CN105902454B - One kind being used for the regenerated Moringa compound Essence of cell repair - Google Patents

One kind being used for the regenerated Moringa compound Essence of cell repair Download PDF

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CN105902454B
CN105902454B CN201610485168.5A CN201610485168A CN105902454B CN 105902454 B CN105902454 B CN 105902454B CN 201610485168 A CN201610485168 A CN 201610485168A CN 105902454 B CN105902454 B CN 105902454B
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parts
moringa
extract
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regenerated
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CN105902454A (en
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杨曼生
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Guangdong Bailichen Biotechnology Co., Ltd.
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Han Zaiman
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36Carboxylic acids; Salts or anhydrides thereof
    • A61K8/365Hydroxycarboxylic acids; Ketocarboxylic acids
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • A61K8/375Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/41Amines
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • A61K8/65Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/735Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/005Antimicrobial preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/04Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations

Abstract

The present invention relates to one kind to be used for the regenerated Moringa compound Essence of cell repair, it is characterized by: according to parts by weight including following raw material: 5-7 parts of moringa oleifera leaf extractive, 2-4 parts of seed oil of Moringa oleigera, native 3-5 parts of seven extract, 1-3 parts of Folium Artemisiae Argyi extract, 1-3 parts of achyranthes bidentata extract, 1-3 parts of Herba speranskiae tuberculatae extract, 5-10 parts of glycerol, 2-4 parts of glycerin monostearate, 1-3 parts of triethanolamine, 5-10 parts of hyaluronic acid, 5-10 parts of collagen, 2-5 parts of 1,3-BDO, 5-10 parts of lactic acid, 0.1 part of essential oil, 0.1 part and pure water 24-65 parts of preservative.It is an advantage of the invention that Essence can penetrate into face's deep layer, face's cell repair is promoted to regenerate, while uvioresistant activity can also be improved, prevented skin aging, and keep certain antibiotic property, protect the safety of skin.

Description

One kind being used for the regenerated Moringa compound Essence of cell repair
[technical field]
The present invention relates to cosmetic fields, in particular to a kind of to be used for the regenerated Moringa compound Essence of cell repair.
[background technique]
Skin, as the age is continuously increased, all gradually tends to aging as other organs.The aging of skin be it is a kind of just It often occurs as, skin aging as a result, other than making the physiological function of skin decline, it is most important that become the appearance of people Change.Aging makes the beauty of human body lose lustre, and therefore, the appearance of aging can generate negative effect to the psychology of people, everybody is intended to keep outer Looks youth, perpetual youth.Prevention and delay skin aging are the important topics of cosmetic dermatology.The aging of skin is endogenous Factor and the common exercising result of exogenous stimulation factor.Endogenous factor is slowing down due to skin cell metabolism, skin Cuticula thicken and cause the dystrophia of skin so that subcutaneous fat storage gradually decreases, cell and fibr tissue nutrition are not It is good, performance decline, and skin is made wrinkle occur.Extrinsic factor is the elasticity because of direct sunlight meeting coup injury deep skin Fiber and collagen, causing skin of face to become, relaxation is matt, and ultraviolet irradiation gently then enables skin darkening thicker, weight It then can lead to cutaneum carcinoma, be that skin is made to do sth. in advance one of arch-criminal of aging.It is especially so to form using high-quality cosmetics The good habit of Essence.
Essence is the superfine product in skin care item, and ingredient is exquisite, effect is powerful, significant effect, remains what it possessed It is noble and mysterious.The effect of Essence has anti-aging, crease-resistant, moisturizing, whitening, despeckle etc..The essence occurred currently on the market The main effect of liquid is moisturizing, whitening and puts aging, and with cell repair regeneration function and effective Essence is basic No.
[summary of the invention]
In view of above content, it is necessary to provide one kind for the regenerated Moringa compound Essence of cell repair, can permeate To face's deep layer, face's cell repair is promoted to regenerate, while uvioresistant activity can also be improved, prevents skin aging, and keep Certain antibiotic property protects the safety of skin.
In order to achieve the above objectives, the technical scheme adopted by the invention is that: one kind is multiple for the regenerated Moringa of cell repair Square Essence includes following raw material according to parts by weight: 5-7 parts of moringa oleifera leaf extractive, 2-4 parts of seed oil of Moringa oleigera, and native seven extracts 3-5 parts, 1-3 parts of Folium Artemisiae Argyi extract, 1-3 parts of achyranthes bidentata extract, 1-3 parts of Herba speranskiae tuberculatae extract, 5-10 parts of glycerol, monostearate is sweet 2-4 parts of grease, 1-3 parts of triethanolamine, 5-10 parts of hyaluronic acid, 5-10 parts of collagen, 2-5 parts of 1,3-BDO, lactic acid 5- 10 parts, 0.1 part of essential oil, 0.1 part and pure water 24-65 parts of preservative.
In the present invention, as further explanation, the moringa oleifera leaf extractive is prepared by the following method: being accurately weighed The leaf of Moringa of 30g, it is 6-12 hours dry at 50-60 DEG C with infrared baking oven, it crushes, crosses 20 mesh sieve, be then added 200mL's Solvent, hot dipping 2-4 hours in 50-70 DEG C of hot bath, filtering extraction filtrate, cooled to room temperature, then with 800-1000r/ The speed of min is centrifuged 5-10 minutes, takes supernatant, and the dehydrated alcohol of 5-8 times of volume is added, and 48 hours is stood, with 800- The speed of 1000r/min is centrifuged 5-10 minutes, is taken precipitating, is washed 2 times with the dehydrated alcohol of 200mL, with infrared baking oven in 50-60 DEG C obtain moringa oleifera leaf extractive within dry 12-24 hours.
In the present invention, as further explanation, the solvent is distilled water water, methanol, ethyl alcohol, isopropanol, positive fourth One of alcohol, ethylene glycol, acetoneand ethyl acetate.
In the present invention, as further explanation, the seed oil of Moringa oleigera is prepared by the following method: weighing 100g Moringa Seed benevolence is put into pulverizer crushing, crosses 10 meshes, puts refluxing extraction device into, and 500mL is added and analyzes pure petroleum ether circumfluence distillation 2- 5 times, each 2-6h merges extracting solution, 50-80 DEG C is put into after suction filtration, 12-24 is concentrated in the vacuum oven of 0.05-0.15MPa Hour, obtain seed oil of Moringa oleigera.
