extremely lacks moisture, so not only influences the water and oil balance of face, and due to lacking moisture, it is easy to increase wrinkle
The chance of generation.Existing moisture saver mask, moisture-keeping efficacy is undesirable.
Dendrobium candidum (Dendrobiumofficinale) is orchid family Dendrobium herbaceos perennial, is that one kind is distributed in
The Chinese medicine plant of karst area, it gains the name because iron green is presented for epidermis, is that the rare danger that relates to of China's emphasis second class protection is planted
Thing.Dendrobium Sw is the important traditional Chinese medicine of China, is confirmed according to pharmacology test, during dendrobium candidum is as being of illnesses and fitness
Medicine is long-standing, Qin Han dynasty《Sheng Nong's herbal classic》Record dendrobium candidum " in main wound, eliminating impediment, lower gas, tonifying five zang organs consumptive disease it is thin
The thick stomach of thin, Qiang Yin, long term usage "；It is classical in Taoist school's medical science before more than 1,000 years into book《Taoist Scriptures》Dendrobium candidum is classified as " China nine
First of big celestial grass "；Li Shizhen (1518-1593 A.D.) exists《Compendium of Materia Medica》Middle evaluation dendrobium candidum " in strong the moon strengthening the essence, thick stomach, benefit never enough, flat stomach
Gas, long muscle, intelligence development is except frightened, macrobiosis of making light of one's life by commiting suicide "；It is among the people to be called " help celestial grass ", rank first of " Chinese nine big celestial grass ", by state
Border medicinal plant circle is referred to as " medicine circle giant panda ".Dendrobium candidum also has external efficacy, and modern scientific research shows, dendrobium candidum
Rich in polysaccharide, dendrobine, free amino acid, vitamin (vitamin A, vitamin C, vitamin E), chlorophyll and various enzymes,
Not only it can also stop blooding by oral absorption, dendrobium candidum, promote wound healing, can be used to repair damaged skin outside.
The content of the invention
In order to make up the defect of prior art, the present invention provides tencel facial mask and its preparation of a kind of composition containing dendrobium candidum
Method.
The technical problems to be solved by the invention are achieved by the following technical programs：
A kind of tencel facial mask of composition containing dendrobium candidum, is formulated by tetra- kinds of component raw materials of A, B, C and D：
Component A：30-45 parts of pure water, 2-5 parts of glycerine, 0.3-0.5 parts of parts of 1,2- pentanediols, 0.2-0.6 parts of 1,2- hexylene glycols,
0.05-0.1 parts of EDTA disodiums, 0.12-0.15 parts of methyl hydroxybenzoate；
B component：1-10 parts of 1,3- propane diols, 0.1-0.6 parts of xanthans, 0.1-1 parts of Tremella fructification extract, hydroxy ethyl fiber
Plain 0.06-0.08 parts, 0.01-0.1 parts of Sodium Hyaluronate；
Component C：0.5-1 parts of trehalose, carbohydrate isomer/pure water/0.1-0.3 parts of citric acid/sodium citrate compound, iron
Skin Herba Dendrobii extract/pure water/2-8 parts of butanediol compound, saccharomycete lysis thing extract/water/Phenoxyethanol compound 1-3
Part, 0.5-2 parts of Gotu Kola P.E, 0.06-0.08 parts of dipotassium glycyrrhizinate, 0.1-0.5 parts of Phenoxyethanol, the 0.05-2 of hexapeptide -11
Part, 0.1-0.5 parts of calcium pantothenate, 0.1-0.2 parts of xanthans, 0.1-1 parts of urea, pungent glycol 0.1-0.25 parts, magnesium lactate 0.06-
0.08 part, 0.1-0.25 parts of Sensiva SC50,0.02-0.05 parts of potassium chloride, 0.02-0.05 parts of potassium lactate, magnesium chloride 0.02-
0.05 part, 0.5-2 parts of glucose；
D components：0-0.04 parts of essence, 0.06-0.09 parts of Cremophor RH40.
