CN107569420A - A kind of delicate fragrance type shower powder containing peony and its preparation method and application - Google Patents
A kind of delicate fragrance type shower powder containing peony and its preparation method and application Download PDFInfo
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Abstract
A kind of delicate fragrance type shower powder containing peony, the shower powder is made up of major ingredient and auxiliary material, according to parts by weight, the major ingredient is made up of 29 parts of 28 36 parts of peony, 4 12 parts of dutchmanspipe root, 4 12 parts of rose, 4 12 parts of Jasmine, 12 20 parts of lopseed, 29 parts of the flower bud of lily magnolia and cacumen biotae, and the auxiliary material is made up of beta cyclodextrin and purified water.Delicate fragrance type shower powder containing peony prepared by the present invention, using pure natural formula, using the fragrant beautiful peony of kind most fragrant in tree peony as major ingredient, selected plurality of raw materials carries out science compounding, take full advantage of the concertedness and compatibility of each raw material, the stability problem of product formula is set to have obtained perfect solution, it is applicable not only to full bath, apply also for maniluvium lavipeditum, and refreshing body clean skin can be brought, dredging the channel, sterilize clearing damp, fragrant body beautification, adjust blood fat, stabilizing blood pressure, toxin-expelling and face nourishing, anti-aging and raising body immunity and other effects, the pruitus that is particularly suitable for use in patient.
Description
Technical field
The present invention relates to a kind of bath agent, specifically a kind of delicate fragrance type shower powder containing peony and preparation method thereof
And application.
Background technology
Tree peony category Ranunculaceae Paeonia, machaka, there is very high ornamental value and pharmaceutical value, it is for a long time, male
The utilization of red deep processed product but seem serious hysteresis that production added value is very low, does not form industrial chain.The Chinese Academy of Sciences
Shown using the result of chemical assay, 8 kinds of amino acid needed by human and a variety of dimensions are contained in peony petal, pistil and pollen
Raw element, carbohydrate and Flavonoid substances, also containing trace element necessary to a variety of enzymes, 7 kinds of macroelements and 5 kinds of human bodies, have
The effects such as anti-cancer, anticancer, regulation blood fat, stabilizing blood pressure, toxin-expelling and face nourishing, anti-aging, raising body immunity.
Shower cream and shower powder have been increasingly becoming the most frequently used, a kind of commodity that consumption is maximum in people's daily life,
As the improvement of people's living standards, requirement of the people for bath product also more and more higher, at present, common shower on the market
Product, it is most of to contain more chemical composition, frequently use, moisture of skin balance can be destroyed, cause skin water shortage, aging etc. to ask
Topic, it is long-term use of, it is unfavorable for the skin health of people, and pure natural bath product species is rare on the market now, kind list
One, expensive, skin effect is not notable.
The content of the invention
The invention provides a kind of delicate fragrance type shower powder containing peony and its preparation method and application, the shower powder is with male
Red flower is major ingredient, and adds Chinese medicine and its compatibility, while cleaning skin can also dredging the channel, sterilization clearing damp, fragrant body beautification.
The present invention be solve the technical scheme that uses of above-mentioned technical problem for：A kind of delicate fragrance type shower powder containing peony,
The shower powder is made up of major ingredient and auxiliary material, and according to parts by weight, the major ingredient is by peony 28-36 parts, dutchmanspipe root 4-12 parts, rose
Rare colored 4-12 parts, Jasmine 4-12 parts, lopseed 12-20 parts, flower bud of lily magnolia 2-9 parts and cacumen biotae 2-9 parts composition, the auxiliary material by β-
Cyclodextrin and purified water composition.
A kind of delicate fragrance type shower powder containing peony, the shower powder are made up of the major ingredient of following parts by weight：Peony 32
8 parts of part, 8 parts of dutchmanspipe root, 8 parts of rose, 8 parts of Jasmine, 16 parts of lopseed, 8 parts of the flower bud of lily magnolia and cacumen biotae.
