CN102641228B - Rhodiola crenulata eye cream with whitening and anti-wrinkle effects - Google Patents

Rhodiola crenulata eye cream with whitening and anti-wrinkle effects Download PDF

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Publication number
CN102641228B
CN102641228B CN 201210155162 CN201210155162A CN102641228B CN 102641228 B CN102641228 B CN 102641228B CN 201210155162 CN201210155162 CN 201210155162 CN 201210155162 A CN201210155162 A CN 201210155162A CN 102641228 B CN102641228 B CN 102641228B
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extracting solution
skin
concentrated
eye cream
rhodiola crenulata
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CN102641228A (en
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卢小红
孔维颖
周军
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Tibet Tibetan Medicine Group Co ltd
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TONGDE GROUP CO Ltd
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Abstract

The invention discloses a rhodiola crenulata eye cream with whitening and anti-wrinkle effects. The rhodiola crenulata eye cream is mainly prepared from rhodiola crenulata root extract, black tea extract, coix seed extract, honeysuckle flower extract and corresponding adjuvants. Rhodiola crenulata can nourish and moisturize skin and keep constant moisture and elasticity of the skin and has anti-oxidation and whitening functions. Known from Compendium of Materia Medica, coix seeds have the functions of 'nourishing facial appearance and keeping youth', whitening and removing freckles, contracting pores, excreting water and slimming bodies. Black tea can moisturize skin, promote blood circulation and activate cells. Honeysuckle flower, also named lonicera japonica, can improve the water keeping capability of the skin and form a natural water keeping screen. The rhodiola crenulata eye cream is prepared from rhodiola crenulata serving as 'monarch', coix seeds serving as 'minister', black tea serving as 'assistant' and honeysuckle flower serving as 'guide' under the support of adjuvants. The rhodiola crenulata eye cream can promote skin metabolism, enhance skin activity, reduce epidermal pigmentation and resist against oxidation and removing oxygen free radicals; and the rhodiola crenulata eye cream is fine and smooth, has certain whitening, moisturizing and anti-wrinkle effects and prevents generation of thin wrinkles near eyes.

Description

A kind of Radix Rhodiolae eye cream with tender white crease-resistant effect
Technical field
The present invention relates to technical field of skin care, be specifically related to a kind of Radix Rhodiolae eye cream with tender white crease-resistant effect and preparation method thereof.
Background technology
Along with the progress of society and improving constantly of expanding economy and living standards of the people, people are also more and more higher to the requirement of beauty and skin care cosmetics, and more and more the direction to " naturalization, nutrient laden, curative effectization " develops.But great majority all contain harmful chemical substance in the various beauty and skin care cosmetics in the market, and as poisonous and harmful substances such as leaded, hydrargyrum, these skin care item cause people's skin allergy easily, and human organ and function are caused damage.From eighties of last century eighties, the skin expert just finds, adds various natural materials in skin care item, skin is had good nourishing effect, and have no side effect, and particularly effective component extracting adds to and has more remarkable effect in the skin care item from plant.Therefore, development is a kind of utilizes pure natural substance to make the beauty and skin care cosmetics that human body skin is had nutrition and a protective effect very important meaning is just arranged.
Summary of the invention
In view of above-mentioned weak point, the object of the present invention is to provide a kind of natural plant extracts that utilizes to have Radix Rhodiolae eye cream of tender white crease-resistant effect and preparation method thereof for what primary raw material made.
The consumption of each raw material of the present invention is also groped to sum up to draw through the inventor in a large number, each raw material consumption all has effect preferably in following weight range: a kind of Radix Rhodiolae eye cream with tender white crease-resistant effect, and this eye cream is to be made by the raw material of following weight distribution ratio:
Radix Rhodiolae root extracting solution 0.8-1.2 part
Black tea extracting solution 0.4-0.6 part
Semen Coicis extracting solution 0.4-0.6 part
Flos Lonicerae extracting solution 0.4-0.6 part
Caprylyl glycol 0.4-0.6 part
Beta glucan 1-3 part
Encircle five polydimethylsiloxane 0.8-1.2 parts
Polydimethylsiloxane 1-3 part
Polydimethylsiloxane/methyl polysilicone alkyl copolymer 6-8 part
Vinyldimethicone/polymethyl siloxane silsesquioxane cross linked polymer 4-6 part
Hyaluronate sodium 0.04-0.06 part
Glycerol 8-12 part
EHA/VP/ polydimethylsiloxane methacrylate copolymer 1-1.5
Butanediol 4-6 part
Water 80-120 part.
