CN107569420B - Faint scent type bath powder containing peony and preparation method and application thereof - Google Patents
Faint scent type bath powder containing peony and preparation method and application thereof Download PDFInfo
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Abstract
The prepared fragrant bath powder containing the peony adopts a pure natural formula, takes the fragrant variety of the peony as the main material, and scientifically compounds various raw materials, fully utilizes the cooperativity and compatibility of the raw materials, and completely solves the stability problem of the product formula, is not only suitable for body bath, but also suitable for hand bath and foot bath, can bring the effects of refreshing body, cleaning skin, dredging channels and collaterals, sterilizing, eliminating dampness, aromatic body beautifying, regulating blood fat, stabilizing blood pressure, expelling toxin, nourishing skin, delaying senescence, improving human body immunity and the like, and is particularly suitable for skin pruritus patients.
Description
Technical Field
The invention relates to a bath agent, in particular to a faint scent bath powder containing peony and a preparation method and application thereof.
Background
The deciduous shrubs of Paeonia of Ranunculaceae have high ornamental value and medical value, and the development and utilization of deep-processed products of Paeonia appears to be seriously lagged for a long time, the production added value is very low, and no industrial chain is formed. The results of chemical measurements adopted by the Chinese academy of sciences show that the peony petals, pistils and pollen contain 8 amino acids, vitamins, saccharides and flavonoids which are necessary for human bodies, and also contain various enzymes, 7 macroelements and 5 trace elements which are necessary for human bodies, and have the effects of preventing cancers, resisting cancers, regulating blood fat, stabilizing blood pressure, expelling toxin, beautifying, delaying senescence, improving the immunity of human bodies and the like.
Shower gel and bath powder have become the most commonly used daily necessities in people's daily life gradually, the consumption is the biggest, along with the improvement of people's standard of living, people also are more and more high to the requirement of bathing product, at present, the shower product that is common on the market, most contain more chemical composition, frequent use, can destroy skin moisture balance, cause skin lack of water, ageing scheduling problem, long-term use, be unfavorable for people's skin health, and the pure natural shower product kind on the market is rare now, the variety is single, and is expensive, the skin care effect is not showing prominently.
Disclosure of Invention
The invention provides a faint scent bath powder containing peony and a preparation method and application thereof.
The invention adopts the technical scheme that the peony-containing faint scent bath powder is prepared from 28-36 parts by weight of peony, 4-12 parts by weight of dutchmanspipe root, 4-12 parts by weight of rose, 4-12 parts by weight of jasmine, 12-20 parts by weight of garden balsam stem, 2-9 parts by weight of magnolia flower and 2-9 parts by weight of cacumen biotae, and the auxiliary materials are β -cyclodextrin and purified water.
The faint scent bath powder containing peony is prepared from the following main materials in parts by weight: 32 parts of peony, 8 parts of dutchmanspipe root, 8 parts of rose, 8 parts of jasmine flower, 16 parts of garden balsam stem, 8 parts of magnolia flower and 8 parts of cacumen biotae.
The method for preparing the faint scent bath powder containing peony provided by the invention comprises the following steps:
step one, weighing the raw materials according to the parts by weight;
step two, drying the weighed aristolochia debilis in a vacuum freeze drying box at the temperature of-40 to-25 ℃ until the water content is 6 to 10 percent, then crushing and sieving the dried aristolochia debilis with a sieve of 200 meshes, and then extracting by adopting a supercritical CO2 fluid extraction technology to obtain the aristolochia debilis extract oil for later use;
removing impurities from the weighed peony, rose, jasmine and magnolia flowers, cleaning the peony, rose, jasmine and magnolia flowers with clear water, adding an ethanol solution with the mass concentration of 70% to soak for 1-5 hours, filtering filtrate, quickly dehydrating and drying petals with a microwave dryer to obtain dry petals, adding the dry petals into the aristolochia debilis extraction oil prepared by the second extraction step with the weight part of 5-10 times of that of the aristolochia debilis extraction oil, stirring to ensure that the dry petals are fully contacted with the aristolochia debilis extraction oil, standing for 24-72 hours, and then performing ultrasonic extraction for 2-4 hours at the temperature of 40-50 ℃ to obtain mixed extraction oil for later use;
