CN106281807A - Oleum Camelliae handmade soap and preparation method thereof - Google Patents
Oleum Camelliae handmade soap and preparation method thereof Download PDFInfo
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- CN106281807A CN106281807A CN201610674933.8A CN201610674933A CN106281807A CN 106281807 A CN106281807 A CN 106281807A CN 201610674933 A CN201610674933 A CN 201610674933A CN 106281807 A CN106281807 A CN 106281807A
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- chakubing
- oleum camelliae
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/48—Superfatting agents
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
- Cosmetics (AREA)
Abstract
The present invention is to provide a kind of Oleum Camelliae handmade soap and preparation method thereof, and it is oil raw material based on Camellia oil, and adds the Multiple components Oleum Cocois that human body is useful, Petiolus Trachycarpi oil, cera alba, CHAKUBING powder etc., it is prepared from including following content of component: Oleum Camelliae 100 120 parts, Oleum Cocois 50 60 parts, Petiolus Trachycarpi oil 50 60 parts, cera alba 57 parts, 35 parts of CHAKUBING powder, NaOH 29 36 parts, 69 86 parts of water, essential oil of the flower of Camellia sinensis 1 1.5 parts.The Oleum Camelliae handmade soap prepared, dynamics of cleaning is strong, and cleaning performance is good, has skin protection to human body skin and moistens defencive function effect, and cleaning length in service life reaches 5 weeks/more than 100 grams, has market prospect and using value widely.
Description
Technical field:
The invention belongs to cosmetics of everyday use technical field, relate to a kind of handmade soap and preparation method thereof, particularly a kind of Oleum Camelliae is manual
Soap and preparation method thereof.
Background technology:
Along with improving constantly of modern people's living standard, various the articles for daily uses used in everyday are required the most increasingly by people
Height, various functional cosmeticses of everyday use also get more and more, and such as various functional milch cow fancy soaps etc., Oleum Camelliae has another name called camellia seed oil, is one
Plant the pure natural plant oil extracted from Semen Camelliae, be a kind of high-grade plant health-care oil, not only there is higher nutriture value
Value, the most also has the highest medical value, is the medicine for external use and beauty and skin care article having no side effect safely.Oleum Camelliae or cry mountain
Rich in abundant vitamin and oleic acid in Oleum Camelliae, it is easier to be absorbed by human body skin；Simultaneously also rich in there being tea saponin in Oleum Camelliae,
Tea polyphenols, the various bioactivators composition such as aminoacid, and the lot of trace mineral element such as potassium, zinc, selenium.Oleum Camelliae also by
It is widely used in cleansing milk, in shampoo etc. skin care item, but, above-mentioned application Oleum Camelliae is all to make the modes such as additive to enter
Row application, function produced by it is limited with useful efficacy effect.
Such as one Oleum Camelliae that Chinese patent notification number is CN103897896A and Jojoba oil and tea essential oil and hydrogen-oxygen
Changing soda soapization and make the preparation method of Oleum Camelliae fancy soap, the Camellia oil soap of preparation, it uses rich in unsaturated fatty acid Camellia oil soap
Change gained sodium palmitate cleaning capacity, foaming characteristic etc. the most poor, and soap body matter is soft at normal temperatures, under conditions of temperature is slightly higher i.e.
Can soften, preserve difficulty.During people's routine use, shower, face cleaning etc. are short for service life, are usually no more than 4 time-of-weeks.Also have
Another patent of invention notification number is CN103333752A
Utilize natural plants Camellia oil and Petiolus Trachycarpi oil etc. for raw material sodium hydroxide and normal saline through low temperature cold system, and add
The camellia oil skin care soap of the effectively skin-care nutrient composition such as Aloe, rich in the Petiolus Trachycarpi oil saponification gained satisfied fatty acid of satisfied fatty acid
Sodium is equipped with mutually with Camellia oil unsaturated fatty acid sodium, the hardness of soap is greatly improved, thus improves the use of this soap body
In the life-span, commonly reach 5 weeks/about 100 grams, but during actual use, its foaming effect has been deposited in cleaning dynamics
In bigger difference, cleaning performance is not ideal enough, and simultaneously in saponification process, the natural glycerin of generation is partially soluble in normal saline
In, cause the loss of glycerol, thus the moist degree having had influence on the using effect of soap body is poor.
Therefore, how to provide a kind of Oleum Camelliae handmade soap, it cleans dynamics by force, and cleaning performance is good, has human body skin
Defencive function effect is moistened in skin protection, and cleaning length in service life reaches Oleum Camelliae handmade soap and the preparation method of 5 weeks/more than 100 grams,
The needs of prebiotic work during to meet current people.