Further, the Radix Rhodiolae eye cream with tender white crease-resistant effect is made by following raw materials in part by weight:
1 part of Radix Rhodiolae root extracting solution
0.5 part of black tea extracting solution
0.5 part of Semen Coicis extracting solution
0.5 part of Flos Lonicerae extracting solution
0.5 part of caprylyl glycol
2 parts of beta glucans
Encircle 1 part of five polydimethylsiloxane
2 parts of polydimethylsiloxane
7 parts of polydimethylsiloxane/methyl polysilicone alkyl copolymer
5 parts of vinyldimethicone/polymethyl siloxane silsesquioxane cross linked polymer
0.05 part of hyaluronate sodium
10 parts of glycerol
1.3 parts of EHAs/VP/ polydimethylsiloxane methacrylate copolymer
5 parts of butanediols
100 parts in water.
Raw materials used among the present invention all can be by commercially available acquisition, wherein Radix Rhodiolae root extracting solution, black tea extracting solution, Semen Coicis extracting solution and Flos Lonicerae extracting solution can also obtain or by following preparation technology's acquisition by the prior art means:
The preparation technology of described Radix Rhodiolae root extracting solution is: get the Radix Rhodiolae root, remove rough bark, add 6-8 and doubly measure the 60%-70% alcohol reflux three times, first and second time 3 hours extracted 2 hours for the third time, filtered, merge extractive liquid,, reclaim ethanol to there not being the alcohol flavor, be concentrated into the thick paste that relative density is 1.25-1.45,60 ℃ of surveys; And then add 3-5 times of water gaging, the water precipitating secondary, each 48 hours, get supernatant, filter, filtrate be concentrated into relative density be 1.03-1.10 concentrated solution namely, 60 ℃ of surveys.
The preparation technology of described black tea extracting solution is: the dry bud-leaf of getting plant of theaceae black tea, add 90 ℃ of water of 10 times of amounts, soaked 15-20 minute, ultrasonic extraction 2 times, each 10-15 minute, filter merging filtrate, filtrate be concentrated into relative density be 1.03-1.10 concentrated solution namely, 60 ℃ of surveys.
The preparation technology of described Semen Coicis extracting solution is: gets Semen Coicis, pulverizes, adds 6-8 times of decocting and boil secondary, and 2 hours for the first time, 1 hour for the second time, filtration, merging filtrate is concentrated into relative density and is the concentrated solution of 1.03-1.10 namely, 60 ℃ of surveys.
The preparation technology of described Flos Lonicerae extracting solution is: gets 6-8 times of decocting of caprifoliaceae plant dry flower of light red Radix Ophiopogonis adding and boils secondary, and 2 hours for the first time, 1 hour for the second time, filter, merging filtrate is concentrated into relative density and is the concentrated solution of 1.03-1.10 namely, 60 ℃ of surveys.
The concrete preparation process for preparing the Radix Rhodiolae eye cream with tender white crease-resistant effect is as follows:
With ring five polydimethylsiloxane, polydimethylsiloxane, polydimethylsiloxane/methyl polysilicone alkyl copolymer, the vinyldimethicone/polymethyl siloxane silsesquioxane cross linked polymer of above-mentioned formula ratio put into be warmed up in the emulsifying pot 45 the degree, get A phase thing; Again hyaluronate sodium, glycerol, butanediol and water are dropped into and be heated to 85 degree dissolvings in the water pot fully, be cooled to obtain B phase thing behind 45 degree, taking out B phase thing goes into the emulsifying pot and mixes with A phase thing, 45 rev/mins of mixing speeds, homogenizing 10 minutes, stir insulation 20 minutes after adding Radix Rhodiolae root extracting solution, black tea extracting solution, Semen Coicis extracting solution, Flos Lonicerae extracting solution and beta glucan, caprylyl glycol at last again, discharging namely gets eye cream behind the evacuation froth breaking.