In the present invention, as further explanation, described is used for the regenerated Moringa compound Essence of cell repair to gold The antibiotic rate of staphylococcus aureus is 77.66-100%, and the antibiotic rate to Escherichia coli is 75.81-91.65%, is read white The antibiotic rate of pearl bacterium is 85.64-100%, and the antibiotic rate to Pseudomonas aeruginosa is 84.99-100%.
In the present invention, as further explanation, described one kind is used for the regenerated Moringa compound Essence of cell repair Preparation method, it is characterised in that: specific steps are as follows:
Successively by load weighted moringa oleifera leaf extractive, seed oil of Moringa oleigera, native seven extracts, Folium Artemisiae Argyi extract, achyranthes bidentata extract, Herba speranskiae tuberculatae extract, glycerol, glycerin monostearate, triethanolamine, 1,3 butylene glycol, lactic acid and pure water are put into emulsion pot In, 60 DEG C are warming up to, turn on agitator is stirred 40 minutes with the speed of 100r/min, is subsequently placed into hyaluronic acid and collagen egg White, stirring after twenty minutes, is cooled to 45 DEG C while stirring, finally puts into essential oil and preservative, and stirring can be prepared by after ten minutes For the regenerated Moringa compound Essence of cell repair.
The effective component of part material is as follows:
Moringa is drought-resistant, impoverishment tolerant, growth are rapid, adaptable, is the quick growing species of trees of subtropical and tropical zones.Moringa Leaf and okra fruit are common woody vegetables in India and south east asia, and Moringa seed is rich in grease, and edible, seed has water purification Function.Leaf of Moringa, seed, bark, moringa root etc. are folk tradition drugs, for health care and treat a variety of diseases.Therefore, Moringa Referred to as " tree of miracle ".
Moringa blade, fruit pod are naturally anti-rich in several mineral materials, vitamin, 20 kinds of amino acid, 46 kinds of antioxygen elements and 36 kinds Scorching body and minerals.Leaf of Moringa powder has hypoglycemic, lipid-loweringing, decompression, antitumor, anti-oxidant, defaecation, diuresis, expelling parasite, improves sleep And other effects, long-term consumption can enhance immune function of human body, delay senescence, prevention disease.Ayurveda thinks that Moringa can prevent 300 kinds of diseases.Especially concern and heat of the Moringa by many research institutions, the developed countries such as America and Europe and consumer in recent years is held in both hands. Often edible leaf of Moringa can strengthen immunity, toxin expelling, body shaping, anti-aging, anticancer and have pole to a variety of chronic and major disease Big improvement effect.Leaf of Moringa is natural green food, and the complete nutrients matter containing needed by human body, it may replace compound dimension Raw element, calcium tablet, cod-liver oil etc..Especially there is good effect to hypertension, hyperlipidemia, diabetes, gout etc..Leaf of Moringa can assist Improve, prevention disease, improves sleep, enhancing memory, delays senescence, may further be used to the special portions such as treatment liver, spleen, channels and collaterals The disease of position.It also has the effects that treat halitosis and sober up.
The type composition of fatty acid is extremely similar to olive oil in seed oil of Moringa oleigera, can be used as after finishing advanced edible Oil.Since oil ben is not oxidizable, has potent washing and make bubble effect, be soapmaking, cosmetics, lubricant, preservative and perfume (or spice) The quality raw materials of material.
Native seven prescription sources: side goes out in " acute filthy disease Alioth " volume, and name is shown under " acute filthy disease pandect " volume.Drug composition: peach kernel, red Chinese herbaceous peony, Herba Lycopi, corydalis tuber, safflower, dried orange peel, the root of three-nerved spicebush, Radix Angelicae Pubescentis.
Folium artemisiae argyi cries wormwood also known as fragrant Chinese mugwort, Chinese mugwort, argy wormwood, for the dried leaf of compositae plant Chinese mugwort.With warming channel for arresting bleeding, cold dispelling stops Bitterly, the effect of wet down desinsection.Suitable for deficient cold type bleeding and abdominal pain, have obviously for women's cold of insufficiency type irregular menstruation, abdominal pain, metrorrhagia and metrostaxis Curative effect.The ventable blood of folium artemisiae argyi, warm channels and collaterals also have effects that anti-bacteria and anti-virus while improving immunity of organisms.
Radix achyranthis bidentatae is in elongated cylindrical, straight and upright or slightly bent, long 15~70cm, 0.4~1cm of diameter.Surface lark is light Brown, the protrusion of the lateral root trace and horizontally long hole skin sample that have the thin vertical wrinkle of micro- distortion, arrangement sparse.Matter is firmly crisp, frangibility, dampness After soften, section is flat, light brown, slightly in cutin sample it is beautiful glossy, center vascular bundle xylem is larger, yellow-white, periphery dissipate There are most yellowish-white color dots.There are dispelling stasis of blood and stimulating the menstrual flow, nourishing liver and kidney, strengthening the bones and muscles, inducing diuresis for treating strangurtia, the effect of ensurining proper downward flow of the blood.
Lopseed also known as medicine Anacamptis pyromaidalis, Staggergrass etc..Perennial herb, it is reddish brown with stem color, without leaf, drying, free from admixture person It is preferred.Annual herb flowers produce the nations of China and India.Property happiness sunlight, be afraid of it is wet, heat-resisting to can not resist cold, adaptability is in loose fertile slightly sour In soil, but it is also barren-resistant.Adaptability is stronger, and transplanting easily survives, and growth is rapid.Also name is impetuous for seed, stem also name lopseed, It can be used as medicine, there is the effect of activating microcirculation and removing stasis medicinal, diuresis removing toxic substances, promoting menstruation is deep.Fresh grass mashes external application, can control the swollen pain of boil, insect-bite Wound.
Glycerol is exactly glycerine, is as watery grease, skin is easy to absorb and 1,3-PD has good moisturizing Effect, may be used as moisturizer.
Glycerin monostearate, nonionic surfactant.It is used as emulsifier in cosmetics and medical paste.White waxy Thin slice or bead solid, it is not soluble in water, it mixes and is dispersed in water through intense oscillations with hot water.
