CN102657589B - Rhodiola crenulata sun cream - Google Patents
Rhodiola crenulata sun cream Download PDFInfo
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- CN102657589B CN102657589B CN 201210155192 CN201210155192A CN102657589B CN 102657589 B CN102657589 B CN 102657589B CN 201210155192 CN201210155192 CN 201210155192 CN 201210155192 A CN201210155192 A CN 201210155192A CN 102657589 B CN102657589 B CN 102657589B
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Abstract
The invention discloses Rhodiola crenulata sun cream which is prepared from a Rhodiola crenulata root extracting solution, palmarosa oil and corresponding auxiliary materials. The Rhodiola crenulata disclosed by the invention can moisturize and keep the constant-wet elasticity of skins; the Rhodiola crenulata has anti-oxidizing and whitening functions and is recorded as a 'gold plant' by Compendium of Materia Medica; palmarosa enables the skin to be recovered to a state of moisturizing, conditions sebum secretion and accelerates cells to be regenerated; and pleasant fragrance has the function of pacifying a mood and also has the invigorating effect. Rhodiola rosea is used as 'monarch' and the palmarosa is used as 'minister'; the corresponding auxiliary materials are mixed to prepare the sun cream; and the sun protect factors are SPF30+ and PA+++. The Rhodiola crenulata sun cream can effectively block and absorb ultraviolet rays, and prevents the skins from being burnt, tanned and aged. The Rhodiola crenulata sun cream can supplement water and nutrients lost by the skins in time so as to recover natural white of the skins.
Description
Technical field
The present invention relates to technical field of skin care, be specifically related to a kind of Radix Rhodiolae sunscreen cream and preparation method thereof.
Background technology
The Exposure to Sunlight of appropriateness can make vasodilation under skin, blood circulation promoting, and helping to build up resistance to produce vitamin D, strengthens skeleton.But be exposed to the sun unbridledly, can cause wrinkle, freckle, drying, the unequal problem of the colour of skin, and the possibility that increases skin carcinoma is arranged, have endless trouble.Only carried out sun-proofly, effectively prevented melanic generation, shine black, shine and do not hinder, could constantly keep skin health moist.Sunscreen product is varied in the market, easy chafe, cause that uncomfortable sensation appears in user, even make skin the diseases such as irritated occur, from eighties of last century eighties, the skin expert just finds, add various natural plant raw materials in skin care item, skin is had good nourishing effect, and have no side effect, particularly effective component extracting adds to and has more remarkable effect in skin care item from plant; Because effective ingredients in plant has performance gentleness, the advantage such as cheap, efficient, and the Chinese medicine decapacitation with anti-sunlight function absorbs outside ultraviolet, the natural sun-prevention agent of extracting from the natural plants clock can effectively absorb ultraviolet, remove oxygen-derived free radicals and freckle removing and whitening effect, therefore develops effective ingredient that a kind of utilization extracts and make sunlight screening skin-protecting product very important meaning is just arranged from plant.
Summary of the invention
In view of above-mentioned weak point, the object of the present invention is to provide a kind of Radix Rhodiolae sunscreen cream that natural plant extracts makes for primary raw material and preparation method thereof that utilizes.
The consumption of each raw material of the present invention is also groped to sum up to draw through the inventor in a large number, and each raw material consumption all has effect preferably in the following weight scope: a kind of Radix Rhodiolae sunscreen cream, this sunscreen cream are to be made by the raw material of following weight portion proportioning:
Radix Rhodiolae root extracting solution 1.0-2.0 part
Palmarosa oil 0.4-0.6 part
1,2-hexanediol 0.4-0.6 part
C14-22 alcohol/C12-20 alkyl androstanediol 3.0-4.0 part
Glyceryl stearate/PEG-100 stearate 2-3 part
Butylated hydroxytoluene 0.1-0.2 part
Polydimethylsiloxane 2-3 part
2-Methylpentadecane 2-3 part
Dicaprylyl carbonate 3-5 part
Zinc oxide 4.5-5.5 part
Titanium dioxide 1-2 part
Glycerol 8-12 part
Propylene glycol 4-6 part
Xanthan gum 0.1-0.2 part
Allantoin 0.1-0.3 part
Octocrilene 3-5 part
Ethylhexyl methoxy cinnamate 6-9 part
Polyacrylamide/C13-14 isoparaffin/laureth-7 0.4-0.6 part
Vinyldimethicone/polymethyl siloxane silsesquioxane cross linked polymer 1-3 part
Water 80-120 part.
