CN105362206A - Maca moisture mask with oxidation-resistant effect and preparation method - Google Patents
Maca moisture mask with oxidation-resistant effect and preparation method Download PDFInfo
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- CN105362206A CN105362206A CN201510062365.1A CN201510062365A CN105362206A CN 105362206 A CN105362206 A CN 105362206A CN 201510062365 A CN201510062365 A CN 201510062365A CN 105362206 A CN105362206 A CN 105362206A
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Abstract
The invention relates to a maca moisture mask with the oxidation-resistant effect and a preparation method. The maca moisture mask comprises konjac refined flour, a purple maca fresh root extract, a pyracantha fortuneana fruit extract, a ginkgo leaf extract, a white fungus extract and a luffa extract. According to the maca mask, the pure natural plant extracts are main components and can supplement rich oxidation-resistant factors for skin. The mask has the effects of delaying senescence and increasing skin elasticity, is soft in texture and good in skin attachment and can absorb and release a large number of nutritional ingredients. As known from mouse anti-aging experiments, the maca moisture mask can remarkably increase the content of hydroxyproline and superoxide dismutase and reduce the content of malondialdehyde and lipofuscin. By means of water retention and skin irritation experiments on skin of healthy females, it is known that the mask has good moisture retention, is free of irritation and has an ideal face beautifying effect, and anaphylaxis is not likely to happen.
Description
Technical field
The invention belongs to cosmetics and skincare product field, be specifically related to a kind of Lepidinm meyenii Walp moisture saver mask and the preparation method with anti-oxidation efficacy.
Background technology
Women thirsts for keeping young, the skin that can break of playing wind and stringing instruments, and does not wish that wrinkle, mottle etc. climb to oneself on the face with the passing of the years.But women is after 35 years old, skin of face is due to outside being chronically exposed to, and through exposing to the weather, Skin Cell just starts to enter aging period.The increase at age and the impact by external environment, the oxygen-derived free radicals in body can increase gradually, superoxide dismutase (SOD) can be made not enough, cause too much oxygen-derived free radicals and skin corium cell to produce oxidation reaction, cause chloasma.
Beautiful spring-time easily dies, appearance is easily old, and this is the rule of the Nature, and we cannot change.But if before skin aging, we just can improve the consciousness of self-improvement skin, improve self Scavenging activity to oxygen-derived free radicals, mottle, obscure, microgroove etc. at least can be allowed to arrive a little later.Therefore, the antioxidation of skin, replenishing water and preserving moisture work just seem very important.And facial film is the most frequently used basic beauty and skin care product, it directly acts on the skin after cleaning, more effectively can infiltrate through skin, utilize the blink covering face, the air that temporary transient isolation is extraneous and pollution, improve skin temperature, the pore expansion of skin, promote sweat gland secretion and metabolism, make the oxygen content of skin increase.Facial film is conducive to the oil substances that skin gets rid of the metabolic product of epidermis cell and accumulation, and the moisture in facial film infiltrates the horny layer of skin epidermis, and skin becomes soft, increases elasticity.
From eighties of last century eighties, skin expert just finds, various natural material is added in skin care item, good nourishing effect is had to skin, and have no side effect, particularly from plant, effective component extracting adds in skin care item and has more remarkable effect, but have not been reported based on the skin care item of new resource food Lepidinm meyenii Walp exploitation.
Summary of the invention
The technical problem to be solved in the present invention is: provide a kind of Lepidinm meyenii Walp moisture saver mask and the preparation method with anti-oxidation efficacy, fills up Lepidinm meyenii Walp blank in the use of skin care industry, solves the various skin problems that the reason such as air pollution, fatigue causes.
The technical scheme that the present invention solves the problem is: provide a kind of Lepidinm meyenii Walp moisture saver mask with anti-oxidation efficacy, described Lepidinm meyenii Walp moisture saver mask comprises following component: konjaku powder, the fresh root extract of purple Lepidinm meyenii Walp, pyracantha fortuneana extract, Folium Ginkgo extract, Tremella extract, Fructus Luffae extract.
In Lepidinm meyenii Walp moisture saver mask provided by the invention, the mass ratio of each component is: konjaku powder 8 ~ 12, the fresh root extract 12 ~ 18 of purple Lepidinm meyenii Walp, pyracantha fortuneana extract 10 ~ 15, Folium Ginkgo extract 5 ~ 10, Tremella extract 1 ~ 5, Fructus Luffae extract 1 ~ 5.
In Lepidinm meyenii Walp moisture saver mask provided by the invention, in described konjaku powder, the content of Rhizoma amorphophalli glucomannan is greater than 90%.
In Lepidinm meyenii Walp moisture saver mask provided by the invention, the preparation method of the fresh root extract of described purple Lepidinm meyenii Walp is: get fresh of purple Lepidinm meyenii Walp, clean up, section, be transferred to extraction vessel after smashing to pieces with pulverizer, add the ethanol water of 70% ~ 90% by solid-liquid ratio 1: 6 ~ 1: 10, at 30 ~ 50 DEG C, stir extraction 1 ~ 3h, be cooled to room temperature, cross leaching filtrate; Residue after filtration extracts twice after the same method; Merge three gained filtrates, be concentrated into the extractum that volume is 10% ~ 20%, obtain the fresh root extract of purple Lepidinm meyenii Walp.
In Lepidinm meyenii Walp moisture saver mask provided by the invention, the preparation method of described pyracantha fortuneana extract is: get fresh pyracantha fortuneana and be placed in refiner, extraction vessel are transferred to, this ethanol water first acid for adjusting pH to 2.0 ~ 4.0 after the ethanol water adding 70% ~ 90% by solid-liquid ratio 1: 6 ~ 1: 10 carries out homogenate; Stir extraction 1 ~ 3h at 30 ~ 50 DEG C, be cooled to room temperature, centrifuging and taking supernatant, be concentrated into the extractum that volume is 10% ~ 20%, obtain pyracantha fortuneana extract.