Further, the preparation method of dendrobium candidum extract is in component C：
The first step：Dendrobium candidum is harvested before blooming, 30~60min is rinsed with purified water, then rinsed 3 times with purified water；So
The segment of 1-3cm length is cut into afterwards, it is freezed completely solid, then carries out vacuum freeze drying more than 24 hours, dried iron
The skin stem of noble dendrobium is placed in oscillatory type ultramicro grinding grinding kneading machine and ultramicro grinding 5-10min is carried out at a temperature of -25 DEG C to -30 DEG C,
Obtain dendrobium candidum ultrafine powder；
Second step, by above-mentioned dendrobium candidum ultrafine powder, according to solid-liquid ratio 1:10~1:40g/ml, adds water and is sufficiently mixed, use
When carrying out separation of solid and liquid, wherein Microwave Extraction after Microwave Extraction, microwave treatment power is 400W, frequency 2450MHz, and the time is
Extract solution A is obtained after 15-20min, separation of solid and liquid and slag A is extracted；
The ethanol that 3rd step, said extracted slag A and volume fraction are 20~100% is according to solid-liquid ratio 1:8~1:12 g/ml are mixed,
Then using ultrasonic wave extraction progress separation of solid and liquid, 20~90 DEG C of Extracting temperature, 1~2h of extraction time, separation of solid and liquid is carried
Take liquid B and extract slag B；
4th step, extract solution B merges after removing ethanol through reduced vacuum concentration with extract solution A, is carried out using miillpore filter
Filter out miscellaneous, obtain liquor C；
5th step, liquor C adds 1~5h of protease hydrolyzed, uses molecular weight ranges for 3000~5000Da nanofiltration membrane enzyme
Liquid is solved, filtrate D is obtained, NF membrane retention part is dendrobium polysaccharide；
6th step, filtrate D adds glycosylhydrolase, digests 1~3h, then will use nanofiltration membrane of the molecular weight for 1000Da,
Filtrate E is obtained, filtrate E is spray-dried to obtain dendrobine；
7th step：The dendrobium polysaccharide obtained in 5th step is mixed with the dendrobine obtained in the 6th step, dendrobium candidum is prepared and carries
Take thing.
The dendrobium candidum extract of the present invention is freeze-dried and low-temperature submicron powder using fresh dendrobium candidum as raw material, first
Broken acquisition dendrobium candidum ultrafine powder, saves the baking operation of traditional dendrobium candidum, and active ingredient is difficult to be destroyed, then carries out respectively
Microwave Extraction and ultrasonic wave extraction, with reference to zymolysis technique and membrane separation technique, coproduction obtains dendrobium polysaccharide and dendrobine, by iron sheet
Dendrobium polysaccharide and dendrobine in the stem of noble dendrobium are fully extracted, and extract high conversion rate, and the active ingredient of dendrobium candidum is easier quilt
Absorption of human body, bioavilability is higher, and extraction process is very gentle, it is to avoid the decomposition of dendrobium candidum active ingredient, gained
Extract impurity content it is less, substantially increase the purity and content of dendrobium polysaccharide and dendrobine in extract, improve pair
The utilization rate of dendrobium candidum, realizes the rational exploitation and utilization to dendrobium candidum.
Further, the preparation method of Tremella fructification extract is in B component：
Tremella fructification dry product is taken, 35-45min is soaked at room temperature with distilled water, is placed in beater and fully crushes, white fungus is made
Slurries；The pH value of white fungus slurries is adjusted to 6.0~8.0, the complex enzyme formulation of mass fraction 0.5~2% is added, at 50~55 DEG C
0.5~1.5h of lower enzyme digestion reaction obtains white fungus enzymolysis liquid, the complex enzyme formulation include 3~7 parts 200,000 U/g neutral proteinases,
And 3~7 parts of 100,000 U/g pectases；To the white fungus enzymolysis liquid kind according to volume ratio 1: 5~1: 10 add distilled water 90~
2~4h, filtering are extracted at 100 DEG C, gained filtrate is concentrated into the medicinal extract that volume is 10%~20%, produces dried tremella extract.
Further, the preparation method of Gotu Kola P.E is in component C：
Centella is taken to be added to CO2In supercritical extract device, ethanol is as entrainer, and entrainer accounts for the volume hundred of total extractant
Divide than being 6%, extracting pressure 20MPa, 38 DEG C of temperature, CO2Flow 2.5ml/g crude drug min, extraction time 180min, obtain accumulated snow
Careless just extract；Extract at the beginning of centella is isolated effective group with AB-8 resin separating columns and with ethanol solution as eluant, eluent
Point, by water, 10%-20% ethanol, 35%-45% ethanol, 55%-70% ethanol sequentially eluting, wherein 35%-45% second
It is the Gotu Kola P.E after the target components concentration that alcohol and 55%-70% ethanol elutions get off.
Further, the present invention also provides the preparation method of the tencel facial mask of the above-mentioned composition containing dendrobium candidum, is specially：
S1：Each component is weighed；
S2：By in component A addition aqueous phase pot, stirring is warming up to 80-85 DEG C, stirs extremely without insulation 15-30 minutes after graininess,
It is standby as A phases；
S3：B component is put into dissolving tank, is stirred for being well mixed, it is standby as B phases；
S4：The temperature for setting emulsification pot is 80-85 DEG C, and above-mentioned A phases first are pumped into emulsification pot, adds B and mixes and stirs,
Open homogeneous 2-5 minutes, be incubated 15 minutes；
S5：Emulsion tank is cooled to 45 DEG C, adds component C, then stirs；
S6：Emulsion tank is cooled to 40 DEG C, adds D components, then stirs；
S7：Emulsion tank is cooled to 35-38 DEG C, then discharges, and stands to obtain facial mask liquid；
S8：Using pure short silk fiber as raw material, real silk non-woven cloth is prepared using spun lacing net-forming technology；Real silk non-woven cloth is taken off
Glue processing, degumming rate is 10%；15- will be soaked in facial mask liquid obtained by real silk non-woven cloth immersion step S7 after degumming process
After 20min take out, then the tencel face paper of moistening is placed in 40-50 DEG C of baking oven bake to its moisture be 30-50% when
Take out and be again dipped into facial mask liquid and soak 10-15min, then Vacuum Package is got product.
