CN114591043A - Double-component tile back glue and preparation method thereof - Google Patents

Double-component tile back glue and preparation method thereof Download PDF

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Publication number
CN114591043A
CN114591043A CN202111662360.4A CN202111662360A CN114591043A CN 114591043 A CN114591043 A CN 114591043A CN 202111662360 A CN202111662360 A CN 202111662360A CN 114591043 A CN114591043 A CN 114591043A
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Prior art keywords
component
parts
powder
liquid
back glue
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CN202111662360.4A
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Chinese (zh)
Inventor
陈乐舟
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Hubei Jeark New Material Co ltd
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Hubei Jeark New Material Co ltd
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Priority to CN202111662360.4A priority Critical patent/CN114591043A/en
Publication of CN114591043A publication Critical patent/CN114591043A/en
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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B28/00Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
    • C04B28/02Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
    • C04B28/04Portland cements
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/00474Uses not provided for elsewhere in C04B2111/00
    • C04B2111/00637Uses not provided for elsewhere in C04B2111/00 as glue or binder for uniting building or structural materials
    • C04B2111/00646Masonry mortars
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/20Resistance against chemical, physical or biological attack
    • C04B2111/27Water resistance, i.e. waterproof or water-repellent materials
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/50Flexible or elastic materials
    • C04B2111/503Elastic materials
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2201/00Mortars, concrete or artificial stone characterised by specific physical values
    • C04B2201/10Mortars, concrete or artificial stone characterised by specific physical values for the viscosity
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2201/00Mortars, concrete or artificial stone characterised by specific physical values
    • C04B2201/50Mortars, concrete or artificial stone characterised by specific physical values for the mechanical strength
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/50Reuse, recycling or recovery technologies
    • Y02W30/91Use of waste materials as fillers for mortars or concrete

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Adhesives Or Adhesive Processes (AREA)
  • Curing Cements, Concrete, And Artificial Stone (AREA)

Abstract

The invention provides a double-component tile back glue which comprises a liquid material component A and a powder material component B, wherein the weight ratio of the liquid material component A to the powder material component B is 1: 1.5-2, and the liquid material component A comprises the following raw materials in parts by weight: 70-140 parts of emulsion, 1-6 parts of waterproof agent and 2-6 parts of auxiliary agent, wherein the powder component B comprises the following raw materials in parts by weight: 35-55 parts of white cement, 35-55 parts of fine sand, 1-10 parts of konjac fine powder and 1-3 parts of an auxiliary agent II. In addition, the invention also provides a preparation method of the bi-component tile back glue, which comprises the following steps: mixing the liquid material component and the powder material component. The bi-component ceramic tile back glue provided by the invention has good water resistance and aging resistance, and the characteristics of the tile after freeze-thaw cycling are not changed greatly.