Summary of the invention:
The present invention is to provide a kind of Oleum Camelliae handmade soap and preparation method thereof, and it is oil raw material based on Camellia oil, and adds people
The Multiple components Oleum Cocois that body is useful, Petiolus Trachycarpi oil, cera alba, CHAKUBING powder etc., the Oleum Camelliae handmade soap prepared, cleans dynamics
By force, cleaning performance is good, has skin protection to human body skin and moistens defencive function effect, and cleaning length in service life reaches 5 weeks/100
More than gram, there is market prospect and using value widely.
In order to realize above goal of the invention, the present invention by the following technical solutions:
A kind of Oleum Camelliae handmade soap, is prepared from including following content of component: Oleum Camelliae 100-120 part, Oleum Cocois 50-60 part, palm fibre
Palmitic acid oil 50-60 part, cera alba 5-7 part, CHAKUBING powder 3-5 part, NaOH 29-36 part, water 69-86 part, essential oil of the flower of Camellia sinensis 1-1.5
Part.
Oleum Camelliae handmade soap of the present invention, described Oleum Camelliae handmade soap the most also includes following content of component: sucrose 5-8
Part, milk 3-5 part；Described milk is milk and/or sheep milk.
The method that it is another object of the present invention to prepare Oleum Camelliae handmade soap as above, its concrete preparation method is:
(1), miscella processed, by the Oleum Camelliae of each mass component, Oleum Cocois, Petiolus Trachycarpi oil, cera alba and remaining each raw material, after mixing every
Water is heated to 45-55 DEG C, after melting completely to cera alba, obtains miscella；
(2), alkali liquor is prepared: by the NaOH of mass parts in proportioning, be slowly added in the aqueous solution that proportioning is good, stirring while adding, extremely
Being completely dissolved and make alkali liquor, the temperature controlling alkali liquor is 45-50 DEG C；
(3), saponification: alkali liquor is slowly added to miscella, and is slowly stirred, add CHAKUBING powder when soap lye gradually becomes thickness
And essential oil of the flower of Camellia sinensis, stir, obtain soap lye；
(4), entering mould, rear processed handmade soap: poured into by soap lye in mould, surface covers, and keeps temperature 30-35 DEG C, after 24-48h
The demoulding；Soap blank stripping and slicing after demoulding, be positioned over cool place, ventilate, be dried place, 30-35 days time, be Oleum Camelliae handmade soap.
The described method preparing Oleum Camelliae handmade soap, its described CHAKUBING powder is prepared as follows:
A), tea making oil cake coarse powder: will after colding pressing and squeezing Oleum Camelliae, remaining CHAKUBING after crushed cross 80-100 mesh sieve, for tea
Oil cake coarse powder；
B), CHAKUBING extractum is prepared: by CHAKUBING coarse powder and water, after the ratio mixing that feed liquid mass ratio is 1:5-10, in
Extract 30-40min at 80-100 DEG C, cool down, be cooled to room temperature, filter cleaner, obtain filtrate and at 60-70 DEG C, continue heating stir
Mix until filtrate is thickness paste, i.e. obtain CHAKUBING extractum；
C), preparation CHAKUBING powder: CHAKUBING extractum is placed in baking oven, dries at a temperature of 50-60 DEG C to constant weight, for CHAKUBING
Extractum block, pulverized 100-150 mesh sieve by CHAKUBING extractum block, obtained CHAKUBING powder.
Essential oil of the flower of Camellia sinensis of the present invention, is prepared as follows:
A), raw material disposal: cross 20-30 mesh sieve after being pulverized by dry Flos Camelliae sinensis, obtain tea plant pollen；
B) Flos Camelliae sinensis extractum, is prepared: by tea plant pollen and solvent petroleum ether, be 1:8-10 mixing by feed liquid mass ratio, through ultrasonic
Extraction, under the conditions of control ultrasonic power is 500-600W, extracts 30-40min, obtains lixiviating solution, by lixiviating solution at 40-45 DEG C
1-2h is concentrated in vacuo, is finally 40-45 DEG C dry to constant weight in temperature, obtains Flos Camelliae sinensis extractum.
C), essential oil of the flower of Camellia sinensis is prepared: by upper step Flos Camelliae sinensis extractum and dehydrated alcohol, be that 5-7:1 joins according to feed liquid mass ratio
Than mixing, filter after extractum is completely dissolved, remove residue, filtrate cold preservation 12-24h at 0-4 DEG C, obtain cold preservation filtrate, by cold
Tibetan filtrate, through vacuum filtration, obtains the essential oil of the flower of Camellia sinensis ethanol solution of clarification, in vacuum 0.1MPA, temperature 35-40 DEG C water-bath rotation
Steam 20-40min, remove ethanol, i.e. obtain essential oil of the flower of Camellia sinensis.