The method for preparing a kind of delicate fragrance type shower powder containing peony of the present invention, comprises the following steps：
Step 1: each raw material is weighed respectively according to above-mentioned parts by weight；
Step 2: drying to water content is in the vacuum freezing drying oven that temperature is -40 ~ -25 DEG C by the dutchmanspipe root weighed
6-10%, then crush and cross 150-200 mesh sieves, dutchmanspipe root extraction is extracted to obtain using supercritical carbon dioxide extraction technology afterwards
Oil, it is standby；
Step 3: the peony weighed, rose, Jasmine and the flower bud of lily magnolia are gone into the removal of impurity, after being cleaned up with clear water, add
Mass concentration is 70% alcohol solution dipping 1-5h, filters out filtrate, dries to obtain by petal fast dewatering with microwave dryer
Dry petal, the step of dry petal is added into 5-10 times of its parts by weight afterwards two, extract in obtained dutchmanspipe root extraction oil, stir
Mixing makes dry petal fully be contacted with dutchmanspipe root extraction oil, then stands 24-72h, afterwards the ultrasonic wave under the conditions of 40-50 DEG C of temperature
2-4h is extracted, obtains hybrid extraction oil, it is standby；
Step 4: take beta-schardinger dextrin to be placed in conical flask, add purified water, heating water bath dissolves beta-schardinger dextrin, afterwards by β-
Cyclodextrin solution is let cool to 40 DEG C, then constant temperature stirring 30-40min, takes step 3 hybrid extraction oil injection beta-schardinger dextrin solution
In, after continuing constant temperature stirring 2-4h, put and 12-24h is refrigerated in refrigerator, take out and filter, obtain oily solid powder, oily solid powder is used
Low temperature drying 12-18h, taking-up dried object crushed 150-200 mesh sieves, obtain β-ring under the conditions of 55-65 DEG C after purifying water washing
Dextrin includes extraction oil solid powder, wherein, hybrid extraction oil, beta-schardinger dextrin and purified water are by weight hybrid extraction oil：
Beta-schardinger dextrin：Purified water=1：6：60；
Step 5: the lopseed weighed and cacumen biotae are cleaned up dry after cut into slices, under 25-30W sterilamps away from 1m at
Irradiate 25-35s and carry out ultraviolet sterilization, be dried and crushed into coarse powder afterwards, add using 8-12 times of concentration measured of coarse powder as 60-70%
Ethanol immersion 12-18h after, ultrasonic extraction 30-35min, ultrasonic temperature be 30-32 DEG C, ultrasonic power 75-85W, ultrasound carries
Take three times, merge extract solution three times and be concentrated under reduced pressure, concentrate is placed in 48-60h in 4 DEG C of refrigerators, filters, must filter out partial pigment
The concentrate of precipitation, afterwards under the conditions of 80 DEG C, relative density 1.31-1.34 is concentrated into, is then dried under reduced pressure, crushing and mistake
1800-2000 mesh sieves, mixing micropowders are obtained, it is standby；
Step 6: micropowders will be mixed made from beta-cyclodextrin inclusion compound extraction oil solid powder and step 5 made from step 4
It is well mixed, encapsulation, produce a kind of delicate fragrance type shower powder containing peony.
As a kind of preferred scheme, the extracting pressure of supercritical carbon dioxide extraction described in step 2 is 25-35MPa, extraction
Temperature is 50-65 DEG C, extraction time 5-7h.
As a kind of preferred scheme, a kind of delicate fragrance type shower powder containing peony is with every bag of 100- made from step 6
150g, the specification wrapped per box 20 are packaged.
As a kind of preferred scheme, the peony is fragrant beautiful peony.
As a kind of preferred scheme, the shower powder is used for partial immersion bath or full bath, and the partial immersion bath is maniluvium, foot
Bath, hip bath, bath in a tub or half bath, the full bath are indoor bathing pool or middle-size and small-size swimming pool, during shower, set water temperature in 38-
40 DEG C, man uses 100g during full bath, and Ms uses 150g shower powder dipping bath 15-25min, and partial immersion bath is washed one's hair using 15-30g
Bath powder dipping bath 5-15min.
Tree peony, there is very high ornamental value and pharmaceutical value, the Chinese Academy of Sciences is shown using the result of chemical assay, male
Containing 8 kinds of amino acid and multivitamin needed by human, carbohydrate and Flavonoid substances in red petal, pistil and pollen, go back
Containing trace element necessary to a variety of enzymes, 7 kinds of macroelements and 5 kinds of human bodies, there is anti-cancer, anticancer, regulation blood fat, stabilised blood
The effects such as pressure, toxin-expelling and face nourishing, anti-aging, raising body immunity.
Fragrant beautiful peony, is kind most fragrant in all tree peonies, the luxurious floral type of the gracefulness of great taste, fragrance god
It is secret and strong, give chemical feeling.
Dutchmanspipe root, gas is fragrant special, bitter, can improve skin oxidation resistance, moreover it is possible to play a part of gentle, delicate fragrance,
There is different degrees of inhibitory action to bacillus such as staphylococcus aureus, green pus, large intestine, deformations, immunity can be improved, also had
There is antitumaous effect.
Rose, acrid flavour, sweet, slightly warm in nature, Return liver, the spleen channel.With regulating the flow of vital energy Xie Yu, dampness elimination is with, promoting blood circulation to remove blood stasis and menstruation regulating
The effect of analgesic, for liver-stomach disharmony, menoxenia, pain caused by ecchymoma, spitting of blood, carbuncle swells or the acute mastitis of spitting blood from the beginning of.In addition, rose
The property of medicine of rare flower as mild as a dove, is capable of the conscience blood vessels of warm foster people, and relax hair strongly fragrant gas in vivo, plays calmness, pacifies, antidepressant work(
Effect.
Jasmine, give off a strong fragrance charming, fragrant and sweet pure and sweet, mood can be stabilized, allayed nervousness.Contain in its pure white petal
There is the nutrient that gas chromatography and vitamin, and sugar and starch etc. are beneficial to human body, for can also be nursed one's health in cosmetics
Dry skin, has a gorgeous appearance of U.S. flesh, strengthening physique, refreshing, is very good cosmetic good merchantable brand the effect of anti-senility.