The Radix Rhodiolae root extract contains effective active compositions such as rhodioloside, butyl alcohol, ketone and rhodosin among the present invention, and Radix Rhodiolae is top grade in the Rhodida plant, is the standards of pharmacopoeia that version Pharmacopoeia of the People's Republic of China Radix Rhodiolae in 2010 is included.Modern scientific research shows in the Radix Rhodiolae rhizome and contains several physiological active substances to have strengthening by means of tonics effects such as anoxia enduring, radioprotective, resisting fatigue, slow down aging, prophylaxis of tumours diffusion.Compositions such as rhodioloside, butyl alcohol, ketone are 5 times of other kind Radix Rhodiolaes in the Caulis et folium clerodendri bungei Herba hylotelephii erythrosticti.Be described as " snowy region Radix Ginseng ", the ability that has good oxidation resistance and remove ultra-oxygen anion free radical is better than hydroxyl radical free radical and greater than vitamin E.Studies show that the Radix Rhodiolae root extract has the ability of vitro inhibition tyrosinase activity, tyrosine changes melanin in the blocking-up skin under the catalysis of tryrosinase, thereby reduces melanic generation, reaches the effect of whitening.And the concentration of suppression ratio and extracting solution becomes positive correlation.Radix Rhodiolae root extract (rhodioloside and total flavones) has the ability of antioxidation in vitro, the Radix Rhodiolae root extract is applied to cosmetic skin care product aspect, mainly possessed defying age, antioxidation, free radical resisting, radioprotective, whiten, anti-effect such as chap.But the delaying human body skin aging keeps the skin vigor, prevents computer and daily Exposure to Sunlight radiation, and it is obscure to improve the skin color and luster, increases skin elasticity, make that skin and muscles are fair, tender, vigor is arranged, can be used as the whitening anti-aging cosmetics additive.
Black tea belongs to full fermentation teas, is that the bud-leaf with Camellia sinensis is raw material, and typical process processes such as (cutting), fermentation, drying are refining forms through withering, kneading.Doing dark brown pool because of it is homophony with the redness with the millet paste that brews, so name black tea.Contain Polyphenols in the black tea, carbohydrate, aminoacid, pectin, theaflavin, thearubigins, multiple materials such as tea polybase and antioxidant, tool refresh oneself disappear tired, replenishing body fluid and clearing away heat pathogen, anti-inflammation and sterilization, detoxifcation, strong skeleton and antioxidation, effects such as slow down aging, result of study shows, antioxidant in the black tea is the propagation path of chemical substance in the destruction of cancer cells thoroughly, the effect of black tea and green tea is roughly suitable, but the antioxidant of black tea than the green tea complexity many, especially useful especially to heart, the USA Magazine report, black tea defying age effect is better than Bulbus Allii head, Caulis et Folium Brassicae capitatae and Radix Dauci Sativae etc.
Flos Lonicerae claims Flos Lonicerae again, is the caprifoliaceae plant alabastrum of Radix Ophiopogonis.Composition contains chlorogenic acid, isochlorogenic acid, neochlorogenic acid, Flavonoid substances, lonicerin, matter, inositol, Saponin etc.Total amino acids content reaches about 8%.The content of water-soluble amino acid is about 0.1%, and the content of water-soluble carbon aquation platform thing is at l more than 8%, and contain at least manganese, chromium, nickel, actinium, zinc, cobalt, silicon, ferrum, etc. eight kinds of trace element of needed by human.Also contain the chemical constituent of volatilization wet goods more than 30 kinds and form, many types wherein can be used for making perfume, edible essence etc.It is used for cosmetics also is to plant Chinese herbal medicine additive preferably.Extract fragrant volatile oil and with the active substance of the Flos Lonicerae of solvent extraction with steam distillation, joining the bathing thinner receives in the product, to not injury of skin, make that foam is abundant, fragrance is soft, take out stains, cleaning skin, nourishing skin, make skin keep higher water content, strengthen the vigor of skin, reach the effect of delaying decrepitude of skin.Seborrheic dermatitis, good skin inflammation also there is certain curative effect.