Triethanolamine, colourless to pale yellow transparent thick liquid, micro- have an ammonia taste, and when low temperature becomes colourless to faint yellow cube System crystals.Color deepens gradually when being placed in air.Soluble easily in water, ethyl alcohol, acetone, glycerol and ethylene glycol etc. are being made up It is used as emulsifier, moisturizer, humidizer, thickener, PH poising agent in product.Triethanolamine is that emulsifier is commonly used in cream preparation, Have lotion fine and smooth with the cream products that triethanolamine emulsifies, the characteristics of lotion brilliant white, another triethanolamine and higher fatty acids or The colloid phase stability that higher aliphatic is formed is good, stable product quality, and it is high can to hold additional ingredients specific gravity.Triethanolamine be containing The most frequently used neutralizer of the acidity high-molecular gel such as carbomer, triethanolamine form and stablize by neutralizing with carboxyls such as carbomers Macromolecular structure, reach the application effect of thickening and moisturizing.
Hyaluronic acid is also known as uronic acid, hyaluronic acid, and basic structure is by two dissacharide units D-Glucose aldehydic acid and N- The large-scale polysaccharide of acetylglucosamine composition.It is different from other mucopolysaccharides, its not sulfur-bearing.Its hyalomitome molecule can carry 500 Times or more moisture be widely applied in skin care products and cosmetics for the best moisturizing ingredient recognized by current.
Collagen is boiomacromolecule, the main component in animal connective tissue, and content is most in the mammalian body Functional protein more, distribution is most wide, accounts for the 25-30% of total protein, certain organisms are even as high as 80% or more.Former egg Bai Yin has good biocompatibility, biodegradable and bioactivity, therefore in food, medicine, organizational project, change The fields such as cosmetic are widely applied.
Lactic acid is a kind of carboxylic acid, and molecular formula is C3H6O3, it is the carboxylic acid containing hydroxyl, therefore is an alpha-hydroxy acid (AHA).Since lactic acid is a part of the intrinsic natural moisturizing factor of skin, it is widely used as moistening for many skin care item Agent.
The invention has the following advantages:
1. a kind of regenerated Moringa compound Essence of cell repair that is used for of the invention has soft skin, cutin generation is improved Thank, repair cell regeneration enhances cell activity, keeps the effect of skin elasticity and pliability, enable skin it is glittering and translucent, full of life Machine.The general flavone in moringa oleifera leaf extractive in the present invention can remove the horny layer of epidermis of aging, promote basal cell hyperplasia, repair Multiple aging collagenous fibres, improve skin tension and elasticity.The Proliferation, Differentiation of horn cells is adjusted, angling process is inhibited, stimulation accelerates The maintenance and regeneration of cell stimulate hyperplasia, promote blood capillary proliferation, accelerate blood circulation;Along with native seven extracts The content of peroxide MDA can be reduced, the activity of superoxide dismutase SOD is improved, eliminates skin in metabolic processes The harmful substance of generation eliminates the obstruction of metabolism, promotes cell repair regeneration to provide power-assisted for general flavone, further The speed for improving the metabolism of skin, improves skin surface gloss, makes skin more bright, compact.
2. a kind of regenerated Moringa compound Essence of cell repair that is used for of the invention has extremely strong inoxidizability and anti-purple Outside line activity, protects skin not by the infringement of ultraviolet light, skin is obscure caused by resisting because of environmental radiation, slows down Skin Cell Aging speed.Dienoic acid and tetraenoic acid in one side seed oil of Moringa oleigera have very strong absorption for shortwave and ultraviolet B radiation, With extremely strong anti-ultraviolet stability;On the other hand along with flavones abundant in moringa oleifera leaf extractive and Folium Artemisiae Argyi extract The strong anti-oxidation that phenolic hydroxyl group in class compound structure has, meanwhile, wormwood extract can effectively remove OH free radical, make Essence of the invention has very strong inoxidizability, and seed oil of Moringa oleigera induction period is 9 times of olive oil, so that of the invention Essence inoxidizability it is very stable, extend antioxidative effective time.
3. a kind of regenerated Moringa compound Essence of cell repair that is used for of the invention has extremely strong antibiotic property, can be fine Protection skin safe, for skin build up together advantageous barrier.Isothiocyanate in moringa oleifera leaf extractive and seed oil of Moringa oleigera Permeability of cell membranes can be destroyed, the respiration of bacterium is hindered, is had for gram-positive bacteria, dermatophyte very strong anti- Bacterium activity;Along in Folium Artemisiae Argyi extract 1,8- Cineole, terpinol, spathulenol, caryophyllene oxide, needle juniper camphor for Various bacteria, fungi and virus have antibacterial action, and synergistic effect between the two greatly strengthens the antibiotic property of Essence, And the polysaccharide all contained very much in moringa oleifera leaf extractive, Herba speranskiae tuberculatae extract and achyranthes bidentata extract filled up Folium Artemisiae Argyi extract for The unabiding disadvantage of antibiotic property, greatly improved the stability of antibacterial effect.
[specific embodiment]
According to parts by weight:
Embodiment 1:
1. moringa oleifera leaf extractive, seed oil of Moringa oleigera, native seven extracts, wormwood extract, achyranthes bidentata extract and lopseed are extracted The preparation of object
Moringa oleifera leaf extractive is prepared by the following method: the leaf of Moringa of 30g is accurately weighed, it is dry at 50 DEG C with infrared baking oven It 6 hours, crushes, crosses 20 mesh sieve, the distilled water of 100mL, the hot dipping 2 hours in 50 DEG C of hot baths is then added, filtering is extracted Filtrate, cooled to room temperature, then be centrifuged 5 minutes with the speed of 800r/min, supernatant is taken, the anhydrous of 5 times of volumes is added Ethyl alcohol stands 48 hours, is centrifuged 5 minutes with the speed of 800r/min, takes precipitating, washed 2 times with the dehydrated alcohol of 200mL, uses Infrared baking oven obtains moringa oleifera leaf extractive in dry 12 hours at 50 DEG C.
Seed oil of Moringa oleigera is prepared by the following method: being weighed 100g moringa seeds benevolence, is put into pulverizer crushing, crosses 10 meshes, put Into refluxing extraction device, pure petroleum ether circumfluence distillation 2 times of 500mL analysis is added, extracting solution is merged, put after suction filtration by each 2h Enter 50 DEG C, the vacuum oven of 0.05MPa is concentrated 12 hours, obtains seed oil of Moringa oleigera.