Description

Double-component tile back glue and preparation method thereof
Technical Field
The invention relates to the technical field of ceramic tile back glue, in particular to double-component ceramic tile back glue and a preparation method thereof.
Background
Ceramic tiles are widely used as decorative building materials, ranging from ceramic tiles, glazed tiles, full-body tiles, ceramic tiles, vitrified tiles, archaized tiles and stone-like tiles, to current thin plates, microlites and full-polished tiles, and the technology of the ceramic tile family is continuously updated, the quality is continuously improved, and the design and color are continuously innovated. As a mate of ceramic tiles, namely a ceramic tile pasting material, the ceramic tile pasting material is correspondingly and continuously upgraded and updated from lime to cement and cement mortar and then to the existing ceramic tile glue and ceramic tile back glue so as to meet the performance requirements of ceramic tile pasting. The ceramic tile back glue can effectively improve the bonding strength of the back of the ceramic tile and cement mortar, and is the most effective interface bonding reinforcing material at present. The ceramic tile back glue is composed of dry powder component and liquid component, when in use, the dry powder component and the liquid component are mixed according to a certain proportion, and the mixture is used for paving the back surface of decorative materials such as ceramic tiles, vitrified tiles, floor tiles and the like, is widely applied to decorative surface decoration places of buildings such as inner and outer wall surfaces, ground surfaces, bathrooms, kitchens and the like, and has the characteristics of high bonding strength, water resistance, freeze-thaw resistance and aging resistance, and is convenient to construct. However, the ceramic tile back glue on the market at present has various varieties and different quality, and the problems of hollowing, peeling, falling off and the like often occur after the ceramic tile back glue is used, for example: the bonded ceramic tile is easy to fall off after being eroded by rainwater; the cold and hot change of the climate leads the gelled material to be influenced by the deformation, so that the interface of the gelled material and the ceramic tile has a crack layer, and the ceramic tile falls off.
Disclosure of Invention
The present invention is directed to solving at least one of the problems of the prior art. Therefore, the invention provides a double-component tile back glue which comprises a liquid material component A and a powder material component B, wherein the weight ratio of the liquid material component A to the powder material component B is 1: 1.5-2,
the liquid material component A comprises the following raw materials in parts by weight:
70-140 parts of an emulsion,
1-6 parts of a water-proofing agent,
2-6 parts of an auxiliary agent,
the powder component B comprises the following raw materials in parts by weight:
Figure BDA0003447671320000021
further, the emulsion is a compound of acrylic emulsion, styrene-butadiene latex and VAE emulsion.
Further, the waterproof agent is tung oil.
Further, the auxiliary agent comprises a towel gourd extract.
Further, the second auxiliary agent comprises sepiolite powder.
In addition, the invention also provides a method for preparing the double-component tile back glue, which comprises the following steps:
s1, fully mixing and uniformly stirring all the components in the liquid material component A to obtain a liquid component material;
s2, fully and uniformly stirring all the components in the powder component B to obtain a dry powder component material;
s3, weighing and placing the liquid component material and the dry powder component material according to the weight ratio of 1: 1.5-2, and then pouring the liquid component material into the dry powder component material to be uniformly stirred without agglomeration, thus obtaining the tile back glue.
The double-component ceramic tile back glue provided by the invention has strong bonding strength, and can effectively solve the problems of hollowing, shelling, falling and the like during the bonding of ceramic tiles. The invention adopts the compound of acrylic emulsion, styrene-butadiene latex and VAE emulsion as the matrix, and endows the ceramic tile back glue with stronger bonding strength, water resistance and elasticity; the konjac fine powder has super-strong water-retaining property, and can effectively prolong the hydration time when the tile gum is contacted with cement mortar, thereby being beneficial to increasing the bonding strength; carboxyl contained in the towel gourd extract can be directionally adsorbed on the surface of cement particles so as to improve the binding property of the tile back glue and cement mortar, thereby further improving the bonding strength of the tile back glue.
Detailed Description
In order to better understand the present invention, the following examples are further provided to illustrate the present invention, but the present invention is not limited to the following examples.
Example 1:
the double-component tile back glue comprises a liquid material component A and a powder material component B, wherein the weight ratio of the liquid material component A to the powder material component B is 1:1.5, and the liquid material component A comprises the following raw materials in parts by weight: 40 parts of acrylic emulsion, 10 parts of butadiene styrene latex, 20 parts of VAE emulsion, 1 part of waterproof agent, 0.5 part of sodium pyrophosphate, 0.2 part of dispersing agent, 0.1 part of defoaming agent, 0.1 part of bactericide and 1.1 part of towel gourd extract; the powder component B comprises the following raw materials in parts by weight: 35 parts of white cement, 35 parts of fine sand, 1 part of konjac powder, 0.5 part of sepiolite powder and 0.5 part of retarder.
The waterproof agent is tung oil, and the gum is endowed with good waterproof performance by the tung oil; the sodium pyrophosphate can adsorb metal ions in the cement mortar, so that the adhesion of the gum and the cement mortar is improved; the sepiolite powder is used as a thickening agent, so that the back glue of the ceramic tile can keep a stable system.
