CN102657590B - Rhodiola crenulata essence with effects of whitening, moisturizing and wrinkle resisting - Google Patents

Rhodiola crenulata essence with effects of whitening, moisturizing and wrinkle resisting Download PDF

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CN102657590B
CN102657590B CN201210155201XA CN201210155201A CN102657590B CN 102657590 B CN102657590 B CN 102657590B CN 201210155201X A CN201210155201X A CN 201210155201XA CN 201210155201 A CN201210155201 A CN 201210155201A CN 102657590 B CN102657590 B CN 102657590B
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extracting solution
skin
essence
concentrated
black tea
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CN102657590A (en
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卢小红
孔维颖
周军
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Tibet Tibetan Medicine Group Co ltd
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TONGDE GROUP CO Ltd
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Abstract

The invention discloses rhodiola crenulata essence with the effects of whitening, moisturizing and wrinkle resisting. The rhodiola crenulata essence is mainly prepared from a rhodiola crenulata root extracting solution, a black tea extracting solution, a blueberry fruit extracting solution, a loniceraflower extracting solution and corresponding auxiliary materials. According to the rhodiola crenulata essence, rhodiola crenulata can moisten, moisturize and maintain the constant humidity and resilience of skin and has the antioxidation and whitening functions; anthocyanin enriched in blueberry is a pure natural and anti-aging nutritional replenishing agent; black tea can moisten the skin, promote blood circulation and activate cells and has the effects of resisting bacteria, refreshing and the like; and the lonicera flower is also named as honeysuckle flower, and can improve the water retention capacity of the skin to ensure that a natural water retention barrier is formed. According to the rhodiola crenulata essence, the rhodiola crenulata is used as a 'monarch' medicine, the blueberry is used as a 'ministerial' medicine, the black tea is used as an 'adjuvant' medicine, and the lonicera flower is used as a 'conductant' medicine, and the rhodiola crenulata essence can enhance the activity of the skin, promote metabolism, remove the damage of oxygen radicals, and improve the resilience of the skin, so that the skin is tight and tender and smooth, a good deep moisturizing effect is achieved, and the wrinkles are reduced.

Description

A kind of Radix Rhodiolae essence with the crease-resistant effect of skin nursing
Technical field
The present invention relates to technical field of skin care, be specifically related to a kind of Radix Rhodiolae essence with the crease-resistant effect of skin nursing and preparation method thereof.
Background technology
Along with the progress of society and improving constantly of expanding economy and living standards of the people, people are also more and more higher to the requirement of beauty and skin care cosmetics, more and more to the future development of " naturalization, nutrient laden, curative effect ".But in various beauty and skin care cosmetics in the market, great majority all contain harmful chemical substance, and as poisonous and harmful substances such as leaded, hydrargyrum, these skin care item easily cause people's skin allergy, to human organ and function injury.From eighties of last century eighties, the skin expert just finds, adds various natural materials in skin care item, skin is had good nourishing effect, and have no side effect, and particularly effective component extracting adds to and has more remarkable effect in skin care item from plant.Therefore, development is a kind of utilizes the effective ingredient extract from plant to make the beauty and skin care cosmetics that human body skin is had nutrition and a protective effect very important meaning is just arranged.
Summary of the invention
In view of above-mentioned weak point, the object of the present invention is to provide a kind of natural plant extracts that utilizes to have Radix Rhodiolae essence of the crease-resistant effect of skin nursing and preparation method thereof for what primary raw material made.
The consumption of each raw material of the present invention is also groped to sum up to draw through the inventor in a large number, each raw material consumption all has effect preferably in the following weight scope: a kind of Radix Rhodiolae essence with the crease-resistant effect of skin nursing, and this essence is to be made by the raw material of following weight distribution ratio:
Radix Rhodiolae root extracting solution 4-6 part
Black tea extracting solution 0.4-0.6 part
Blue berry extracting solution 0.4-0.6 part
Flos Lonicerae extract 0.4-0.6 part
1,2-hexanediol 0.4-0.6 part
Carbomer 0.1-0.2 part
Propylene glycol 4-8 part
Hyaluronate sodium 0.04-0.06 part
Butanediol 10-15 part
Beta glucan 1-3 part
Triethanolamine 0.1-0.2 part
Water 80-120 part.