Further, the Radix Rhodiolae sunscreen cream is to be made by the raw material of following weight distribution ratio:
1 part of Radix Rhodiolae root extracting solution
0.5 part of palmarosa oil
0.5 part of 1,2-hexanediol
C14-22 alcohol/3.5 parts of C12-20 alkyl androstanediol
Glyceryl stearate/2 parts of PEG-100 stearates
0.1 part of butylated hydroxytoluene
2 parts of polydimethylsiloxane
2 parts of 2-Methylpentadecanes
4 parts of dicaprylyl carbonate
4.75 parts of zinc oxide
1.5 parts of titanium dioxide
10 parts of glycerol
5 parts of propylene glycol
0.1 part of xanthan gum
0.2 part of allantoin
4 parts of octocrilenes
7.5 parts of ethylhexyl methoxy cinnamates
Polyacrylamide/C13-14 isoparaffin/laureth-7 0.5 part
Vinyldimethicone/2 parts of polymethyl siloxane silsesquioxane cross linked polymers
100 parts, water.
Raw materials used in the present invention all can be by commercially available acquisition, wherein palmarosa oil and Radix Rhodiolae root extracting solution can also obtain or by following preparation technology's acquisition by the prior art means:
The preparation technology of described Radix Rhodiolae root extract is: get the Radix Rhodiolae root, remove rough bark, add 6-8 doubly to measure the 60%-70% alcohol reflux three times, first and second time 3 hours extracted 2 hours for the third time, filtered, merge extractive liquid,, reclaim ethanol to without the alcohol flavor, be concentrated into the thick paste that relative density is 1.25-1.45,60 ℃ of surveys; And then add 3-5 times of water gaging, and the water precipitating secondary, each 48 hours, get supernatant, filter, filtrate is concentrated into the concentrated solution that relative density is 1.03-1.10,60 ℃ of surveys.
The preparation technology of described palmarosa oil is: get and dry Cymbopogon martini, put in the volatile oil extraction pot, soaked 30-45 minute, decoct with water three Yi ﹑ secondaries and add water 6-8 and doubly measure, each 2 hours, 4-5 doubly measured for the third time, extracted 1 hour, and collected volatile oil, and get final product.
The method for preparing the Radix Rhodiolae sunscreen cream, its concrete preparation process is as follows:
with C14-22 alcohol/C12-20 alkyl androstanediol, glyceryl stearate/PEG-100 stearate, butylated hydroxytoluene, polydimethylsiloxane, 2-Methylpentadecane, dicaprylyl carbonate, zinc oxide and titanium dioxide are put into and are warmed up to 80 in the oil phase pot and spend to get A thing mutually, with glycerol, propylene glycol, xanthan gum, allantoin and water drop into and are heated to 85 degree dissolve completes in the water pot and get B thing mutually, first with B phase thing suction emulsifying pot, again with A phase thing also suction emulsifying pot, mix and blend, added octocrilene and ethylhexyl methoxy cinnamate homogenizing 6 minutes, then add polyacrylamide/C13-14 isoparaffin/laureth-7 and vinyldimethicone/polymethyl siloxane silsesquioxane cross linked polymer homogenizing 2 minutes again, stir insulation 20 minutes, be cooled to 45 degree and add Radix Rhodiolae root extracting solution, palmarosa oil and 1, the discharging that stirs of 2-hexanediol, get sunscreen cream.