Several effect components contained in the cleawhite pack provided below the present invention are introduced：
Dendrobium candidum extract is rich in dendrobium polysaccharide and dendrobine, promotes the regeneration, activation, effect of maintenance of cell, persistently protects
It is wet moisten, softening skin, with good anti-aging and compact skin the effects such as, strengthen elasticity of skin, deep layer repair skin, allow
Skin is dynamic.
Tremella fructification extract is rich in polysaccharide compound, it is possible to increase cuticula moisture, and soft to skin
Soft sensation, improves skin electric conductivity integrated value, improves the water holding capacity of skin, and reduction water release constant improves the screen of skin
Hinder function, prevent evaporation of the moisture from skin.
Saccharomycete lysis thing extract is tissue respiratory factor, can improve cell aerobic respiration ability, strengthens cellular respiration,
Strengthen cell viability, promote cell turnover, Hydrolyzed Protein is crease-resistant, reparation effect, and effectively facilitates the absorption of active matter, is production
The multiplier of product effect.
Gotu Kola P.E has a conditioning skin health state, the skin that compacts, the work(such as promote the regeneration of aging skin, anti-floating swollen
Effect.
1,3-PD is a kind of transparent, colourless, tool stickiness and hygroscopic straight-chain fatty alcohol liquid, being commonly used for
In adornment water and Essence, in addition to moisture-retaining capacity, active ingredient can be helped to permeate, antiseptic power is also helped in addition, belong to small molecule
Moisturizing ingredient, can stay in cuticula by moisture.
Trehalose, is a kind of natural carbohydrate, and it can effectively protect epidermal cell membrane structure, and activating cell nurses one's health flesh
Skin, makes skin health natural, flexible.Trehalose can keep skin former in cell surface layer one layer of special diaphragm of formation
Nutritious and moisture, the mucus separated out from film can gently Glycerin make bright skin jade-like stone, it is gloss, tender.
Sodium Hyaluronate, supplement flesh bottom moisture helps to slow down skin TYR enzyme activity.
The application method of face mask of traditional Chinese medicine of the present invention containing the stem of noble dendrobium is：Before facial mask, first deeply cleaning is facial, then
Facial mask is overlying on face, enters facial mask and pastes skin, after 15-25 minutes, facial mask active material is absorbed by the skin, and takes facial mask, nothing
Need washing；
The present invention has the advantages that：
（1）The present invention is equipped with Tremella fructification extract, saccharomycete molten using dendrobium candidum extract as main active component
Born of the same parents' thing extract and Gotu Kola P.E, four kinds of component collaborations work, and go deep into skin bottom and keep the skin wet, strengthen skin moisturizing energy
Power, can make moisture content in skin keep appropriate, improve skin cell metabolism, conditioning skin microcirculation, and mending
Water lock while water, promotes skin to recover good barrier function, effectively reduces water loss, pins moisture, is kept for 24 hours
Long-acting water profit, so as to strengthen skin moisturizing degree, elasticity and suppleness, careful nourishing skin, scaly dry skin of releiving and itch so that
The natural regulating power of skin is recovered.
（2）The present invention is also containing 1,3- propane diols, glycerine, trehalose, 1,2- pentanediols, 1,2- hexylene glycols, same point of carbohydrate
Isomers, Sodium Hyaluronate, it is acted synergistically with other components of the present invention, and moisture needed for skin can be effectively caught after application, plus
Strong moisturizing, maintenance fiber desalinates wrinkle, lifting elasticity of skin and degree of compacting, repairs skin barrier function, makes skin smooth, soft
Soft and high resilience, while layer protecting film can be built up on skin, so as to play water lock moisturizing, the work of smooth microgroove
With so as to improve skin various problems caused by water shortage, being effectively improved skin state.
（3）Real silk non-woven cloth is handled, in addition to powerful water suction moisture retention, additionally it is possible to adsorb above-mentioned face
Film liquid, being adjacent to after skin of face slowly to discharge, and improve preserving moisture and protecting skin effect, not the used time be also easy to peel off.
（4）The preparation method that the present invention is provided, different raw material needs to add within the scope of different temperature, because good
It keeps the temperature of activity to be conditional to many active components, and temperature is too high to destroy its activity, and temperature is too low and can not be fine
Fully merged with other components, therefore different raw materials needs to select to add at suitable temperature, and abundant after adding
Stir so that various raw materials are sufficiently mixed, than more uniform, final its assimilation effect of obtained product also can be relatively good.