Further, having the Radix Rhodiolae essence of the crease-resistant effect of skin nursing, is to be made by following raw materials in part by weight:
5 parts of Radix Rhodiolae root extracting solution
0.5 part of black tea extracting solution
0.5 part of blue berry extracting solution
0.5 part of Flos Lonicerae extracting solution
0.5 part of 1,2-hexanediol
0.1 part of carbomer
6 parts of propylene glycol
0.05 part of hyaluronate sodium
12 parts of butanediols
2 parts of beta glucans
0.1 part of triethanolamine
100 parts, water.
Raw materials used in the present invention all can be by commercially available acquisition, wherein Radix Rhodiolae root extracting solution, black tea extracting solution, blue berry extracting solution and Flos Lonicerae extracting solution can also obtain or by following preparation technology's acquisition by the prior art means:
The preparation technology of described Radix Rhodiolae root extracting solution is: get the Radix Rhodiolae root, remove rough bark, add 6-8 doubly to measure the 60%-70% alcohol reflux three times, first and second time 3 hours extracted 2 hours for the third time, filtered, merge extractive liquid,, reclaim ethanol to without the alcohol flavor, be concentrated into the thick paste that relative density is 1.25-1.45,60 ℃ of surveys; And then add 3-5 times of water gaging, and the water precipitating secondary, each 48 hours, get supernatant, filter, filtrate is concentrated into relative density to be the concentrated solution of 1.03-1.10 and to get final product 60 ℃ of surveys.
The preparation technology of described black tea extracting solution is: the dry bud-leaf of getting plant of theaceae black tea, add 90 ℃ of water of 10 times of amounts, soaked 15-20 minute, ultrasonic extraction 2 times, each 10-15 minute, filter merging filtrate, filtrate is concentrated into relative density to be the concentrated solution of 1.03-1.10 and to get final product 60 ℃ of surveys.
The preparation technology of described blue berry extracting solution is: get the blue berry making beating, get the blue berry serosity, add 10 times of amount 60-75% ethanol, ultrasonic extraction three times, each 30 minutes, sucking filtration, centrifugal, decompression recycling ethanol, filtrate are concentrated into relative density to be the concentrated solution of 1.03-1.10 and to get final product 60 ℃ of surveys.
The preparation technology of described Flos Lonicerae extracting solution is: gets caprifoliaceae plant dry flower of light red Radix Ophiopogonis and adds 6-8 times of decocting to boil secondary, and 2 hours for the first time, 1 hour for the second time, filter, merging filtrate, to be concentrated into relative density be the concentrated solution of 1.03-1.10 and get final product 60 ℃ of surveys.
The concrete preparation process for preparing the Radix Rhodiolae essence with the crease-resistant effect of skin nursing is as follows:
Carbomer, propylene glycol, hyaluronate sodium, butanediol and the water of above-mentioned formula ratio are inserted vessel in heating to 85 degree, be dissolved to transparent heat-insulation 10 minutes, add the triethanolamine neutralization, progressively be cooled to 45 degree and then add Radix Rhodiolae root extracting solution, black tea extracting solution, blue berry extracting solution, Flos Lonicerae extracting solution and beta glucan and 1, the 2-hexanediol stirs and gets final product discharging, gets essence.
