CN106309260B

CN106309260B - A kind of Radix Notoginseng is preserved youthful looks facial mask

Info

Publication number: CN106309260B
Application number: CN201610994075.5A
Authority: CN
Inventors: 王萍; 罗渝杰; 罗开珍; 况金妍
Original assignee: YUNNAN REN XIU HUA COSMETICS Co Ltd
Current assignee: Yunnan Qianrong Biotechnology Co ltd
Priority date: 2016-11-11
Filing date: 2016-11-11
Publication date: 2019-03-05
Anticipated expiration: 2036-11-11
Also published as: CN106309260A

Abstract

It preserves youthful looks facial mask the present invention relates to a kind of Radix Notoginseng, belongs to cosmetic technical field；Radix Notoginseng facial mask of preserving youthful looks includes following components: Notogineng Extract, Salvia root P.E, angelica extract, bupleurum extract, Radix et Caulis Opuntiae Dillenii extract, Radix Oenotherae erythrosepalae extract, hyaluronic acid, glycine betaine, xanthan gum, methylisothiazolinone, glycerol, propylene glycol, hydrolytic collagen, deionized water, preparation method includes the following steps: (1) obtaining Notogineng Extract；(2) Salvia root P.E is obtained；(3) angelica extract is obtained；(4) Radix et Caulis Opuntiae Dillenii extract is obtained；(5) mixture is obtained；(6) pH is adjusted；(7) finished product is obtained.The present invention can remove superoxide anion, oxidation resistance with super strength；It is not only able to maintain the original nutrition of skin and moisture, avoids skin sunburn and melanin deposition, moreover it is possible to smooth face's microgroove, efficiently supplement and lock moisture in cuticula；It can promote the generation of collagen in skin hyaluronic acid and epidermal cell, promote skin to assign and live.

Description

A kind of Radix Notoginseng is preserved youthful looks facial mask

Technical field

It preserves youthful looks facial mask the present invention relates to a kind of Radix Notoginseng, belongs to cosmetic technical field.

Background technique

As the continuous increase and people of people's life and work pressure face computer for a long time, day is accumulated the moon in sunlight irradiation Tired, the radiation such as ultraviolet light, electromagnetism generates grievous injury to skin, and environmental pollution is serious in addition, and skin occur in numerous people Problem is mainly manifested in the following aspects: (1) skin is tight or even fuel-displaced, this is the performance of skin extreme dehydration；(2) face On start chloasma or light black patch occur, the colour of skin is uneven, this be skin for a long time by radiate and skin lack nutrition Performance；(3) there is smooth cut in the positions such as canthus, mouth border, and skin elasticity weakens, this is local skin aging, and resistivity is weak Performance；(4) chin nearby grows acne, cannot eliminate for a long time, this is skin anti-irritant and the table that self-regeneration function reduces It is existing.

Numerous skin problems reminds us to need that advantageous measures is taken to protect our skin, in recent years, facial mask by Consumers, it is well known that the principle of facial mask is temporarily isolating extraneous sky exactly using the of short duration time for being covered on face Gas and pollution, improve skin temperature, and the pore expansion of skin promotes sweat gland secretion and metabolism, makes in the oxygen content of skin It rises, is conducive to skin and excludes the product of epidermal cell metabolism and the oil substances of accumulation, the moisture in facial mask penetrates into table The cuticula of skin, skin become soft, and skin is naturally bright flexible.

China is Chinese herbal medicine kingdom, has only day to obtain thick Chinese herbal medicine resource, in recent years Chinese herbal medicine cosmetic meet the tendency of and Raw, pure natural pollution-free with its, effective advantage obtains the favor of many consumers, therefore, utilizes Study of Medicinal Herbs one It kind can safely and effectively supplement and the facial mask for lockking the moisture and beauty and skin care in face's cuticula is imperative.

Summary of the invention

Against the above technical problems, it is an object of the invention to break through the deficiency of existing facial mask, provides a kind of Radix Notoginseng and stays Face film is equipped with various plants essence using the Radix Notoginseng essential ingredient extracted in Radix Notoginseng, by the proportion of science, has fine Pro-skin it is aqueous, carry skin makeup nutritional ingredient abundant, cooperate natural silk film, deep layer is releived while keeping the skin wet for skin Moisturizing strengthens skin natural moisture barrier, nutrition skin while enhancing skin respiration, cooperates with hyaluronic acid, micro- Penetrate into skin, can effectively improve phenomena such as skin is obscure, coarse, pore is coarse, dry, make skin it is smooth, it is delicate, rich in light Pool, it may also be used for after-sun restorative.

In order to achieve the above objectives, the invention provides the following technical scheme:

Radix Notoginseng facial mask of preserving youthful looks includes following components: Notogineng Extract, Salvia root P.E, angelica extract, radix bupleuri Extract, Radix et Caulis Opuntiae Dillenii extract, Radix Oenotherae erythrosepalae extract, hyaluronic acid, glycine betaine, xanthan gum, methylisothiazolinone, glycerol, Propylene glycol, hydrolytic collagen, deionized water.