Embodiment
With reference to embodiment, the present invention will be described in detail, and embodiment is only the preferred embodiment of the present invention,
It is not limitation of the invention.
Embodiment 1
A kind of tencel facial mask of composition containing dendrobium candidum, is formulated by tetra- kinds of component raw materials of A, B, C and D：
Component A：30 parts of pure water, 2 parts of glycerine, 0.3 part of 1,2- pentanediols, 0.2 part of 1,2- hexylene glycols, 0.05 part of EDTA disodiums, hydroxyl
0.12 part of benzene methyl；
B component：1 part of 1,3- propane diols, 0.1 part of xanthans, 0.1 part of Tremella fructification extract, 0.06 part of hydroxyethyl cellulose,
0.01 part of Sodium Hyaluronate；
Component C：0.5 part of trehalose, carbohydrate isomer/pure water/0.1 part of citric acid/sodium citrate compound, dendrobium candidum
Extract/pure water/2 parts of butanediol compound, saccharomycete lysis thing extract/water/1 part of Phenoxyethanol compound, centella carry
Take 0.5 part of thing, 0.06 part of dipotassium glycyrrhizinate, 0.1 part of Phenoxyethanol, 0.05 part of hexapeptide -11,0.1 part of calcium pantothenate, xanthans 0.1
Part, 0.1 part of urea, 0.1 part of pungent glycol, 0.06 part of magnesium lactate, 0.1 part of Sensiva SC50,0.02 part of potassium chloride, potassium lactate
0.02 part, 0.02 part of magnesium chloride, 0.5 part of glucose；
D components：0.06 part of Cremophor RH40；
The preparation method of the tencel facial mask of the composition containing dendrobium candidum, be specially：
S1：Each component is weighed；
S2：By in component A addition aqueous phase pot, stirring is warming up to 80-85 DEG C, stirs extremely without insulation 15-30 minutes after graininess,
It is standby as A phases；
S3：B component is put into dissolving tank, is stirred for being well mixed, it is standby as B phases；
S4：The temperature for setting emulsification pot is 80-85 DEG C, and above-mentioned A phases first are pumped into emulsification pot, adds B and mixes and stirs,
Open homogeneous 2-5 minutes, be incubated 15 minutes；
S5：Emulsion tank is cooled to 45 DEG C, adds component C, then stirs；
S6：Emulsion tank is cooled to 40 DEG C, adds D components, then stirs；
S7：Emulsion tank is cooled to 35-38 DEG C, then discharges, and stands to obtain facial mask liquid；
S8：Using pure short silk fiber as raw material, real silk non-woven cloth is prepared using spun lacing net-forming technology；Real silk non-woven cloth is taken off
Glue processing, degumming rate is 10%；15- will be soaked in facial mask liquid obtained by real silk non-woven cloth immersion step S7 after degumming process
After 20min take out, then the tencel face paper of moistening is placed in 40-50 DEG C of baking oven bake to its moisture be 30-50% when
Take out and be again dipped into facial mask liquid and soak 10-15min, then Vacuum Package is got product.
Embodiment 2
A kind of tencel facial mask of composition containing dendrobium candidum, is formulated by tetra- kinds of component raw materials of A, B, C and D：
Component A：45 parts of pure water, 5 parts of glycerine, 0.5 part of part of 1,2- pentanediols, 0.6 part of 1,2- hexylene glycols, 0.1 part of EDTA disodiums,
0.15 part of methyl hydroxybenzoate；
B component：10 parts of 1,3- propane diols, 0.6 part of xanthans, 1 part of Tremella fructification extract, 0.08 part of hydroxyethyl cellulose,
0.1 part of Sodium Hyaluronate；
Component C：1 part of trehalose, carbohydrate isomer/pure water/0.3 part of citric acid/sodium citrate compound, dendrobium candidum are carried
Thing/pure water/8 parts of butanediol compound, saccharomycete lysis thing extract/water/3 parts of Phenoxyethanol compound, centella is taken to extract
2 parts of thing, 0.08 part of dipotassium glycyrrhizinate, 0.5 part of Phenoxyethanol, 2 parts of hexapeptide -11,0.5 part of calcium pantothenate, 0.2 part of xanthans, urea
1 part, 0.25 part of pungent glycol, 0.08 part of magnesium lactate, 0.25 part of Sensiva SC50,0.05 part of potassium chloride, 0.05 part of potassium lactate, chlorine
Change 0.05 part of magnesium, 2 parts of glucose；
D components：0.04 part of essence, 0.09 part of Cremophor RH40；
Wherein, the preparation method of dendrobium candidum extract is：
The first step：Dendrobium candidum is harvested before blooming, 30~60min is rinsed with purified water, then rinsed 3 times with purified water；So
The segment of 1-3cm length is cut into afterwards, it is freezed completely solid, then carries out vacuum freeze drying more than 24 hours, dried iron
The skin stem of noble dendrobium is placed in oscillatory type ultramicro grinding grinding kneading machine and ultramicro grinding 5-10min is carried out at a temperature of -25 DEG C to -30 DEG C,
Obtain dendrobium candidum ultrafine powder；