Semen Coicis rich in proteins, lipid, vitamin B1, B2, glucosan and acidic polysaccharose, Compendium of Material Medica meaning Semen Coicis " invigorating spleen and reinforcing stomach, tonifying the lung heat clearing away, expelling wind and dampness, skin care are stayed and held, make light of one's life by commiting suicide and prolong life ".Semen Coicis can promote the metabolism of body inner blood and moisture.Semen Coicis makes skin smooth because of rich in proteins, vitamin B1, B2, reduce wrinkle, eliminate the effect of pigment spot, can assist to eliminate mottle, make skin more fair, can also reach the effect of Glycerin, can treat brown patch, freckle, pimples when whitening, speckle is disappeared and Glycerin.To the tangible curative effect of having of face acne and pachylosis, also ultraviolet there is absorbability simultaneously in addition, also can reaches sun-proof and effect anti-ultraviolet in its extractive matter adding cosmetics.
Among the present invention, Radix Rhodiolae can moisten to support preserves moisture, and keeps the constant humidity elasticity of skin, and has antioxidation and whitening function, is recited as " gold plant " by Compendium of Material Medica.Compendium of Material Medica meaning Semen Coicis " skin care is stayed and held ", energy whitening and speckle dispelling, receipts fine, soft fur hole, draining weight reducing.Make skin smooth, reduce wrinkle, eliminate pigment.Black tea can skin care, blood circulation promoting, and activating cell has antibiotic, effect such as refresh oneself simultaneously.Flos Lonicerae claims Flos Lonicerae again.It can promote the skin water holding capacity, forms natural lock water barrier.Be " monarch " with Radix Rhodiolae, Semen Coicis is " minister ", " assistant " with black tea, " making " can promote skin metabolism with Flos Lonicerae, strengthen skin activity, alleviate the epidermis pigmentation, antioxidation and removing oxygen-derived free radicals are fine and smooth moist, have certain tender white, preserve moisture and anti-wrinkle effect, prevent the generation of eye microgroove.
The specific embodiment
Below we will do a detailed explanation to the present invention in conjunction with specific embodiments.
Embodiment 1
In the present embodiment, raw material components and consumption that preparation has the Radix Rhodiolae eye cream of tender white crease-resistant effect are:
Radix Rhodiolae root extracting solution 10g
Black tea extracting solution 5g
Semen Coicis extracting solution 5g
Flos Lonicerae extracting solution 5g
Caprylyl glycol 5g
Beta glucan 20g
Encircle five polydimethylsiloxane 10g
Polydimethylsiloxane 20g
Polydimethylsiloxane/methyl polysilicone alkyl copolymer 70g
Vinyldimethicone/polymethyl siloxane silsesquioxane cross linked polymer 50g
Hyaluronate sodium 0.5g
Glycerol 100g
EHA/VP/ polydimethylsiloxane methacrylate copolymer 13g
Butanediol 50g
Water 1000g.
Its preparation process is: ring five polydimethylsiloxane, polydimethylsiloxane, polydimethylsiloxane/methyl polysilicone alkyl copolymer, the vinyldimethicone/polymethyl siloxane silsesquioxane cross linked polymer of above-mentioned formula ratio are put into be warmed up to 45 degree in the emulsifying pot, get A phase thing; Again hyaluronate sodium, glycerol, butanediol and water are dropped into and be heated to 85 degree dissolvings in the water pot fully, be cooled to obtain B phase thing behind 45 degree, taking out B phase thing goes into the emulsifying pot and mixes with A phase thing, 45 rev/mins of mixing speeds, homogenizing 10 minutes, stir insulation 20 minutes after adding Radix Rhodiolae root extracting solution, black tea extracting solution, Semen Coicis extracting solution, Flos Lonicerae extracting solution and beta glucan, caprylyl glycol at last again, discharging namely gets eye cream behind the evacuation froth breaking.
Embodiment 2
Preparation process is with embodiment 1, and different is that raw material components and consumption with Radix Rhodiolae eye cream of tender white crease-resistant effect are:
Radix Rhodiolae root extracting solution 8g
Black tea extracting solution 4g
Semen Coicis extracting solution 4g
Flos Lonicerae extracting solution 4g
Caprylyl glycol 4g
Beta glucan 10g
Encircle five polydimethylsiloxane 8g
Polydimethylsiloxane 10g
Polydimethylsiloxane/methyl polysilicone alkyl copolymer 60g
Vinyldimethicone/polymethyl siloxane silsesquioxane cross linked polymer 40g
Hyaluronate sodium 0.4g
Glycerol 80g
EHA/VP/ polydimethylsiloxane methacrylate copolymer 10g
Butanediol 40g
Water 800g.
