CN105543013A - Makeup removing soap with plant botanical component extracting solution and manufacturing method for same - Google Patents
Makeup removing soap with plant botanical component extracting solution and manufacturing method for same Download PDFInfo
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- CN105543013A CN105543013A CN201510917328.4A CN201510917328A CN105543013A CN 105543013 A CN105543013 A CN 105543013A CN 201510917328 A CN201510917328 A CN 201510917328A CN 105543013 A CN105543013 A CN 105543013A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/06—Inorganic compounds
- C11D9/18—Water-insoluble compounds
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
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Abstract
The invention provides a makeup removing soap with plant component extracting solution and a manufacturing method for the same. Organic solution and inorganic solution are employed; a vacuumizing decompression extracting method is employed to make a makeup removing soap with Barbary wolfberry extracting solution, saponaria officinalis extracting solution, houttuynia cordata solution, artichokes extracting solution and liquorice extracting solution; the makeup removing soap has effects of whitening and shrinking enlarged pores, warming and anti-aging as well as killing inflammation; certain effects are taken to skin diseases such as allergic dermatitis and acne.
Description
Technical field
The invention relates to a kind of containing medlar extract liquid, Saponaria officinalis extracting solution, Herba Houttuyniae extract, makeup removing soap of the plant component extraction liquid such as arithoke extracting solution and licorice extract and preparation method thereof, specifically comprise, using as the wolfberry fruit of plant material, Saponaria officinalis, Herba Houttuyniae, arithoke, Radix Glycyrrhizae shredding stage respectively; The mix stages of organic solution and inorganic solution is added in described chippy material of vegetable origin; By the stage that the described plant material being mixed with organic solution and inorganic solution homogenizes; Plant material after described homogenizing is carried out the stage of ultrasonic disruption; Plant material after described ultrasonic disruption is carried out the stage of vacuum decompression extraction; Plant material after described extraction is carried out the stage of filtering; Plant extraction liquid after described filtration is carried out the stage that is concentrated and powdered; Soap base (Soapnoodle) is added, the mix stages of titanium dioxide (Titaniumdioxide) and spices in each plant extraction liquid after described powdered; And the stirring sizing stage of described mixed mixed solution; Soap containing plant material comprising above step and preparation method thereof.
In more detail, the invention provides a kind of makeup removing soap containing plant component extraction liquid and preparation method thereof, employ organic solution and inorganic solution, and undertaken extracting by vacuum decompression extraction method with the addition of medlar extract liquid, Saponaria officinalis extracting solution, Herba Houttuyniae extract, the makeup removing soap of arithoke extracting solution and licorice extract, not only there is whitening effect, pore refining effect, humidity-holding effect and anti-aging effects, also there is antiinflammation, for a kind of makeup removing soap containing plant component extraction liquid that the sensitive skin such as allergic dermatitis and acne problem is also effective and preparation method thereof.
Background technology
Day by day become easily living environment as modern, environmental pollution and fast-food are main dietetic life, and it is allergic that pressure and irregular living habit etc. cause.Therefore, recent dermatosis increases severely, and under situation like this, the substantially Clean-exploitation utilizing crude substance to make day by day is risen.
Take cleaning skin as the general soap that order uses, by means of basic salt and abundant foam and the clean power of its higher fatty acid contained, just be used widely before for a long time, soap be by various animal raw fat and vegetative grease by with sodium hydroxide generation saponification reaction after, make containing 12 ~ 15% moisture neat soap after, in order to dispel the foul smell that allows people feel under the weather and add spices, in order to reach the object of skin moisture-keeping and lubrication, with the addition of the various additives required for other such as softening agent and wetting Agent for Printing Inks, make formed solid-state.
The making method of the soap used for order with cleaning skin generally can be divided into saponification method (Saponification), neutralisation (Neutralization) and methyl esters saponification method (MethylesterSaponification).Saponification method utilizes grease to be hydrolyzed under the effect of alkali to obtain carboxylate salt and alcohol.Neutralisation utilizes grease under the effect of the catalyzer of acid or metalloid oxide compound etc., and after high temperature, high pressure, lower hydrolysis obtains alcohol and lipid acid, the method after this lipid acid refining, alcohol being neutralized.Methyl esters saponification method is after utilizing grease to make methyl esters soap under the effect of methyl alcohol, obtains the method for carboxylate salt and methyl alcohol after methyl esters soap and alkali reaction.