Preferably, the Radix Notoginseng is preserved youthful looks, facial mask includes following components by weight percent: 8-14 parts of Notogineng Extract, Radix Salviae Miltiorrhizae extract 8-10 parts of object, 8-10 parts of angelica extract, 8-10 parts of bupleurum extract, 6-8 parts of Radix et Caulis Opuntiae Dillenii extract, Radix Oenotherae erythrosepalae extract 6-8 Part, 3-5 parts of hyaluronic acid, 3-5 parts of glycine betaine, 2-4 parts of xanthan gum, 3-5 parts of methylisothiazolinone, 2-4 parts of glycerol, propylene glycol 2-4 parts, 4-6 parts of hydrolytic collagen, 100-185 parts of deionized water.

Preferably, the Radix Notoginseng is preserved youthful looks, facial mask includes following components by weight percent: 11 parts of Notogineng Extract, Salvia root P.E 9 parts, 9 parts of angelica extract, 9 parts of bupleurum extract, 7 parts of Radix et Caulis Opuntiae Dillenii extract, 7 parts of Radix Oenotherae erythrosepalae extract, 4 parts of hyaluronic acid, 4 parts of glycine betaine, 3 parts of xanthan gum, 4 parts of methylisothiazolinone, 3 parts of glycerol, 3 parts of propylene glycol, 5 parts of hydrolytic collagen, deionized water 145 parts.

Above-described Radix Notoginseng preserve youthful looks facial mask preparation method specifically includes the following steps:

(1) preparation of Notogineng Extract: the ethyl alcohol of 50%-60% is added in selected Roots of Panax Notoginseng powder, impregnates 30-50min, returns Stream extracts 2-3 times, each 100-150min, and merging filtrate is stand-by；

(2) preparation of Salvia root P.E: selected Radix Salviae Miltiorrhizae is ground into 30-50 mesh after cleaning drying, is packed into extraction kettle barrel In, extraction kettle, separating still are heated respectively, open cooling water water-bath refrigeration, at 40-50 DEG C to be achieved, opens CO₂Gas Bottle, is forced into 20-30MPa to system by high-pressure pump, while opening entrainer pump, squeezes into entrainer to accurate quantitative analysis, is allowed to Become fluid-mixing with carbon dioxide, reaches static immersing 28-32min after extraction conditions, dynamic extraction is then carried out, every 1- 1.5h takes a sample, stand-by after concentration；

(3) preparation of angelica extract: selected Radix Angelicae Sinensis is ground into 10-20 mesh after cleaning drying, with " double formulations " in normal pressure Three times, combined extract adds 100-120 mesh to filter respectively, 3000r/min's to lower heating and refluxing extraction with 3-5 layers of gauze It is centrifuged 10-20 minutes in centrifuge, it is stand-by to merge supernatant；

(4) preparation of Radix et Caulis Opuntiae Dillenii extract: selected cactus dry powder is put into extractor, and cactus dry powder weight is added 18-22 times of water and the cellulase of cactus dry powder weight 0.8-1.5% are heated to 45-55 DEG C and maintain this temperature Degree adjusts pH to 4-6, after digesting 50-70min, is cooled to 22-26 DEG C, 1.5-2.5h is stirred with 2 lattice revolving speeds, using 4000r/ The centrifuge of min is centrifuged 8-12min, merges supernatant, and the active carbon of supernatant quality 4-6% is added, stand after 20-30h from The heart removes active carbon, and it is stand-by to merge Aqueous extracts；

(5) by the hyaluronic acid of formula ratio, glycine betaine, xanthan gum, methylisothiazolinone, glycerol, propylene glycol, hydrolysis glue The Notogineng Extract, pellet of the step of original, deionized water addition emulsion tank internal emulsification are uniform, add formula ratio (1)-(4) preparation Conopsea extraction, angelica extract, Radix et Caulis Opuntiae Dillenii extract and formula ratio bupleurum extract, Radix Oenotherae erythrosepalae extract stir and evenly mix Afterwards, the homogeneous 30-45min in homogenizer obtains emulsifying uniform mixture；

(6) pH for the mixture that regulating step (5) obtains is to faintly acid, obtains Radix Notoginseng and preserves youthful looks facial mask liquid；

(7) step (6) resulting Radix Notoginseng facial mask liquid of preserving youthful looks is sterilized 24-32 minutes in disinfection cabinet, then by molding day Right silk film mask sheet is soaked in the Radix Notoginseng after disinfection and preserves youthful looks in facial mask liquid 18-26 minutes, then by natural silk film mask sheet Packaging seal is got product.

Preferably, amount of alcohol added is 6-10 times of Roots of Panax Notoginseng powder weight in step (1).

Preferably, in step (2), the ethyl alcohol that entrainer is 95%, dosage 350-450ml/h.

Preferably, in step (2), the condition of dynamic extraction are as follows: pressure 20-30MPa, temperature are 40-50 DEG C.