In the present invention: Radix Rhodiolae root extract (liquid) contains the effective active compositions such as rhodioloside, butyl alcohol, ketone and rhodosin, and Radix Rhodiolae is top grade in Rhodida plant, is the standards of pharmacopoeia that version Pharmacopoeia of the People's Republic of China Radix Rhodiolae in 2010 is included.Modern scientific research shows in the Radix Rhodiolae rhizome and contains several physiological active substances to have the strengthening by means of tonics effects such as anoxia enduring, radioprotective, resisting fatigue, slow down aging, prophylaxis of tumours diffusion.In the Caulis et folium clerodendri bungei Herba hylotelephii erythrosticti, the compositions such as rhodioloside, butyl alcohol, ketone are 5 times of other kind Radix Rhodiolaes.Be described as " snowy region Radix Ginseng ", the ability that has good oxidation resistance and remove ultra-oxygen anion free radical is better than hydroxyl radical free radical and greater than vitamin E.The Radix Rhodiolae extracting solution extracts refining forming through advanced technologies, contain the antioxidant such as a large amount of rhodiolosides and Rosavin and abundant nutritional labeling, have good radioprotective and anti-oxidation efficacy, can effectively reduce x radiation x or radioprotective to the damage of Skin Cell.Studies show that, the Radix Rhodiolae root extract has the ability of vitro inhibition tyrosinase activity, and in blocking-up skin, tyrosine changes melanin under the catalysis of tryrosinase, thereby reduces melanic generation, reaches the effect of whitening.And the concentration of suppression ratio and extracting solution becomes positive correlation.Radix Rhodiolae root extract (rhodioloside and total flavones) has the ability of antioxidation in vitro, the Radix Rhodiolae root extract is applied to cosmetic skin care product aspects, mainly possessed defying age, antioxidation, free radical resisting, radioprotective, whitening, the anti-effect such as chap.But the delaying human body skin aging keeps the skin vigor, prevents computer and daily Exposure to Sunlight radiation, improves the skin color and luster obscure, increases skin elasticity, make that skin and muscles are fair, tender, vigor is arranged, can be used as the whitening anti-aging cosmetics additive.
Described palmarosa oil contains abundant natural complex C, GLA, protein, mineral etc.Skin moisture-keeping, antibacterial action with highly significant, energy whitening effect, soft skin smooth microgroove, and the prevention wrinkle can promote skin regeneration, make skin keep elasticity and gloss.Be fit to various skin quality, xerosis cutis, mottle, cicatrix, wound, burn and scald, sunburn, eczema, aging skin are all had splendid effect.
The present invention is effectively composite to together with Radix Rhodiolae root extract (liquid) and palmarosa oil, and assistant is learnt from other's strong points to offset one's weaknesses, and groped in a large number to sum up under the detailed consumption of each component that draws the inventor with adjuvant, finally obtains the Radix Rhodiolae sunscreen cream.
In the present invention, Radix Rhodiolae can moisten foster moisturizing, keep the constant humidity elasticity of skin, and have antioxidation and a whitening function, be recited as " gold plant " by Compendium of Material Medica, Cymbopogon martini can make skin recover the state of moisturizing, and the conditioning sebum secretion promotes cell regeneration, its pleasant fragrance has been pacified effect to emotion, and the effect that improves is also arranged.Take Radix Rhodiolae as " monarch ", Cymbopogon martini is " minister ", then coordinates corresponding adjuvant to make sunscreen cream, SPF (sun protection factor) is SPF30+, and PA+++ can effectively intercept and absorb ultraviolet, prevent skin sunburn, tanned and aging, in time replenish moisture and the nutrient that skin runs off, recover the skin natural whiting.
The specific embodiment
Below we do a detailed explanation in connection with specific embodiment to the present invention.
Embodiment 1
In the present embodiment, raw material components and the consumption of preparation Radix Rhodiolae sunscreen cream are:
Radix Rhodiolae root extracting solution 10g
Palmarosa oil 5g
1,2-hexanediol 5g
C14-22 alcohol/C12-20 alkyl androstanediol 35g
Glyceryl stearate/PEG-100 stearate 20g
Butylated hydroxytoluene 1g
Polydimethylsiloxane 20g
2-Methylpentadecane 20g
Dicaprylyl carbonate 40g
Zinc oxide 47.5g
Titanium dioxide 15g
Glycerol 100g
Propylene glycol 50g
Xanthan gum 1g
Allantoin 2g
Octocrilene 40g
Ethylhexyl methoxy cinnamate 75g
Polyacrylamide/C13-14 isoparaffin/laureth-7 5g
Vinyldimethicone/polymethyl siloxane silsesquioxane cross linked polymer 20g
Water 1000g.
its preparation process is: with the disodiumedetate of above-mentioned formula ratio, cocoyl-glucoside sulfosuccinate disodium, it is transparent to each material dissolution that sodium laureth sulfate and water are inserted the insulation of vessel in heating to 85 degree, and then add the pure and mild stearic acid of cetearyl alcohol until after dissolving fully, progressively cool to again 50 degree, next add again methyl glucose dioleate and cocamido propyl betaine, until stirring and dissolving is complete, add palmarosa oil after being cooled to 40 degree, Radix Rhodiolae root extracting solution and sodium chloride, stir and get final product discharging, get cleansing milk.