In the general soap made by described method, with the addition of the tensio-active agent in chemical additive, edta edta (ethylenediaminetetraaceticacid), antioxidant, high spices, the material that sanitas and artificial color etc. add when soap makes, though not talkative useful to human body, but when chemical substance enter into eyes or in the mouth when, though can a part be discharged, also can retain the part that cannot discharge and stay in the body.Tensio-active agent in chemical additive enters blood by cytolemma, and then is circulated to whole body, causes brain, heart, liver, the cell disorders of spleen etc.Cause body immunity to weaken thus, infer the reason namely producing disease allergic dermatitis.
Based on the danger that the problems referred to above are brought, the user demand of natural soap increases sharply, and the situation that oneself making natural soap also uses at home is also increasing.Owing to having lacked the tensio-active agent in chemical soap in the general making method of natural soap, the microorganism of its inside just can be decomposed in one day, can't environmental problem be produced.
The invention provides the natural soap of a kind of non-pigment and preservative-free, wherein with the addition of medlar extract liquid, Saponaria officinalis extracting solution, Herba Houttuyniae extract, arithoke extracting solution and licorice extract, for allergic skin or sensitive skin, a kind of soap containing vegetable material provided and preparation method thereof.
It is below the simple introduction as raw-material wolfberry fruit of the present invention, Saponaria officinalis, Herba Houttuyniae, arithoke, Radix Glycyrrhizae.
Wolfberry fruit (Lyciumchinense) is machaka, belongs to Solanaceae, and be the fruit of matrimony vine tree, it is distributed in the whole Asia similar with Korea S.Composition comprises trimethyl-glycine (Betaine), maize quality (Zeazanthin), carotene (Carotene), VitB1 (Thiamine), vitamin A, B1, B2, C etc., it contains a large amount of skin care vitamins Cs and abundant cellulosic.
Saponaria officinalis (Saponariaofficinalis) belongs to Caryophyllaceae Soapwort morphological specificity, and per nnial herb, is distributed in Korea S various places.Root contains saponin(e (Saponin), can be used as medicine, and can be used as treatment chronic dermatosis in autumn.Stem and leaf can be used as soap and substitute articles for use for clean wool or silk.
Herba Houttuyniae (Houttuyniacordata) is distributed widely in Korea S (Yu Ling island, sleeping island, Ju Jidao), Japan, China, Himalaya and Java, and history was more than 300 years.Main component is, containing 0.005% essential oil and methyl nonyl ketone (Methylnonylketone), and myrcene (Myrcene).Decanoylacetaldehyde (Decanoylacetaldehyde) and lauric acid have niff, because containing aldehyde (Laurinaldehyd).Containing Quercitroside (Quercitrin) on leaf, in flower and fruit fringe, contain isoquercitrin (Isoquercitrin).
Arithoke (Cynarascolymus) belongs to chrysanthemum section, under happiness is grown on the weather of maritime gentleness, only has southern areas can grow out summer in Korea S, can cultivate easily at the southern coast of Korea S and Jizhou Island.Containing protein, vitamin A, C, calcium, iron, phosphorus, sugar, inulin (Inulin), selenium (selenium).Selenium can be imitated and prevented the aging of skin and diminish inflammation, and it, by reducing intracellular peroxide concentrations, prevents the generation of free radical.
Radix Glycyrrhizae (Glycyrrhizauralensis) belongs to a kind of per nnial herb, be also called Glycyrrhiza uralensis Fisch. and Radix Glycyrrhizae, distribute and cultivate in Russia (siberian), Iran, Afghanistan, Pakistan, the Central Asia,, also there is cultivation in China (Gansu, Xinjiang) and Mongolia in Korea S.Glycyrrhiza glabra is distributed in southern Europe, the Central Asia, China.Containing Methionin (Glycyrrhizin) and sucrose (Sucrose), glucose (Glucose), liquirtin (Liquiritin), licoricidin (Licoricidin).Methionin (Glycyrrhizin) is for diphtheria toxin, and tetanus toxin, Codeine Hydrochloride, vauqueline nitric acid, snake venom, while tetrodotoxin etc. have detoxification, also has the anti-inflammatory action suppressing oedema.In addition, eczema and severe face acnes, together take Radix Glycyrrhizae and Japanese Honeysuckle and also can play result for the treatment of.