Folium Artemisiae Argyi extract, achyranthes bidentata extract, native seven extracts and Herba speranskiae tuberculatae extract are prepared by the following method: being weighed respectively Folium artemisiae argyi, the radix achyranthis bidentatae, seven and each 30g of lopseed of soil that crushed 20 mesh sieve, are respectively put into 200mL beaker, and 150mL is added and steams Distilled water places it in electric-heated thermostatic water bath, and temperature is controlled at 80 DEG C, hot dipping 3 hours, filters, puts the filtrate into other In 500mL large beaker: it repeats to extract 3 times with same method, merges 3 filtrates, be concentrated into 10-20mL with rotary evaporator, After being cooled to room temperature, 60mL ethyl alcohol being added, stands 24 hours at backlight, filters, filter cake is successively washed 2 times with ethyl alcohol and ether, Respectively obtain Folium Artemisiae Argyi extract, achyranthes bidentata extract, native seven extracts and Herba speranskiae tuberculatae extract.
2. the preparation of Moringa compound Essence
According to parts by weight, successively by 5 parts of moringa oleifera leaf extractives, 2 parts of seed oil of Moringa oleigera, 3 parts of seven extracts of soil, 1 portion of folium artemisiae argyi Extract, 1 part of achyranthes bidentata extract, 1 part of Herba speranskiae tuberculatae extract, 2 parts of seed oil of Moringa oleigera, 5 parts of glycerol, 2 parts of glycerin monostearates, 1 Part triethanolamine, 1 part of 1,3-BDO, 5 parts of lactic acid and 65 parts of pure water are put into emulsion pot, are warming up to 60 DEG C, unlatching is stirred Device is mixed, is stirred 40 minutes with the speed of 100r/min, 5 parts of hyaluronic acids and 5 parts of collagens are subsequently placed into, is stirred 20 minutes Afterwards, it is cooled to 45 DEG C while stirring, finally puts into 0.1 part of essential oil and 0.1 portion of preservative, stirring can be prepared by being used for after ten minutes The regenerated Moringa compound Essence of cell repair.
Embodiment 2:
1. moringa oleifera leaf extractive, seed oil of Moringa oleigera, native seven extracts, wormwood extract, achyranthes bidentata extract and lopseed are extracted The preparation of object
Moringa oleifera leaf extractive is prepared by the following method: the leaf of Moringa of 30g is accurately weighed, it is dry at 55 DEG C with infrared baking oven It 7 hours, crushes, crosses 20 mesh sieve, the ethyl alcohol of 120mL, the hot dipping 2 hours in 50 DEG C of hot baths is then added, filter is extracted in filtering Liquid, cooled to room temperature, then be centrifuged 6 minutes with the speed of 800r/min, supernatant is taken, the anhydrous second of 5 times of volumes is added Alcohol stands 48 hours, is centrifuged 6 minutes with the speed of 800r/min, takes precipitating, washed 2 times with the dehydrated alcohol of 200mL, use is red Outer baking oven obtains moringa oleifera leaf extractive in dry 14 hours at 55 DEG C.
Seed oil of Moringa oleigera is prepared by the following method: being weighed 100g moringa seeds benevolence, is put into pulverizer crushing, crosses 10 meshes, put Into refluxing extraction device, pure petroleum ether circumfluence distillation 2 times of 500mL analysis is added, extracting solution is merged, put after suction filtration by each 3h Enter 55 DEG C, the vacuum oven of 0.05MPa is concentrated 14 hours, obtains seed oil of Moringa oleigera.
Folium Artemisiae Argyi extract, achyranthes bidentata extract, native seven extracts and Herba speranskiae tuberculatae extract are prepared by the following method: being weighed respectively Folium artemisiae argyi, the radix achyranthis bidentatae, seven and each 30g of lopseed of soil that crushed 20 mesh sieve, are respectively put into 200mL beaker, and 150mL is added and steams Distilled water places it in electric-heated thermostatic water bath, and temperature is controlled at 80 DEG C, hot dipping 3 hours, filters, puts the filtrate into other In 500mL large beaker: it repeats to extract 3 times with same method, merges 3 filtrates, be concentrated into 10-20mL with rotary evaporator, After being cooled to room temperature, 60mL ethyl alcohol being added, stands 24 hours at backlight, filters, filter cake is successively washed 2 times with ethyl alcohol and ether, Respectively obtain Folium Artemisiae Argyi extract, achyranthes bidentata extract, native seven extracts and Herba speranskiae tuberculatae extract.
2. the preparation of Moringa compound Essence
According to parts by weight, successively by 5 parts of moringa oleifera leaf extractives, 2.5 parts of seed oil of Moringa oleigera, 3.5 parts of seven extracts of soil, 1.5 Part Folium Artemisiae Argyi extract, 1.5 parts of achyranthes bidentata extracts, 1.5 parts of Herba speranskiae tuberculatae extracts, 2 parts of seed oil of Moringa oleigera, 6 parts of glycerol, 2 parts of single tristearin Acid glyceride, 1 part of triethanolamine, 1 part of 1,3-BDO, 6 parts of lactic acid and 58 parts of pure water are put into emulsion pot, are warming up to 60 DEG C, turn on agitator is stirred 40 minutes with the speed of 100r/min, is subsequently placed into 6 parts of hyaluronic acids and 6 parts of collagens, stirs It mixes after twenty minutes, is cooled to 45 DEG C while stirring, finally put into 0.1 part of essential oil and 0.1 portion of preservative, stirring is after ten minutes It is made for the regenerated Moringa compound Essence of cell repair.
Embodiment 3:
1. moringa oleifera leaf extractive, seed oil of Moringa oleigera, native seven extracts, wormwood extract, achyranthes bidentata extract and lopseed are extracted The preparation of object
Moringa oleifera leaf extractive is prepared by the following method: the leaf of Moringa of 30g is accurately weighed, it is dry at 65 DEG C with infrared baking oven It 8 hours, crushes, crosses 20 mesh sieve, the methanol of 120mL, the hot dipping 3 hours in 60 DEG C of hot baths is then added, filter is extracted in filtering Liquid, cooled to room temperature, then be centrifuged 7 minutes with the speed of 850r/min, supernatant is taken, the anhydrous second of 6 times of volumes is added Alcohol stands 48 hours, is centrifuged 7 minutes with the speed of 850r/min, takes precipitating, washed 3 times with the dehydrated alcohol of 200mL, use is red Outer baking oven obtains moringa oleifera leaf extractive in dry 16 hours at 65 DEG C.