placing β -cyclodextrin into a conical flask, adding purified water, heating in a water bath to dissolve β -cyclodextrin, cooling β -cyclodextrin solution to 40 ℃, stirring at constant temperature for 30-40min, injecting the mixed extract oil obtained in the step three into β -cyclodextrin solution, continuously stirring at constant temperature for 2-4h, refrigerating for 12-24h in a refrigerator, taking out, filtering to obtain oil solid powder, washing the oil solid powder with purified water, drying at low temperature of 55-65 ℃ for 12-18h, taking out the dried product, crushing, and sieving with a 150-mesh sieve with 200 meshes to obtain β -cyclodextrin inclusion extract oil solid powder, wherein the weight ratio of the mixed extract oil, β -cyclodextrin and the purified water is β -cyclodextrin, and the weight ratio of purified water is 1: 6: 60;
step five, cleaning, airing and slicing the weighed garden balsam stems and Chinese arborvitae twig, irradiating 25-35s to 1m under a 25-30W disinfection lamp for ultraviolet sterilization, then drying and crushing the garden balsam stems and Chinese arborvitae twig into coarse powder, adding 8-12 times of ethanol with the concentration of 60-70% of the coarse powder for soaking for 12-18h, ultrasonically extracting for 30-35min at the ultrasonic temperature of 30-32 ℃ and the ultrasonic power of 75-85W for three times, combining the three extracting solutions and concentrating the extracting solutions under reduced pressure, placing the concentrated solution in a refrigerator at 4 ℃ for 48-60h, performing suction filtration to obtain a concentrated solution with part of pigment precipitates filtered, then concentrating the concentrated solution to the relative density of 1.31-1.34 at the temperature of 80 ℃, then drying under reduced pressure, crushing and sieving the concentrated solution through a 1800-mesh sieve 2000 sieve to obtain mixed superfine powder for later use;
and step six, uniformly mixing the β -cyclodextrin inclusion extract oil solid powder prepared in the step four and the mixed superfine powder prepared in the step five, and packaging to obtain the faint scent bath powder containing the peony.
As a preferable scheme, the extraction pressure of the supercritical CO2 fluid extraction in the second step is 25-35MPa, the extraction temperature is 50-65 ℃, and the extraction time is 5-7 h.
Preferably, the faint scent bath powder containing peony prepared in the sixth step is packaged according to the specification of 100-150g per bag and 20 bags per box.
As a preferred scheme, the peony is fragrant jade peony.
Preferably, the bath powder is used for local bath or whole body bath, the local bath is hand bath, foot bath, hip bath, basin bath or half body bath, the whole body bath is an indoor bath or a medium-small swimming pool, the water temperature is set to be 38-40 ℃ when bathing, 100g of bath powder is used by men when bathing the whole body, 150g of bath powder is used by women when bathing the whole body for 15-25min, and 15-30g of bath powder is used by local bath for 5-15 min.
The peony has high ornamental value and medical value, and the chemical measurement results adopted by Chinese academy of sciences show that peony petals, pistils and pollen contain 8 amino acids, vitamins, saccharides and flavonoids which are necessary for human bodies, and also contain enzymes, 7 macroelements and 5 trace elements which are necessary for human bodies, and has the effects of preventing and resisting cancers, regulating blood fat, stabilizing blood pressure, expelling toxin, beautifying, delaying senescence, improving human immunity and the like.
The peony is the most fragrant variety of all peonies, has elegant and luxurious flower fragrance with mysterious and strong fragrance, and gives people a wonderful feeling.
The birthwort root has special aroma and bitter taste, can improve the oxidation resistance of skin, has the functions of mildness and faint scent, has different degrees of inhibiting bacillus such as staphylococcus aureus, pyocyanea, large intestine, deformation and the like, can improve the immunity, and also has the anticancer function.
Rose flower, pungent and sweet in flavor, warm in nature, enters liver and spleen meridians. Has effects of regulating qi-flowing, resolving stagnation, eliminating dampness, regulating stomach, promoting blood circulation, removing blood stasis, regulating menstruation and relieving pain, and can be used for treating incoordination between liver and stomach, menoxenia, blood stasis swelling pain, hematemesis hemoptysis, carbuncle swelling or acute mastitis. In addition, the rose is very mild in drug property, can warm and nourish heart, liver and blood vessels of people, soothes depression in the body, and has the effects of calming, soothing and resisting depression.
The jasmine flower has strong fragrance, is charming, sweet and mellow, and can calm mood and eliminate nervous tension. The white petals contain various organic matters, vitamins, sugar, starch and other nutrient elements beneficial to human bodies, can be used in cosmetics to condition dry skin, has the effects of beautifying the skin, building bodies, refreshing, resisting aging and resisting aging, and is an ideal good beauty product.
The garden balsam stem, the part used as the medicine, is the whole plant, has the efficacies of promoting blood circulation by removing blood stasis, promoting urination and removing toxicity, and dredging channels and penetrating bones, and also has one of the important efficacies of oxidation resistance.
Flos Magnoliae has the effect of dispelling wind cold, is also a rare spice and chemical material, and contains a large amount of volatile oil with aromatic smell.