Preferably, in step (4), the production method of cactus dry powder are as follows: selected fresh cactus, cutting after cleaning Processing, is freeze-dried 3-6h in subzero 60-80 degrees Celsius of low temperature refrigerator, is 20Pa-40Pa in vacuum degree, sublimation temperature is 2-4h is dried in vacuum sublimation under conditions of 40-60 DEG C, 80-100 mesh is crushed in pulverizer, at subzero 65-75 degrees Celsius, very Reciprocal of duty cycle is vacuum freeze drying under conditions of 20Pa-40Pa, obtains cactus dry powder.

Preferably, the water content of cactus xeraphium is 6-10% in step (4).

Preferably, the additional amount of glycerol and propylene glycol is 1:0.5-1:1 in step (5).

Preferably, the pH of mixture is adjusted to 4.5-6.5 in step (6).

Preferably, the additional amount of glycerol is the 30-50% of Radix et Caulis Opuntiae Dillenii extract in step (5).

The function of each traditional Chinese medicine ingredients is as follows in the present invention:

Notogineng Extract: having The flat liver of heat-clearing, mental-tranquilization, and moistening lung preserves youth anti-aging, elimination and reduces wrinkle of skin And senile plaque and other effects, it is the most natural good beauty and skin care beauty treatment product of women, its energy anti-aging protects skin, improves skin Skin appearance makes skin emolliency and increases elasticity.

Angelica extract: it is living that amino acid, vitamin, natural moisturizing factor, microelement and other biological abundant are included Property substance, can inhibit tyrosinase activity, prevent from tyrosinase from aoxidizing to form pigment, have promoting circulation of blood and enriching blood, antibacterial, itching analgesic Effect, moreover it is possible to delay skin aging.

Salvia root P.E: having and adjust endocrine function, promotes skin metabolism, and activate blood circulation and disperse blood clots freckle removing and whitening, pigment of dispelling, Have the effects that extremely strong calm, anti-inflammatory sterilization, relieving swelling and reddness of eye.

Bupleurum extract: saikosaponin saikoside therein not only has the function of the proliferation activity of promotion skin fiber sprout cell, And it can also be effectively facilitated the generation of collagen in skin hyaluronic acid and epidermal cell, this skin assigns effect living, energy The light aging or natural aging with delaying skin are effectively improved, enhances the elasticity of skin, reduces the appearance of skin smooth cut, allows flesh Skin restores careful, elastic and tender.

Radix et Caulis Opuntiae Dillenii extract: the chemical components such as amino acid, superoxide dismutase (SOD) and polysaccharide for being wherein rich in all are To the active constituent of skin Yellow Gentian Extract, and its contained vitamin C abundant has the ability removed and inhibit free radical, The superpower water conservation ingredient contained can be such that moisture rests in skin for a long time, enhance the natural water holding capacity of skin, keep for a long time The tender state of skin water.

Radix Oenotherae erythrosepalae extract: its most important ingredient is γ-linolenic acid (GLA), its energy synthesis of prostaglandins inhibits Anaphylactoid inflammation phenomenon improves the allergic symptoms such as asthma, Atopic dermatitis, and contained linolenic acid, it can make skin Cell retains more moisture, there is moistening effect.

Beneficial effects of the present invention:

(1) present invention uses the active constituent of natural plants as raw material, using the reasonable compatibility between Chinese herbal medicine, significantly The effect of each active constituent is improved, and without any side effects, can be used for a long time；Notogineng Extract can protect skin, change Kind skin appearance, makes skin emolliency and increases elasticity, reasonable compatibility Salvia root P.E can not only play Radix Salviae Miltiorrhizae and activate blood circulation and disperse blood clots, dispel The effects of speckles, beautification and white, calmness, anti-inflammatory sterilization, relieving swelling and reddness of eye, moreover it is possible to significantly increase the oxidation resistance of Radix Notoginseng, remove super oxygen yin from Son, meanwhile, Radix Notoginseng can increase the stability of effective component in Salvia root P.E.

(2) angelica extract includes the bioactivity such as amino acid abundant, vitamin, natural moisturizing factor, microelement Substance, the Radix et Caulis Opuntiae Dillenii extract of the chemical components such as amino acid, superoxide dismutase (SOD) and polysaccharide that compatibility is rich in, not only It is able to maintain the original nutrition of skin and moisture, skin sunburn and melanin deposition is avoided, is effective against skin aging, moreover it is possible to smooth The microgroove of face efficiently supplements and locks moisture in cuticula, dispels freckle, with Radix Oenotherae erythrosepalae extract compatibility, sensitive skin Also it can easily use, be not inhibited.

(3) bupleurum extract compatibility with Danshen extract can promote collagen in skin hyaluronic acid and epidermal cell It generates, promotes skin to assign and live, bupleurum extract compatibility Radix et Caulis Opuntiae Dillenii extract can control cortex secretion, prevent acne, radix bupleuri mentions Object compatibility angelica extract is taken, there is the effect of blood circulation promoting and enriching.

Specific embodiment

Below in conjunction with the embodiment of the present invention and comparative example, technical solution in the embodiment of the present invention carries out clear, complete Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other Embodiment shall fall within the protection scope of the present invention.