In the present invention, the Radix Rhodiolae root extract contains the effective active compositions such as rhodioloside, butyl alcohol, ketone and rhodosin, and Radix Rhodiolae is top grade in Rhodida plant, is the standards of pharmacopoeia that version Pharmacopoeia of the People's Republic of China Radix Rhodiolae in 2010 is included.Modern scientific research shows in the Radix Rhodiolae rhizome and contains several physiological active substances to have the strengthening by means of tonics effects such as anoxia enduring, radioprotective, resisting fatigue, slow down aging, prophylaxis of tumours diffusion.In the Caulis et folium clerodendri bungei Herba hylotelephii erythrosticti, the compositions such as rhodioloside, butyl alcohol, ketone are 5 times of other kind Radix Rhodiolaes.Be described as " snowy region Radix Ginseng ", the ability that has good oxidation resistance and remove ultra-oxygen anion free radical is better than hydroxyl radical free radical and greater than vitamin E.Studies show that, the Radix Rhodiolae root extract has the ability of vitro inhibition tyrosinase activity, and in blocking-up skin, tyrosine changes melanin under the catalysis of tryrosinase, thereby reduces melanic generation, reaches the effect of whitening.And the concentration of suppression ratio and extracting solution becomes positive correlation.Radix Rhodiolae root extract (rhodioloside and total flavones) has the ability of antioxidation in vitro, the Radix Rhodiolae root extract is applied to cosmetic skin care product aspects, mainly possessed defying age, antioxidation, free radical resisting, radioprotective, whitening, the anti-effect such as chap.But the delaying human body skin aging keeps the skin vigor, prevents computer and daily Exposure to Sunlight radiation, improves the skin color and luster obscure, increases skin elasticity, make that skin and muscles are fair, tender, vigor is arranged, can be used as the whitening anti-aging cosmetics additive.
Black tea belongs to full fermentation teas, be bud-leaf take Camellia sinensis as raw material, through withering, knead (cutting), fermentation, it is dry etc. that the typical process processes are refining forms.Because of its do dark brown pool and the millet paste that brews take redness as homophony, therefore named black tea.contain Polyphenols in black tea, carbohydrate, aminoacid, pectin, theaflavin, thearubigins, the many kinds of substances such as tea polybase and antioxidant, tool refresh oneself disappear tired, replenishing body fluid and clearing away heat pathogen, anti-inflammation and sterilization, detoxifcation, strong skeleton and antioxidation, the effects such as slow down aging, result of study shows, antioxidant in black tea is the propagation path of chemical substance in destruction of cancer cells thoroughly, the effect of black tea and green tea is roughly suitable, but the antioxidant of black tea than the green tea complexity many, especially useful especially to heart, the USA Magazine report, black tea defying age effect is better than Bulbus Allii head, Caulis et Folium Brassicae capitatae and Radix Dauci Sativae etc.
Blue berry, the formal name used at school Pericarpium Citri tangerinae belongs to Ericaceae genus vaccinium plant.It is blue that fruit is, and drape layer white fruit powder, and sarcocarp is fine and smooth, and fruity is sour-sweet, unique flavor, and the content of anthocyanidin is very high; Contain abundant nutritional labeling in Blueberry, it not only has good nutrition health-care functions, also has the functions such as the cranial nerve of preventing is aging, heart tonifying, anticancer vessel softening, enhancing human organism immunity.Except sugar, acid and the Vc of routine, be rich in VE, VA, VB, SOD, arbutin, protein, anthocyanin, edible fiber and abundant K, Fe, the mineral elements such as Zn, Ca in Blueberry.Containing a large amount of purple compositions in blue berry, is exactly anthocyanidin.Anthocyanidin is the anti-aging and nutritive supplement of pure natural, studies have shown that it is that mankind nowadays is found the most effective antioxidant.The antioxygenic property of anthocyanidin is higher 50 times than vitamin E, than ten times of vitamin C Senior Two.It is that absolutely different from other antioxidant is that anthocyanidin can pass through blood brain barrier, directly protects brain and nervous system to the biological effectiveness of human body.The blue berry extract is that in present all Anthocyanins, effect is the best, range of application is the widest, side effect is minimum, is also the most expensive kind of price.The bioavailability of the blue or green plain molecule of flower blue berry extract is high.In the blue berry extract, not only the molecule of anthocyanidin is superior, and containing the special dietary compositions such as abundant organic germanium, organic selenium, Arbutin, aminoacid, fruit acid and vitamin, these special dietary materials just have useful especially effect to Human Physiology in free state; If be embedded in oligomer anthocyanidin molecule, along with the raising of bioavailability, its effect is more obvious.