Oleum Camelliae of the present invention can select Camellia oil, and the unsaturated fatty acid content in its Oleum Camelliae is up to more than 90%, n-
3, the unsaturated fatty acid of n-6 series, and polyene unsaturated fatty acid.Also rich in there being tea soap in the CHAKUBING coarse powder of the present invention
The several mineral materials compositions such as element, tea polyphenols, the bioactive substance such as arachidonic acid and aminoacid, and potassium, zinc, selenium.This
In bright added multicomponent as Oleum Camelliae and tea saponin etc. be in cleansing milk, shampoo, skin care item, all have a large amount of interpolation.
Therefore the Oleum Camelliae handmade soap that prepared by the present invention has that cleaning force is strong, and cleaning performance is good, bubbles abundant, and use for up to 5 weeks/
More than 100 grams.
Following table is Oleum Camelliae handmade soap prepared by the inventive method, each technical specification after testing, table 1,
Table 1,
Illustrate: the experiment service condition explanation of Oleum Camelliae handmade soap prepared by the inventive method: in order to verify that Oleum Camelliae of the present invention is manual
The personnel of 60 various skins of different nature existing are divided into four groups by the using effect of soap, wherein dry skin, oiliness skin,
The skin of Combination skin and sensitivity totally four groups, each group of people person is 15, carries out face cleaning voluntarily or shower uses, to detect it
Using effect, the use time is 6-8 week.
Using effect illustrates: using through person on probation, the Oleum Camelliae handmade soap hardness of the present invention is moderate, and cleaning force is strong, bubble
Exquisiteness, abundant, performance is gentle, refrigerant skin smoothing, and moisturizing is satisfactory for result, without being dried tight sense, occurs without allergic conditions, uses
Rear skin is the finest and the smoothest glossy, and the raw perfume of skin, has quintessence oil and the fragrance of milk taste；
Cleaning rate: cleaning rate=wash mixed dirt weight/mixed dirt original weight.
Detailed description of the invention: the inventive method is described in further detail below in conjunction with embodiment, following embodiment party
Case uses mass parts or mass percent.
Embodiment 1
One Oleum Camelliae handmade soap of the present invention, its each content of component composition is as follows: Oleum Camelliae 100-120 part, Oleum Cocois 50-60 part,
Petiolus Trachycarpi oil 50-60 part, cera alba 5-7 part, CHAKUBING powder 3-5 part, NaOH 29-36 part, water 69-86 part, essential oil of the flower of Camellia sinensis 1-
1.5 part.
It is preferably added sucrose 5-8 part, milk 3-5 part；Described milk is selected as milk.
Embodiment 2
In addition in place of the description below, undeclared part is the most same as Example 1,
Oleum Camelliae 110 parts, Oleum Cocois 55-part, Petiolus Trachycarpi oil 50 parts, cera alba 6 parts, 5 parts of CHAKUBING powder, NaOH 30 parts, 80 parts of water,
Essential oil of the flower of Camellia sinensis 1.5 parts, sucrose 5, milk 5 parts；
The milk that the present embodiment is selected is milk and the mixing of sheep milk each point 50% mass ratio.
The NaOH used in the various embodiments described above is its aqueous solution, and NaOH and water are made NaOH solution.In embodiment
The water used can be advisable spring-warm syndrome spring selenium-rich mineral water.
A kind of Oleum Camelliae handmade soap of the present invention, its concrete preparation method is:
(1), miscella processed, by the Oleum Camelliae of each mass component, Oleum Cocois, Petiolus Trachycarpi oil, cera alba and remaining each raw material sucrose 5, milk
Liquid 5 parts；After mixing, water proof is heated to 45-55 DEG C, after melting completely to cera alba, obtains miscella；
(2) alkali liquor, is prepared: by the NaOH of mass parts in proportioning, being slowly added in the aqueous solution that proportioning is good, limit adds stirring, extremely
Being completely dissolved and make alkali liquor, the temperature controlling alkali liquor is 45-50 DEG C；
(3), saponification: alkali liquor is slowly added to miscella, and is slowly stirred, add CHAKUBING powder when soap lye gradually becomes thickness
And essential oil of the flower of Camellia sinensis, stir, obtain soap lye；
(4), entering mould, rear processed handmade soap: poured into by soap lye in mould, surface covers, and keeps temperature 30-35 DEG C, after 24-48h
The demoulding；Soap blank stripping and slicing after demoulding, be positioned over cool place, ventilate, be dried place, 30-35 days time, be Oleum Camelliae handmade soap.