In prior art related to the present invention, propose one, soap, the mixed extract of radix bupleuri and angelica in Korean Patent No. 10-1079915 (prior art document 1), it contains the make-up composition of surface active composition.A kind of medicinal herbs soap being added with South Korea medicinal herbs is proposed in No. 10-1209189th, Korean Patent (prior art document 2).A kind of natural soap constituent containing the improved skin of South Korea's extract and South Korea's powder is proposed in No. 10-2014-0071570th, Korean Patent (prior art document 3).
Describe in prior art document 1, the mixed extract of radix bupleuri and angelica can be used as natural tensio-active agent.
Describe a kind of by, the extraction juice in 300 Herba Houttuyniaes in prior art document 2, Herba Centellae, sewage, water-soluble plant bacteriocidin, purslane, kuh-seng, Fructus Cnidii, gold, the medicinal herbs stoste extracted in Radix Angelicae Sinensis and ginseng, the medicinal herbs soap made.
Describe in prior art document 3 a kind of by, Chinese medicine herbal medicine powder extracts and rosemary extract, pine extract, phytoncide, apricot seed extract, camomile extract, seed of Radix Oenotherae erythrosepalae extract, Citrus bergamia extract, eucalyptus extracts, wormwood extract, the brown fungus extract of birch, buckwheat extract, Semen Cassiae extract, Herba Houttuyniae extract, wolfberry fruit extract, Radix Angelicae Sinensis extract, Radix Glycyrrhizae extract, Pericarpium Citri Reticulatae extract, Radix Puerariae extract, aloe, oligochitosan, xanthohumol, sprout brown rice, turmeric, Ligusticum wallichii, mulberry leaf, the seed of Job's tears, mung bean and green tea, for the one of raw material is improved effect Natural toilet soap to skin.
Existing document has but comprises the wolfberry fruit extract used in one or more the present invention, soap alkaline extraction thing, Herba Houttuyniae extract, cynara scolymus extracts, Radix Glycyrrhizae extract, but does not comprise all, does not emphasize the effective constituent of cynara scolymus extracts especially.Therefore, in effect, prior art is only mentioned antibacterial, humidity-holding effect, and not mentioned skin whitening effects, and restrain pore effect and other more significant effects.
Earlier application document
(prior art document 0001) No. 10-1079915th, Korean Patent (2011.10.28)
(prior art document 0002) No. 10-1209189th, Korean Patent (2012.12.06)
(prior art document 0003) No. 10-2014-0071570th, Korean Patent (2014.06.12)
Summary of the invention
The object of this invention is to provide one, not only there is makeup removing effect, whitening effect, pore refining effect, humidity-holding effect, anti-aging effects, have antiinflammation, the one also effective for the sensitive skin such as allergic dermatitis and acne problem contains medlar extract liquid, Saponaria officinalis extracting solution, Herba Houttuyniae extract, makeup removing soap of the plant component extraction liquid such as arithoke extracting solution and licorice extract and preparation method thereof.
The technique means of technical solution problem
The present invention by following means, using as the wolfberry fruit of plant material, Saponaria officinalis, Herba Houttuyniae, arithoke, Radix Glycyrrhizae shredding stage respectively; The mix stages of organic solution and inorganic solution is added in described chippy material of vegetable origin; By the stage that the described plant material being mixed with organic solution and inorganic solution homogenizes; Plant material after described homogenizing is carried out the stage of ultrasonic disruption; Plant material after described ultrasonic disruption is carried out the stage of vacuum decompression extraction; Plant material after described extraction is carried out the stage of filtering; Plant extraction liquid after described filtration is carried out the stage that is concentrated and powdered; Soap base (Soapnoodle) is added, the mix stages of titanium dioxide (Titaniumdioxide) and spices in each plant extraction liquid after described powdered; And the stirring sizing stage of described mixed mixed solution; Soap containing plant material comprising above step and preparation method thereof, solves technical problem by aforesaid method.
The invention provides a kind of makeup removing soap containing plant component extraction liquid and preparation method thereof, employ organic solution and inorganic solution, and undertaken extracting by vacuum decompression extraction method with the addition of medlar extract liquid, Saponaria officinalis extracting solution, Herba Houttuyniae extract, the makeup removing soap of arithoke extracting solution and licorice extract, not only there is whitening effect, pore refining effect, humidity-holding effect and anti-aging effects, also there is antiinflammation, for the sensitive skin such as allergic dermatitis and acne problem a kind of makeup removing soap containing plant component extraction liquid also with effect and preparation method thereof, technical problem is solved by aforesaid method.