Flos Lonicerae claims again Flos Lonicerae, is the caprifoliaceae plant alabastrum of Radix Ophiopogonis.Composition contains chlorogenic acid, isochlorogenic acid, neochlorogenic acid, Flavonoid substances, lonicerin, matter, inositol, Saponin etc.Total amino acids content reaches 8% left and right.The content of water-soluble amino acid is in 0.1% left and right, and the content of water solublity carbohydrate is at l more than 8%, and contain at least manganese, chromium, nickel, actinium, zinc, cobalt, silicon, ferrum, etc. eight kinds of trace element of needed by human.Also contain the chemical composition of volatilization wet goods more than 30 kinds and form, many types wherein can be used for making perfume, edible essence etc.It is used for cosmetics is also to plant Chinese herbal medicine additive preferably.With extraction by steam distillation fragrance volatile oil with the active substance of the Flos Lonicerae of solvent extraction, join in showering agent receipts product, to not injury of skin, make that foam is abundant, fragrance is soft, take out stains, cleaning skin, nourishing skin, make skin keep higher water content, strengthen the vigor of skin, reach the effect of delay skin aging.Seborrheic dermatitis, good skin inflammation also there is certain curative effect.
In the present invention, Radix Rhodiolae can moisten foster moisturizing, keeps the constant humidity elasticity of skin, and has antioxidation and whitening function, is recited as " gold plant " by Compendium of Material Medica.Blue berry is described as " oral cosmetics for skin ", the anti-aging and nutritive supplement that its anthocyanidin that is rich in is pure natural.Black tea can skin care, blood circulation promoting, and activating cell has antibiotic, the effect such as refresh oneself simultaneously.Flos Lonicerae claims again Flos Lonicerae.It can promote the skin water holding capacity, forms natural lock water barrier.Shennong's Herbal points out that it can regulate female incretion, removes yellow gas and mottle, makes appearance moist.Take Radix Rhodiolae as " monarch ", blue berry is " minister ", and " assistant " with black tea, " making " is with Flos Lonicerae, be equipped with adjuvant and make essence, can strengthen skin activity, enhance metabolism, remove the oxygen-derived free radicals injury, promote skin elasticity, more the consolidation children is sliding to make skin, and the deep moisturizing effect, reduce wrinkle and generate preferably.
The specific embodiment
Below we do a detailed explanation in connection with specific embodiment to the present invention.
Embodiment 1
In the present embodiment, raw material components and consumption that preparation has the Radix Rhodiolae essence of the crease-resistant effect of skin nursing are:
Radix Rhodiolae root extracting solution 50g
Black tea extracting solution 5g
Blue berry extracting solution 5g
Flos Lonicerae extracting solution 5g
1,2-hexanediol 5g
Carbomer 1g
Propylene glycol 60g
Hyaluronate sodium 0.5g
Butanediol 120g
Beta glucan 20g
Triethanolamine 1g
Water 1000g.
Its preparation process is: carbomer, glycerol polymethacrylates/propylene glycol, hyaluronate sodium, butanediol and the water of above-mentioned formula ratio are inserted vessel in heating to 85 degree, be dissolved to transparent heat-insulation 10 minutes, add the triethanolamine neutralization, progressively be cooled to 45 degree and then add Radix Rhodiolae root extracting solution, black tea extracting solution, blue berry extracting solution, Flos Lonicerae extracting solution and beta glucan and 1, the 2-hexanediol stirs and gets final product discharging, gets essence.
Embodiment 2
Preparation process is with embodiment 1, and different is that the raw material components and the consumption that prepare the Radix Rhodiolae essence with the crease-resistant effect of skin nursing are:
Radix Rhodiolae root extracting solution 40g
Black tea extracting solution 4g
Blue berry extracting solution 4g
Flos Lonicerae extracting solution 4g
1,2-hexanediol 4g
Carbomer 1g
Propylene glycol 60g
Hyaluronate sodium 0.4g
Butanediol 100g
Beta glucan 10g
Triethanolamine 1g
Water 800g.