Further CHAKUBING powder of the present invention is prepared as follows:
A), tea making oil cake coarse powder: will after colding pressing and squeezing Oleum Camelliae, remaining CHAKUBING after crushed cross 80-100 mesh sieve, for tea
Oil cake coarse powder；
B), CHAKUBING extractum is prepared: by CHAKUBING coarse powder and water, after the ratio mixing that feed liquid mass ratio is 1:5-10, in
Extract 30-40min at 80-100 DEG C, cool down, be cooled to room temperature, filter cleaner, obtain filtrate and at 60-70 DEG C, continue heating stir
Mix until filtrate is thickness paste, i.e. obtain CHAKUBING extractum；
C), preparation CHAKUBING powder: CHAKUBING extractum is placed in baking oven, dries at a temperature of 50-60 DEG C to constant weight, for CHAKUBING
Extractum block, pulverized 100-150 mesh sieve by CHAKUBING extractum block, obtained CHAKUBING powder.
Further essential oil of the flower of Camellia sinensis of the present invention, is prepared as follows:
A), raw material disposal: cross 20-30 mesh sieve after being pulverized by dry Flos Camelliae sinensis, obtain tea plant pollen；
B) Flos Camelliae sinensis extractum, is prepared: by tea plant pollen and solvent petroleum ether, be 1:8-10 mixing by feed liquid mass ratio, through ultrasonic
Extraction, under the conditions of control ultrasonic power is 500-600W, extracts 30-40min, obtains lixiviating solution, by lixiviating solution at 40-45 DEG C
1-2h is concentrated in vacuo, is finally 40-45 DEG C dry to constant weight in temperature, obtains Flos Camelliae sinensis extractum.
C), essential oil of the flower of Camellia sinensis is prepared: by upper step Flos Camelliae sinensis extractum and dehydrated alcohol, be that 5-7:1 joins according to feed liquid mass ratio
Than mixing, filter after extractum is completely dissolved, remove residue, filtrate cold preservation 12-24h at 0-4 DEG C, obtain cold preservation filtrate, by cold
Tibetan filtrate, through vacuum filtration, obtains the essential oil of the flower of Camellia sinensis ethanol solution of clarification, in vacuum 0.1MPA, temperature 35-40 DEG C water-bath rotation
Steam 20-40min, remove ethanol, i.e. obtain essential oil of the flower of Camellia sinensis.
Utilizing Oleum Camelliae handmade soap prepared by the inventive method, have cleaning force strong, bubble exquisiteness, abundant, performance is gentle, clearly
Nice and cool skin, moisturizing is satisfactory for result, without being dried tight sense, uses rear skin the finest and the smoothest glossy, and the raw perfume of skin, has quintessence oil
And the fragrance of milk taste.
Claims (5)
1. an Oleum Camelliae handmade soap, is prepared from including following content of component: Oleum Camelliae 100-120 part, Oleum Cocois 50-60 part,
Petiolus Trachycarpi oil 50-60 part, cera alba 5-7 part, CHAKUBING powder 3-5 part, NaOH 29-36 part, water 69-86 part, essential oil of the flower of Camellia sinensis 1-
1.5 part.
Oleum Camelliae handmade soap the most according to claim 1, is characterized in that described Oleum Camelliae handmade soap also includes following mass parts group
Point: sucrose 5-8 part, milk 3-5 part；Described milk is milk and/or sheep milk.
3. the method preparing Oleum Camelliae handmade soap as claimed in claim 1, its concrete preparation method is:
(1), miscella processed, by the Oleum Camelliae of each mass component, Oleum Cocois, Petiolus Trachycarpi oil, cera alba and remaining each raw material, after mixing every
Water is heated to 45-55 DEG C, after melting completely to cera alba, obtains miscella；
(2), alkali liquor is prepared: by the NaOH of mass parts in proportioning, be slowly added in the aqueous solution that proportioning is good, stirring while adding, extremely
Being completely dissolved and make alkali liquor, the temperature controlling alkali liquor is 45-50 DEG C；
(3), saponification: alkali liquor is slowly added to miscella, and is slowly stirred, add CHAKUBING powder when soap lye gradually becomes thickness
And essential oil of the flower of Camellia sinensis, stir, obtain soap lye；
(4), entering mould, rear processed handmade soap: poured into by soap lye in mould, surface covers, and keeps temperature 30-35 DEG C, after 24-48h
The demoulding；Soap blank stripping and slicing after demoulding, be positioned over cool place, ventilate, be dried place, 30-35 days time, be Oleum Camelliae handmade soap.