Embodiment 2
Preparation process is with embodiment 1, and different is that the raw material components and the consumption that prepare the Radix Rhodiolae sunscreen cream are:
Radix Rhodiolae root extracting solution 10g
Palmarosa oil 4g
1,2-hexanediol 4g
C14-22 alcohol/C12-20 alkyl androstanediol 30g
Glyceryl stearate/PEG-100 stearate 20g
Butylated hydroxytoluene 1g
Polydimethylsiloxane 20g
2-Methylpentadecane 20g
Dicaprylyl carbonate 30g
Zinc oxide 45g
Titanium dioxide 10g
Glycerol 80g
Propylene glycol 40g
Xanthan gum 1g
Allantoin 1g
Octocrilene 30g
Ethylhexyl methoxy cinnamate 60g
Polyacrylamide/C13-14 isoparaffin/laureth-7 4g
Vinyldimethicone/polymethyl siloxane silsesquioxane cross linked polymer 10g
Water 80g.
Embodiment 3
Preparation process is with embodiment 1, and different is that the raw material components and the consumption that prepare the Radix Rhodiolae sunscreen cream are:
Radix Rhodiolae root extracting solution 20g
Palmarosa oil 6g
1,2-hexanediol 6g
C14-22 alcohol/C12-20 alkyl androstanediol 40g
Glyceryl stearate/PEG-100 stearate 30g
Butylated hydroxytoluene 2g
Polydimethylsiloxane 30g
2-Methylpentadecane 30g
Dicaprylyl carbonate 50g
Zinc oxide 55g
Titanium dioxide 20g
Glycerol 120g
Propylene glycol 60g
Xanthan gum 2g
Allantoin 3g
Octocrilene 50g
Ethylhexyl methoxy cinnamate 90g
Polyacrylamide/C13-14 isoparaffin/laureth-7 (match Bick) 6g
Vinyldimethicone/polymethyl siloxane silsesquioxane cross linked polymer 30g
Water 1200g.
In the various embodiments described above, raw materials used all can be by commercially available acquisition, as C14-22 alkylol/C12-20 alkyl androstanediol (trade name: Montanov L) available from match BIC Corp; Glyceryl stearate/PEG-100 stearate (trade name:
Arlacel 165Also can be expressed as: glyceryl stearate (with) the PEG-100 stearate) available from Britain standing grain major company; Polyacrylamide/C13-14 isoparaffin/laureth-7 are also available from match BIC Corp; Radix Rhodiolae root extracting solution and palmarosa oil can also obtain or obtain by following preparation technology by the prior art means:
The preparation technology of Radix Rhodiolae root extract is: the preparation technology of described Radix Rhodiolae root extract is: get the Radix Rhodiolae root, remove rough bark, add 6-8 doubly to measure the 60%-70% alcohol reflux three times, first and second time 3 hours extracted 2 hours for the third time, filtered, merge extractive liquid,, reclaim ethanol to without the alcohol flavor, be concentrated into the thick paste that relative density is 1.25-1.45,60 ℃ of surveys; And then add 3-5 times of water gaging, and the water precipitating secondary, each 48 hours, get supernatant, filter, filtrate is concentrated into the concentrated solution that relative density is 1.03-1.10,60 ℃ of surveys.
The preparation technology of palmarosa oil is: get and dry Cymbopogon martini, put in the volatile oil extraction pot, soaked 30-45 minute, decoct with water three times, Yi ﹑ secondary adds water 6-8 doubly to be measured, and each 2 hours, 4-5 doubly measured for the third time, extracts 1 hour, collects volatile oil, and get final product.