The cacumen biotae can eliminate harmful free radicals, inhibit pigmentation, deeply moisten skin, cool blood, stop bleeding, expel wind-damp and dissipate toxic swelling.
Compared with the prior art, the invention has the following beneficial effects:
(1) the invention provides a faint scent bath powder containing peony and a preparation method and application thereof, the bath powder adopts a pure natural formula, the fragrant variety of peony in peony is taken as a main material, multiple raw materials are carefully selected for scientific compounding, the cooperativity and compatibility of the raw materials are fully utilized, the stability problem of the product formula is perfectly solved, the bath powder is not only suitable for a whole body bath, but also suitable for a hand bath and foot bath, and has the effects of refreshing body, cleaning skin, dredging channels and collaterals, sterilizing, eliminating dampness, perfuming body, regulating blood fat, stabilizing blood pressure, expelling toxin, beautifying, delaying senescence, improving human immunity and the like, and is particularly suitable for patients with skin pruritus;
(2) according to the invention, a large amount of volatile oil components in the dutchmanspipe root are subjected to supercritical extraction to obtain the extracted oil, the yield of the volatile oil components is improved to the maximum extent on the premise of not damaging the volatile oil components, the dutchmanspipe root can improve the oxidation resistance of skin and has the effects of being mild and fragrant, and the volatile oil components in the dutchmanspipe root play a non-negligible role in the aspect of exerting the drug effects of the dutchmanspipe root, so that the application range of the dutchmanspipe root is expanded, and the commercial value of the dutchmanspipe root is also improved;
(3) the extraction and separation processes are carried out at normal temperature or low temperature, low boiling point substances in the raw materials can be guaranteed not to be damaged, effective ingredients in the raw materials can be better protected, β -cyclodextrin is utilized to include the volatile oil, the fragrance of the aromatic plants can be prevented from being too strong, the solid powder of the liquid volatile oil can be made into powder, the stability is improved, and the drug effect can be favorably exerted;
(4) the invention provides a faint scent type bath powder containing peony and a preparation method and application thereof, wherein garden balsam stem and Chinese arborvitae twig are treated to filter out pigment precipitates, so that the phenomenon that the bath powder enters wounds to cause the pigment precipitates when the bath powder is used for scar skin is avoided, and meanwhile, the faint scent type bath powder can improve skin metabolism, promote skin blood circulation, increase skin nutrition, effectively remove free radicals, eliminate the pigment precipitates, is high in antioxidant activity and long in storage time; the ultrafine powder is crushed into ultrafine powder, and the ultrafine powder after ultrafine crushing can reach the nanometer level, is beneficial to the mutual matching of all raw materials, has small particle diameter, can directly permeate into the human body through the skin, and greatly improves the physiological action.
Detailed Description
The present invention is described in detail with reference to the following embodiments, which are provided in the present invention as a premise of the technical solution of the present invention, and the detailed implementation manner and the specific operation process are provided in the present embodiment.
The faint scent bath powder is prepared from 28-36 parts by weight of peony, 4-12 parts by weight of dutchmanspipe root, 4-12 parts by weight of rose, 4-12 parts by weight of jasmine flower, 12-20 parts by weight of garden balsam stem, 2-9 parts by weight of magnolia flower and 2-9 parts by weight of cacumen biotae, and the auxiliary material is prepared from β -cyclodextrin and purified water.
The faint scent bath powder containing peony is prepared from the following main materials in parts by weight: 32 parts of peony, 8 parts of dutchmanspipe root, 8 parts of rose, 8 parts of jasmine flower, 16 parts of garden balsam stem, 8 parts of magnolia flower and 8 parts of cacumen biotae.