In Lepidinm meyenii Walp moisture saver mask provided by the invention, the preparation method of described Folium Ginkgo extract is: get green fresh Folium Ginkgo, dries and is less than 10% to moisture, pulverize after cleaning at putting into 45 ~ 60 DEG C, drying baker, crosses 20 mesh sieves and obtains Ginkgo Leaf; Dropped into by Ginkgo Leaf and extract vessel, such as round-bottomed flask, add the ethanol water of 50 ~ 80% by solid-liquid ratio 1: 5 ~ 1: 10,70 ~ 85 DEG C of reflux, extract, 1 ~ 3h, are cooled to room temperature, cross leaching supernatant; Residue after filtration extracts twice after the same method; Merge three gained supernatant, being concentrated into volume is 10% ~ 20%, and the distilled water adding 1 ~ 3 times of volume carries out water precipitating, and after room temperature leaves standstill 24 ~ 48h, filter, gained filtrate is concentrated into the extractum that volume is 10% ~ 20%, obtains Folium Ginkgo extract.
In Lepidinm meyenii Walp moisture saver mask provided by the invention, the preparation method of described Tremella extract is: get Tremella fructification dry product, soaks 30 ~ 50min with under distilled water room temperature, is placed in beater fully broken, obtained Tremella serosity; Regulate pH value to 6.0 ~ 8.0 of Tremella serosity, add the compound enzymic preparation of mass fraction 0.5 ~ 2%, at 50 ~ 55 DEG C, enzyme digestion reaction 0.5 ~ 1.5h obtains Tremella enzymolysis solution, and described compound enzymic preparation comprises the 200000 U/g neutral protease of 3 ~ 7 parts and the 100000 U/g pectases of 3 ~ 7 parts; Lixiviate 2 ~ 4h at adding distilled water 90 ~ 100 DEG C according to volume ratio 1: 5 ~ 1: 10 to this Tremella enzymolysis solution kind, filter, gained filtrate is concentrated into the extractum that volume is 10% ~ 20%, obtains Tremella extract.
In Lepidinm meyenii Walp moisture saver mask provided by the invention, the preparation method of described Fructus Luffae extract is: cleaned by fresh Fructus Luffae, grind after chopping, adds the ethanol water of 70 ~ 90% by solid-liquid ratio 1: 5 ~ 1: 10, reflux, extract, 4 ~ 6h at 60 ~ 70 DEG C, crosses leaching supernatant; Residue after filtration extracts once after the same method; Merge twice gained supernatant, be concentrated into the extractum that volume is 10% ~ 20%, obtain Fructus Luffae extract.
The present invention also provides a kind of preparation method with the Lepidinm meyenii Walp moisture saver mask of anti-oxidation efficacy, and described preparation method comprises:
The selection of S1, konjaku powder: select the konjaku powder that the content of Rhizoma amorphophalli glucomannan is greater than 90%;
The preparation method of S2, the fresh root extract of purple Lepidinm meyenii Walp: get fresh of purple Lepidinm meyenii Walp, clean up, section, extraction vessel are transferred to after smashing to pieces with pulverizer, add the ethanol water (note: the ethanol water in various embodiments of the present invention all uses percent by volume to represent) of 70% ~ 90% (v/v) by solid-liquid ratio 1: 6 ~ 1: 10, stir extraction 1 ~ 3h at 30 ~ 50 DEG C, be cooled to room temperature, cross leaching filtrate, use the mode such as sucking filtration, plate-and-frame filtration; Residue after filtration extracts twice after the same method; Merge three gained filtrates, be concentrated into the extractum that volume is 10% ~ 20%, obtain the fresh root extract of purple Lepidinm meyenii Walp;
The preparation method of S3, pyracantha fortuneana extract: get fresh pyracantha fortuneana and be placed in refiner, extraction vessel are transferred to after the ethanol water adding 70% ~ 90% by solid-liquid ratio 1: 6 ~ 1: 10 carries out homogenate, this ethanol water first acid for adjusting pH to 2.0 ~ 4.0, the chemical stability of polyphenol isoreactivity material in protection pyracantha fortuneana; Stir extraction 1 ~ 3h at 30 ~ 50 DEG C, be cooled to room temperature, centrifuging and taking supernatant, centrifugal rotational speed 3000rpm, be concentrated into the extractum that volume is 10% ~ 20%, obtain pyracantha fortuneana extract;
The preparation method of S4, Folium Ginkgo extract: get green fresh Folium Ginkgo, dries at putting into 45 ~ 60 DEG C, drying baker and is less than 10% to moisture, pulverize after cleaning, crosses 20 mesh sieves and obtains Ginkgo Leaf; Dropped into by Ginkgo Leaf and extract vessel, such as round-bottomed flask, add the ethanol water of 50 ~ 80% by solid-liquid ratio 1: 5 ~ 1: 10,70 ~ 85 DEG C of reflux, extract, 1 ~ 3h, are cooled to room temperature, cross leaching supernatant; Residue after filtration extracts twice after the same method; Merge three gained supernatant, being concentrated into volume is 10% ~ 20%, and the distilled water adding 1 ~ 3 times of volume carries out water precipitating, and after room temperature leaves standstill 24 ~ 48h, filter, gained filtrate is concentrated into the extractum that volume is 10% ~ 20%, obtains Folium Ginkgo extract;
The preparation method of S5, Tremella extract: get Tremella fructification dry product, soaks 30 ~ 50min with under distilled water room temperature, is placed in beater fully broken, obtained Tremella serosity; Regulate pH value to 6.0 ~ 8.0 of Tremella serosity, add the compound enzymic preparation of mass fraction 0.5 ~ 2%, at 50 ~ 55 DEG C, enzyme digestion reaction 0.5 ~ 1.5h obtains Tremella enzymolysis solution, and described compound enzymic preparation comprises the 200000 U/g neutral protease of 3 ~ 7 parts and the 100000 U/g pectases of 3 ~ 7 parts; Lixiviate 2 ~ 4h at adding distilled water 90 ~ 100 DEG C according to volume ratio 1: 5 ~ 1: 10 to this Tremella enzymolysis solution kind, filter, gained filtrate is concentrated into the extractum that volume is 10% ~ 20%, obtains Tremella extract;
The preparation method of S6, Fructus Luffae extract: cleaned by fresh Fructus Luffae, grind after chopping, adds the ethanol water of 70 ~ 90% by solid-liquid ratio 1: 5 ~ 1: 10, reflux, extract, 4 ~ 6h at 60 ~ 70 DEG C, crosses leaching supernatant; Residue after filtration extracts once after the same method; Merge twice gained supernatant, be concentrated into the extractum that volume is 10% ~ 20%, obtain Fructus Luffae extract;
S7, prepare described Lepidinm meyenii Walp moisture saver mask by following mass ratio: konjaku powder 8 ~ 12, the fresh root extract 12 ~ 18 of purple Lepidinm meyenii Walp, pyracantha fortuneana extract 10 ~ 15, Folium Ginkgo extract 5 ~ 10, Tremella extract 1 ~ 5, Fructus Luffae extract 1 ~ 5.