Second step, by above-mentioned dendrobium candidum ultrafine powder, according to solid-liquid ratio 1:10~1:40g/ml, adds water and is sufficiently mixed, use
When carrying out separation of solid and liquid, wherein Microwave Extraction after Microwave Extraction, microwave treatment power is 400W, frequency 2450MHz, and the time is
Extract solution A is obtained after 15-20min, separation of solid and liquid and slag A is extracted；
The ethanol that 3rd step, said extracted slag A and volume fraction are 20~100% is according to solid-liquid ratio 1:8~1:12 g/ml are mixed,
Then using ultrasonic wave extraction progress separation of solid and liquid, 20~90 DEG C of Extracting temperature, 1~2h of extraction time, separation of solid and liquid is carried
Take liquid B and extract slag B；
4th step, extract solution B merges after removing ethanol through reduced vacuum concentration with extract solution A, is carried out using miillpore filter
Filter out miscellaneous, obtain liquor C；
5th step, liquor C adds 1~5h of protease hydrolyzed, uses molecular weight ranges for 3000~5000Da nanofiltration membrane enzyme
Liquid is solved, filtrate D is obtained, NF membrane retention part is dendrobium polysaccharide；
6th step, filtrate D adds glycosylhydrolase, digests 1~3h, then will use nanofiltration membrane of the molecular weight for 1000Da,
Filtrate E is obtained, filtrate E is spray-dried to obtain dendrobine.
7th step：The dendrobium polysaccharide obtained in 5th step is mixed with the dendrobine obtained in the 6th step, iron sheet stone is prepared
Dry measure used in former times extract.
The preparation method of the tencel facial mask of the composition containing dendrobium candidum, be specially：
S1：Each component is weighed；
S2：By in component A addition aqueous phase pot, stirring is warming up to 80-85 DEG C, stirs extremely without insulation 15-30 minutes after graininess,
It is standby as A phases；
S3：B component is put into dissolving tank, is stirred for being well mixed, it is standby as B phases；
S4：The temperature for setting emulsification pot is 80-85 DEG C, and above-mentioned A phases first are pumped into emulsification pot, adds B and mixes and stirs,
Open homogeneous 2-5 minutes, be incubated 15 minutes；
S5：Emulsion tank is cooled to 45 DEG C, adds component C, then stirs；
S6：Emulsion tank is cooled to 40 DEG C, adds D components, then stirs；
S7：Emulsion tank is cooled to 35-38 DEG C, then discharges, and stands to obtain facial mask liquid；
S8：Using pure short silk fiber as raw material, real silk non-woven cloth is prepared using spun lacing net-forming technology；Real silk non-woven cloth is taken off
Glue processing, degumming rate is 10%；15- will be soaked in facial mask liquid obtained by real silk non-woven cloth immersion step S7 after degumming process
After 20min take out, then the tencel face paper of moistening is placed in 40-50 DEG C of baking oven bake to its moisture be 30-50% when
Take out and be again dipped into facial mask liquid and soak 10-15min, then Vacuum Package is got product.
Embodiment 3
A kind of tencel facial mask of composition containing dendrobium candidum, is formulated by tetra- kinds of component raw materials of A, B, C and D：
Component A：40 parts of pure water, 3 parts of glycerine, 0.4 part of part of 1,2- pentanediols, 0.5 part of 1,2- hexylene glycols, 0.08 part of EDTA disodiums,
0.13 part of methyl hydroxybenzoate；
B component：5 parts of 1,3- propane diols, 0.4 part of xanthans, 0.6 part of Tremella fructification extract, 0.07 part of hydroxyethyl cellulose,
0.06 part of Sodium Hyaluronate；
Component C：0.3 part of trehalose, carbohydrate isomer/pure water/0.12 part of citric acid/sodium citrate compound, iron sheet stone
Dry measure used in former times extract/pure water/5 parts of butanediol compound, saccharomycete lysis thing extract/water/2 parts of Phenoxyethanol compound, centella
1 part of extract, 0.07 part of dipotassium glycyrrhizinate, 0.3 part of Phenoxyethanol, 1 part of hexapeptide -11,0.3 part of calcium pantothenate, xanthans 0.15
Part, 0.6 part of urea, 0.15 part of pungent glycol, 0.07 part of magnesium lactate, 0.15 part of Sensiva SC50,0.03 part of potassium chloride, potassium lactate
0.03 part, 0.03 part of magnesium chloride, 1 part of glucose；
D components：0.02 part of essence, 0.07 part of Cremophor RH40；
Wherein, the preparation method of dendrobium candidum extract is：
The first step：Dendrobium candidum is harvested before blooming, 30~60min is rinsed with purified water, then rinsed 3 times with purified water；So
The segment of 1-3cm length is cut into afterwards, it is freezed completely solid, then carries out vacuum freeze drying more than 24 hours, dried iron
The skin stem of noble dendrobium is placed in oscillatory type ultramicro grinding grinding kneading machine and ultramicro grinding 5-10min is carried out at a temperature of -25 DEG C to -30 DEG C,