The method for preparing the faint scent bath powder containing peony provided by the invention comprises the following steps:
step one, weighing the raw materials according to the parts by weight;
step two, drying the weighed aristolochia debilis in a vacuum freeze drying box at the temperature of-40 to-25 ℃ until the water content is 6 to 10 percent, then crushing and sieving the dried aristolochia debilis with a sieve of 150 meshes and 200 meshes, and then extracting the aristolochia debilis extract oil by adopting a supercritical CO2 fluid extraction technology, wherein the extraction pressure of the supercritical CO2 fluid extraction is 25 to 35MPa, the extraction temperature is 50 to 65 ℃, and the extraction time is 5 to 7 hours for later use;
removing impurities from the weighed peony, rose, jasmine and magnolia flowers, cleaning the peony, rose, jasmine and magnolia flowers with clear water, adding an ethanol solution with the mass concentration of 70% to soak for 1-5 hours, filtering filtrate, quickly dehydrating and drying petals with a microwave dryer to obtain dry petals, adding the dry petals into the aristolochia debilis extraction oil prepared by the second extraction step with the weight part of 5-10 times of that of the aristolochia debilis extraction oil, stirring to ensure that the dry petals are fully contacted with the aristolochia debilis extraction oil, standing for 24-72 hours, and then performing ultrasonic extraction for 2-4 hours at the temperature of 40-50 ℃ to obtain mixed extraction oil for later use;
placing β -cyclodextrin into a conical flask, adding purified water, heating in a water bath to dissolve β -cyclodextrin, cooling β -cyclodextrin solution to 40 ℃, stirring at constant temperature for 30-40min, injecting the mixed extract oil obtained in the step three into β -cyclodextrin solution, continuously stirring at constant temperature for 2-4h, refrigerating for 12-24h in a refrigerator, taking out, filtering to obtain oil solid powder, washing the oil solid powder with purified water, drying at low temperature of 55-65 ℃ for 12-18h, taking out the dried product, crushing, and sieving with a 150-mesh sieve with 200 meshes to obtain β -cyclodextrin inclusion extract oil solid powder, wherein the weight ratio of the mixed extract oil, β -cyclodextrin and the purified water is β -cyclodextrin, and the weight ratio of purified water is 1: 6: 60;
step five, cleaning, airing and slicing the weighed garden balsam stems and Chinese arborvitae twig, irradiating 25-35s to 1m under a 25-30W disinfection lamp for ultraviolet sterilization, then drying and crushing the garden balsam stems and Chinese arborvitae twig into coarse powder, adding 8-12 times of ethanol with the concentration of 60-70% of the coarse powder for soaking for 12-18h, ultrasonically extracting for 30-35min at the ultrasonic temperature of 30-32 ℃ and the ultrasonic power of 75-85W for three times, combining the three extracting solutions and concentrating the extracting solutions under reduced pressure, placing the concentrated solution in a refrigerator at 4 ℃ for 48-60h, performing suction filtration to obtain a concentrated solution with part of pigment precipitates filtered, then concentrating the concentrated solution to the relative density of 1.31-1.34 at the temperature of 80 ℃, then drying under reduced pressure, crushing and sieving the concentrated solution through a 1800-mesh sieve 2000 sieve to obtain mixed superfine powder for later use;
step six, evenly mixing the β -cyclodextrin inclusion extraction oil solid powder prepared in the step four and the mixed superfine powder prepared in the step five, and then packaging and packaging the mixture according to the specification of 100 g/bag and 150 g/box and 20 bags/box to obtain the faint scent type bath powder containing the peony.
As a preferred scheme, the peony is fragrant jade peony.
Preferably, the bath powder is used for local bath or whole body bath, the local bath is hand bath, foot bath, hip bath, basin bath or half body bath, the whole body bath is an indoor bath or a medium-small swimming pool, the water temperature is set to be 38-40 ℃ when bathing, 100g of bath powder is used by men when bathing the whole body, 150g of bath powder is used by women when bathing the whole body for 15-25min, and 15-30g of bath powder is used by local bath for 5-15 min.
Example one
The peony-containing faint scent bath powder is prepared from 28 parts by weight of peony, 4 parts by weight of dutchmanspipe root, 4 parts by weight of rose, 4 parts by weight of jasmine, 12 parts by weight of garden balsam stem, 2 parts by weight of magnolia flower and 2 parts by weight of cacumen biotae, and the auxiliary materials are β -cyclodextrin and purified water.
The method for preparing the faint scent bath powder containing peony provided by the invention comprises the following steps:
step one, weighing the raw materials according to the parts by weight;
step two, drying the weighed aristolochia debilis in a vacuum freeze drying oven at the temperature of-40 ℃ until the water content is 6%, then crushing and sieving by a 150-mesh sieve, and then extracting by adopting a supercritical CO2 fluid extraction technology to obtain the aristolochia debilis extract oil, wherein the extraction pressure of the supercritical CO2 fluid extraction is 25MPa, the extraction temperature is 50 ℃, and the extraction time is 5 hours for later use;
removing impurities from the weighed peony, rose, jasmine and magnolia flowers, cleaning the peony, rose, jasmine and magnolia flowers with clear water, adding an ethanol solution with the mass concentration of 70% to soak for 1 hour, filtering filtrate, quickly dehydrating and drying the petals with a microwave dryer to obtain dry petals, adding the dry petals into the aristolochia debilis extraction oil prepared by the extraction in the step two with the weight part of 5 times of that of the dried petals, stirring to ensure that the dry petals are fully contacted with the aristolochia debilis extraction oil, standing for 24 hours, and then performing ultrasonic extraction for 2 hours at the temperature of 40 ℃ to obtain mixed extraction oil for later use;