Embodiment 1

Radix Notoginseng facial mask of preserving youthful looks includes following components by weight percent: 8 parts of Notogineng Extract, 8 parts of Salvia root P.E, Radix Angelicae Sinensis mention Take 8 parts of object, 8 parts of bupleurum extract, 6 parts of Radix et Caulis Opuntiae Dillenii extract, 6 parts of Radix Oenotherae erythrosepalae extract, 3 parts of hyaluronic acid, 3 parts of glycine betaine, 2 parts of xanthan gum, 3 parts of methylisothiazolinone, 2 parts of glycerol, 2 parts of propylene glycol, 4 parts of hydrolytic collagen, 100 parts of deionized water.

(1) preparation of Notogineng Extract: the ethyl alcohol of 50%-60% is added in selected Roots of Panax Notoginseng powder, and amount of alcohol added is Radix Notoginseng 6 times of root powder weight, immersion 30-50min, refluxing extraction 2-3 times, each 100-150min, merging filtrate are stand-by；

(2) preparation of Salvia root P.E: selected Radix Salviae Miltiorrhizae is ground into 30-50 mesh after cleaning drying, is packed into extraction kettle barrel In, extraction kettle, separating still are heated respectively, open cooling water water-bath refrigeration, at 40-50 DEG C to be achieved, opens CO₂Gas Bottle, is forced into 20-30MPa to system by high-pressure pump, while opening entrainer pump, squeezes into accurate quantitative analysis entrainer, carries secretly The addition of agent, can be improved extraction efficiency, promote the precipitation of effective component, the ethyl alcohol that entrainer is 95%, dosage 350/h, It is allowed to become fluid-mixing with carbon dioxide, pressure reaches 20MPa, static immersing 28-32min after temperature reaches 50 DEG C, then Dynamic extraction is carried out, takes a sample every 1-1.5h, it is stand-by after concentration；

(4) preparation of Radix et Caulis Opuntiae Dillenii extract: the 1. preparation of cactus dry powder: selected fresh cactus, after cleaning at cutting Reason, is freeze-dried 3-6h in subzero 60-80 degrees Celsius of low temperature refrigerator, is 20Pa-40Pa in vacuum degree, sublimation temperature is 2-4h is dried in vacuum sublimation under conditions of 40-60 DEG C, 80-100 mesh is crushed in pulverizer, at subzero 65-75 degrees Celsius, very Reciprocal of duty cycle is vacuum freeze drying under conditions of 20Pa-40Pa, and drying to water content is 6%, obtains cactus dry powder, is freeze-dried The forfeiture of beneficiating ingredient in cactus can be prevented with lyophilization, it is ensured that the reservation of beneficiating ingredient in cactus, in addition, freezing Dry and vacuum sublimation drying can promote cell wall embrittlement, conducive to the extraction of subsequent beneficiating ingredient；2. selected cactus dry powder, It is put into extractor, 18-22 times of weight of cactus dry powder of water and the fiber of cactus dry powder weight 0.8-1.5% is added Plain enzyme is heated to 45-55 DEG C and maintains this temperature, the excessively high internal structure that can destroy cactus powder of temperature, cause effectively at Divide and be destroyed, adjust pH to 4-6, after digesting 50-70min, be cooled to 22-26 DEG C, stirs 1.5-2.5h with 2 lattice revolving speeds, use The centrifuge of 4000r/min is centrifuged 8-12min, merges supernatant, and the active carbon of supernatant quality 4-6% is added, and stands 20- Active carbon is centrifuged off after 30h, merging Aqueous extracts are stand-by, are digested before extracting, digest the cactus powder water of assisted extraction Extracting solution has good stability, and indices are better than common Aqueous extracts；

(6) pH to 4.5 for the mixture that regulating step (5) obtains obtains Radix Notoginseng and preserves youthful looks facial mask liquid；

Embodiment 2

Radix Notoginseng facial mask of preserving youthful looks includes following components by weight percent: 11 parts of Notogineng Extract, 9 parts of Salvia root P.E, Radix Angelicae Sinensis 9 parts of extract, 9 parts of bupleurum extract, 7 parts of Radix et Caulis Opuntiae Dillenii extract, 7 parts of Radix Oenotherae erythrosepalae extract, 4 parts of hyaluronic acid, glycine betaine 4 Part, 3 parts of xanthan gum, 4 parts of methylisothiazolinone, 3 parts of glycerol, 2 parts of propylene glycol, 5 parts of hydrolytic collagen, 145 parts of deionized water.