Obtain dendrobium candidum ultrafine powder；
Second step, by above-mentioned dendrobium candidum ultrafine powder, according to solid-liquid ratio 1:10~1:40g/ml, adds water and is sufficiently mixed, use
When carrying out separation of solid and liquid, wherein Microwave Extraction after Microwave Extraction, microwave treatment power is 400W, frequency 2450MHz, and the time is
Extract solution A is obtained after 15-20min, separation of solid and liquid and slag A is extracted；
The ethanol that 3rd step, said extracted slag A and volume fraction are 20~100% is according to solid-liquid ratio 1:8~1:12 g/ml are mixed,
Then using ultrasonic wave extraction progress separation of solid and liquid, 20~90 DEG C of Extracting temperature, 1~2h of extraction time, separation of solid and liquid is carried
Take liquid B and extract slag B；
4th step, extract solution B merges after removing ethanol through reduced vacuum concentration with extract solution A, is carried out using miillpore filter
Filter out miscellaneous, obtain liquor C；
5th step, liquor C adds 1~5h of protease hydrolyzed, uses molecular weight ranges for 3000~5000Da nanofiltration membrane enzyme
Liquid is solved, filtrate D is obtained, NF membrane retention part is dendrobium polysaccharide；
6th step, filtrate D adds glycosylhydrolase, digests 1~3h, then will use nanofiltration membrane of the molecular weight for 1000Da,
Filtrate E is obtained, filtrate E is spray-dried to obtain dendrobine.
7th step：The dendrobium polysaccharide obtained in 5th step is mixed with the dendrobine obtained in the 6th step, iron sheet stone is prepared
Dry measure used in former times extract.
Wherein, the preparation method of Tremella fructification extract is in B component：Tremella fructification dry product is taken, with distillation hydroecium
The lower immersion 35-45min of temperature, is placed in beater and fully crushes, white fungus slurries are made；Adjust the pH value of white fungus slurries to 6.0~
8.0, the complex enzyme formulation of mass fraction 0.5~2% is added, 0.5~1.5h of enzyme digestion reaction obtains white fungus enzymolysis at 50~55 DEG C
Liquid, the complex enzyme formulation includes 3~7 parts of 200,000 U/g neutral proteinases and 3~7 parts of 100,000 U/g pectases；To
The white fungus enzymolysis liquid kind is added according to volume ratio 1: 5~1: 10 extracts 2~4h at 90~100 DEG C of distilled water, filtering, gained filtrate
The medicinal extract that volume is 10%~20% is concentrated into, dried tremella extract is produced.
Wherein, the preparation method of Gotu Kola P.E is in component C：Centella is taken to be added to CO2In supercritical extract device,
Ethanol is as entrainer, and the percent by volume that entrainer accounts for total extractant is 6%, extracting pressure 20MPa, 38 DEG C of temperature, CO2
Flow 2.5ml/g crude drug min, extraction time 180min, obtain centella just extract；By extract at the beginning of centella with AB-8 trees
Fat splitter and as eluant, eluent active principle is isolated with ethanol solution, by water, 10%-20% ethanol, 35%-45% second
The target group that the sequentially eluting of alcohol, 55%-70% ethanol, wherein 35%-45% ethanol and 55%-70% ethanol elutions get off
Divide after concentration is the Gotu Kola P.E.
The preparation method of the tencel facial mask of the composition containing dendrobium candidum, be specially：
S1：Each component is weighed；
S2：By in component A addition aqueous phase pot, stirring is warming up to 80-85 DEG C, stirs extremely without insulation 15-30 minutes after graininess,
It is standby as A phases；
S3：B component is put into dissolving tank, is stirred for being well mixed, it is standby as B phases；
S4：The temperature for setting emulsification pot is 80-85 DEG C, and above-mentioned A phases first are pumped into emulsification pot, adds B and mixes and stirs,
Open homogeneous 2-5 minutes, be incubated 15 minutes；
S5：Emulsion tank is cooled to 45 DEG C, adds component C, then stirs；
S6：Emulsion tank is cooled to 40 DEG C, adds D components, then stirs；
S7：Emulsion tank is cooled to 35-38 DEG C, then discharges, and stands to obtain facial mask liquid；
S8：Using pure short silk fiber as raw material, real silk non-woven cloth is prepared using spun lacing net-forming technology；Real silk non-woven cloth is taken off
Glue processing, degumming rate is 10%；15- will be soaked in facial mask liquid obtained by real silk non-woven cloth immersion step S7 after degumming process
After 20min take out, then the tencel face paper of moistening is placed in 40-50 DEG C of baking oven bake to its moisture be 30-50% when
Take out and be again dipped into facial mask liquid and soak 10-15min, then Vacuum Package is got product.