In the preparation method of Lepidinm meyenii Walp moisture saver mask provided by the invention, also comprise after described step S7:
S8, above-mentioned substance proportionally to be mixed, after distilled water allotment, obtain emulsion and pour in facial film mould, first leave standstill 10 ~ 14h, then in steamer, steam 30 ~ 50min ripening molding, then in-20 ~-30 DEG C of washings of thawing after freezing 3 ~ 5 days, until pH is 6.0 ~ 8.0, spin-dry, is placed in the ozone sterilization treatment 20 ~ 40min of 0.5 ~ 1.5ppm, is packaged into bag and get final product.
Implement the present invention, there is following beneficial effect: active component is all extract from pure natural plant, effectively can improve the oxidation resistance of skin, and inject sufficient moisture for skin, prevent the moisture in keratodermatitis from evaporate, make the plant essence of load be easy to absorption, face is kept to moisten, avoid face skin accelerated ageing, reduce facial wrinkles, there is desirable antioxidation, the effect of slow down aging.Meanwhile, the mask carriers be made up of konjaku powder is a kind of sponge structure, except having powerful water suction moisture retention, the elite of said extracted thing can also be adsorbed, being adjacent to after skin of face can slow releasing, and improve preserving moisture and protecting skin effect, the used time is not easy to peel off yet.
Detailed description of the invention
In order to make object of the present invention, technical scheme and advantage clearly understand, below in conjunction with embodiment, the present invention is further elaborated.Should be appreciated that specific embodiment described herein only in order to explain the present invention, be not intended to limit the present invention.
Lepidinm meyenii Walp (Maca) belongs to the herbaceous plant of Cruciferae separate row Vegetable spp, originates in the mountain area, Andean of Peru height above sea level 3500 ~ 4500m.There is resisting fatigue, relieving stress, antioxidation, slow down aging, raising fertility, alleviate many-sided effects such as climacteric syndrome.Existing a lot of research shows, Lepidinm meyenii Walp, as a kind of nutritious medicine food dual purpose plant, has remarkable effect in antioxidation.The mechanism of the antioxidant activity of maca polysaccharide may be due to maca polysaccharide molecule having reproducibility group, can with oxidant-active oxygen generation redox reaction.Some researcheres are also had to compare the antioxidant effect of three kinds of different colours Lepidinm meyenii Walp, result shows, and the Lepidinm meyenii Walp of purple, yellow, black three kinds of different coat color all presents antioxidant activity, but purple best results, its antioxidation mechanism is because purple Lepidinm meyenii Walp inhibits lipid peroxidation active.Therefore, the present invention just selects the fresh root extract of purple Lepidinm meyenii Walp as the main active of facial film.
The Lepidinm meyenii Walp moisture saver mask with anti-oxidation efficacy of the present invention, comprises following component: konjaku powder, the fresh root extract of purple Lepidinm meyenii Walp, pyracantha fortuneana extract, Folium Ginkgo extract, Tremella extract, Fructus Luffae extract.
Rhizoma amorphophalli is Araeceae Amorphophallus, belongs to herbaceos perennial.In Rhizoma amorphophalli, topmost active component is Rhizoma amorphophalli glucomannan (KGM), konjak portuguese gansu polyose glycan molecule be about by mol ratio 1: 1.6 D-Glucose and the natural polysaccharide that is combined into of D-MANNOSE.KGM has good chemical stability and biocompatibility, hygroscopicity, hydrophilic and biodegradability etc., and thus it is with a wide range of applications in fields such as medicine, weaving, food, chemical industry, agriculturals.Rhizoma amorphophalli glucomannan KGM can Fast-swelling, and be dissolved in water, can form a kind of hydrosol of thickness, its water absorbing capacity reaches 80 ~ 120 times.In the present invention, use konjaku powder as mask carriers, the elite of said extracted thing while water suction, moisture retention, can also be adsorbed, promote the release of skin of face.Preferably, in konjaku powder, the content of Rhizoma amorphophalli glucomannan is greater than 90%.
Pyracantha fortuneana has another name called Fructus Pyracanthae (Fructus Pyracanthae Fortuneanae), torch fruit etc., is mainly distributed in mountain region and the hilly country in the regions such as China southeast, southwest and northwest.Pyracantha fortuneana nutrient composition content enriches: amino acid classes is complete, is rich in soluble sugar, protein, the vitamin such as VC, VE, the mineral elements such as selenium; The antioxidant reductases such as highly active superoxide dismutase (SOD), glutathion peroxidase (GSH-Px); The flavonoid components content such as anthocyanidin are high.The anthocyanidin that pyracantha fortuneana is rich in is the anti-aging and nutritive supplement of pure natural; research proves that anthocyanidin is that mankind nowadays finds the most effective antioxidant; it can protect human body from the damage of the harmful substances such as free radical; its antioxygenic property exceeds 50 times than vitamin E; it can also by making skin become smooth and high resilience to the suppression of elastoser and Collagenase; the skin injury because excessive Exposure to Sunlight causes can be prevented; inflammation-inhibiting and allergy, have radiation-resistant effect.