A method for preparing the double-component tile back glue comprises the following steps:
s1, fully mixing and uniformly stirring all the components in the liquid material component A to obtain a liquid component material;
s2, fully and uniformly stirring all the components in the powder component B to obtain a dry powder component material;
s3, weighing and placing the liquid component material and the dry powder component material according to the weight ratio of 1:1.5, and then pouring the liquid component material into the dry powder component material to be uniformly stirred without agglomeration, thus obtaining the tile back glue.
Example 2:
the double-component tile back glue comprises a liquid component A and a powder component B, wherein the weight ratio of the liquid component A to the powder component B is 1:2, and the liquid component A comprises the following raw materials in parts by weight: 70 parts of acrylic emulsion, 30 parts of butadiene styrene latex, 40 parts of VAE emulsion, 6 parts of a waterproof agent, 1 part of sodium pyrophosphate, 0.4 part of a dispersing agent, 0.3 part of a defoaming agent, 0.3 part of a bactericide and 4 parts of a towel gourd extract; the powder component B comprises the following raw materials in parts by weight: 55 parts of white cement, 55 parts of fine sand, 10 parts of konjac fine powder, 2 parts of sepiolite powder and 1 part of retarder.
Wherein the waterproof agent is tung oil.
A method for preparing the double-component tile back glue comprises the following steps:
s1, fully mixing and uniformly stirring all the components in the liquid material component A to obtain a liquid component material;
s2, fully and uniformly stirring all the components in the powder component B to obtain a dry powder component material;
s3, weighing and placing the liquid component material and the dry powder component material according to the weight ratio of 1:2, and then pouring the liquid component material into the dry powder component material to be uniformly stirred without agglomeration, thus obtaining the tile back glue.
Example 3:
the double-component tile back glue comprises a liquid material component A and a powder material component B, wherein the weight ratio of the liquid material component A to the powder material component B is 1:1.5, and the liquid material component A comprises the following raw materials in parts by weight: 50 parts of acrylic emulsion, 15 parts of butadiene styrene latex, 30 parts of VAE emulsion, 3 parts of a waterproof agent, 0.75 part of sodium pyrophosphate, 0.3 part of a dispersing agent, 0.2 part of a defoaming agent, 0.2 part of a bactericide and 2 parts of a towel gourd extract; the powder component B comprises the following raw materials in parts by weight: 40 parts of white cement, 45 parts of fine sand, 7 parts of konjac fine powder, 1 part of sepiolite powder and 0.5 part of retarder.
Wherein the waterproof agent is tung oil.
A method for preparing the double-component tile back glue comprises the following steps:
s1, fully mixing and uniformly stirring all the components in the liquid material component A to obtain a liquid component material;
s2, fully and uniformly stirring all the components in the powder component B to obtain a dry powder component material;
s3, weighing and placing the liquid component material and the dry powder component material according to the weight ratio of 1:1.5, and then pouring the liquid component material into the dry powder component material to be uniformly stirred without agglomeration, thus obtaining the tile back glue.
Example 4:
the double-component tile back glue comprises a liquid material component A and a powder material component B, wherein the weight ratio of the liquid material component A to the powder material component B is 1:2, and the liquid material component A comprises the following raw materials in parts by weight: 60 parts of acrylic emulsion, 30 parts of butadiene styrene latex, 35 parts of VAE emulsion, 4 parts of a waterproof agent, 0.7 part of sodium pyrophosphate, 0.2 part of a dispersing agent, 0.3 part of a defoaming agent, 0.2 part of a bactericide and 2.6 parts of a towel gourd extract; the powder component B comprises the following raw materials in parts by weight: 50 parts of white cement, 4 parts of fine sand, 6 parts of konjac powder, 1.2 parts of sepiolite powder and 0.7 part of retarder.
Wherein the waterproof agent is tung oil.
A method for preparing the double-component tile back glue comprises the following steps:
s1, fully mixing and uniformly stirring all the components in the liquid material component A to obtain a liquid component material;
s2, fully and uniformly stirring all the components in the powder component B to obtain a dry powder component material;
s3, weighing and placing the liquid component material and the dry powder component material according to the weight ratio of 1:2, and then pouring the liquid component material into the dry powder component material to be uniformly stirred without agglomeration, thus obtaining the tile back glue.
Comparative example:
comparative example 1 differs from example 4 in that: no konjac powder is produced;
comparative example 2 differs from example 4 in that: no loofah extract.
Example 5:
the tile back glue prepared in the above examples 1 to 4 and comparative examples 1 and 2 was subjected to a performance test, and the tile back glue was subjected to a performance test according to the criteria of JC/T547-2017 ceramic tile adhesive, and the results are shown in the following table 1:
TABLE 1
Figure BDA0003447671320000051
As can be seen from the performance test structure in Table 1, the dual-component tile back glue provided by the invention not only has better water resistance and aging resistance, but also has little change of the characteristics after freeze-thaw cycling, and the comprehensive performance of the tile back glue prepared by the invention is far better than that of the tile back glue commonly used in the market.
While embodiments of the invention have been shown and described, it will be understood by those of ordinary skill in the art that: various changes, modifications, substitutions and alterations can be made to the embodiments without departing from the principles and spirit of the invention, the scope of which is defined by the claims and their equivalents.