(1) preparation of Notogineng Extract: the ethyl alcohol of 50%-60% is added in selected Roots of Panax Notoginseng powder, and amount of alcohol added is Radix Notoginseng 8 times of root powder weight, immersion 30-50min, refluxing extraction 2-3 times, each 100-150min, merging filtrate are stand-by；

(2) preparation of Salvia root P.E: selected Radix Salviae Miltiorrhizae is ground into 30-50 mesh after cleaning drying, is packed into extraction kettle barrel In, extraction kettle, separating still are heated respectively, open cooling water water-bath refrigeration, at 40-50 DEG C to be achieved, opens CO₂Gas Bottle, is forced into 20-30MPa to system by high-pressure pump, while opening entrainer pump, squeezes into accurate quantitative analysis entrainer, carries secretly The addition of agent, can be improved extraction efficiency, promote the precipitation of effective component, the ethyl alcohol that entrainer is 95%, dosage 400ml/ H is allowed to become fluid-mixing with carbon dioxide, and pressure reaches 25MPa, and temperature is static immersing 28-32min after 45 DEG C, then Dynamic extraction is carried out, takes a sample every 1-1.5h, it is stand-by after concentration；

(4) preparation of Radix et Caulis Opuntiae Dillenii extract: cactus dry powder is 1. prepared: selected fresh cactus, cutting processing after cleaning, It is freeze-dried 3-6h in subzero 60-80 degrees Celsius of low temperature refrigerator, is 20Pa-40Pa, sublimation temperature 40-60 in vacuum degree 2-4h is dried in vacuum sublimation under conditions of DEG C, and 80-100 mesh is crushed in pulverizer, at subzero 65-75 degrees Celsius, vacuum degree For vacuum freeze drying under conditions of 20Pa-40Pa, drying to water content is 8%, obtains cactus dry powder, freeze-drying and liter Magnificent drying can prevent the forfeiture of beneficiating ingredient in cactus, it is ensured that the reservation of beneficiating ingredient in cactus, in addition, freeze-drying It can promote cell wall embrittlement with vacuum sublimation drying, conducive to the extraction of subsequent beneficiating ingredient；2. selected cactus dry powder, is put into In extractor, 18-22 times of weight of cactus dry powder of water and the cellulase of cactus dry powder weight 0.8-1.5% is added, It is heated to 45-55 DEG C and maintains this temperature, the excessively high internal structure that can destroy cactus powder of temperature causes effective component to be broken It is bad, pH to 4-6, E/S 1% are adjusted, after digesting 50-70min, is cooled to 22-26 DEG C, 1.5-2.5h is stirred with 2 lattice revolving speeds, adopts It is centrifuged 8-12min with the centrifuge of 4000r/min, merges supernatant, the active carbon of supernatant quality 4-6% is added, stand 20- Active carbon is centrifuged off after 30h, merging Aqueous extracts are stand-by, are digested before extracting, digest the cactus powder water of assisted extraction Extracting solution has good stability, and indices are better than common Aqueous extracts；

(6) pH to pH for the mixture that regulating step (5) obtains is adjusted to 5.5, obtains Radix Notoginseng and preserves youthful looks facial mask liquid；

Embodiment 3

Radix Notoginseng facial mask of preserving youthful looks includes following components by weight percent: 14 parts of Notogineng Extract, 10 parts of Salvia root P.E, Radix Angelicae Sinensis 10 parts of extract, 10 parts of bupleurum extract, 8 parts of Radix et Caulis Opuntiae Dillenii extract, 8 parts of Radix Oenotherae erythrosepalae extract, 5 parts of hyaluronic acid, glycine betaine 5 Part, 4 parts of xanthan gum, 5 parts of methylisothiazolinone, 4 parts of glycerol, 2 parts of propylene glycol, 6 parts of hydrolytic collagen, 185 parts of deionized water.

(1) preparation of Notogineng Extract: the ethyl alcohol of 50%-60% is added in selected Roots of Panax Notoginseng powder, and amount of alcohol added is Radix Notoginseng 10 times of root powder weight, immersion 30-50min, refluxing extraction 2-3 times, each 100-150min, merging filtrate are stand-by；

(2) preparation of Salvia root P.E: selected Radix Salviae Miltiorrhizae is ground into 30-50 mesh after cleaning drying, is packed into extraction kettle barrel In, extraction kettle, separating still are heated respectively, open cooling water water-bath refrigeration, at 40-50 DEG C to be achieved, opens CO₂Gas Bottle, is forced into 20-30MPa to system by high-pressure pump, while opening entrainer pump, squeezes into accurate quantitative analysis entrainer, carries secretly The addition of agent, can be improved extraction efficiency, promote the precipitation of effective component, the ethyl alcohol that entrainer is 95%, dosage 450ml/ H is allowed to become fluid-mixing with carbon dioxide, and pressure reaches 30MPa, static immersing 28-32min after temperature reaches 50 DEG C, so Laggard Mobile state extraction, takes a sample every 1-1.5h, stand-by after concentration；