Semen Ginkgo, has another name called Semen Ginkgo, Gong Sunshu, Cortex schefflerae octophyllae etc., deciduous tree, belongs to gymnosperm Semen Ginkgo door unique existing species, and the every other species of its fellow disciple have become extinct all, are therefore called as botanic " living fossil ".Semen Ginkgo originates in China, now extensively plants in the whole world.It has multiple use, can be used as traditional medicine purposes and food.Flavone component contained in Folium Ginkgo can hinder pigment in the formation of skin corium and calmness, reaches skin whitening and the effect preventing and treating pigment speckle.Except flavone, the trace element such as the zinc in Folium Ginkgo, manganese, molybdenum, also can scavenging activated oxygen and check melanin growth.Flavonoid glycoside in Folium Ginkgo and flavonol are all the street cleaners of free radical, can protect skin corium cell, improve blood circulation, prevent the oxidized generation wrinkle of cell.
Tremella is put down, sweet in the mouth, light, nontoxic, and function profit the five internal organs, fill blood.Be applicable to the five internal organs weakness, insufficiency of vital energy and blood, lusterless complexion, hair not damp.Tremella polysaccharide is the main component of Tremella, and tremella polysaccharide is as natural extract, and having moisturizing and antioxidative activity, is a kind of excellent skin care product additive; In addition, be also rich in natural characteristic colloid, life-time service, the metabolism of people can be made to strengthen, and blood circulation is vigorous, and the function of each histoorgan improves, and the elasticity of skin strengthens, and subcutaneous tissue is plentiful, and wrinkle shoals and even disappears, and skin becomes delicate smooth.But nowadays under allegro life, a lot of people has no time tonic, and the nutritional labeling extracting Tremella is in facial film, is also a good beauty method.
Fructus Luffae extract fluidity is sweet, gentle, and scalable face sebum secretion, has clearly to skin of face, convergence, calm, the function of balance.TCM investigation finds, also be rich in the Moisture factor of natural plants essence, saponins, carbohydrate, wood glue, lymphatic temperament, vitamin, citrulline, xylan and interferon and mineral (ferrum, calcium, potassium, phosphorus, magnesium, zinc etc.) etc. in Fructus Luffae and effectively take good care of composition, these nutritional labelings of Fructus Luffae, easily be absorbed by the skin, skin moisture can be kept, alleviate wrinkle, improve coarse, dispel black speck, maintain the soft bullet of skin sliding, beautiful ruddy, have simultaneously refresh oneself, refrigerant effect, moist especially to the skin after Exposure to Sunlight.
In a preferred embodiment of Lepidinm meyenii Walp moisture saver mask of the present invention, the mass ratio of each component is: konjaku powder 8 ~ 12, the fresh root extract 12 ~ 18 of purple Lepidinm meyenii Walp, pyracantha fortuneana extract 10 ~ 15, Folium Ginkgo extract 5 ~ 10, Tremella extract 1 ~ 5, Fructus Luffae extract 1 ~ 5.In the present embodiment, konjaku powder has adsorbed sufficient moisture, and fully load pyracantha fortuneana, Folium Ginkgo, Tremella, Fructus Luffae etc. can have the pure natural plant extract of antioxidant activity, play its synergism, realize superpower antioxidant effect, keep face to moisten, avoid face skin accelerated ageing, reduce facial wrinkles, there is desirable antioxidation, the effect of slow down aging.
The preparation of embodiment 1 Lepidinm meyenii Walp moisture saver mask
The selection of S1, konjaku powder: select the konjaku powder that the content of Rhizoma amorphophalli glucomannan is greater than 90%;
The preparation method of S2, the fresh root extract of purple Lepidinm meyenii Walp: get fresh of purple Lepidinm meyenii Walp, clean up, section, be transferred to extraction vessel after smashing to pieces with pulverizer, add the ethanol water of 70% by solid-liquid ratio 1: 6, stir at 30 DEG C and extract 3h, be cooled to room temperature, cross leaching filtrate; Residue after filtration extracts twice after the same method; Merge three gained filtrates, be concentrated into the extractum that volume is 10%, obtain the fresh root extract of purple Lepidinm meyenii Walp;
The preparation method of S3, pyracantha fortuneana extract: get fresh pyracantha fortuneana and be placed in refiner, is transferred to extraction vessel, this ethanol water first acid for adjusting pH to 2.0 after the ethanol water adding 70% carries out homogenate by solid-liquid ratio 1: 6; Stir at 30 DEG C and extract 3h, be cooled to room temperature, centrifuging and taking supernatant, be concentrated into the extractum that volume is 10%, obtain pyracantha fortuneana extract;
The preparation method of S4, Folium Ginkgo extract: get green fresh Folium Ginkgo, dries at putting into 45 DEG C, drying baker and is less than 10% to moisture, pulverize after cleaning, crosses 20 mesh sieves and obtains Ginkgo Leaf; Ginkgo Leaf is dropped into round-bottomed flask, adds the ethanol water of 50% by solid-liquid ratio 1: 5,70 DEG C of reflux, extract, 3h, are cooled to room temperature, cross leaching supernatant; Residue after filtration extracts twice after the same method; Merge three gained supernatant, being concentrated into volume is 10%, and the distilled water adding 3 times of volumes carries out water precipitating, and after room temperature leaves standstill 24h, filter, gained filtrate is concentrated into the extractum that volume is 10%, obtains Folium Ginkgo extract;