Seed oil of Moringa oleigera is prepared by the following method: being weighed 100g moringa seeds benevolence, is put into pulverizer crushing, crosses 10 meshes, put Into refluxing extraction device, pure petroleum ether circumfluence distillation 3 times of 500mL analysis is added, extracting solution is merged, put after suction filtration by each 3h Enter 60 DEG C, the vacuum oven of 0.1MPa is concentrated 16 hours, obtains seed oil of Moringa oleigera.
Folium Artemisiae Argyi extract, achyranthes bidentata extract, native seven extracts and Herba speranskiae tuberculatae extract are prepared by the following method: being weighed respectively Folium artemisiae argyi, the radix achyranthis bidentatae, seven and each 30g of lopseed of soil that crushed 20 mesh sieve, are respectively put into 200mL beaker, and 150mL is added and steams Distilled water places it in electric-heated thermostatic water bath, and temperature is controlled at 80 DEG C, hot dipping 3 hours, filters, puts the filtrate into other In 500mL large beaker: it repeats to extract 3 times with same method, merges 3 filtrates, be concentrated into 10-20mL with rotary evaporator, After being cooled to room temperature, 60mL ethyl alcohol being added, stands 24 hours at backlight, filters, filter cake is successively washed 2 times with ethyl alcohol and ether, Respectively obtain Folium Artemisiae Argyi extract, achyranthes bidentata extract, native seven extracts and Herba speranskiae tuberculatae extract.
2. the preparation of Moringa compound Essence
According to parts by weight, successively by 6 parts of moringa oleifera leaf extractives, 3 parts of seed oil of Moringa oleigera, 3.5 parts of seven extracts of soil, 1.5 parts Folium Artemisiae Argyi extract, 1.5 parts of achyranthes bidentata extracts, 1.5 parts of Herba speranskiae tuberculatae extracts, 3 parts of seed oil of Moringa oleigera, 7 parts of glycerol, 3 parts of monostearates Glyceride, 2 parts of triethanolamines, 2 parts of 1,3-BDOs, 7 parts of lactic acid and 48 parts of pure water are put into emulsion pot, are warming up to 60 DEG C, turn on agitator is stirred 40 minutes with the speed of 100r/min, is subsequently placed into 7 parts of hyaluronic acids and 7 parts of collagens, stirs It mixes after twenty minutes, is cooled to 45 DEG C while stirring, finally put into 0.1 part of essential oil and 0.1 portion of preservative, stirring is after ten minutes It is made for the regenerated Moringa compound Essence of cell repair.
Embodiment 4:
1. moringa oleifera leaf extractive, seed oil of Moringa oleigera, native seven extracts, wormwood extract, achyranthes bidentata extract and lopseed are extracted The preparation of object
Moringa oleifera leaf extractive is prepared by the following method: the leaf of Moringa of 30g is accurately weighed, it is dry at 70 DEG C with infrared baking oven It 9 hours, crushes, crosses 20 mesh sieve, the ethylene glycol of 150mL, the hot dipping 3 hours in 65 DEG C of hot baths is then added, filtering is extracted Filtrate, cooled to room temperature, then be centrifuged 8 minutes with the speed of 900r/min, supernatant is taken, the anhydrous of 7 times of volumes is added Ethyl alcohol stands 48 hours, is centrifuged 8 minutes with the speed of 900r/min, takes precipitating, washed 3 times with the dehydrated alcohol of 200mL, uses Infrared baking oven obtains moringa oleifera leaf extractive in dry 18 hours at 70 DEG C.
Seed oil of Moringa oleigera is prepared by the following method: being weighed 100g moringa seeds benevolence, is put into pulverizer crushing, crosses 10 meshes, put Into refluxing extraction device, pure petroleum ether circumfluence distillation 3 times of 500mL analysis is added, extracting solution is merged, put after suction filtration by each 4h Enter 65 DEG C, the vacuum oven of 0.1MPa is concentrated 18 hours, obtains seed oil of Moringa oleigera.
Folium Artemisiae Argyi extract, achyranthes bidentata extract, native seven extracts and Herba speranskiae tuberculatae extract are prepared by the following method: being weighed respectively Folium artemisiae argyi, the radix achyranthis bidentatae, seven and each 30g of lopseed of soil that crushed 20 mesh sieve, are respectively put into 200mL beaker, and 150mL is added and steams Distilled water places it in electric-heated thermostatic water bath, and temperature is controlled at 80 DEG C, hot dipping 3 hours, filters, puts the filtrate into other In 500mL large beaker: it repeats to extract 3 times with same method, merges 3 filtrates, be concentrated into 10-20mL with rotary evaporator, After being cooled to room temperature, 60mL ethyl alcohol being added, stands 24 hours at backlight, filters, filter cake is successively washed 2 times with ethyl alcohol and ether, Respectively obtain Folium Artemisiae Argyi extract, achyranthes bidentata extract, native seven extracts and Herba speranskiae tuberculatae extract.
2. the preparation of Moringa compound Essence
According to parts by weight, successively by 6.5 parts of moringa oleifera leaf extractives, 3 parts of seed oil of Moringa oleigera, 4 parts of seven extracts of soil, 2 parts of Chinese mugworts Leaf extract, 2 parts of achyranthes bidentata extracts, 2 parts of Herba speranskiae tuberculatae extracts, 3 parts of seed oil of Moringa oleigera, 8 parts of glycerol, 3 parts of glycerin monostearates, 2 parts of triethanolamines, 2 parts of 1,3-BDOs, 8 parts of lactic acid and 42 parts of pure water are put into emulsion pot, are warming up to 60 DEG C, unlatching is stirred Device is mixed, is stirred 40 minutes with the speed of 100r/min, 8 parts of hyaluronic acids and 8 parts of collagens are subsequently placed into, is stirred 20 minutes Afterwards, it is cooled to 45 DEG C while stirring, finally puts into 0.1 part of essential oil and 0.1 portion of preservative, stirring can be prepared by being used for after ten minutes The regenerated Moringa compound Essence of cell repair.