(4) preparation of Radix et Caulis Opuntiae Dillenii extract: cactus dry powder is 1. prepared: selected fresh cactus, cutting processing after cleaning, It is freeze-dried 3-6h in subzero 60-80 degrees Celsius of low temperature refrigerator, is 20Pa-40Pa, sublimation temperature 40-60 in vacuum degree 2-4h is dried in vacuum sublimation under conditions of DEG C, and 80-100 mesh is crushed in pulverizer, at subzero 65-75 degrees Celsius, vacuum degree For vacuum freeze drying under conditions of 20Pa-40Pa, dry to water content is 10%, obtains cactus dry powder, freeze-drying and Lyophilization can prevent the forfeiture of beneficiating ingredient in cactus, it is ensured that the reservation of beneficiating ingredient in cactus, in addition, freezing is dry Dry and vacuum sublimation drying can promote cell wall embrittlement, conducive to the extraction of subsequent beneficiating ingredient；2. selected cactus dry powder, puts Enter in extractor, 18-22 times of weight of cactus dry powder of water and the cellulose of cactus dry powder weight 0.8-1.5% is added Enzyme is heated to 45-55 DEG C and maintains this temperature, and the excessively high internal structure that can destroy cactus powder of temperature leads to effective component It is destroyed, adjusts pH to 4-6, E/S 1.2%, after digesting 50-70min, be cooled to 22-26 DEG C, stir 1.5- with 2 lattice revolving speeds 2.5h is centrifuged 8-12min using the centrifuge of 4000r/min, merges supernatant, the active carbon of supernatant quality 4-6% is added, It is centrifuged off active carbon after standing 20-30h, merging Aqueous extracts are stand-by, are digested before extracting, digest the celestial being of assisted extraction Palm powder aqueous extract has good stability, and indices are better than common Aqueous extracts；

(5) by the hyaluronic acid of formula ratio, glycine betaine, xanthan gum, methylisothiazolinone, glycerol, propylene glycol, hydrolysis glue Original, deionized water addition emulsion tank internal emulsification are uniform, and the additional amount of glycerol and propylene glycol is 1:0.7, add the step of formula ratio Suddenly the radix bupleuri of the Notogineng Extract, Salvia root P.E, angelica extract of (1)-(4) preparation, Radix et Caulis Opuntiae Dillenii extract and formula ratio After extract, Radix Oenotherae erythrosepalae extract stir and evenly mix, the homogeneous 30-45min in homogenizer obtains emulsifying uniform mixture；

(6) pH to pH for the mixture that regulating step (5) obtains is adjusted to 6.5, obtains Radix Notoginseng and preserves youthful looks facial mask liquid；

Experimental analysis:

Experiment one: keratoderma water content test

1, experimental subjects: voluntarily signature informed consent form, health, the age 20~54 years old 80 women volunteer for selection Subject carries out facial mask observation on probation, volunteer's stochastic averagina is divided into 4 groups, every group of 20 people, every group includes 20-28,29- 37, the subject of 38-54 three phases.Informed consent form is signed with study subject and limits receiving and exclusion criteria.It is tested right As recipient's standard be 20~54 years old health, through interrogation eligible；Study subject eliminator's standard is to tested cosmetics Allergy sufferers, in addition, there is the severe primaries disease such as conscience kidney and hemopoietic system, mental patient does not use according to regulations tested material, Can not determining effect or data, umbra does not ring effect judgement person, does not meet and receives standard.

2, experiment arranges: 4 groups of subjects, the daily life system time consistency during test, diet is consistent, early during test Morning uses same skin care item, and dosage is identical, clears up face using same mildy wash cooperation warm water, cleaning is completed at 9 points at night Afterwards, it is applied using facial mask made of embodiment 1 in face for first group, film cloth is smoothed, it is quiet to enjoy 15-20min, nothing is used after removing eye mask Name finger belly gently massages eye circumference 2-3min；Second group uses facial mask made of embodiment 2, and application method is identical as first group； For third group using facial mask made of embodiment 3, application method is identical as first group；4th group using it is commercially available, with the Ministry of Public Health batch The a certain brand facial mask of quasi- code, application method it is identical as first group (it is when first used once every three days, a piece of daily, it is subsequent every Week uses 2-3 times, the time consistency of every group of subject's face mask film).

3, experimental method: (1) short-acting test: volunteer after 9 face cleanings, uniformly smears the facial mask of same dose at night, point Not in using preceding 0h, using rear 1h, 2h, 4h and 6h, surveyed using moisture tester Corneometer (CM825, German CK company) Volunteer's left and right face cheek position water content of stratum corneum is measured, measures 3 times and is averaged；(2) long-acting test: volunteer every night 9 Point face cleaning after, uniformly smear same dose facial mask, continuous 8 weeks, use first 0 week, using 2 weeks, 4 weeks, 6 weeks, 8 weeks, respectively make Volunteer's left and right face cheek position water content of stratum corneum is measured with moisture tester Corneometer (CM825, German CK company), It measures 3 times and is averaged.(it is required that subject per's test is the same time in the daytime)

4, experimental result: the results are shown in Table 1 for 4 groups of subjects or so cheek moisture measurement:

The keratoderma water content statistical form of 1 experimental group of table, control group

As can be seen from Table 1: either short-acting test or long-acting test, volunteer use three made of embodiment 1-3 Seven preserve youthful looks after facial mask, and keratoderma water content is above common facial mask commercially available, with Ministry of Public Health's authentication code.

Experiment two: anti-wrinkle effect test

1, experimental subjects: identical as the experimental subjects selection criteria of experiment one.