The preparation method of S5, Tremella extract: get Tremella fructification dry product, soaks 30min with under distilled water room temperature, is placed in beater fully broken, obtained Tremella serosity; Regulate the pH value to 6.0 of Tremella serosity, add the compound enzymic preparation of mass fraction 0.5%, at 50 DEG C, enzyme digestion reaction 1.5h obtains Tremella enzymolysis solution, and described compound enzymic preparation comprises the 200000 U/g neutral protease of 7 parts and the 100000 U/g pectases of 3 parts; Lixiviate 2h at adding distilled water 100 DEG C according to volume ratio 1: 10 to this Tremella enzymolysis solution kind, filter, gained filtrate is concentrated into the extractum that volume is 10%, obtains Tremella extract;
The preparation method of S6, Fructus Luffae extract: cleaned by fresh Fructus Luffae, grind after chopping, adds the ethanol water of 70% by solid-liquid ratio 1: 5, reflux, extract, 6h at 60 DEG C, crosses leaching supernatant; Residue after filtration extracts once after the same method; Merge twice gained supernatant, be concentrated into the extractum that volume is 10%, obtain Fructus Luffae extract;
S7, prepare described Lepidinm meyenii Walp moisture saver mask by following mass ratio: konjaku powder 8, the fresh root extract 12 of purple Lepidinm meyenii Walp, pyracantha fortuneana extract 15, Folium Ginkgo extract 10, Tremella extract 5, Fructus Luffae extract 5;
S8, above-mentioned substance proportionally to be mixed, after distilled water allotment, obtain emulsion and pour in facial film mould, first leave standstill 10h, in steamer, then steam 30min ripening molding, then in-20 DEG C of washings of thawing after freezing 5 days, until pH is 6.0, spin-dry, is placed in the ozone sterilization treatment 20min of 0.5ppm, is packaged into bag and get final product.
The preparation of embodiment 2 Lepidinm meyenii Walp moisture saver mask
The selection of S1, konjaku powder: select the konjaku powder that the content of Rhizoma amorphophalli glucomannan is greater than 90%;
The preparation method of S2, the fresh root extract of purple Lepidinm meyenii Walp: get fresh of purple Lepidinm meyenii Walp, clean up, section, be transferred to extraction vessel after smashing to pieces with pulverizer, add the ethanol water of 90% by solid-liquid ratio 1: 10, stir at 50 DEG C and extract 1h, be cooled to room temperature, cross leaching filtrate; Residue after filtration extracts twice after the same method; Merge three gained filtrates, be concentrated into the extractum that volume is 20%, obtain the fresh root extract of purple Lepidinm meyenii Walp;
The preparation method of S3, pyracantha fortuneana extract: get fresh pyracantha fortuneana and be placed in refiner, is transferred to extraction vessel, this ethanol water first acid for adjusting pH to 4.0 after the ethanol water adding 90% carries out homogenate by solid-liquid ratio 1: 10; Stir at 50 DEG C and extract 1h, be cooled to room temperature, centrifuging and taking supernatant, be concentrated into the extractum that volume is 20%, obtain pyracantha fortuneana extract;
The preparation method of S4, Folium Ginkgo extract: get green fresh Folium Ginkgo, dries at putting into 60 DEG C, drying baker and is less than 10% to moisture, pulverize after cleaning, crosses 20 mesh sieves and obtains Ginkgo Leaf; Ginkgo Leaf is dropped into round-bottomed flask, adds the ethanol water of 80% by solid-liquid ratio 1: 10,85 DEG C of reflux, extract, 1h, are cooled to room temperature, cross leaching supernatant; Residue after filtration extracts twice after the same method; Merge three gained supernatant, being concentrated into volume is 20%, and the distilled water adding 1 times of volume carries out water precipitating, and after room temperature leaves standstill 48h, filter, gained filtrate is concentrated into the extractum that volume is 20%, obtains Folium Ginkgo extract;
The preparation method of S5, Tremella extract: get Tremella fructification dry product, soaks 50min with under distilled water room temperature, is placed in beater fully broken, obtained Tremella serosity; Regulate the pH value to 8.0 of Tremella serosity, add the compound enzymic preparation of mass fraction 2%, at 55 DEG C, enzyme digestion reaction 0.5h obtains Tremella enzymolysis solution, and described compound enzymic preparation comprises the 200000 U/g neutral protease of 3 parts and the 100000 U/g pectases of 7 parts; Lixiviate 4h at adding distilled water 90 DEG C according to volume ratio 1: 5 to this Tremella enzymolysis solution kind, filter, gained filtrate is concentrated into the extractum that volume is 20%, obtains Tremella extract;
The preparation method of S6, Fructus Luffae extract: cleaned by fresh Fructus Luffae, grind after chopping, adds the ethanol water of 90% by solid-liquid ratio 1: 10, reflux, extract, 4h at 70 DEG C, crosses leaching supernatant; Residue after filtration extracts once after the same method; Merge twice gained supernatant, be concentrated into the extractum that volume is 20%, obtain Fructus Luffae extract;
S7, prepare described Lepidinm meyenii Walp moisture saver mask by following mass ratio: konjaku powder 12, the fresh root extract 18 of purple Lepidinm meyenii Walp, pyracantha fortuneana extract 10, Folium Ginkgo extract 5, Tremella extract 1, Fructus Luffae extract 1;
S8, above-mentioned substance proportionally to be mixed, after distilled water allotment, obtain emulsion and pour in facial film mould, first leave standstill 14h, in steamer, then steam 50min ripening molding, then in-30 DEG C of washings of thawing after freezing 3 days, until pH is 8.0, spin-dry, is placed in the ozone sterilization treatment 40min of 1.5ppm, is packaged into bag and get final product.