Meet the pertinent regulations requirement of defending No. the 0680th, the special word (2005) of adornment through check product of the present invention, sense index (color and luster, fragrance, outward appearance) meets the industry regulation, and physical and chemical index (PH, heat-resisting, cold-resistant) meets industry and stipulates.
Radix Rhodiolae effective ingredient in the present invention has ultra-violet radiation resisting in skin nursing, resist the pigementation that harm ray causes, accelerates protein excretion, prevents skin aging, immunomodulating, the effect that improves the skin self-protection ability.After testing, product of the present invention has SPF30+, the PA+++ SPF (sun protection factor).
Choose 50 examples and have 2 hours at least and be in the experimenter that the sun directly shines operation under environment every days, the sunscreen cream that adopts embodiment 1 to make is protected skin, uses continuously 60 days, and concrete outcome is as follows:
Table one statistics compares:
Judgment criteria as a result:
Effectively: the experimenter feels very satisfied, can well intercept and absorb ultraviolet, and skin is without sunburn, tanned phenomenon, and skin is fine and smooth moist, the soft and smooth gloss of the lasting water profit of skin, and fragile muscle and skin is bright in vain.
Produce effects: the experimenter feels general satisfaction, substantially can intercept and absorb ultraviolet, and skin is substantially without sunburn, tanned phenomenon, and skin is essentially smooth moist, and the basic non-pigment of epidermis is calm.
Invalid: the experimenter feels dissatisfied, can not effectively intercept and absorb ultraviolet, and skin has slight sunburn and tanned phenomenon, and the coarse dry sensation of skin is without obvious improvement, and the epidermis pigmentation is without any improvement.
The experimenter is all without irritated or other toxicities.
Same, embodiment 2 and 3 has also been done corresponding effect evaluation test, the effect evaluation test result of result of the test and embodiment 1 is not stated therefore do not do to apply at this without significant difference.
Claims (3)
1. Radix Rhodiolae sunscreen cream, it is characterized in that: this sunscreen cream is to be made by the raw material of following weight portion proportioning:
Radix Rhodiolae root extracting solution 1.0-2.0 part
Palmarosa oil 0.4-0.6 part
1,2-hexanediol 0.4-0.6 part
C14-22 alcohol/C12-20 alkyl androstanediol 3.0-4.0 part
Glyceryl stearate/PEG-100 stearate 2-3 part
Butylated hydroxytoluene 0.1-0.2 part
Polydimethylsiloxane 2-3 part
2-Methylpentadecane 2-3 part
Dicaprylyl carbonate 3-5 part
Zinc oxide 4.5-5.5 part
Titanium dioxide 1-2 part
Glycerol 8-12 part
Propylene glycol 4-6 part
Xanthan gum 0.1-0.2 part
Allantoin 0.1-0.3 part
Octocrilene 3-5 part
Ethylhexyl methoxy cinnamate 6-9 part
Polyacrylamide/C13-14 isoparaffin/laureth-7 0.4-0.6 part
Vinyldimethicone/polymethyl siloxane silsesquioxane cross linked polymer 1-3 part
Water 80-120 part;
The preparation technology of described Radix Rhodiolae root extracting solution is: get the Radix Rhodiolae root, remove rough bark, add 6-8 doubly to measure the 60%-70% alcohol reflux three times, first and second time 3 hours extracted 2 hours for the third time, filtered, merge extractive liquid,, reclaim ethanol to without the alcohol flavor, be concentrated into the thick paste that relative density is 1.25-1.45,60 ℃ of surveys; And then add 3-5 times of water gaging, and the water precipitating secondary, each 48 hours, get supernatant, filter, filtrate is concentrated into the concentrated solution that relative density is 1.03-1.10,60 ℃ of surveys;
The preparation technology of described palmarosa oil is: get and dry Cymbopogon martini, put in the volatile oil extraction pot, soaked 30-45 minute, decoct with water three Yi ﹑ secondaries and add water 6-8 and doubly measure, each 2 hours, 4-5 doubly measured for the third time, extracted 1 hour, and collected volatile oil, and get final product.