2, experiment arranges: identical as the experiment arrangement of experiment one.

3, experimental method: using the skin elasticity of Courage+Khazaka company, Germany (German CK company) manufacture CotometerMPA580 host, used probe are Reviscometer RV600 elastic fibrous tissue test probes, survey five It is secondary to be averaged.Test zone: place between the eyebrows middle up 2cm forehead region, lower lip middle 2cm chin area, nose down Point and left and right cheek region at pupil intersection.The blank value (R2, R5, R7) of 30min after being tested region clean is first measured, so Regulation subject adheres to preserve youthful looks using Radix Notoginseng made of embodiment 1-3 facial mask and common commercially available facial mask sooner or later daily afterwards, surveys respectively (negative pressure is constant in test process is test zone skin elasticity index R2, R5, R7 value after examination 2 weeks, 4 weeks, 6 weeks, 8 weeks 450mbar)。

4, experimental index illustrates: for skin elasticity index R2, R5, R7 closer to 1, the elasticity of skin is better.

R2=Ua/Uf；R5=Ur/Ue；R7=Ur/Uf；Wherein:

Uf --- skin maximum tension amount

Ue --- after constant negative pressure is added on skin, the amount of tension of skin, positioning elastic part amount of tension at 0.1 second.

Ur --- after cancelling negative pressure, skin will restore to the original state rapidly state, equally be divided into elastic portion score value Ur, that is, cancel negative Pressure is after 0.1 second, the recovery value and visco-elastic portions value or plastic value of skin.

Ua --- from cancellation negative pressure to the recovery value of skin when follow-on test skin surface adds negative pressure again next time.

5, experimental result: by experimental group and the anti-wrinkle effect of control group statistics in table 2.

The anti-wrinkle effect statistical form of 2 experimental group of table, control group

As can be seen from Table 2: after volunteer is using facial mask made of embodiment 1-3, skin elasticity index R2, R5, R7 is equal Higher than common commercially available facial mask, i.e. anti-wrinkle effect is better than common commercially available facial mask.

Experiment three: whitening effect test

3, experimental result: using before facial mask, tester's cheek position is shot with VISIA digital skin analyzer (U.S.) Image, obtain initial absolute score value, 2 weeks, 4 weeks, 6 weeks and 8 weeks same time in the daytime, 20 DEG C of room temperature of control after application facial mask ± 2 DEG C, relative humidity (RH) 55% ± 3%, tester 30min before survey enters quiet to be measured in test environment, 10min before surveying Face slightly cleans, and cleaning finishes the image for using VISIA digital skin analyzer (U.S.) to shoot tester's cheek position after 1h (analyzed area avoids laugh line, retroreflective regions, black mole and hair as far as possible) is tied test using absolute score value item as analytical standard Fruit counts in table 3.Wherein, the improvement of skin-whitening is with the absolute score value of color spot, ultraviolet spot, chloasma and red area, black The change rate of red pigment value is measured, that is: change rate=test value-control value/control value × 100%.

The whitening effect table of comparisons of 3 experimental group of table, control group

As can be seen from Table 3: volunteer is better than common commercially available face using whitening effect after facial mask made of embodiment 1-3 Film, wherein color spot, ultraviolet spot, chloasma fading effect be better than common commercially available facial mask eye sticker, red area reduces area and is greater than Common commercially available facial mask.

Invention using the active constituent of natural plants as raw material, using the reasonable compatibility between Chinese herbal medicine, The effect of each active constituent is significantly improved, and without any side effects, can be used for a long time；Notogineng Extract can protect skin Skin improves skin appearance, makes skin emolliency and increase elasticity, reasonable compatibility Salvia root P.E can not only play Radix Salviae Miltiorrhizae promoting blood circulationization The effects of silt, freckle removing and whitening, calmness, anti-inflammatory sterilization, relieving swelling and reddness of eye, moreover it is possible to significantly increase the oxidation resistance of Radix Notoginseng, remove super Oxygen anion, meanwhile, Radix Notoginseng can increase the stability of effective component in Salvia root P.E.Angelica extract includes ammonia abundant The bioactive substances such as base acid, vitamin, natural moisturizing factor, microelement, amino acid that compatibility is rich in, superoxide dismutase The Radix et Caulis Opuntiae Dillenii extract of the chemical components such as enzyme (SOD) and polysaccharide, can not only keep the original nutrition of skin and moisture, avoid skin Solarization injures melanin deposition, is effective against skin aging, moreover it is possible to smooth the microgroove of face, efficiently supplement and lock in cuticula Moisture dispels freckle, and with Radix Oenotherae erythrosepalae extract compatibility, sensitive skin also can be used easily, is not inhibited.Bupleurum extract compatibility Salvia root P.E can promote the generation of collagen in skin hyaluronic acid and epidermal cell, promote skin to assign and live, radix bupleuri extracts Object compatibility Radix et Caulis Opuntiae Dillenii extract can control cortex secretion, prevent acne, bupleurum extract compatibility angelica extract has promoting blood circulation The effect of enriching blood.