The preparation of embodiment 3 Lepidinm meyenii Walp moisture saver mask
The selection of S1, konjaku powder: select the konjaku powder that the content of Rhizoma amorphophalli glucomannan is greater than 90%;
The preparation method of S2, the fresh root extract of purple Lepidinm meyenii Walp: get fresh of purple Lepidinm meyenii Walp, clean up, section, be transferred to extraction vessel after smashing to pieces with pulverizer, add the ethanol water of 80% by solid-liquid ratio 1: 8, stir at 40 DEG C and extract 2h, be cooled to room temperature, cross leaching filtrate; Residue after filtration extracts twice after the same method; Merge three gained filtrates, be concentrated into the extractum that volume is 15%, obtain the fresh root extract of purple Lepidinm meyenii Walp;
The preparation method of S3, pyracantha fortuneana extract: get fresh pyracantha fortuneana and be placed in refiner, is transferred to extraction vessel, this ethanol water first acid for adjusting pH to 3.0 after the ethanol water adding 80% carries out homogenate by solid-liquid ratio 1: 8; Stir at 40 DEG C and extract 2h, be cooled to room temperature, centrifuging and taking supernatant, be concentrated into the extractum that volume is 15%, obtain pyracantha fortuneana extract;
The preparation method of S4, Folium Ginkgo extract: get green fresh Folium Ginkgo, dries at putting into 50 DEG C, drying baker and is less than 10% to moisture, pulverize after cleaning, crosses 20 mesh sieves and obtains Ginkgo Leaf; Dropped into by Ginkgo Leaf and extract vessel, add the ethanol water of 70% by solid-liquid ratio 1: 8,80 DEG C of reflux, extract, 2h, are cooled to room temperature, cross leaching supernatant; Residue after filtration extracts twice after the same method; Merge three gained supernatant, being concentrated into volume is 15%, and the distilled water adding 2 times of volumes carries out water precipitating, and after room temperature leaves standstill 36h, filter, gained filtrate is concentrated into the extractum that volume is 15%, obtains Folium Ginkgo extract
The preparation method of S5, Tremella extract: get Tremella fructification dry product, soaks 40min with under distilled water room temperature, is placed in beater fully broken, obtained Tremella serosity; Regulate the pH value to 7.0 of Tremella serosity, add the compound enzymic preparation of mass fraction 1%, at 52 DEG C, enzyme digestion reaction 1h obtains Tremella enzymolysis solution, and described compound enzymic preparation comprises the 200000 U/g neutral protease of 5 parts and the 100000 U/g pectases of 5 parts; Lixiviate 3h at adding distilled water 95 DEG C according to volume ratio 1: 8 to this Tremella enzymolysis solution kind, filter, gained filtrate is concentrated into the extractum that volume is 15%, obtains Tremella extract;
The preparation method of S6, Fructus Luffae extract: cleaned by fresh Fructus Luffae, grind after chopping, adds the ethanol water of 80% by solid-liquid ratio 1: 8, reflux, extract, 5h at 65 DEG C, crosses leaching supernatant; Residue after filtration extracts once after the same method; Merge twice gained supernatant, be concentrated into the extractum that volume is 15%, obtain Fructus Luffae extract;
S7, prepare described Lepidinm meyenii Walp moisture saver mask by following mass ratio: konjaku powder 10, the fresh root extract 15 of purple Lepidinm meyenii Walp, pyracantha fortuneana extract 12, Folium Ginkgo extract 8, Tremella extract 3, Fructus Luffae extract 3;
S8, above-mentioned substance proportionally to be mixed, after distilled water allotment, obtain emulsion and pour in facial film mould, first leave standstill 12h, in steamer, then steam 40min ripening molding, then in-25 DEG C of washings of thawing after freezing 4 days, until pH is 7.0, spin-dry, is placed in the ozone sterilization treatment 30min of 1.0ppm, is packaged into bag and get final product.
Embodiment 4 effectiveness is verified
What use the Lepidinm meyenii Walp moisture saver mask of preparation in embodiment 3 carries out effectiveness checking, and evaluates its safety.
1, Antisenility Experiment
Select aged 12 the month female Kunming mouses 60 of nature, be divided into matched group (N group) and each 30 of experimental group (M group) at random, separately 30 3 month female Kunming mouses contrasted as few age group (Y group).Mice is by group sub-cage rearing, and under clean, ventilation, drying, room temperature (22 ± 2) DEG C condition, routine raises food drinking-water, and adaptability starts to test after raising.Test front shaver and slough hair 3cm × 3cm between mouse back two omoplate on skin, M group application Lepidinm meyenii Walp moisture saver mask, every day 1 time; N group and Y group mouse back application equivalent infiltrate the non-woven fabrics compression facial film of substrate astringent.Respectively at experiment 15,30, during 45d, three treated animals respectively get 10, cervical dislocation gets its drug effect area skin after putting to death, and measures the content of equivalent areas of skin weight and hydroxyproline (HYP), superoxide dismutase (SOD), lipid peroxide metabolite malonaldehyde (MDA) and lipofuscin (LF).
Experimental result shows, during application facial film 15d, M group and Y group skin weight and hydroxyproline content have increase trend, but not statistically significant.During application 30d and 45d, compared with N group, S group, the skin weight of M group and SOD vigor, HYP content obviously increase, and the content of MDA and LF then obviously reduces (P<0.05 and P<0.01).Illustrate that Lepidinm meyenii Walp moisture saver mask of the present invention has significant antioxidation, anti-aging effects.
2, moisture retention and skin irritation test
Select 25 tested volunteers of healthy women, the mean age is 26.87 ± 5.24 years old, without any skin and systemic disease, in the past to skin care item without allergies, recipient site is without scytitis person.Before experiment, experimenter need unify clean both hands inner forearm, by dry medicated napkin wiped clean.After clean, choosing upper and lower two ends area at experimenter right-hand man's inner forearm is that measurement markers is carried out in the region of (3 × 3cm2).Before official testing, require experimenter in temperature for (22 ± 2) DEG C, humidity is that the metastable constant temperature and humidity efficacy test laboratory of (50 ± 5) % is sat quietly at least 30min, can not drink water, forearm exposes, and places, keep loosening in test mode.