Lopseed, part of being used as medicine be plant herb, have the effect of promoting blood circulation and removing blood stasis, diuresis detoxify, stimulate the menstrual flow it is deep, it is anti-oxidant
It is one of its important effect.
The flower bud of lily magnolia, there is the effect of dispersing wind and cold, is a kind of rare spices and industrial chemicals again, contains a large amount of volatile oil smells virtue
It is fragrant.
Cacumen biotae, harmful free radicals are removed, suppress pigment and formed, deep layer Glycerin, cool blood, hemostasis, wind-damp dispelling, dissipated swollen
Poison.
Compared with prior art, the invention has the advantages that：
（1）The invention provides a kind of delicate fragrance type shower powder containing peony and its preparation method and application, the shower powder uses
Pure natural formula, using the fragrant beautiful peony of kind most fragrant in tree peony as major ingredient, selected plurality of raw materials carries out science compounding, fully profit
With the concertedness and compatibility of each raw material, the stability problem of product formula has been obtained perfect solution, be applicable not only to complete
Body is bathed, and applies also for maniluvium lavipeditum, and can bring refreshing body clean skin, dredging the channel, sterilizes clearing damp, fragrant body beautification, regulation blood fat, steady
Determine blood pressure, toxin-expelling and face nourishing, anti-aging and improve body immunity and other effects, the pruitus that is particularly suitable for use in patient；
（2）The present invention has carried out supercritical extract to a large amount of volatile oil compositions contained in dutchmanspipe root and has obtained extraction oil, is protecting
On the premise of staying volatile oil composition not destroyed, its yield is improved to greatest extent, dutchmanspipe root, can improve skin antioxygen
Change ability, plays a part of gentle, delicate fragrance, and the volatile oil composition in dutchmanspipe root plays in terms of dutchmanspipe root plays these drug effects
Considerable effect, therefore, the use range of dutchmanspipe root was both expanded, and improved the commercial value of dutchmanspipe root again；
（3）The present invention uses alcohol solution dipping peony, rose, Jasmine and this kind of fragrant plant of the flower bud of lily magnolia, can be effective
The worm's ovum being attached in petal surface is removed, using dutchmanspipe root volatile oil as Extraction solvent, the volatile oil allowed in dry petal fills
Divide and be dissolved into dutchmanspipe root volatile oil, extraction yield is high, and the shower powder prepared has light fragrance of a flower taste, can after shower
Reach the fragrance of flowers assails one's nose, refreshing effect, and lasting fragrance；The extraction of the present invention and separating technology are all under normal temperature or low temperature
Carry out, can guarantee that the low-boiling point material in each raw material is not destroyed, preferably protect the active ingredient in each raw material, will utilize β-
Cyclodextrin encapsulated volatile oil, both it had been avoided that the fragrance of fragrant plant was excessively strong, and can makes the oily solid powdering that evaporates, and carries
High stability, be advantageous to the performance of drug effect；
（4）The invention provides a kind of delicate fragrance type shower powder containing peony and its preparation method and application, to lopseed and side
CedarLeaves are handled, and filter out pigementation, are avoided when scar skin uses shower powder, shower powder enters wound, causes pigment
Precipitation, meanwhile, skin metabolism can be improved, promote skin blood circulation, increase skin-nourishing, free radical is effectively removed, disappear
Depigmentation precipitates, and antioxidation activity is high, holding time length；Micropowders are ground into, the micropowders after ultramicro grinding can
To reach nanoscale, be advantageous to the mutual cooperation between each raw material, particle diameter is small, can directly penetrate into people's by skin
In vivo, its physiological action is greatly improved.
Embodiment
The present invention is elaborated with reference to specific embodiment, the present embodiment premised on technical solution of the present invention,
Give detailed embodiment and specific operating process.
A kind of delicate fragrance type shower powder containing peony, the shower powder is made up of major ingredient and auxiliary material, described according to parts by weight
Major ingredient is by peony 28-36 parts, dutchmanspipe root 4-12 parts, rose 4-12 parts, Jasmine 4-12 parts, lopseed 12-20 parts, the flower bud of lily magnolia
2-9 parts and cacumen biotae 2-9 parts composition, the auxiliary material are made up of beta-schardinger dextrin and purified water.
A kind of delicate fragrance type shower powder containing peony, the shower powder are made up of the major ingredient of following parts by weight：Peony 32
8 parts of part, 8 parts of dutchmanspipe root, 8 parts of rose, 8 parts of Jasmine, 16 parts of lopseed, 8 parts of the flower bud of lily magnolia and cacumen biotae.