Finally, the above examples are only used to illustrate the technical scheme of the present invention and are not limiting, although through the foregoing embodiment The present invention is described in detail, however, those skilled in the art should understand that, can be right in the form and details It makes various changes, without departing from claims of the present invention limited range.

Claims

The facial mask 1. a kind of Radix Notoginseng is preserved youthful looks, it is characterised in that: Radix Notoginseng facial mask of preserving youthful looks includes following components: Notogineng Extract, Salvia root P.E, angelica extract, bupleurum extract, Radix et Caulis Opuntiae Dillenii extract, Radix Oenotherae erythrosepalae extract, hyaluronic acid, glycine betaine, Huang Virgin rubber, methylisothiazolinone, glycerol, propylene glycol, hydrolytic collagen, deionized water；The Radix Notoginseng is preserved youthful looks the preparation method of facial mask, Specifically includes the following steps:

(1) preparation of Notogineng Extract: the ethyl alcohol of 50%-60% is added in selected Roots of Panax Notoginseng powder, impregnates 30-50min, refluxing extraction 2-3 times, each 100-150min, merging filtrate is stand-by；

(2) preparation of Salvia root P.E: selected Radix Salviae Miltiorrhizae is ground into 30-50 mesh after cleaning drying, is fitted into extraction kettle barrel, point It is other that extraction kettle, separating still are heated, cooling water water-bath refrigeration is opened, at 40-50 DEG C to be achieved, opens CO₂Gas cylinder passes through High-pressure pump is forced into 20-30MPa to system, while opening entrainer pump, squeezes into entrainer to accurate quantitative analysis, is allowed to and titanium dioxide Carbon becomes fluid-mixing, reaches static immersing 28-32 min after extraction conditions, then carries out dynamic extraction, take every 1-1.5h Sample, it is stand-by after concentration；

(3) preparation of angelica extract: selected Radix Angelicae Sinensis is ground into 10-20 mesh after cleaning drying, is added under normal pressure with " double formulations " Three times, combined extract adds 100-120 mesh to filter respectively, in the centrifugation of 3000r/min to circumfluence distillation with 3-5 layers of gauze It is centrifuged 10-20 minutes in machine, it is stand-by to merge supernatant；

(4) preparation of Radix et Caulis Opuntiae Dillenii extract: selected cactus dry powder is put into extractor, and cactus dry powder weight 18-22 is added The cellulase of water again and cactus dry powder weight 0.8-1.5%, is heated to 45-55 DEG C and maintains this temperature, adjusts PH to 4-6 is cooled to 22-26 DEG C after digesting 50-70min, stirs 1.5-2.5h with 2 lattice revolving speeds, using 4000r/min from Scheming is centrifuged 8-12min, merges supernatant, and the active carbon of supernatant quality 4-6% is added, and is centrifuged off work after standing 20-30h Property charcoal, merge Aqueous extracts it is stand-by；

(5) by the hyaluronic acid of formula ratio, glycine betaine, xanthan gum, methylisothiazolinone, glycerol, propylene glycol, hydrolytic collagen, The Notogineng Extract, Radix Salviae Miltiorrhizae of the step of deionized water addition emulsion tank internal emulsification is uniform, adds formula ratio (1)-(4) preparation mention After taking the bupleurum extract of object, angelica extract, Radix et Caulis Opuntiae Dillenii extract and formula ratio, Radix Oenotherae erythrosepalae extract to stir and evenly mix, Homogeneous 30-45min in homogenizer obtains emulsifying uniform mixture；

(6) pH for the mixture that regulating step (5) obtains is to faintly acid, obtains Radix Notoginseng and preserves youthful looks facial mask liquid；

(7) step (6) resulting Radix Notoginseng facial mask liquid of preserving youthful looks is sterilized 24-32 minutes in disinfection cabinet, then by molding natural silkworm The Radix Notoginseng that cortina mask sheet is soaked in after disinfection is preserved youthful looks in facial mask liquid 18-26 minute, then by natural silk film mask sheet packaging Sealing is got product.
The facial mask 2. Radix Notoginseng according to claim 1 is preserved youthful looks, it is characterised in that: in step (1), amount of alcohol added is Radix Notoginseng 6-10 times of root powder weight.
The facial mask 3. Radix Notoginseng according to claim 1 is preserved youthful looks, it is characterised in that: in step (2), entrainer be 95% second Alcohol, dosage 350-450ml/h.
The facial mask 4. Radix Notoginseng according to claim 1 is preserved youthful looks, it is characterised in that: in step (4), the production of cactus dry powder Method are as follows: selected fresh cactus, cutting processing, is freeze-dried 3- in subzero 60-80 degrees Celsius of low temperature refrigerator after cleaning 6h is 20Pa-40Pa in vacuum degree, the dry 2-4h of vacuum sublimation, the powder in pulverizer under conditions of sublimation temperature is 40-60 DEG C It is broken to 80-100 mesh, at subzero 65-75 degrees Celsius, vacuum degree is vacuum freeze drying under conditions of 20Pa-40Pa, obtains celestial being Slap dry powder.