Embodiment 5:
1. moringa oleifera leaf extractive, seed oil of Moringa oleigera, native seven extracts, wormwood extract, achyranthes bidentata extract and lopseed are extracted The preparation of object
Moringa oleifera leaf extractive is prepared by the following method: the leaf of Moringa of 30g is accurately weighed, it is dry at 75 DEG C with infrared baking oven It 10 hours, crushes, crosses 20 mesh sieve, the ethyl acetate of 150mL, the hot dipping 3.5 hours in 65 DEG C of hot baths, filtering is then added Filtrate, cooled to room temperature are extracted, then is centrifuged 9 minutes with the speed of 950r/min, supernatant is taken, 8 times of volumes is added Dehydrated alcohol stands 48 hours, is centrifuged 9 minutes with the speed of 950r/min, takes precipitating, wash 4 with the dehydrated alcohol of 200mL It is secondary, moringa oleifera leaf extractive is obtained within dry 20 hours at 75 DEG C with infrared baking oven.
Seed oil of Moringa oleigera is prepared by the following method: being weighed 100g moringa seeds benevolence, is put into pulverizer crushing, crosses 10 meshes, put Into refluxing extraction device, pure petroleum ether circumfluence distillation 4 times of 500mL analysis is added, extracting solution is merged, put after suction filtration by each 5h Enter 70 DEG C, the vacuum oven of 0.12MPa is concentrated 20 hours, obtains seed oil of Moringa oleigera.
Folium Artemisiae Argyi extract, achyranthes bidentata extract, native seven extracts and Herba speranskiae tuberculatae extract are prepared by the following method: being weighed respectively Folium artemisiae argyi, the radix achyranthis bidentatae, seven and each 30g of lopseed of soil that crushed 20 mesh sieve, are respectively put into 200mL beaker, and 150mL is added and steams Distilled water places it in electric-heated thermostatic water bath, and temperature is controlled at 80 DEG C, hot dipping 3 hours, filters, puts the filtrate into other In 500mL large beaker: it repeats to extract 3 times with same method, merges 3 filtrates, be concentrated into 10-20mL with rotary evaporator, After being cooled to room temperature, 60mL ethyl alcohol being added, stands 24 hours at backlight, filters, filter cake is successively washed 2 times with ethyl alcohol and ether, Respectively obtain Folium Artemisiae Argyi extract, achyranthes bidentata extract, native seven extracts and Herba speranskiae tuberculatae extract.
2. the preparation of Moringa compound Essence
According to parts by weight, successively by 6.5 parts of moringa oleifera leaf extractives, 3.5 parts of seed oil of Moringa oleigera, 4.5 parts of seven extracts of soil, 2.5 parts of Folium Artemisiae Argyi extracts, 2.5 parts of achyranthes bidentata extracts, 2.5 parts of Herba speranskiae tuberculatae extracts, 4 parts of seed oil of Moringa oleigera, 9 parts of glycerol, 4 parts of lists are hard Glycerol, 3 parts of triethanolamines, 3 parts of 1,3-BDOs, 9 parts of lactic acid and 32 parts of pure water are put into emulsion pot, are warming up to 60 DEG C, turn on agitator is stirred 40 minutes with the speed of 100r/min, is subsequently placed into 9 parts of hyaluronic acids and 9 parts of collagens, Stirring after twenty minutes, is cooled to 45 DEG C while stirring, finally puts into 0.1 part of essential oil and 0.1 portion of preservative, and stirring is after ten minutes It can be made for the regenerated Moringa compound Essence of cell repair.
Embodiment 6:
1. moringa oleifera leaf extractive, seed oil of Moringa oleigera, native seven extracts, wormwood extract, achyranthes bidentata extract and lopseed are extracted The preparation of object
Moringa oleifera leaf extractive is prepared by the following method: the leaf of Moringa of 30g is accurately weighed, it is dry at 80 DEG C with infrared baking oven It 12 hours, crushes, crosses 20 mesh sieve, the acetone of 200mL, the hot dipping 4 hours in 70 DEG C of hot baths is then added, filter is extracted in filtering Liquid, cooled to room temperature, then be centrifuged 10 minutes with the speed of 1000r/min, supernatant is taken, the anhydrous of 8 times of volumes is added Ethyl alcohol stands 48 hours, is centrifuged 10 minutes with the speed of 1000r/min, takes precipitating, washed 5 times with the dehydrated alcohol of 200mL, Moringa oleifera leaf extractive is obtained within dry 24 hours at 80 DEG C with infrared baking oven.
Seed oil of Moringa oleigera is prepared by the following method: being weighed 100g moringa seeds benevolence, is put into pulverizer crushing, crosses 10 meshes, put Into refluxing extraction device, pure petroleum ether circumfluence distillation 5 times of 500mL analysis is added, extracting solution is merged, put after suction filtration by each 6h Enter 80 DEG C, the vacuum oven of 0.15MPa is concentrated 24 hours, obtains seed oil of Moringa oleigera.
Folium Artemisiae Argyi extract, achyranthes bidentata extract, native seven extracts and Herba speranskiae tuberculatae extract are prepared by the following method: being weighed respectively Folium artemisiae argyi, the radix achyranthis bidentatae, seven and each 30g of lopseed of soil that crushed 20 mesh sieve, are respectively put into 200mL beaker, and 150mL is added and steams Distilled water places it in electric-heated thermostatic water bath, and temperature is controlled at 80 DEG C, hot dipping 3 hours, filters, puts the filtrate into other In 500mL large beaker: it repeats to extract 3 times with same method, merges 3 filtrates, be concentrated into 10-20mL with rotary evaporator, After being cooled to room temperature, 60mL ethyl alcohol being added, stands 24 hours at backlight, filters, filter cake is successively washed 2 times with ethyl alcohol and ether, Respectively obtain Folium Artemisiae Argyi extract, achyranthes bidentata extract, native seven extracts and Herba speranskiae tuberculatae extract.
2. the preparation of Moringa compound Essence
According to parts by weight, successively by 7 parts of moringa oleifera leaf extractives, 4 parts of seed oil of Moringa oleigera, 5 parts of seven extracts of soil, 3 portions of folium artemisiae argyis Extract, 3 parts of achyranthes bidentata extracts, 3 parts of Herba speranskiae tuberculatae extracts, 4 parts of seed oil of Moringa oleigera, 10 parts of glycerol, 4 parts of glycerin monostearates, 3 Part triethanolamine, 3 parts of 1,3-BDOs, 10 parts of lactic acid and 24 parts of pure water are put into emulsion pot, are warming up to 60 DEG C, unlatching is stirred Device is mixed, is stirred 40 minutes with the speed of 100r/min, 10 parts of hyaluronic acids and 10 parts of collagens are subsequently placed into, is stirred 20 minutes Afterwards, it is cooled to 45 DEG C while stirring, finally puts into 0.1 part of essential oil and 0.1 portion of preservative, stirring can be prepared by being used for after ten minutes The regenerated Moringa compound Essence of cell repair.