In experiment, test products (Lepidinm meyenii Walp moisture saver mask of the present invention) applies at random in experimenter's left and right arm.Use CorneometerCM825PC tester probe, each area test 5 times, using meansigma methods as test value.First measure the blank value in tested region, then sample facial film is applied in tested region, skin massages 1min gently, with the residue that warm water removing adheres to after removing facial film, and in removing rear 0.5h, 1h, 2h, 3h and 4h, use the moisture content of skin of the tested region of probe measurement and white space, and record test result, calculate moisture of skin percentage change (seeing the following form 1) in different time points; Observe the skin variations in tested region, the left and right sides respectively, result shows simultaneously, application Lepidinm meyenii Walp moisture saver mask region there is no rubescent, swelling, pruritus, drying, tight, have goose pimples and the abnormal phenomena such as small red dot or blister.
Result is known, and after application Lepidinm meyenii Walp moisture saver mask of the present invention, the tested area skin water content of volunteer has had and significantly promotes after 0.5h, illustrates that product has good moistening effect.At 1h thereafter, 2h, 3h and 4h, although tested area skin water content decreases, but still far above blank value, illustrate that product of the present invention has good moisture retention.Meanwhile, this result of the test absolutely proves that Lepidinm meyenii Walp moisture saver mask of the present invention has no side effect to skin, safe and reliable.
Table 1. moisture of skin result of variations
Claims (10)
1. have a Lepidinm meyenii Walp moisture saver mask for anti-oxidation efficacy, it is characterized in that, described Lepidinm meyenii Walp moisture saver mask comprises following component: konjaku powder, the fresh root extract of purple Lepidinm meyenii Walp, pyracantha fortuneana extract, Folium Ginkgo extract, Tremella extract, Fructus Luffae extract.
2. Lepidinm meyenii Walp moisture saver mask according to claim 1, it is characterized in that, the mass ratio of each component is: konjaku powder 8 ~ 12, the fresh root extract 12 ~ 18 of purple Lepidinm meyenii Walp, pyracantha fortuneana extract 10 ~ 15, Folium Ginkgo extract 5 ~ 10, Tremella extract 1 ~ 5, Fructus Luffae extract 1 ~ 5.
3. Lepidinm meyenii Walp moisture saver mask according to claim 2, is characterized in that, in described konjaku powder, the content of Rhizoma amorphophalli glucomannan is greater than 90%.
4. Lepidinm meyenii Walp moisture saver mask according to claim 2, it is characterized in that, the preparation method of the fresh root extract of described purple Lepidinm meyenii Walp is: get fresh of purple Lepidinm meyenii Walp, clean up, section, is transferred to extraction vessel with pulverizer after smashing to pieces, the ethanol water of 70% ~ 90% is added by solid-liquid ratio 1: 6 ~ 1: 10, stir extraction 1 ~ 3h at 30 ~ 50 DEG C, be cooled to room temperature, cross leaching filtrate; Residue after filtration extracts twice after the same method; Merge three gained filtrates, be concentrated into the extractum that volume is 10% ~ 20%, obtain the fresh root extract of purple Lepidinm meyenii Walp.
5. Lepidinm meyenii Walp moisture saver mask according to claim 2, it is characterized in that, the preparation method of described pyracantha fortuneana extract is: get fresh pyracantha fortuneana and be placed in refiner, extraction vessel are transferred to, this ethanol water first acid for adjusting pH to 2.0 ~ 4.0 after the ethanol water adding 70% ~ 90% by solid-liquid ratio 1: 6 ~ 1: 10 carries out homogenate; Stir extraction 1 ~ 3h at 30 ~ 50 DEG C, be cooled to room temperature, centrifuging and taking supernatant, be concentrated into the extractum that volume is 10% ~ 20%, obtain pyracantha fortuneana extract.
6. Lepidinm meyenii Walp moisture saver mask according to claim 2, it is characterized in that, the preparation method of described Folium Ginkgo extract is: get green fresh Folium Ginkgo, dries to moisture and be less than 10% after cleaning at putting into 45 ~ 60 DEG C, drying baker, pulverize, cross 20 mesh sieves and obtain Ginkgo Leaf; Dropped into by Ginkgo Leaf and extract vessel, add the ethanol water of 50 ~ 80% by solid-liquid ratio 1: 5 ~ 1: 10,70 ~ 85 DEG C of reflux, extract, 1 ~ 3h, are cooled to room temperature, cross leaching supernatant; Residue after filtration extracts twice after the same method; Merge three gained supernatant, being concentrated into volume is 10% ~ 20%, and the distilled water adding 1 ~ 3 times of volume carries out water precipitating, and after room temperature leaves standstill 24 ~ 48h, filter, gained filtrate is concentrated into the extractum that volume is 10% ~ 20%, obtains Folium Ginkgo extract.
7. Lepidinm meyenii Walp moisture saver mask according to claim 2, is characterized in that, the preparation method of described Tremella extract is: get Tremella fructification dry product, soaks 30 ~ 50min with under distilled water room temperature, is placed in beater fully broken, obtained Tremella serosity; Regulate pH value to 6.0 ~ 8.0 of Tremella serosity, add the compound enzymic preparation of mass fraction 0.5 ~ 2%, at 50 ~ 55 DEG C, enzyme digestion reaction 0.5 ~ 1.5h obtains Tremella enzymolysis solution, and described compound enzymic preparation comprises the 200000 U/g neutral protease of 3 ~ 7 parts and the 100000 U/g pectases of 3 ~ 7 parts; Lixiviate 2 ~ 4h at adding distilled water 90 ~ 100 DEG C according to volume ratio 1: 5 ~ 1: 10 to this Tremella enzymolysis solution kind, filter, gained filtrate is concentrated into the extractum that volume is 10% ~ 20%, obtains Tremella extract.