The method for preparing a kind of delicate fragrance type shower powder containing peony of the present invention, comprises the following steps：
Step 1: each raw material is weighed respectively according to above-mentioned parts by weight；
Step 2: drying to water content is in the vacuum freezing drying oven that temperature is -40 ~ -25 DEG C by the dutchmanspipe root weighed
6-10%, then crush and cross 150-200 mesh sieves, dutchmanspipe root extraction is extracted to obtain using supercritical carbon dioxide extraction technology afterwards
Oil, the extracting pressure of the supercritical carbon dioxide extraction is 25-35MPa, and extraction temperature is 50-65 DEG C, extraction time 5-
7h, it is standby；
Step 3: the peony weighed, rose, Jasmine and the flower bud of lily magnolia are gone into the removal of impurity, after being cleaned up with clear water, add
Mass concentration is 70% alcohol solution dipping 1-5h, filters out filtrate, dries to obtain by petal fast dewatering with microwave dryer
Dry petal, the step of dry petal is added into 5-10 times of its parts by weight afterwards two, extract in obtained dutchmanspipe root extraction oil, stir
Mixing makes dry petal fully be contacted with dutchmanspipe root extraction oil, then stands 24-72h, afterwards the ultrasonic wave under the conditions of 40-50 DEG C of temperature
2-4h is extracted, obtains hybrid extraction oil, it is standby；
Step 4: take beta-schardinger dextrin to be placed in conical flask, add purified water, heating water bath dissolves beta-schardinger dextrin, afterwards by β-
Cyclodextrin solution is let cool to 40 DEG C, then constant temperature stirring 30-40min, takes step 3 hybrid extraction oil injection beta-schardinger dextrin solution
In, after continuing constant temperature stirring 2-4h, put and 12-24h is refrigerated in refrigerator, take out and filter, obtain oily solid powder, oily solid powder is used
Low temperature drying 12-18h, taking-up dried object crushed 150-200 mesh sieves, obtain β-ring under the conditions of 55-65 DEG C after purifying water washing
Dextrin includes extraction oil solid powder, wherein, hybrid extraction oil, beta-schardinger dextrin and purified water are by weight hybrid extraction oil：
Beta-schardinger dextrin：Purified water=1：6：60；
Step 5: the lopseed weighed and cacumen biotae are cleaned up dry after cut into slices, under 25-30W sterilamps away from 1m at
Irradiate 25-35s and carry out ultraviolet sterilization, be dried and crushed into coarse powder afterwards, add using 8-12 times of concentration measured of coarse powder as 60-70%
Ethanol immersion 12-18h after, ultrasonic extraction 30-35min, ultrasonic temperature be 30-32 DEG C, ultrasonic power 75-85W, ultrasound carries
Take three times, merge extract solution three times and be concentrated under reduced pressure, concentrate is placed in 48-60h in 4 DEG C of refrigerators, filters, must filter out partial pigment
The concentrate of precipitation, afterwards under the conditions of 80 DEG C, relative density 1.31-1.34 is concentrated into, is then dried under reduced pressure, crushing and mistake
1800-2000 mesh sieves, mixing micropowders are obtained, it is standby；
Step 6: micropowders will be mixed made from beta-cyclodextrin inclusion compound extraction oil solid powder and step 5 made from step 4
Well mixed, afterwards with every bag of 100-150g, the specification wrapped per box 20 is packaged encapsulation, produces a kind of delicate fragrance containing peony
Type shower powder.
As a kind of preferred scheme, the peony is fragrant beautiful peony.
As a kind of preferred scheme, the shower powder is used for partial immersion bath or full bath, and the partial immersion bath is maniluvium, foot
Bath, hip bath, bath in a tub or half bath, the full bath are indoor bathing pool or middle-size and small-size swimming pool, during shower, set water temperature in 38-
40 DEG C, man uses 100g during full bath, and Ms uses 150g shower powder dipping bath 15-25min, and partial immersion bath is washed one's hair using 15-30g
Bath powder dipping bath 5-15min.
Embodiment one
A kind of delicate fragrance type shower powder containing peony, the shower powder is made up of major ingredient and auxiliary material, according to parts by weight, the major ingredient
It is made up of 2 parts of 28 parts of peony, 4 parts of dutchmanspipe root, 4 parts of rose, 4 parts of Jasmine, 12 parts of lopseed, 2 parts of the flower bud of lily magnolia and cacumen biotae,
The auxiliary material is made up of beta-schardinger dextrin and purified water.