Comparative example 1:
Test to improving and removing scar:
Changed using no scar that is measured microscopically with camera shooting.Test object is 50 volunteers (25 women, 25 male Property), between 15-65 years old, there is scar at the age.Test carries out under the supervision of dermatologist.Compare be not used Essence and Using product of the present invention twice a day morning and evening, it is applied to scarring areas and measures its repair rate after continuous use 45 days, Comparing result is shown in Table 1.
Table 1:
Mild scar Moderate scar Severe scar
Essence is not used 85% 65% 25%
Embodiment 1 100% 70% 40%
Embodiment 2 100% 72% 43%
Embodiment 3 100% 77% 50%
Embodiment 4 100% 85% 55%
Embodiment 5 100% 80% 52%
Embodiment 6 100% 80% 50%
Table 1 the result shows that: using implement 1-6 Essence volunteer scar repair rate significantly larger than be not used Essence Volunteer scar repair rate, wherein mild scar repair rate arranges from high to low are as follows: embodiment 1=embodiment 2=implement Example 3=embodiment 4=embodiment 5=embodiment 6 > Essence is not used;Moderate scar repair rate arranges from high to low are as follows: implements 2 > embodiment of example 4 > embodiment 5=embodiment 6 > embodiment, 3 > embodiment 1 > Essence is not used;Severe scar repair rate is from height To low arrangement are as follows: 2 > embodiment of embodiment 4 > embodiment, 5 > embodiment 6=3 > embodiment of embodiment 1 > Essence is not used.
Comparative example 2:
Unused Essence and embodiment 1-6 sample is taken to measure maximum absorption wavelength 212nm in ultraviolet specrophotometer Absorbance after place's measurement 10min and 120min, the results are shown in Table 2.
Table 2:
Table 2 the result shows that: it is stronger than the absorbance of the sample of unused Essence using the sample of embodiment 1-6, and The result of the absorbance of 120min and 10min is not much different, and the absorbance of 10min test arranges from high to low are as follows: and embodiment 4 > 2 > embodiment of embodiment 5 > embodiment, 6 > embodiment, 3 > embodiment 1 > Essence is not used;120min test absorbance from height to Low arrangement are as follows: 2 > embodiment of embodiment 4 > embodiment, 5 > embodiment, 6 > embodiment, 3 > embodiment 1 > Essence is not used.
Comparative example 3:
Essence will be not added with and add the sample progress antibiotic property test of each embodiment, antibiotic rate the results are shown in Table 3.
Table 3:
Table 3 the result shows that: embodiment 1-6 has staphylococcus aureus, Escherichia coli, Candida albicans, Pseudomonas aeruginosa The sample of Essence is not used to staphylococcus aureus, Escherichia coli, Candida albicans, green pus bar in preferable antibacterial effect Bacterium does not have antibacterial effect.To the arrangement of the antibiotic rate of staphylococcus aureus from high to low are as follows: embodiment 4=embodiment 5=is real Apply 2 > embodiment of example 6 > embodiment, 3 > embodiment 1 > unused Essence;To the arrangement of the antibiotic rates of Escherichia coli from high to low Are as follows: 2 > embodiment of embodiment 4 > embodiment, 5 > embodiment, 6 > embodiment, 3 > embodiment 1 > Essence is not used;To Candida albicans Antibiotic rate arrangement from high to low are as follows: 2 > embodiment of embodiment 3=embodiment 4=embodiment 5=6 > embodiment of embodiment 1 > Essence is not used;To the arrangement of the antibiotic rate of Pseudomonas aeruginosa from high to low are as follows: embodiment 4=embodiment 5=embodiment 6 > reality Apply 3 > embodiment of example, 2 > embodiment 1 > unused Essence;
In a kind of better embodiment of the invention
1. moringa oleifera leaf extractive, seed oil of Moringa oleigera, native seven extracts, wormwood extract, achyranthes bidentata extract and lopseed are extracted The preparation of object
Moringa oleifera leaf extractive is prepared by the following method: the leaf of Moringa of 30g is accurately weighed, it is dry at 70 DEG C with infrared baking oven It 9 hours, crushes, crosses 20 mesh sieve, the ethylene glycol of 150mL, the hot dipping 3 hours in 65 DEG C of hot baths is then added, filtering is extracted Filtrate, cooled to room temperature, then be centrifuged 8 minutes with the speed of 900r/min, supernatant is taken, the anhydrous of 7 times of volumes is added Ethyl alcohol stands 48 hours, is centrifuged 8 minutes with the speed of 900r/min, takes precipitating, washed 3 times with the dehydrated alcohol of 200mL, uses Infrared baking oven obtains moringa oleifera leaf extractive in dry 18 hours at 70 DEG C.
Seed oil of Moringa oleigera is prepared by the following method: being weighed 100g moringa seeds benevolence, is put into pulverizer crushing, crosses 10 meshes, put Into refluxing extraction device, pure petroleum ether circumfluence distillation 3 times of 500mL analysis is added, extracting solution is merged, put after suction filtration by each 4h Enter 65 DEG C, the vacuum oven of 0.1MPa is concentrated 18 hours, obtains seed oil of Moringa oleigera.
Folium Artemisiae Argyi extract, achyranthes bidentata extract, native seven extracts and Herba speranskiae tuberculatae extract are prepared by the following method: being weighed respectively Folium artemisiae argyi, the radix achyranthis bidentatae, seven and each 30g of lopseed of soil that crushed 20 mesh sieve, are respectively put into 200mL beaker, and 150mL is added and steams Distilled water places it in electric-heated thermostatic water bath, and temperature is controlled at 80 DEG C, hot dipping 3 hours, filters, puts the filtrate into other In 500mL large beaker: it repeats to extract 3 times with same method, merges 3 filtrates, be concentrated into 10-20mL with rotary evaporator, After being cooled to room temperature, 60mL ethyl alcohol being added, stands 24 hours at backlight, filters, filter cake is successively washed 2 times with ethyl alcohol and ether, Respectively obtain Folium Artemisiae Argyi extract, achyranthes bidentata extract, native seven extracts and Herba speranskiae tuberculatae extract.