Embodiment 3
Preparation process is with embodiment 1, and different is that raw material components and consumption with Radix Rhodiolae eye cream of tender white crease-resistant effect are:
Radix Rhodiolae root extracting solution 12g
Black tea extracting solution 6g
Semen Coicis extracting solution 6g
Flos Lonicerae extracting solution 6g
Caprylyl glycol 6g
Beta glucan 30g
Encircle five polydimethylsiloxane 12g
Polydimethylsiloxane 30g
Polydimethylsiloxane/methyl polysilicone alkyl copolymer 80g
Vinyldimethicone/polymethyl siloxane silsesquioxane cross linked polymer 60g
Hyaluronate sodium 0.6g
Glycerol 120g
EHA/VP/ polydimethylsiloxane methacrylate copolymer 15g
Butanediol 60g
Water 1200g.
Each embodiment is raw materials used among the present invention all can be by commercially available acquisition, as ring five polydimethylsiloxane among the above-mentioned embodiment available from DOW CORNING (lot number: 2012060105), polydimethylsiloxane/methyl polysilicone alkyl copolymer is available from DOW CORNING (lot number: 2012022904), vinyldimethicone/polymethyl siloxane silsesquioxane cross linked polymer is available from the U.S. fluosilicic new material company limited (lot number: 2011100203) of mark, EHA/VP/ polydimethylsiloxane methacrylate copolymer available from Ke Laien (lot number: 2012022804), Radix Rhodiolae root extracting solution wherein, the black tea extracting solution, the Semen Coicis extracting solution, the Flos Lonicerae extracting solution can also obtain or obtain by following preparation technology by the prior art means:
The preparation technology of Radix Rhodiolae root extracting solution is: get the Radix Rhodiolae root, remove rough bark, add 6-8 and doubly measure the 60%-70% alcohol reflux three times, first and second time 3 hours extracted 2 hours for the third time, filtered, merge extractive liquid,, reclaim ethanol to there not being the alcohol flavor, be concentrated into the thick paste that relative density is 1.25-1.45,60 ℃ of surveys; And then add 3-5 times of water gaging, the water precipitating secondary, each 48 hours, get supernatant, filter, filtrate be concentrated into relative density be 1.03-1.10 concentrated solution namely, 60 ℃ of surveys.
The preparation technology of black tea extracting solution is: get the dry bud-leaf of plant of theaceae black tea, add 90 ℃ of water of 10 times of amounts, soaked 15-20 minute, ultrasonic extraction 2 times each 10-15 minute, is filtered, merging filtrate, filtrate be concentrated into relative density be 1.03-1.10 concentrated solution namely, 60 ℃ of surveys.
The preparation technology of Semen Coicis extracting solution is: gets Semen Coicis, pulverizes, adds 6-8 times of decocting and boil secondary, and 2 hours for the first time, 1 hour for the second time, filtration, merging filtrate is concentrated into relative density and is the concentrated solution of 1.03-1.10 namely, 60 ℃ of surveys.
The preparation technology of Flos Lonicerae extracting solution is: gets caprifoliaceae plant dry flower of light red Radix Ophiopogonis and adds 6-8 times of decocting and boil secondary, and 2 hours for the first time, 1 hour for the second time, filter, merging filtrate is concentrated into relative density and is the concentrated solution of 1.03-1.10 namely, 60 ℃ of surveys.
Through the pertinent regulations requirement of check this product accord with Q B/T 1857-2004, sense index (color and luster, fragrance, structure) meets the industry regulation, and physical and chemical index (PH, heat-resisting, cold-resistant, active matter) meets the industry regulation.
Product of the present invention is carried out following test:
Cutis laxa, pigmentation are many near the eyes to choose 50 examples, the experimenter that the eye microgroove is many, and the age is between between 30-55 year, sooner or later behind the clean skin, the eye cream that embodiment 1 is made is applied in skin around the eyes equably, sooner or later respectively once, used 60 days continuously, concrete outcome is as follows:
Table one statistics compares:
Figure 826794DEST_PATH_IMAGE002
Judgment criteria as a result:
Effectively: the experimenter feels very satisfied, and skin has more consolidation children cunning of elasticity near the eyes, and skin is fine and smooth moist, and the eye microgroove obviously reduces, and the colour of skin obviously bleaches near the eyes; Microscopically skin texture density near the eyes obviously reduces.