The method for preparing a kind of delicate fragrance type shower powder containing peony of the present invention, comprises the following steps：
Step 1: each raw material is weighed respectively according to above-mentioned parts by weight；
Step 2: it is 6% that the dutchmanspipe root weighed is dried to water content in the vacuum freezing drying oven that temperature is -40 DEG C, so
Crush afterwards and cross 150 mesh sieves, dutchmanspipe root extraction oil is extracted to obtain using supercritical carbon dioxide extraction technology afterwards, it is described overcritical
The extracting pressure of CO2 fluid extractions is 25MPa, and extraction temperature is 50 DEG C, extraction time 5h, standby；
Step 3: the peony weighed, rose, Jasmine and the flower bud of lily magnolia are gone into the removal of impurity, after being cleaned up with clear water, add
Mass concentration is 70% alcohol solution dipping 1h, filters out filtrate, dries petal fast dewatering with microwave dryer and done
Petal, the step of dry petal is added into 5 times of its parts by weight afterwards two, are extracted in obtained dutchmanspipe root extraction oil, and stirring makes to do
Petal is fully contacted with dutchmanspipe root extraction oil, then stands 24h, and the ultrasonic wave extraction 2h under the conditions of 40 DEG C of temperature, is obtained mixed afterwards
Extraction oil is closed, it is standby；
Step 4: take beta-schardinger dextrin to be placed in conical flask, add purified water, heating water bath dissolves beta-schardinger dextrin, afterwards by β-
Cyclodextrin solution is let cool to 40 DEG C, then constant temperature stirring 30min, is taken in step 3 hybrid extraction oil injection beta-schardinger dextrin solution,
After continuing constant temperature stirring 2h, put and 12h is refrigerated in refrigerator, take out and filter, obtain oily solid powder, oily solid powder is washed with purifying
Low temperature drying 12h, taking-up dried object crushed 150 mesh sieves, obtain beta-cyclodextrin inclusion compound extraction oil solid under the conditions of 55 DEG C after washing
Powder, wherein, hybrid extraction oil, beta-schardinger dextrin and purified water are by weight hybrid extraction oil：Beta-schardinger dextrin：Purified water=1：
6：60；
Step 5: the lopseed weighed and cacumen biotae are cleaned up dry after cut into slices, under 25W sterilamps away from 1m irradiate
25s carries out ultraviolet sterilization, is dried and crushed into coarse powder afterwards, adds and soaks 12h by 60% ethanol of the concentration of 8 times of amounts of coarse powder
Afterwards, ultrasonic extraction 30min, ultrasonic temperature are 30 DEG C, ultrasonic power 75W, and ultrasonic extraction three times, merges extract solution three times and subtracted
Pressure concentration, concentrate are placed in 48h in 4 DEG C of refrigerators, filter, and the concentrate of partial pigment precipitation must be filtered out, afterwards in 80 DEG C of conditions
Under, relative density 1.31 is concentrated into, is then dried under reduced pressure, crushes and crosses 1800 mesh sieves, obtain mixing micropowders, it is standby；
Step 6: micropowders will be mixed made from beta-cyclodextrin inclusion compound extraction oil solid powder and step 5 made from step 4
Well mixed, afterwards with every bag of 100g, the specification wrapped per box 20 is packaged encapsulation, produces a kind of delicate fragrance type containing peony and wash one's hair
Bath powder.
As a kind of preferred scheme, the shower powder is used for partial immersion bath or full bath, and the partial immersion bath is maniluvium, foot
Bath, hip bath, bath in a tub or half bath, the full bath are indoor bathing pool or middle-size and small-size swimming pool, during shower, set water temperature 38
DEG C, man uses 100g during full bath, and Ms uses 150g shower powder dipping bath 15min, and partial immersion bath uses 15g shower powder dipping baths
5min。
Embodiment two
A kind of delicate fragrance type shower powder containing peony, the shower powder is made up of major ingredient and auxiliary material, according to parts by weight, the major ingredient
By 9 parts of 36 parts of peony, 12 parts of dutchmanspipe root, 12 parts of rose, 12 parts of Jasmine, 20 parts of lopseed, 9 parts of the flower bud of lily magnolia and cacumen biotae groups
Into the auxiliary material is made up of beta-schardinger dextrin and purified water.
The method for preparing a kind of delicate fragrance type shower powder containing peony of the present invention, comprises the following steps：
Step 1: each raw material is weighed respectively according to above-mentioned parts by weight；
Step 2: it is 10% that the dutchmanspipe root weighed is dried to water content in the vacuum freezing drying oven that temperature is -25 DEG C,
Then crush and cross 200 mesh sieves, dutchmanspipe root extraction oil is extracted to obtain using supercritical carbon dioxide extraction technology afterwards, it is described super to face
The extracting pressure of boundary's CO2 fluid extractions is 35MPa, and extraction temperature is 65 DEG C, extraction time 7h, standby；
Step 3: the peony weighed, rose, Jasmine and the flower bud of lily magnolia are gone into the removal of impurity, after being cleaned up with clear water, add
Mass concentration is 70% alcohol solution dipping 5h, filters out filtrate, dries petal fast dewatering with microwave dryer and done
Petal, the step of dry petal is added into 10 times of its parts by weight afterwards two, are extracted in obtained dutchmanspipe root extraction oil, and stirring makes
Dry petal is fully contacted with dutchmanspipe root extraction oil, then stands 72h, and the ultrasonic wave extraction 4h under the conditions of temperature 50 C, is obtained afterwards
Hybrid extraction oil, it is standby；
Step 4: take beta-schardinger dextrin to be placed in conical flask, add purified water, heating water bath dissolves beta-schardinger dextrin, afterwards by β-
Cyclodextrin solution is let cool to 40 DEG C, then constant temperature stirring 40min, is taken in step 3 hybrid extraction oil injection beta-schardinger dextrin solution,
After continuing constant temperature stirring 4h, put and 24h is refrigerated in refrigerator, take out and filter, obtain oily solid powder, oily solid powder is washed with purifying
Low temperature drying 18h, taking-up dried object crushed 200 mesh sieves, obtain beta-cyclodextrin inclusion compound extraction oil solid under the conditions of 65 DEG C after washing
Powder, wherein, hybrid extraction oil, beta-schardinger dextrin and purified water are by weight hybrid extraction oil：Beta-schardinger dextrin：Purified water=1：
6：60；
Step 5: the lopseed weighed and cacumen biotae are cleaned up dry after cut into slices, under 30W sterilamps away from 1m irradiate
35s carries out ultraviolet sterilization, is dried and crushed into coarse powder afterwards, adds and is soaked by 70% ethanol of the concentration of 12 times of amounts of coarse powder
After 18h, ultrasonic extraction 35min, ultrasonic temperature is 32 DEG C, ultrasonic power 85W, and ultrasonic extraction three times, merges extract solution three times
And be concentrated under reduced pressure, concentrate is placed in 60h in 4 DEG C of refrigerators, filters, and the concentrate of partial pigment precipitation must be filtered out, afterwards at 80 DEG C
Under the conditions of, relative density 1.34 is concentrated into, is then dried under reduced pressure, crushes and crosses 2000 mesh sieves, obtain mixing micropowders, it is standby；
Step 6: micropowders will be mixed made from beta-cyclodextrin inclusion compound extraction oil solid powder and step 5 made from step 4
Well mixed, afterwards with every bag of 150g, the specification wrapped per box 20 is packaged encapsulation, produces a kind of delicate fragrance type containing peony and wash one's hair
Bath powder.