step four, placing β -cyclodextrin into a conical flask, adding purified water, heating in a water bath to dissolve β -cyclodextrin, cooling β -cyclodextrin solution to 40 ℃, stirring at a constant temperature for 30min, injecting the mixed extract oil obtained in the step three into β -cyclodextrin solution, continuously stirring at a constant temperature for 2h, refrigerating in a refrigerator for 12h, taking out, filtering to obtain oil solid powder, washing the oil solid powder with purified water, drying at a low temperature of 55 ℃ for 12h, taking out the dried product, crushing, and sieving with a 150-mesh sieve to obtain β -cyclodextrin inclusion extract oil solid powder, wherein the mixed extract oil, β -cyclodextrin and the purified water are mixed extract oil, namely β -cyclodextrin and purified water, in a weight ratio of 1: 6: 60;
step five, cleaning and airing weighed garden balsam stems and Chinese arborvitae twig, slicing, irradiating 25s away from a position of 1m under a 25W disinfection lamp for ultraviolet sterilization, drying and crushing to obtain coarse powder, adding 8 times of 60% ethanol of the coarse powder for soaking for 12h, ultrasonically extracting for 30min at the ultrasonic temperature of 30 ℃ and the ultrasonic power of 75W for three times, combining the three extracting solutions, decompressing and concentrating, placing the concentrated solution in a refrigerator at 4 ℃ for 48h, filtering to obtain a concentrated solution with part of pigment precipitates filtered out, concentrating to the relative density of 1.31 at 80 ℃, decompressing and drying, crushing and sieving by a 1800-mesh sieve to obtain mixed superfine powder for later use;
step six, evenly mixing the β -cyclodextrin inclusion extraction oil solid powder prepared in the step four and the mixed superfine powder prepared in the step five, and then packaging and packaging the mixture according to the specification of 100g per bag and 20 bags per box to obtain the faint scent type bath powder containing the peony.
Preferably, the bath powder is used for a local bath or a whole body bath, wherein the local bath is a hand bath, a foot bath, a hip bath, a basin bath or a half body bath, the whole body bath is an indoor bath or a medium-small swimming pool, the water temperature is set at 38 ℃ during bath, 100g of the bath powder is used for men during the whole body bath, 150g of the bath powder is used for bathing for women for 15min, and 15g of the bath powder is used for the local bath for 5 min.
Example two
The peony-containing faint scent bath powder is prepared from main materials and auxiliary materials, wherein the main materials comprise, by weight, 36 parts of peony, 12 parts of dutchmanspipe root, 12 parts of rose, 12 parts of jasmine, 20 parts of garden balsam stem, 9 parts of magnolia flower and 9 parts of cacumen biotae, and the auxiliary materials comprise β -cyclodextrin and purified water.
The method for preparing the faint scent bath powder containing peony provided by the invention comprises the following steps:
step one, weighing the raw materials according to the parts by weight;
step two, drying the weighed aristolochia debilis in a vacuum freeze drying oven at the temperature of-25 ℃ until the water content is 10%, then crushing and sieving by a 200-mesh sieve, and then extracting by adopting a supercritical CO2 fluid extraction technology to obtain the aristolochia debilis extract oil, wherein the extraction pressure of the supercritical CO2 fluid extraction is 35MPa, the extraction temperature is 65 ℃, and the extraction time is 7 hours for later use;
removing impurities from the weighed peony, rose, jasmine and magnolia flowers, cleaning the peony, rose, jasmine and magnolia flowers with clear water, adding an ethanol solution with the mass concentration of 70% to soak for 5 hours, filtering filtrate, quickly dehydrating and drying the petals with a microwave dryer to obtain dry petals, adding the dry petals into the aristolochia debilis extraction oil prepared by the extraction in the step two with the weight part of 10 times of that of the dried petals, stirring to ensure that the dry petals are fully contacted with the aristolochia debilis extraction oil, standing for 72 hours, and then performing ultrasonic extraction at the temperature of 50 ℃ for 4 hours to obtain mixed extraction oil for later use;
step four, placing β -cyclodextrin into a conical flask, adding purified water, heating in a water bath to dissolve β -cyclodextrin, cooling β -cyclodextrin solution to 40 ℃, stirring at a constant temperature for 40min, injecting the mixed extract oil obtained in the step three into β -cyclodextrin solution, continuously stirring at a constant temperature for 4h, refrigerating in a refrigerator for 24h, taking out, filtering to obtain oil solid powder, washing the oil solid powder with purified water, drying at a low temperature of 65 ℃ for 18h, taking out the dried product, crushing, and sieving with a 200-mesh sieve to obtain β -cyclodextrin inclusion extract oil solid powder, wherein the mixed extract oil, β -cyclodextrin and the purified water are mixed extract oil, namely β -cyclodextrin and purified water, in a weight ratio of 1: 6: 60;
step five, cleaning and airing weighed garden balsam stems and Chinese arborvitae twig, slicing, irradiating for 35s under a 30W disinfection lamp at a distance of 1m for ultraviolet sterilization, drying and crushing into coarse powder, adding 12 times of 70% ethanol of the coarse powder for soaking for 18h, ultrasonically extracting for 35min at the ultrasonic temperature of 32 ℃ and the ultrasonic power of 85W for three times, combining the three extracting solutions, decompressing and concentrating, placing the concentrated solution in a refrigerator at 4 ℃ for 60h, filtering to obtain a concentrated solution with part of pigment precipitates filtered out, concentrating to the relative density of 1.34 at 80 ℃, decompressing and drying, crushing and sieving by a 2000-mesh sieve to obtain mixed fine powder for later use;
step six, evenly mixing the β -cyclodextrin inclusion extraction oil solid powder prepared in the step four and the mixed superfine powder prepared in the step five, and then packaging and packaging the mixture according to the specification of 150g per bag and 20 packets per box to obtain the faint scent type bath powder containing the peony.