Embodiment 3
Preparation process is with embodiment 1, and different is that the raw material components and the consumption that prepare the Radix Rhodiolae essence with the crease-resistant effect of skin nursing are:
Radix Rhodiolae root extracting solution 60g
Black tea extracting solution 6g
Blue berry extracting solution 6g
Flos Lonicerae extracting solution 6g
1,2-hexanediol 6g
Carbomer 2g
Propylene glycol 80g
Hyaluronate sodium 0.6g
Butanediol 150g
Beta glucan 30g
Triethanolamine 2g
Water 1200g.
In the present invention, each embodiment is raw materials used all can be by commercially available acquisition, and wherein Radix Rhodiolae root extracting solution, black tea extracting solution, blue berry extracting solution, Flos Lonicerae extracting solution can also obtain or obtain by following preparation technology by the prior art means:
The preparation technology of Radix Rhodiolae root extracting solution is: get the Radix Rhodiolae root, remove rough bark, add 6-8 doubly to measure the 60%-70% alcohol reflux three times, first and second time 3 hours extracted 2 hours for the third time, filtered, merge extractive liquid,, reclaim ethanol to without the alcohol flavor, be concentrated into the thick paste that relative density is 1.25-1.45,60 ℃ of surveys; And then add 3-5 times of water gaging, and the water precipitating secondary, each 48 hours, get supernatant, filter, filtrate is concentrated into relative density to be the concentrated solution of 1.03-1.10 and to get final product 60 ℃ of surveys.
The preparation technology of black tea extracting solution is: get the dry bud-leaf of plant of theaceae black tea, add 90 ℃ of water of 10 times of amounts, soaked 15-20 minute, ultrasonic extraction 2 times each 10-15 minute, is filtered, merging filtrate, filtrate are concentrated into relative density to be the concentrated solution of 1.03-1.10 and to get final product 60 ℃ of surveys.
The preparation technology of blue berry extracting solution is: get the blue berry making beating, get the blue berry serosity, add 10 times of amount 60-75% ethanol, ultrasonic extraction three times, each 30 minutes, sucking filtration, centrifugal, decompression recycling ethanol, filtrate are concentrated into relative density to be the concentrated solution of 1.03-1.10 and to get final product 60 ℃ of surveys.
The preparation technology of Flos Lonicerae extracting solution is: gets caprifoliaceae plant dry flower of light red Radix Ophiopogonis and adds 6-8 times of decocting to boil secondary, and 2 hours for the first time, 1 hour for the second time, filter, merging filtrate, to be concentrated into relative density be the concentrated solution of 1.03-1.10 and get final product 60 ℃ of surveys.
Meet the pertinent regulations requirement of QB/T 2660-2004 through check this product, sense index (color and luster, fragrance, structure) meets the industry regulation, and physical and chemical index (PH, heat-resisting, cold-resistant, active matter) meets the industry regulation.
Product of the present invention is carried out following test:
Choose 50 routine experimenters, the age, smears the essence that embodiment 1 makes on skin after thorough clean skin equably between between 30-55 year, uses once every other day, uses continuously 60 days, and concrete outcome is as follows:
Table one statistics compares:
Figure 554684DEST_PATH_IMAGE001
Judgment criteria as a result:
Effectively: the experimenter feels very satisfied, and skin has elasticity, and more the consolidation children is sliding, and skin is fine and smooth moist, the soft and smooth gloss of the lasting water profit of skin, and the colour of skin obviously bleaches, and wrinkle obviously reduces; Microscopically skin texture density obviously reduces, and skin color obviously shoals.
Produce effects: the experimenter feels general satisfaction, and skin elasticity gloss lubricity increases to some extent, and the colour of skin bleaches to some extent; Wrinkle reduces to some extent; Microscopically skin texture density reduces to some extent, and skin color shoals.