The method preparing Oleum Camelliae handmade soap the most according to claim 3, is characterized in that described CHAKUBING powder as follows
Preparation:
A), tea making oil cake coarse powder: will after colding pressing and squeezing Oleum Camelliae, remaining CHAKUBING after crushed cross 80-100 mesh sieve, for tea
Oil cake coarse powder；
B), CHAKUBING extractum is prepared: by CHAKUBING coarse powder and water, after the ratio mixing that feed liquid mass ratio is 1:5-10, in
Extract 30-40min at 80-100 DEG C, cool down, be cooled to room temperature, filter cleaner, obtain filtrate and at 60-70 DEG C, continue heating stir
Mix until filtrate is thickness paste, i.e. obtain CHAKUBING extractum；
C), preparation CHAKUBING powder: CHAKUBING extractum is placed in baking oven, dries at a temperature of 50-60 DEG C to constant weight, for CHAKUBING
Extractum block, pulverized 100-150 mesh sieve by CHAKUBING extractum block, obtained CHAKUBING powder.
The method preparing Oleum Camelliae handmade soap the most according to claim 3, is characterized in that described essential oil of the flower of Camellia sinensis, by as follows
Prepared by method:
A), raw material disposal: cross 20-30 mesh sieve after being pulverized by dry Flos Camelliae sinensis, obtain tea plant pollen；
B) Flos Camelliae sinensis extractum, is prepared: by tea plant pollen and solvent petroleum ether, be 1:8-10 mixing by feed liquid mass ratio, through ultrasonic
Extraction, under the conditions of control ultrasonic power is 500-600W, extracts 30-40min, obtains lixiviating solution, by lixiviating solution at 40-45 DEG C
1-2h is concentrated in vacuo, is finally 40-45 DEG C dry to constant weight in temperature, obtains Flos Camelliae sinensis extractum；
C), essential oil of the flower of Camellia sinensis is prepared: by upper step Flos Camelliae sinensis extractum and dehydrated alcohol, be that 5-7:1 proportioning is mixed according to feed liquid mass ratio
Close, after extractum is completely dissolved filter, remove residue, filtrate at 0-4 DEG C, cold preservation 12-24h, obtain cold preservation filtrate, by cold preservation filter
Liquid, through vacuum filtration, obtains the essential oil of the flower of Camellia sinensis ethanol solution of clarification, steams 20-in vacuum 0.1MPA, temperature 35-40 DEG C water-bath rotation
40min, removes ethanol, i.e. obtains essential oil of the flower of Camellia sinensis.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610674933.8A CN106281807A (en) | 2016-08-17 | 2016-08-17 | Oleum Camelliae handmade soap and preparation method thereof |
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| CN201610674933.8A CN106281807A (en) | 2016-08-17 | 2016-08-17 | Oleum Camelliae handmade soap and preparation method thereof |
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| CN106281807A true CN106281807A (en) | 2017-01-04 |
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| CN201610674933.8A Pending CN106281807A (en) | 2016-08-17 | 2016-08-17 | Oleum Camelliae handmade soap and preparation method thereof |
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| CN108004060A (en) * | 2017-12-15 | 2018-05-08 | 浙江海洋大学 | A kind of intestines Enteromorpha skin care soap and preparation method thereof |
| CN111363640A (en) * | 2020-04-13 | 2020-07-03 | 湖南润农生态茶油有限公司 | Tea oil handmade soap and preparation method thereof |
| CN112111343A (en) * | 2020-09-28 | 2020-12-22 | 李贺 | Tea flower antibacterial skin care soap and preparation method thereof |
| CN115386438A (en) * | 2022-08-05 | 2022-11-25 | 金辉 | Portable handmade essential oil soap and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108004060A (en) * | 2017-12-15 | 2018-05-08 | 浙江海洋大学 | A kind of intestines Enteromorpha skin care soap and preparation method thereof |
| CN111363640A (en) * | 2020-04-13 | 2020-07-03 | 湖南润农生态茶油有限公司 | Tea oil handmade soap and preparation method thereof |
| CN112111343A (en) * | 2020-09-28 | 2020-12-22 | 李贺 | Tea flower antibacterial skin care soap and preparation method thereof |
| CN115386438A (en) * | 2022-08-05 | 2022-11-25 | 金辉 | Portable handmade essential oil soap and preparation method thereof |
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Application publication date: 20170104 |