As a kind of preferred scheme, the shower powder is used for partial immersion bath or full bath, and the partial immersion bath is maniluvium, foot
Bath, hip bath, bath in a tub or half bath, the full bath are indoor bathing pool or middle-size and small-size swimming pool, during shower, set water temperature 40
DEG C, man uses 100g during full bath, and Ms uses 150g shower powder dipping bath 25min, and partial immersion bath uses 30g shower powder dipping baths
15min。
Embodiment three
A kind of delicate fragrance type shower powder containing peony, the shower powder is made up of major ingredient and auxiliary material, according to parts by weight, the major ingredient
By 7 parts of 34 parts of peony, 10 parts of dutchmanspipe root, 10 parts of rose, 10 parts of Jasmine, 18 parts of lopseed, 7 parts of the flower bud of lily magnolia and cacumen biotae groups
Into the auxiliary material is made up of beta-schardinger dextrin and purified water.
The method for preparing a kind of delicate fragrance type shower powder containing peony of the present invention, comprises the following steps：
Step 1: each raw material is weighed respectively according to above-mentioned parts by weight；
Step 2: it is 8% that the dutchmanspipe root weighed is dried to water content in the vacuum freezing drying oven that temperature is -30 DEG C, so
Crush afterwards and cross 180 mesh sieves, dutchmanspipe root extraction oil is extracted to obtain using supercritical carbon dioxide extraction technology afterwards, it is described overcritical
The extracting pressure of CO2 fluid extractions is 30MPa, and extraction temperature is 60 DEG C, extraction time 6h, standby；
Step 3: the peony weighed, rose, Jasmine and the flower bud of lily magnolia are gone into the removal of impurity, after being cleaned up with clear water, add
Mass concentration is 70% alcohol solution dipping 3h, filters out filtrate, dries petal fast dewatering with microwave dryer and done
Petal, the step of dry petal is added into 8 times of its parts by weight afterwards two, are extracted in obtained dutchmanspipe root extraction oil, and stirring makes to do
Petal fully contacts with dutchmanspipe root extraction oil, then stands 48h, afterwards the ultrasonic wave extraction 3h under the conditions of temperature 45 C, obtains mixed
Extraction oil is closed, it is standby；
Step 4: take beta-schardinger dextrin to be placed in conical flask, add purified water, heating water bath dissolves beta-schardinger dextrin, afterwards by β-
Cyclodextrin solution is let cool to 40 DEG C, then constant temperature stirring 35min, is taken in step 3 hybrid extraction oil injection beta-schardinger dextrin solution,
After continuing constant temperature stirring 3h, put and 18h is refrigerated in refrigerator, take out and filter, obtain oily solid powder, oily solid powder is washed with purifying
Low temperature drying 15h, taking-up dried object crushed 180 mesh sieves, obtain beta-cyclodextrin inclusion compound extraction oil solid under the conditions of 60 DEG C after washing
Powder, wherein, hybrid extraction oil, beta-schardinger dextrin and purified water are by weight hybrid extraction oil：Beta-schardinger dextrin：Purified water=1：
6：60；
Step 5: the lopseed weighed and cacumen biotae are cleaned up dry after cut into slices, under 28W sterilamps away from 1m irradiate
30s carries out ultraviolet sterilization, is dried and crushed into coarse powder afterwards, adds and is soaked by 65% ethanol of the concentration of 10 times of amounts of coarse powder
After 15h, ultrasonic extraction 32min, ultrasonic temperature is 31 DEG C, ultrasonic power 80W, and ultrasonic extraction three times, merges extract solution three times
And be concentrated under reduced pressure, concentrate is placed in 55h in 4 DEG C of refrigerators, filters, and the concentrate of partial pigment precipitation must be filtered out, afterwards at 80 DEG C
Under the conditions of, relative density 1.31-1.34 is concentrated into, is then dried under reduced pressure, crushes and crosses 1800 mesh sieves, obtain mixing micropowders,
It is standby；
Step 6: micropowders will be mixed made from beta-cyclodextrin inclusion compound extraction oil solid powder and step 5 made from step 4
Well mixed, afterwards with every bag of 120g, the specification wrapped per box 20 is packaged encapsulation, produces a kind of delicate fragrance type containing peony and wash one's hair
Bath powder.