Invalid: the experimenter feels dissatisfied, and the scaly dry skin sense is without obvious improvement, and wrinkle is without minimizing, and skin elasticity gloss lubricity is without increase; Microscopically skin texture density is without obvious improvement, and the epidermis pigmentation is without obvious improvement.
The experimenter is all without irritated or other toxicities.
Natural activity extract and the collagen protein such as Radix Rhodiolae, black tea, blue berry, Flos Lonicerae are rich in the present invention, can infiltrate into skin bottom and promote skin metabolism, enhanced activity, the injury of removing oxygen-derived free radicals, promote skin elasticity, more the consolidation children is sliding to make skin, and the deep moisturizing effect, reduce wrinkle and generate preferably.
Same, embodiment 2 and 3 has also been done corresponding effect evaluation test, the effect evaluation test result of result of the test and embodiment 1 is not stated therefore do not do to apply at this without significant difference.

Claims (2)

1. Radix Rhodiolae essence with the crease-resistant effect of skin nursing, it is characterized in that: this essence is to be made by following raw materials in part by weight:
5 parts of Radix Rhodiolae root extracting solution
0.5 part of black tea extracting solution
0.5 part of blue berry extracting solution
0.5 part of Flos Lonicerae extracting solution
0.5 part of 1,2-hexanediol
0.1 part of carbomer
6 parts of propylene glycol
0.05 part of hyaluronate sodium
12 parts of butanediols
2 parts of beta glucans
0.1 part of triethanolamine
100 parts, water;
The preparation technology of described Radix Rhodiolae root extracting solution is: get the Radix Rhodiolae root, remove rough bark, add 6-8 doubly to measure the 60%-70% alcohol reflux three times, first and second time 3 hours extracted 2 hours for the third time, filtered, merge extractive liquid,, reclaim ethanol to without the alcohol flavor, be concentrated into the thick paste that relative density is 1.25-1.45,60 ℃ of surveys; And then add 3-5 times of water gaging, and the water precipitating secondary, each 48 hours, get supernatant, filter, filtrate is concentrated into relative density to be the concentrated solution of 1.03-1.10 and to get final product 60 ℃ of surveys;
The preparation technology of described black tea extracting solution is: the dry bud-leaf of getting plant of theaceae black tea, add 90 ℃ of water of 10 times of amounts, soaked 15-20 minute, ultrasonic extraction 2 times, each 10-15 minute, filter merging filtrate, filtrate is concentrated into relative density to be the concentrated solution of 1.03-1.10 and to get final product 60 ℃ of surveys;
The preparation technology of described blue berry extracting solution is: get the blue berry making beating, get the blue berry serosity, add 10 times of amount 60-75% ethanol, ultrasonic extraction three times, each 30 minutes, sucking filtration, centrifugal, decompression recycling ethanol, filtrate are concentrated into relative density to be the concentrated solution of 1.03-1.10 and to get final product 60 ℃ of surveys;
The preparation technology of described Flos Lonicerae extracting solution is: gets caprifoliaceae plant dry flower of light red Radix Ophiopogonis and adds 6-8 times of decocting to boil secondary, and 2 hours for the first time, 1 hour for the second time, filter, merging filtrate, to be concentrated into relative density be the concentrated solution of 1.03-1.10 and get final product 60 ℃ of surveys.
2. a method for preparing essence claimed in claim 1, is characterized in that, its concrete preparation process is as follows:
Carbomer, propylene glycol, hyaluronate sodium, butanediol and the water of above-mentioned formula ratio are inserted vessel in heating to 85 degree, be dissolved to transparent heat-insulation 10 minutes, add the triethanolamine neutralization, progressively be cooled to 45 degree and then add Radix Rhodiolae root extracting solution, black tea extracting solution, blue berry extracting solution, Flos Lonicerae extracting solution and beta glucan and 1, the 2-hexanediol stirs and gets final product discharging, gets essence.
CN201210155201XA 2012-05-18 2012-05-18 Rhodiola crenulata essence with effects of whitening, moisturizing and wrinkle resisting Expired - Fee Related CN102657590B (en)

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