Preferably, the bath powder is used for a local bath or a whole body bath, wherein the local bath is a hand bath, a foot bath, a hip bath, a basin bath or a half body bath, the whole body bath is an indoor bath or a medium-small swimming pool, the water temperature is set at 40 ℃ during bath, 100g of the bath powder is used for men during the whole body bath, 150g of the bath powder is used for the women during the bath, and 30g of the bath powder is used for the local bath for 15 min.
EXAMPLE III
The peony-containing faint scent bath powder is prepared from a main material and an auxiliary material, wherein the main material comprises, by weight, 34 parts of peony, 10 parts of dutchmanspipe root, 10 parts of rose, 10 parts of jasmine, 18 parts of garden balsam stem, 7 parts of magnolia flower and 7 parts of cacumen biotae, and the auxiliary material comprises β -cyclodextrin and purified water.
The method for preparing the faint scent bath powder containing peony provided by the invention comprises the following steps:
step one, weighing the raw materials according to the parts by weight;
step two, drying the weighed aristolochia debilis in a vacuum freeze drying oven at the temperature of-30 ℃ until the water content is 8%, then crushing and sieving by a 180-mesh sieve, and then extracting by adopting a supercritical CO2 fluid extraction technology to obtain the aristolochia debilis extract oil, wherein the extraction pressure of the supercritical CO2 fluid extraction is 30MPa, the extraction temperature is 60 ℃, and the extraction time is 6 hours for later use;
removing impurities from the weighed peony, rose, jasmine and magnolia flowers, cleaning the peony, rose, jasmine and magnolia flowers with clear water, adding an ethanol solution with the mass concentration of 70% to soak for 3 hours, filtering filtrate, quickly dehydrating and drying the petals with a microwave dryer to obtain dry petals, adding the dry petals into the aristolochia debilis extraction oil prepared by the second extraction step with the weight part of 8 times of that of the dried petals, stirring to fully contact the dry petals with the aristolochia debilis extraction oil, standing for 48 hours, and performing ultrasonic extraction for 3 hours at the temperature of 45 ℃ to obtain mixed extraction oil for later use;
step four, placing β -cyclodextrin into a conical flask, adding purified water, heating in a water bath to dissolve β -cyclodextrin, cooling β -cyclodextrin solution to 40 ℃, stirring at a constant temperature for 35min, injecting the mixed extract oil obtained in the step three into β -cyclodextrin solution, continuously stirring at a constant temperature for 3h, refrigerating in a refrigerator for 18h, taking out, filtering to obtain oil solid powder, washing the oil solid powder with purified water, drying at a low temperature of 60 ℃ for 15h, taking out the dried product, crushing, and sieving with a sieve of 180 meshes to obtain β -cyclodextrin inclusion extract oil solid powder, wherein the mixed extract oil, β -cyclodextrin and the purified water are mixed extract oil, namely β -cyclodextrin and purified water, in a weight ratio of 1: 6: 60;
step five, cleaning and airing weighed garden balsam stems and Chinese arborvitae twig, slicing, irradiating 30s of the slices at a position 1m away from a 28W disinfection lamp for ultraviolet sterilization, drying and crushing the slices into coarse powder, adding ethanol with the concentration of 65% which is 10 times of the coarse powder, soaking the coarse powder for 15h, carrying out ultrasonic extraction for 32min at the ultrasonic temperature of 31 ℃ and the ultrasonic power of 80W, carrying out ultrasonic extraction for three times, combining the three extracting solutions, carrying out reduced pressure concentration, placing the concentrated solution in a refrigerator at the temperature of 4 ℃ for 55h, carrying out suction filtration to obtain a concentrated solution with part of pigment precipitates filtered out, then concentrating the concentrated solution to the relative density of 1.31-1.34 at the temperature of 80 ℃, then carrying out reduced pressure drying, crushing and sieving by a 1800-mesh sieve to obtain mixed;
step six, evenly mixing the β -cyclodextrin inclusion extraction oil solid powder prepared in the step four and the mixed superfine powder prepared in the step five, and then packaging and packaging the mixture according to the specification of 120g per bag and 20 bags per box to obtain the faint scent type bath powder containing the peony.