2. the preparation of Moringa compound Essence
According to parts by weight, successively by 6.5 parts of moringa oleifera leaf extractives, 3 parts of seed oil of Moringa oleigera, 4 parts of seven extracts of soil, 2 parts of Chinese mugworts Leaf extract, 2 parts of achyranthes bidentata extracts, 2 parts of Herba speranskiae tuberculatae extracts, 3 parts of seed oil of Moringa oleigera, 8 parts of glycerol, 3 parts of glycerin monostearates, 2 parts of triethanolamines, 2 parts of 1,3-BDOs, 8 parts of lactic acid and 42 parts of pure water are put into emulsion pot, are warming up to 60 DEG C, unlatching is stirred Device is mixed, is stirred 40 minutes with the speed of 100r/min, 8 parts of hyaluronic acids and 8 parts of collagens are subsequently placed into, is stirred 20 minutes Afterwards, it is cooled to 45 DEG C while stirring, finally puts into 0.1 part of essential oil and 0.1 portion of preservative, stirring can be prepared by being used for after ten minutes The regenerated Moringa compound Essence of cell repair.
Above description is the detailed description for the present invention preferably possible embodiments, but embodiment is not limited to this hair Bright patent claim, it is all the present invention suggested by technical spirit under completed same changes or modifications change, should all belong to In the covered the scope of the patents of the present invention.

Claims (5)

1. one kind is used for the regenerated Moringa compound Essence of cell repair, it is characterised in that: according to parts by weight include following original Material: 5-7 parts of moringa oleifera leaf extractive, 2-4 parts of seed oil of Moringa oleigera, native 3-5 parts of seven extract, 1-3 parts of Folium Artemisiae Argyi extract, achyranthes bidentata extract 1-3 parts, 1-3 parts of Herba speranskiae tuberculatae extract, 5-10 parts of glycerol, 2-4 parts of glycerin monostearate, 1-3 parts of triethanolamine, hyaluronic acid 5-10 parts, 5-10 parts of collagen, 2-5 parts of 1,3-BDO, 5-10 parts of lactic acid, 0.1 part of essential oil, 0.1 part of preservative and pure 24-65 parts of water;The moringa oleifera leaf extractive is prepared by the following method: being accurately weighed the leaf of Moringa of 30g, is existed with infrared baking oven It is 6-12 hours dry at 50-80 DEG C, it crushes, crosses 20 mesh sieve, the solvent of 100-200mL is then added, in 50-70 DEG C of hot bath Middle hot dipping 2-4 hours, filtrate, cooled to room temperature were extracted in filtering, then are divided with the speed centrifugation 5-10 of 800-1000r/min Clock takes supernatant, and the dehydrated alcohol of 5-8 times of volume is added, and stands 48 hours, is centrifuged 5- with the speed of 800-1000r/min 10 minutes, precipitating is taken, is washed 2-5 times with the dehydrated alcohol of 200mL, is obtained within dry 12-24 hours with infrared baking oven at 50-80 DEG C Moringa oleifera leaf extractive;Folium Artemisiae Argyi extract, achyranthes bidentata extract, native seven extracts and the Herba speranskiae tuberculatae extract is by following methods system It is standby: the folium artemisiae argyi that crushed 20 mesh sieve, radix achyranthis bidentatae, seven and each 30g of lopseed of soil are weighed respectively, are respectively put into 200mL beaker, 150mL distilled water is added, places it in electric-heated thermostatic water bath, temperature is controlled at 80 DEG C, hot dipping 3 hours, is filtered, by filtrate It is put into other 500mL large beaker: repeating to extract 3 times with same method, merge 3 filtrates, be concentrated with rotary evaporator To 10-20mL, after being cooled to room temperature, 60mL ethyl alcohol is added, stands 24 hours at backlight, filter, filter cake successively use ethyl alcohol with Ether is washed 2 times, that is, respectively obtains Folium Artemisiae Argyi extract, achyranthes bidentata extract, native seven extracts and Herba speranskiae tuberculatae extract.
2. according to claim 1 a kind of for the regenerated Moringa compound Essence of cell repair, it is characterised in that: described Solvent be one of water, methanol, ethyl alcohol, isopropanol, n-butanol, ethylene glycol, acetoneand ethyl acetate.
3. according to claim 1 a kind of for the regenerated Moringa compound Essence of cell repair, it is characterised in that: described Seed oil of Moringa oleigera be prepared by the following method: weigh 100g moringa seeds benevolence, be put into pulverizer crushing, cross 10 meshes, put reflux into Pure petroleum ether circumfluence distillation 2-5 times of 500mL analysis is added in extractor, and extracting solution is merged, is put into after suction filtration by each 2-6h 50-80 DEG C, the vacuum oven of 0.05-0.15MPa is concentrated 12-24 hours, obtains seed oil of Moringa oleigera.
4. according to claim 1 a kind of for the regenerated Moringa compound Essence of cell repair, it is characterised in that: described Be 77.66-100% to the antibiotic rate of staphylococcus aureus for the regenerated Moringa compound Essence of cell repair, to big The antibiotic rate of enterobacteria is 75.81-91.65%, and the antibiotic rate to Candida albicans is 85.64-100%, to Pseudomonas aeruginosa Antibiotic rate is 84.99-100%.
5. a kind of system for the regenerated Moringa compound Essence of cell repair described in any one of -4 according to claim 1 Preparation Method, it is characterised in that: specific steps are as follows:
Successively by load weighted moringa oleifera leaf extractive, seed oil of Moringa oleigera, native seven extracts, Folium Artemisiae Argyi extract, achyranthes bidentata extract, deep Careless extract, glycerol, glycerin monostearate, triethanolamine, 1,3-BDO, lactic acid and pure water are put into emulsion pot, 60 DEG C are warming up to, turn on agitator is stirred 40 minutes with the speed of 100r/min, is subsequently placed into hyaluronic acid and collagen, Stirring after twenty minutes, is cooled to 45 DEG C while stirring, finally puts into essential oil and preservative, and stirring can be prepared by being used for after ten minutes The regenerated Moringa compound Essence of cell repair.
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CN105434233A (en) * 2015-12-08 2016-03-30 广州市花安堂生物科技有限公司 Keratin repair essence and preparation method thereof

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