Produce effects: the experimenter feels general satisfaction, and skin elasticity gloss lubricity increases slightly near the eyes, and the colour of skin bleaches to some extent near the eyes, and the eye microgroove reduces to some extent, and microscopically skin texture density near the eyes reduces slightly.
Invalid: the experimenter feels dissatisfied, and skin elasticity gloss lubricity does not have increase near the eyes; The eye microgroove does not have obvious improvement, and microscopically skin texture density does not near the eyes have improvement, and the epidermis pigmentation does not have improvement.
Natural activity extracts such as Radix Rhodiolae, black tea, Semen Coicis, Flos Lonicerae are rich in the present invention, can promote skin metabolism, enhanced activity, alleviate the epidermis pigmentation, antioxidation and removing oxygen-derived free radicals, fine and smooth moist, have certain tender white, antioxidation, preserve moisture and anti-wrinkle effect, prevent the generation of eye microgroove.
The experimenter does not all have allergy or other toxicities.
Same, embodiment 2 and 3 has also been done corresponding effect evaluation test, the effect evaluation test result of result of the test and embodiment 1 does not have significant difference, so do not do deposited stating at this.

Claims (1)

1. Radix Rhodiolae eye cream with tender white crease-resistant effect, it is characterized in that: this eye cream is to be made by following raw materials in part by weight:
1 part of Radix Rhodiolae root extracting solution
0.5 part of black tea extracting solution
0.5 part of Semen Coicis extracting solution
0.5 part of Flos Lonicerae extracting solution
0.5 part of caprylyl glycol
2 parts of beta glucans
Encircle 1 part of five polydimethylsiloxane
2 parts of polydimethylsiloxane
7 parts of polydimethylsiloxane/methyl polysilicone alkyl copolymer
5 parts of vinyldimethicone/polymethyl siloxane silsesquioxane cross linked polymer
0.05 part of hyaluronate sodium
10 parts of glycerol
1.3 parts of EHAs/VP/ polydimethylsiloxane methacrylate copolymer
5 parts of butanediols
100 parts in water;
The preparation technology of described Radix Rhodiolae root extracting solution is: get the Radix Rhodiolae root, remove rough bark, add 6-8 and doubly measure the 60%-70% alcohol reflux three times, first and second time 3 hours extracted 2 hours for the third time, filtered, merge extractive liquid,, reclaim ethanol to there not being the alcohol flavor, be concentrated into the thick paste that relative density is 1.25-1.45,60 ℃ of surveys; And then add 3-5 times of water gaging, the water precipitating secondary, each 48 hours, get supernatant, filter, filtrate be concentrated into relative density be 1.03-1.10 concentrated solution namely, 60 ℃ of surveys;
The preparation technology of described black tea extracting solution is: the dry bud-leaf of getting plant of theaceae black tea, add 90 ℃ of water of 10 times of amounts, soaked 15-20 minute, ultrasonic extraction 2 times, each 10-15 minute, filter merging filtrate, filtrate be concentrated into relative density be 1.03-1.10 concentrated solution namely, 60 ℃ of surveys;
The preparation technology of described Semen Coicis extracting solution is: gets Semen Coicis, pulverizes, adds 6-8 times of decocting and boil secondary, and 2 hours for the first time, 1 hour for the second time, filtration, merging filtrate is concentrated into relative density and is the concentrated solution of 1.03-1.10 namely, 60 ℃ of surveys;
The preparation technology of described Flos Lonicerae extracting solution is: gets 6-8 times of decocting of caprifoliaceae plant dry flower of light red Radix Ophiopogonis adding and boils secondary, and 2 hours for the first time, 1 hour for the second time, filter, merging filtrate is concentrated into relative density and is the concentrated solution of 1.03-1.10 namely, 60 ℃ of surveys.
CN 201210155162 2012-05-18 2012-05-18 Rhodiola crenulata eye cream with whitening and anti-wrinkle effects Expired - Fee Related CN102641228B (en)

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