Claims (6)

1. The double-component tile back glue is characterized by comprising a liquid material component A and a powder material component B, wherein the weight ratio of the liquid material component A to the powder material component B is 1: 1.5-2,
the liquid material component A comprises the following raw materials in parts by weight:
70-140 parts of an emulsion,
1-6 parts of a water-proofing agent,
2-6 parts of an auxiliary agent,
the powder component B comprises the following raw materials in parts by weight:
Figure FDA0003447671310000011
2. the two-component tile backsize according to claim 1, wherein the emulsion is a combination of an acrylic emulsion, a styrene-butadiene latex, and a VAE emulsion.
3. The two-component tile backsize of claim 1, wherein the water-proofing agent is tung oil.
4. The two-component tile backsize of claim 1, wherein the adjuvant comprises Luffa cylindrica extract.
5. The two-component tile backsize according to claim 1, wherein the second aid comprises sepiolite powder.
6. A process for preparing the two-component tile backsize according to any one of claims 1 to 5, comprising the steps of:
s1, fully mixing and uniformly stirring all the components in the liquid material component A to obtain a liquid component material;
s2, fully and uniformly stirring all the components in the powder component B to obtain a dry powder component material;
s3, weighing and placing the liquid component material and the dry powder component material according to the weight ratio of 1: 1.5-2, and then pouring the liquid component material into the dry powder component material to be uniformly stirred without agglomeration, thus obtaining the tile back glue.
CN202111662360.4A 2021-12-30 2021-12-30 Double-component tile back glue and preparation method thereof Pending CN114591043A (en)

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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20010018326A (en) * 1999-08-18 2001-03-05 여소현 The process of making a luffa extract
CN105037812A (en) * 2015-08-21 2015-11-11 广西大学 Antimicrobial degradable packaging material and preparation method thereof
CN105130341A (en) * 2015-09-29 2015-12-09 武汉利勤新材料有限公司 Stone gum protection material
CN105362206A (en) * 2015-02-05 2016-03-02 武汉华士特工业生物技术开发有限公司 Maca moisture mask with oxidation-resistant effect and preparation method
JP2018027917A (en) * 2016-08-18 2018-02-22 森永製菓株式会社 METHOD OF STABILIZING GLUCOSE p-COUMARIC ACID GLYCOSIDE, AND METHOD OF PRODUCING GLUCOSE p-COUMARIC ACID GLYCOSIDE SOLUTION USING THE SAME
CN112851209A (en) * 2021-01-15 2021-05-28 湖北民族大学 Novel tile glue and preparation method thereof

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20010018326A (en) * 1999-08-18 2001-03-05 여소현 The process of making a luffa extract
CN105362206A (en) * 2015-02-05 2016-03-02 武汉华士特工业生物技术开发有限公司 Maca moisture mask with oxidation-resistant effect and preparation method
CN105037812A (en) * 2015-08-21 2015-11-11 广西大学 Antimicrobial degradable packaging material and preparation method thereof
CN105130341A (en) * 2015-09-29 2015-12-09 武汉利勤新材料有限公司 Stone gum protection material
JP2018027917A (en) * 2016-08-18 2018-02-22 森永製菓株式会社 METHOD OF STABILIZING GLUCOSE p-COUMARIC ACID GLYCOSIDE, AND METHOD OF PRODUCING GLUCOSE p-COUMARIC ACID GLYCOSIDE SOLUTION USING THE SAME
CN112851209A (en) * 2021-01-15 2021-05-28 湖北民族大学 Novel tile glue and preparation method thereof

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Application publication date: 20220607