Embodiment described above only expresses embodiments of the present invention, and it describes more specific and detailed, but can not
Therefore the limitation to the scope of the claims of the present invention is interpreted as, as long as the skill obtained using the form of equivalent substitution or equivalent transformation
Art scheme, all should fall within the scope and spirit of the invention.
Claims (5)
1. the tencel facial mask of a kind of composition containing dendrobium candidum, it is characterised in that it is prepared by tetra- kinds of component raw materials of A, B, C and D
Form：
Component A：30-45 parts of pure water, 2-5 parts of glycerine, 0.3-0.5 parts of 1,2- pentanediols, 0.2-0.6 parts of 1,2- hexylene glycols, EDTA
0.05-0.1 parts of disodium, 0.12-0.15 parts of methyl hydroxybenzoate；
B component：1-10 parts of 1,3- propane diols, 0.1-0.6 parts of xanthans, 0.1-1 parts of Tremella fructification extract, hydroxy ethyl fiber
Plain 0.06-0.08 parts, 0.01-0.1 parts of Sodium Hyaluronate；
Component C：0.5-1 parts of trehalose, carbohydrate isomer/pure water/0.1-0.3 parts of citric acid/sodium citrate compound, iron
Skin Herba Dendrobii extract/pure water/2-8 parts of butanediol compound, saccharomycete lysis thing extract/water/Phenoxyethanol compound 1-3
Part, 0.5-2 parts of Gotu Kola P.E, 0.06-0.08 parts of dipotassium glycyrrhizinate, 0.1-0.5 parts of Phenoxyethanol, the 0.05-2 of hexapeptide -11
Part, 0.1-0.5 parts of calcium pantothenate, 0.1-0.2 parts of xanthans, 0.1-1 parts of urea, pungent glycol 0.1-0.25 parts, magnesium lactate 0.06-
0.08 part, 0.1-0.25 parts of Sensiva SC50,0.02-0.05 parts of potassium chloride, 0.02-0.05 parts of potassium lactate, magnesium chloride 0.02-
0.05 part, 0.5-2 parts of glucose；
D components：0-0.04 parts of essence, 0.06-0.09 parts of Cremophor RH40.
2. the tencel facial mask of the composition as claimed in claim 1 containing dendrobium candidum, it is characterised in that dendrobium candidum is carried in component C
The preparation method for taking thing is：
The first step：Dendrobium candidum is harvested before blooming, 30~60min is rinsed with purified water, then rinsed 3 times with purified water；So
The segment of 1-3cm length is cut into afterwards, it is freezed completely solid, then carries out vacuum freeze drying more than 24 hours, dried iron
The skin stem of noble dendrobium is placed in oscillatory type ultramicro grinding grinding kneading machine and ultramicro grinding 5-10min is carried out at a temperature of -25 DEG C to -30 DEG C,
Obtain dendrobium candidum ultrafine powder；
Second step, by above-mentioned dendrobium candidum ultrafine powder, according to solid-liquid ratio 1:10~1:40g/ml, adds water and is sufficiently mixed, use
When carrying out separation of solid and liquid, wherein Microwave Extraction after Microwave Extraction, microwave treatment power is 400W, frequency 2450MHz, and the time is
Extract solution A is obtained after 15-20min, separation of solid and liquid and slag A is extracted；
The ethanol that 3rd step, said extracted slag A and volume fraction are 20~100% is according to solid-liquid ratio 1:8~1:12 g/ml are mixed,
Then using ultrasonic wave extraction progress separation of solid and liquid, 20~90 DEG C of Extracting temperature, 1~2h of extraction time, separation of solid and liquid is carried
Take liquid B and extract slag B；
4th step, extract solution B merges after removing ethanol through reduced vacuum concentration with extract solution A, is carried out using miillpore filter
Filter out miscellaneous, obtain liquor C；
5th step, liquor C adds 1~5h of protease hydrolyzed, uses molecular weight ranges for 3000~5000Da nanofiltration membrane enzyme
Liquid is solved, filtrate D is obtained, NF membrane retention part is dendrobium polysaccharide；
6th step, filtrate D adds glycosylhydrolase, digests 1~3h, then will use nanofiltration membrane of the molecular weight for 1000Da,
Filtrate E is obtained, filtrate E is spray-dried to obtain dendrobine；
7th step：The dendrobium polysaccharide obtained in 5th step is mixed with the dendrobine obtained in the 6th step, dendrobium candidum is prepared and carries
Take thing.