8. Lepidinm meyenii Walp moisture saver mask according to claim 2, it is characterized in that, the preparation method of described Fructus Luffae extract is: cleaned by fresh Fructus Luffae, grind after chopping, the ethanol water of 70 ~ 90% is added by solid-liquid ratio 1: 5 ~ 1: 10, reflux, extract, 4 ~ 6h at 60 ~ 70 DEG C, crosses leaching supernatant; Residue after filtration extracts once after the same method; Merge twice gained supernatant, be concentrated into the extractum that volume is 10% ~ 20%, obtain Fructus Luffae extract.
9. have a preparation method for the Lepidinm meyenii Walp moisture saver mask of anti-oxidation efficacy, it is characterized in that, described preparation method comprises:
The selection of S1, konjaku powder: select the konjaku powder that the content of Rhizoma amorphophalli glucomannan is greater than 90%;
The preparation method of S2, the fresh root extract of purple Lepidinm meyenii Walp: get fresh of purple Lepidinm meyenii Walp, clean up, section, extraction vessel are transferred to after smashing to pieces with pulverizer, the ethanol water of 70% ~ 90% is added by solid-liquid ratio 1: 6 ~ 1: 10, stir extraction 1 ~ 3h at 30 ~ 50 DEG C, be cooled to room temperature, cross leaching filtrate; Residue after filtration extracts twice after the same method; Merge three gained filtrates, be concentrated into the extractum that volume is 10% ~ 20%, obtain the fresh root extract of purple Lepidinm meyenii Walp;
The preparation method of S3, pyracantha fortuneana extract: get fresh pyracantha fortuneana and be placed in refiner, extraction vessel are transferred to, this ethanol water first acid for adjusting pH to 2.0 ~ 4.0 after the ethanol water adding 70% ~ 90% by solid-liquid ratio 1: 6 ~ 1: 10 carries out homogenate; Stir extraction 1 ~ 3h at 30 ~ 50 DEG C, be cooled to room temperature, centrifuging and taking supernatant, be concentrated into the extractum that volume is 10% ~ 20%, obtain pyracantha fortuneana extract;
The preparation method of S4, Folium Ginkgo extract: get green fresh Folium Ginkgo, dries at putting into 45 ~ 60 DEG C, drying baker and is less than 10% to moisture, pulverize after cleaning, crosses 20 mesh sieves and obtains Ginkgo Leaf; Dropped into by Ginkgo Leaf and extract vessel, add the ethanol water of 50 ~ 80% by solid-liquid ratio 1: 5 ~ 1: 10,70 ~ 85 DEG C of reflux, extract, 1 ~ 3h, are cooled to room temperature, cross leaching supernatant; Residue after filtration extracts twice after the same method; Merge three gained supernatant, being concentrated into volume is 10% ~ 20%, and the distilled water adding 1 ~ 3 times of volume carries out water precipitating, and after room temperature leaves standstill 24 ~ 48h, filter, gained filtrate is concentrated into the extractum that volume is 10% ~ 20%, obtains Folium Ginkgo extract;
The preparation method of S5, Tremella extract: get Tremella fructification dry product, soaks 30 ~ 50min with under distilled water room temperature, is placed in beater fully broken, obtained Tremella serosity; Regulate pH value to 6.0 ~ 8.0 of Tremella serosity, add the compound enzymic preparation of mass fraction 0.5 ~ 2%, at 50 ~ 55 DEG C, enzyme digestion reaction 0.5 ~ 1.5h obtains Tremella enzymolysis solution, and described compound enzymic preparation comprises the 200000 U/g neutral protease of 3 ~ 7 parts and the 100000 U/g pectases of 3 ~ 7 parts; Lixiviate 2 ~ 4h at adding distilled water 90 ~ 100 DEG C according to volume ratio 1: 5 ~ 1: 10 to this Tremella enzymolysis solution kind, filter, gained filtrate is concentrated into the extractum that volume is 10% ~ 20%, obtains Tremella extract;
The preparation method of S6, Fructus Luffae extract: cleaned by fresh Fructus Luffae, grind after chopping, adds the ethanol water of 70 ~ 90% by solid-liquid ratio 1: 5 ~ 1: 10, reflux, extract, 4 ~ 6h at 60 ~ 70 DEG C, crosses leaching supernatant; Residue after filtration extracts once after the same method; Merge twice gained supernatant, be concentrated into the extractum that volume is 10% ~ 20%, obtain Fructus Luffae extract;
S7, prepare described Lepidinm meyenii Walp moisture saver mask by following mass ratio: konjaku powder 8 ~ 12, the fresh root extract 12 ~ 18 of purple Lepidinm meyenii Walp, pyracantha fortuneana extract 10 ~ 15, Folium Ginkgo extract 5 ~ 10, Tremella extract 1 ~ 5, Fructus Luffae extract 1 ~ 5.
10. the preparation method of Lepidinm meyenii Walp moisture saver mask according to claim 9, is characterized in that, also comprises after described step S7:
S8, above-mentioned substance proportionally to be mixed, after distilled water allotment, obtain emulsion and pour in facial film mould, first leave standstill 10 ~ 14h, then in steamer, steam 30 ~ 50min ripening molding, then in-20 ~-30 DEG C of washings of thawing after freezing 3 ~ 5 days, until pH is 6.0 ~ 8.0, spin-dry, is placed in the ozone sterilization treatment 20 ~ 40min of 0.5 ~ 1.5ppm, is packaged into bag and get final product.
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| FR3138039A1 (en) | 2022-07-21 | 2024-01-26 | Basf Beauty Care Solutions France Sas | Cosmetic or dermatological use of an extract of Pyracantha fortuneana |
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