Preferably, the bath powder is used for local bath or whole body bath, the local bath is hand bath, foot bath, hip bath, basin bath or half body bath, the whole body bath is an indoor bath or a medium-small swimming pool, the water temperature is set to be 38-40 ℃ when bathing, 100g of bath powder is used by men when bathing the whole body, 150g of bath powder is used by women when bathing the whole body for 15-25min, and 15-30g of bath powder is used by local bath for 5-15 min.
Experimental study data
The application effect of the faint scent bath powder containing peony prepared by the preparation method is evaluated. The test population: 300 subjects with 18-60 years old no-heritage medical history are selected, the specific sex composition and age composition are randomly determined, the improvement condition of the skin itch condition of the subjects after use is recorded, 100 subjects in group 1, group 2 and group 3 respectively use the faint scent type bath powder containing peony flowers prepared in example 1, example 2 and example 3. Using the composition 2-3 times per week, and evaluating the effect of the composition on a subject who is continuously used for 1 month, wherein the evaluation criteria of the effect comprise cure, effectiveness and ineffectiveness, the cure is disappearance of skin pruritus symptoms, and no recurrence is caused within 1 year; the effect is that the skin itch is improved to a certain extent, and is basically improved, but still needs to be consolidated; the ineffectiveness is no improvement of skin itch, and other treatment modes are required, and the results are shown in table 1:
as can be seen from Table 1, the bath powder has remarkable curative effect on the skin itch problem, most of the skin itch problems can be effectively solved after any one of the examples 1-3 of the invention is continuously used for 1 month, the problems of pimple, dry skin and the like are gradually improved, and clinical verification shows that the cure and effective rate of the bath powder prepared by the formula of the invention for treating the skin itch is as high as 97.7%.
Although the present invention has been described with reference to the preferred embodiments, it is not intended to be limited to the embodiments, and various changes and modifications can be made by one skilled in the art without departing from the scope of the invention.
Claims (6)
1. The faint scent bath powder containing the peony is characterized by being prepared from main materials and auxiliary materials, wherein the main materials comprise, by weight, 28-36 parts of the peony, 4-12 parts of dutchmanspipe root, 4-12 parts of rose, 4-12 parts of jasmine flower, 12-20 parts of garden balsam stem, 2-9 parts of biond magnolia flower and 2-9 parts of cacumen biotae, and the auxiliary materials comprise β -cyclodextrin and purified water;
the preparation method of the bath powder comprises the following steps:
step one, weighing the raw materials according to the parts by weight;
step two, drying the weighed aristolochia debilis in a vacuum freeze drying box at the temperature of-40 to-25 ℃ until the water content is 6 to 10 percent, then crushing and sieving the dried aristolochia debilis with a sieve of 200 meshes, and then extracting by adopting a supercritical CO2 fluid extraction technology to obtain the aristolochia debilis extract oil for later use;
removing impurities from the weighed peony, rose, jasmine and magnolia flowers, cleaning the peony, rose, jasmine and magnolia flowers with clear water, adding an ethanol solution with the mass concentration of 70% to soak for 1-5 hours, filtering filtrate, quickly dehydrating and drying petals with a microwave dryer to obtain dry petals, adding the dry petals into the aristolochia debilis extraction oil prepared by the second extraction step with the weight part of 5-10 times of that of the aristolochia debilis extraction oil, stirring to ensure that the dry petals are fully contacted with the aristolochia debilis extraction oil, standing for 24-72 hours, and then performing ultrasonic extraction for 2-4 hours at the temperature of 40-50 ℃ to obtain mixed extraction oil for later use;
placing β -cyclodextrin into a conical flask, adding purified water, heating in a water bath to dissolve β -cyclodextrin, cooling β -cyclodextrin solution to 40 ℃, stirring at constant temperature for 30-40min, injecting the mixed extract oil obtained in the step three into β -cyclodextrin solution, continuously stirring at constant temperature for 2-4h, refrigerating for 12-24h in a refrigerator, taking out, filtering to obtain oil solid powder, washing the oil solid powder with purified water, drying at low temperature of 55-65 ℃ for 12-18h, taking out the dried product, crushing, and sieving with a 150-mesh sieve with 200 meshes to obtain β -cyclodextrin inclusion extract oil solid powder, wherein the weight ratio of the mixed extract oil, β -cyclodextrin and the purified water is β -cyclodextrin, and the weight ratio of purified water is 1: 6: 60;
step five, cleaning, airing and slicing the weighed garden balsam stems and Chinese arborvitae twig, irradiating 25-35s to 1m under a 25-30W disinfection lamp for ultraviolet sterilization, then drying and crushing the garden balsam stems and Chinese arborvitae twig into coarse powder, adding 8-12 times of ethanol with the concentration of 60-70% of the coarse powder for soaking for 12-18h, ultrasonically extracting for 30-35min at the ultrasonic temperature of 30-32 ℃ and the ultrasonic power of 75-85W for three times, combining the three extracting solutions and concentrating the extracting solutions under reduced pressure, placing the concentrated solution in a refrigerator at 4 ℃ for 48-60h, performing suction filtration to obtain a concentrated solution with part of pigment precipitates filtered, then concentrating the concentrated solution to the relative density of 1.31-1.34 at the temperature of 80 ℃, then drying under reduced pressure, crushing and sieving the concentrated solution through a 1800-mesh sieve 2000 sieve to obtain mixed superfine powder for later use;
and step six, uniformly mixing the β -cyclodextrin inclusion extract oil solid powder prepared in the step four and the mixed superfine powder prepared in the step five, and packaging to obtain the faint scent bath powder containing the peony.