As a kind of preferred scheme, the shower powder is used for partial immersion bath or full bath, and the partial immersion bath is maniluvium, foot
Bath, hip bath, bath in a tub or half bath, the full bath are indoor bathing pool or middle-size and small-size swimming pool, during shower, set water temperature in 38-
40 DEG C, man uses 100g during full bath, and Ms uses 150g shower powder dipping bath 15-25min, and partial immersion bath is washed one's hair using 15-30g
Bath powder dipping bath 5-15min.
Experimental study data
A kind of delicate fragrance type shower powder using effect containing peony prepared using preparation method of the present invention is assessed.It is tested
Crowd：18-60 year is chosen without the people of heredity medication history subject 300, specific sex composition and age composition determine at random, remember respectively
The improvement situation that subject uses rear pruitus situation is recorded, group 1, group 2 and group 3 are respectively 100 people, respectively use embodiment 1, real
Apply a kind of delicate fragrance type shower powder containing peony that example 2 and embodiment 3 are prepared.Use 2-3 times weekly, to continuous use 1
Month subject's using effect assess wherein, curative effect evaluation standard include cure, it is effective and invalid, the healing is pruitus
Symptom disappears, and without recurrence in 1 year；It is described effectively to be made moderate progress for pruitus, turn for the better by and large, but still need to consolidate；The nothing
Imitate be pruitus without improvement, other modes treatment need to be used instead, be as a result specifically shown in Table 1：
As shown in Table 1, the present invention has the effect of notable to pruitus problem, and appointing in 1-3 of the embodiment of the present invention is used continuously
Meaning one is after 1 month, and pruitus problem majority is effectively solved, papule, gradually improves the problems such as dry skin, through clinic
Checking, the shower powder prepared using inventive formulation, the healing and effective percentage for treating pruitus are up to 97.7%.
The above described is only a preferred embodiment of the present invention, any formal limitation not is made to the present invention, though
So the present invention is described as above with preferred embodiment, but is not limited to the present invention, any to be familiar with this professional technology people
Member, without departing from the scope of the present invention, when a little change or modification made using technology contents described above
It is the equivalent embodiment of equivalent variations, as long as being the technical spirit according to the present invention without departing from technical solution of the present invention content
Any simple modification, equivalent change and modification made to above example, in the range of still falling within technical solution of the present invention.
Claims (7)
- A kind of 1. delicate fragrance type shower powder containing peony, it is characterised in that：The shower powder is made up of major ingredient and auxiliary material, according to weight Number, the major ingredient is by peony 28-36 parts, dutchmanspipe root 4-12 parts, rose 4-12 parts, Jasmine 4-12 parts, lopseed 12- 20 parts, flower bud of lily magnolia 2-9 parts and cacumen biotae 2-9 parts composition, the auxiliary material are made up of beta-schardinger dextrin and purified water.
- A kind of 2. delicate fragrance type shower powder containing peony according to claim 1, it is characterised in that：The shower powder is by following The major ingredient of parts by weight is made：32 parts of peony, 8 parts of dutchmanspipe root, 8 parts of rose, 8 parts of Jasmine, 16 parts of lopseed, the flower bud of lily magnolia 8 8 parts of part and cacumen biotae.