3. the tencel facial mask of the composition as claimed in claim 1 containing dendrobium candidum, it is characterised in that Tremella fructification in B component
The preparation method of extract is：Tremella fructification dry product is taken, 35-45min is soaked at room temperature with distilled water, is placed in beater and fills
Divide broken, white fungus slurries are made；The pH value of white fungus slurries is adjusted to 6.0~8.0, the complex enzyme of mass fraction 0.5~2% is added
Preparation, 0.5~1.5h of enzyme digestion reaction obtains white fungus enzymolysis liquid at 50~55 DEG C, and the complex enzyme formulation includes the 20 of 3~7 parts
Ten thousand U/g neutral proteinases and 3~7 parts of 100,000 U/g pectases；To the white fungus enzymolysis liquid kind according to volume ratio 1: 5~1:
2~4h, filtering are extracted at 10 90~100 DEG C of distilled water of addition, gained filtrate is concentrated into the medicinal extract that volume is 10%~20%, i.e.,
Obtain dried tremella extract.
4. the tencel facial mask of the composition as claimed in claim 1 containing dendrobium candidum, it is characterised in that centella is extracted in component C
The preparation method of thing is：Centella is taken to be added to CO2In supercritical extract device, ethanol is as entrainer, and entrainer accounts for total extraction
The percent by volume of solvent is 6%, extracting pressure 20MPa, 38 DEG C of temperature, CO2Flow 2.5ml/g crude drug min, extraction time
180min, obtains centella just extract；Extract at the beginning of centella is regard as elution with AB-8 resin separating columns and with ethanol solution
Active principle is isolated in agent, by water, 10%-20% ethanol, 35%-45% ethanol, 55%-70% ethanol sequentially eluting, its
It is the Gotu Kola P.E after the target components concentration that middle 35%-45% ethanol and 55%-70% ethanol elutions get off.
5. the preparation method of the tencel facial mask of the composition containing dendrobium candidum as described in claim any one of 1-4, it is characterised in that its
Preparation method is：
S1：Each component is weighed；
S2：By in component A addition aqueous phase pot, stirring is warming up to 80-85 DEG C, stirs extremely without insulation 15-30 minutes after graininess,
It is standby as A phases；
S3：B component is put into dissolving tank, is stirred for being well mixed, it is standby as B phases；
S4：The temperature for setting emulsification pot is 80-85 DEG C, and above-mentioned A phases first are pumped into emulsification pot, adds B and mixes and stirs,
Open homogeneous 2-5 minutes, be incubated 15 minutes；
S5：Emulsion tank is cooled to 45 DEG C, adds component C, then stirs；
S6：Emulsion tank is cooled to 40 DEG C, adds D components, then stirs；
S7：Emulsion tank is cooled to 35-38 DEG C, then discharges, and stands to obtain facial mask liquid；
S8：Using pure short silk fiber as raw material, real silk non-woven cloth is prepared using spun lacing net-forming technology；Real silk non-woven cloth is taken off
Glue processing, degumming rate is 10%；15- will be soaked in facial mask liquid obtained by real silk non-woven cloth immersion step S7 after degumming process
After 20min take out, then the tencel face paper of moistening is placed in 40-50 DEG C of baking oven bake to its moisture be 30-50% when
Take out and be again dipped into facial mask liquid and soak 10-15min, then Vacuum Package is got product.
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| CN109998947A (en) * | 2019-04-29 | 2019-07-12 | 深圳津梁生活科技有限公司 | Tremella skin care freeze-drying facial mask without preservative and preparation method thereof |
| CN111374926A (en) * | 2020-03-30 | 2020-07-07 | 浙江森宇有限公司 | Dendrobium officinale lifting and tightening mask and preparation method thereof |
| CN111388361A (en) * | 2020-03-06 | 2020-07-10 | 王小平 | Preparation method of ultrafine black fungus powder, black fungus mask prepared from ultrafine black fungus powder and preparation method of black fungus mask |
| CN113476389A (en) * | 2021-08-25 | 2021-10-08 | 四川干邦亚农业科技有限公司 | Dendrobium moisturizing and repairing mask and preparation method thereof |
| CN115154382A (en) * | 2022-06-30 | 2022-10-11 | 常州琉璃光生物科技有限公司 | Herba centellae efficient repairing mask and preparation method thereof |
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| CN111374926A (en) * | 2020-03-30 | 2020-07-07 | 浙江森宇有限公司 | Dendrobium officinale lifting and tightening mask and preparation method thereof |
| CN113476389A (en) * | 2021-08-25 | 2021-10-08 | 四川干邦亚农业科技有限公司 | Dendrobium moisturizing and repairing mask and preparation method thereof |
| CN115154382A (en) * | 2022-06-30 | 2022-10-11 | 常州琉璃光生物科技有限公司 | Herba centellae efficient repairing mask and preparation method thereof |
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Application publication date: 20170905 |