2. Radix Rhodiolae sunscreen cream according to claim 1, it is characterized in that: this sunscreen cream is to be made by the raw material of following weight portion proportioning:
1.0 parts of Radix Rhodiolae root extracting solution
0.5 part of palmarosa oil
0.5 part of 1,2-hexanediol
C14-22 alcohol/3.5 parts of C12-20 alkyl androstanediol
Glyceryl stearate/2 parts of PEG-100 stearates
0.1 part of butylated hydroxytoluene
2 parts of polydimethylsiloxane
2 parts of 2-Methylpentadecanes
4 parts of dicaprylyl carbonate
4.75 parts of zinc oxide
1.5 parts of titanium dioxide
10 parts of glycerol
5 parts of propylene glycol
0.1 part of xanthan gum
0.2 part of allantoin
4 parts of octocrilenes
7.5 parts of ethylhexyl methoxy cinnamates
Polyacrylamide/C13-14 isoparaffin/laureth-7 0.5 part
Vinyldimethicone/2 parts of polymethyl siloxane silsesquioxane cross linked polymers
100 parts, water.
3. method for preparing claim 1 or 2 described sunscreen cream, it is characterized in that, its concrete preparation process is as follows: with C14-22 alcohol/C12-20 alkyl androstanediol, glyceryl stearate/PEG-100 stearate, butylated hydroxytoluene, polydimethylsiloxane, 2-Methylpentadecane, dicaprylyl carbonate, zinc oxide and titanium dioxide are put into and are warmed up to 80 in the oil phase pot and spend to get A thing mutually, with glycerol, propylene glycol, xanthan gum, allantoin and water drop into and are heated to 85 degree dissolve completes in the water pot and get B thing mutually, first with B phase thing suction emulsifying pot, again with A phase thing also suction emulsifying pot, mix and blend, added octocrilene and ethylhexyl methoxy cinnamate homogenizing 6 minutes, then add polyacrylamide/C13-14 isoparaffin/laureth-7 and vinyldimethicone/polymethyl siloxane silsesquioxane cross linked polymer homogenizing 2 minutes again, stir insulation 20 minutes, be cooled to 45 degree and add Radix Rhodiolae root extracting solution, palmarosa oil and 1, the discharging that stirs of 2-hexanediol, get sunscreen cream.
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| CN 201210155192 CN102657589B (en) | 2012-05-18 | 2012-05-18 | Rhodiola crenulata sun cream |
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| CN 201210155192 CN102657589B (en) | 2012-05-18 | 2012-05-18 | Rhodiola crenulata sun cream |
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| CN104382833B (en) * | 2014-10-28 | 2015-11-18 | 广东碧嫄化妆品有限公司 | Plant protein peptide stock solution and its preparation method and application |
| EP3233027B1 (en) * | 2014-12-15 | 2021-10-13 | Unilever IP Holdings B.V. | Compositions for providing improved sunscreen protection |
| CN108969407A (en) * | 2018-09-03 | 2018-12-11 | 芜湖凌梦电子商务有限公司 | Sun-proof essence cream and preparation method thereof |
| KR102186533B1 (en) * | 2019-03-11 | 2020-12-03 | 주식회사 자연인 | A cosmetic composition for skin whitening comprising Rosa Damascena Flower Oil and Rhodiola Rosea root extract |
| CN112120988A (en) * | 2020-11-06 | 2020-12-25 | 广州市科能化妆品科研有限公司 | Whitening sunscreen lotion and preparation method thereof |
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| CN1561957A (en) * | 2004-03-19 | 2005-01-12 | 刘巍然 | Method for preparing rhodilarosea skin-care liquid |
| CN100381113C (en) * | 2005-03-29 | 2008-04-16 | 上海应用技术学院 | Sunscreen milk containing natural plant sunscreen component and its preparation method |
| CN102302436A (en) * | 2011-09-14 | 2012-01-04 | 高小娜 | Sun block stick added with natural nutrient substances |
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Effective date of registration: 20191119 Address after: Lhasa City Jinzhu West Road No. 189 850000 Tibet Autonomous Region Patentee after: TIBET TIBETAN MEDICINE GROUP Co.,Ltd. Address before: Jinjiang District Fuxing street in Chengdu City, Sichuan province 610020 No. 1 Patentee before: Tongde Group Co.,Ltd. |
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