2. The peony-containing fen-flavor bath powder as claimed in claim 1, wherein: the bath powder is prepared from the following main materials in parts by weight: 32 parts of peony, 8 parts of dutchmanspipe root, 8 parts of rose, 8 parts of jasmine flower, 16 parts of garden balsam stem, 8 parts of magnolia flower and 8 parts of cacumen biotae.
3. The peony-containing fen-flavor bath powder as claimed in claim 1, wherein: and the supercritical CO2 fluid extraction in the second step has the extraction pressure of 25-35MPa, the extraction temperature of 50-65 ℃ and the extraction time of 5-7 h.
4. The peony-containing fen-flavor bath powder as claimed in claim 1, wherein: and sixthly, packaging the prepared faint scent type bath powder containing the peony in the specification of 100-150g per bag and 20 bags per box.
5. The peony-containing fen-flavor bath powder as claimed in claim 1, wherein: the peony is fragrant jade peony.
6. The application of the peony-containing fen-flavor bath powder as claimed in claim 1, wherein the peony-containing fen-flavor bath powder comprises the following components: the bath powder is used for local bath or whole body bath, wherein the local bath is hand bath, foot bath, hip bath, basin bath or half body bath, the whole body bath is indoor bath or middle and small swimming pool, the water temperature is 38-40 deg.C, the bath powder is used for 15-25min for male when the bath is carried out on the whole body, the bath powder is used for 150g for female when the bath is carried out on the whole body, and the bath powder is used for 15-30g for the local bath and the bath is carried out on the half body for 5-15 min.
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| CN113575617B (en) * | 2021-09-22 | 2022-06-21 | 宁夏农林科学院植物保护研究所（宁夏植物病虫害防治重点实验室） | Application of costus root in biological control, biological control medicament and preparation method thereof |
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| CN1255330A (en) * | 1998-11-30 | 2000-06-07 | 刘玉仁 | Health-care lotion for foot bath |
| CN101422551A (en) * | 2007-10-29 | 2009-05-06 | 吉楠 | Traditional Chinese medicine body scenting and building liquid |
| CN104172155A (en) * | 2014-07-07 | 2014-12-03 | 李�杰 | Ultra-micro peony flower powder as well as preparation method and application thereof |
| CN104248544A (en) * | 2013-06-26 | 2014-12-31 | 昆山鹿康贸易有限公司 | Beauty-treatment herbal medicine formula |
| CN105168261A (en) * | 2015-09-30 | 2015-12-23 | 河南行知专利服务有限公司 | Preparation method of aromatic decocting-free traditional Chinese medicine agent |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1255330A (en) * | 1998-11-30 | 2000-06-07 | 刘玉仁 | Health-care lotion for foot bath |
| CN101422551A (en) * | 2007-10-29 | 2009-05-06 | 吉楠 | Traditional Chinese medicine body scenting and building liquid |
| CN104248544A (en) * | 2013-06-26 | 2014-12-31 | 昆山鹿康贸易有限公司 | Beauty-treatment herbal medicine formula |
| CN104172155A (en) * | 2014-07-07 | 2014-12-03 | 李�杰 | Ultra-micro peony flower powder as well as preparation method and application thereof |
| CN105168261A (en) * | 2015-09-30 | 2015-12-23 | 河南行知专利服务有限公司 | Preparation method of aromatic decocting-free traditional Chinese medicine agent |
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