- 3. prepare a kind of method of the delicate fragrance type shower powder containing peony as claimed in claim 1, it is characterised in that including with Lower step：Step 1: each raw material is weighed respectively according to above-mentioned parts by weight；Step 2: drying to water content is in the vacuum freezing drying oven that temperature is -40 ~ -25 DEG C by the dutchmanspipe root weighed 6-10%, then crush and cross 150-200 mesh sieves, dutchmanspipe root extraction is extracted to obtain using supercritical carbon dioxide extraction technology afterwards Oil, it is standby；Step 3: the peony weighed, rose, Jasmine and the flower bud of lily magnolia are gone into the removal of impurity, after being cleaned up with clear water, add Mass concentration is 70% alcohol solution dipping 1-5h, filters out filtrate, dries to obtain by petal fast dewatering with microwave dryer Dry petal, the step of dry petal is added into 5-10 times of its parts by weight afterwards two, extract in obtained dutchmanspipe root extraction oil, stir Mixing makes dry petal fully be contacted with dutchmanspipe root extraction oil, then stands 24-72h, afterwards the ultrasonic wave under the conditions of 40-50 DEG C of temperature 2-4h is extracted, obtains hybrid extraction oil, it is standby；Step 4: take beta-schardinger dextrin to be placed in conical flask, add purified water, heating water bath dissolves beta-schardinger dextrin, afterwards by β- Cyclodextrin solution is let cool to 40 DEG C, then constant temperature stirring 30-40min, takes step 3 hybrid extraction oil injection beta-schardinger dextrin solution In, after continuing constant temperature stirring 2-4h, put and 12-24h is refrigerated in refrigerator, take out and filter, obtain oily solid powder, oily solid powder is used Low temperature drying 12-18h, taking-up dried object crushed 150-200 mesh sieves, obtain β-ring under the conditions of 55-65 DEG C after purifying water washing Dextrin includes extraction oil solid powder, wherein, hybrid extraction oil, beta-schardinger dextrin and purified water are by weight hybrid extraction oil： Beta-schardinger dextrin：Purified water=1：6：60；Step 5: the lopseed weighed and cacumen biotae are cleaned up dry after cut into slices, under 25-30W sterilamps away from 1m at Irradiate 25-35s and carry out ultraviolet sterilization, be dried and crushed into coarse powder afterwards, add using 8-12 times of concentration measured of coarse powder as 60-70% Ethanol immersion 12-18h after, ultrasonic extraction 30-35min, ultrasonic temperature be 30-32 DEG C, ultrasonic power 75-85W, ultrasound carries Take three times, merge extract solution three times and be concentrated under reduced pressure, concentrate is placed in 48-60h in 4 DEG C of refrigerators, filters, must filter out partial pigment The concentrate of precipitation, afterwards under the conditions of 80 DEG C, relative density 1.31-1.34 is concentrated into, is then dried under reduced pressure, crushing and mistake 1800-2000 mesh sieves, mixing micropowders are obtained, it is standby；Step 6: micropowders will be mixed made from beta-cyclodextrin inclusion compound extraction oil solid powder and step 5 made from step 4 It is well mixed, encapsulation, produce a kind of delicate fragrance type shower powder containing peony.
- A kind of 4. preparation method of delicate fragrance type shower powder containing peony according to claim 3, it is characterised in that：Step The extracting pressure of two supercritical carbon dioxide extractions is 25-35MPa, and extraction temperature is 50-65 DEG C, extraction time 5-7h.
- A kind of 5. preparation method of delicate fragrance type shower powder containing peony according to claim 3, it is characterised in that：Step With every bag of 100-150g, the specification wrapped per box 20 is packaged a kind of delicate fragrance type shower powder containing peony made from six.
- A kind of 6. delicate fragrance type shower powder containing peony according to claim 1, it is characterised in that：The peony is perfume Beautiful peony.
- A kind of 7. application of delicate fragrance type shower powder containing peony according to claim 1, it is characterised in that：The shower powder For partial immersion bath or full bath, the partial immersion bath is maniluvium, lavipeditum, hip bath, bath in a tub or half bath, and the full bath is room Interior bathing pool or middle-size and small-size swimming pool, during shower, water temperature man at 38-40 DEG C, full bath is set use 100g, Ms's use 150g shower powder dipping bath 15-25min, partial immersion bath use 15-30g shower powder dipping baths 5-15min.
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Cited By (2)
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| CN113388460A (en) * | 2021-07-27 | 2021-09-14 | 河南省商业科学研究所有限责任公司 | Faint scent type perfumed soap containing peony flowers and preparation method thereof |
| CN113575617A (en) * | 2021-09-22 | 2021-11-02 | 宁夏农林科学院植物保护研究所（宁夏植物病虫害防治重点实验室） | Application of costus root in biological control, biological control medicament and preparation method thereof |
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| CN104172155A (en) * | 2014-07-07 | 2014-12-03 | 李�杰 | Ultra-micro peony flower powder as well as preparation method and application thereof |
| CN104248544A (en) * | 2013-06-26 | 2014-12-31 | 昆山鹿康贸易有限公司 | Beauty-treatment herbal medicine formula |
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| CN1255330A (en) * | 1998-11-30 | 2000-06-07 | 刘玉仁 | Health-care lotion for foot bath |
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| CN113388460A (en) * | 2021-07-27 | 2021-09-14 | 河南省商业科学研究所有限责任公司 | Faint scent type perfumed soap containing peony flowers and preparation method thereof |
| CN113575617A (en) * | 2021-09-22 | 2021-11-02 | 宁夏农林科学院植物保护研究所（宁夏植物病虫害防治重点实验室） | Application of costus root in biological control, biological control medicament and preparation method thereof |
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| CN107569420B (en) | 2020-07-03 |
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Effective date of registration: 20201012 Address after: 471000 unit 2, building 7, Zhonghong Zhuoyue City, Jianxi District, Luoyang City, Henan Province 1704 Patentee after: Luoyang Green Peony Technology Co.,Ltd. Address before: The peony bridge Xigong District 471000 Henan city of Luoyang Province east side building the East District No. 2-10 Patentee before: LUOYANG XIGONG SHENDU MUDAN PERFUME MILL |