Soap provided by the present invention, containing medlar extract liquid, Saponaria officinalis extracting solution, Herba Houttuyniae extract, the plant component extraction liquid such as arithoke extracting solution and licorice extract, it has makeup removing effect, whitening effect, pore contractive effect, humidity-holding effect, anti-aging effects.Further, also there is antiinflammation, also there is effect for the sensitive skin such as allergic dermatitis and acne problem.
Accompanying drawing explanation
Fig. 1 is of the present invention containing medlar extract liquid, Saponaria officinalis extracting solution, Herba Houttuyniae extract, the schema of an embodiment of the makeup removing soap making method of the plant component extraction liquid such as arithoke extracting solution and licorice extract.
Embodiment
The meaning expressed by vocabulary used in this specification sheets and claim is not intended to limit the present invention, and contriver is described, based on the implication of technical elements of the present invention and concept according to the most preferred mode of oneself invention.
Be clearly and completely described technical scheme of the present invention below in conjunction with accompanying drawing, obviously, described embodiment is the present invention's part embodiment, instead of whole embodiments.Based on the embodiment in the present invention, those of ordinary skill in the art, not making the every other embodiment obtained under creative work prerequisite, belong to the scope of protection of the invention.
The invention provides a kind of makeup removing soap containing plant component extraction liquid and preparation method thereof, employ organic solution and inorganic solution, and extracted by vacuum decompression extraction method, and with the addition of medlar extract liquid, Saponaria officinalis extracting solution, Herba Houttuyniae extract, arithoke extracting solution and licorice extract.
First, medlar extract liquid, Saponaria officinalis extracting solution, Herba Houttuyniae extract, arithoke extracting solution and licorice extract are by obtain after the next stage, pulverize material of vegetable origin wolfberry fruit respectively, Saponaria officinalis, Herba Houttuyniae, arithoke, the shredding stage of Radix Glycyrrhizae, the mix stages of organic solution and inorganic solution is added in described chippy material of vegetable origin, by the stage that the described plant material being mixed with organic solution and inorganic solution homogenizes, plant material after described homogenizing is carried out the stage of ultrasonic disruption, plant material after described ultrasonic disruption is carried out the stage of vacuum decompression extraction, plant material after described extraction is carried out the stage of filtering, plant extraction liquid after described filtration is carried out the stage that is concentrated and powdered.
Secondly, by adding soap base (Soapnoodle) in each plant extraction liquid after described powdered, the mix stages of titanium dioxide (Titaniumdioxide) and spices, and the stirring sizing stage of described mixed mixed solution, make the soap containing plant material.
Embodiment 1. soap making method
(1) shredding stage
Material of vegetable origin wolfberry fruit, Saponaria officinalis, Herba Houttuyniae, arithoke, Radix Glycyrrhizae are carried out shredding stage.
Following instrument is selected to pulverize as required, gyratory crusher (Rotarycrusher), jaw crusher (Jawcrusher), roller crusher (Rollcrusher), cone crusher (Conecrusher), hammer mill (Hammercrusher), impact crusher (Impactcrusher), beater grinder (Hammermill), rod mill (Rodmill), ball mill (Ballmill), raymond mill (Raymondmill), supper micron mill (Supermill), roller crusher (Rollmi), needle mill (Pinmill), airflow type mill (Jetmill), conical bell mill (Conicalballmill) or vibrating mill (Vibrationmill).
Be ground into 1 ~ 100mesh size, diversified setting can be carried out according to design conditions.
For situation about cannot pulverize completely under different imposing a condition, shredding stage needs repeatedly to perform more than 2 times.
(2) solution mix stages
The mix stages of organic solution and inorganic solution is added in chippy material of vegetable origin.
Using the stage of organic solution and inorganic solution, in order to improve the extraction yield of solution, and the solution that selection component is different.
Select following organic solution as required, ethanol (ethanol), methyl alcohol (methanol), fatty oil (fattyoil), glycerine (glycerin), propylene glycol (propyleneglycol), ether (ether), chloroform (chloroform), sherwood oil (petroleumether), hexane (hexane), benzene (benzene), methylene dichloride (methylenechloride), ethyl acetate (ethylacetate), acetone (acetone), select in propyl carbinol (butanol) and Virahol (isopropanol), inorganic solvent can from water, liquefied ammonia (liquidammonia), butter of antimony (antimonytrichloride) and hydrogen fluoride (hydrogenfluoride).
When choosing ethanol as organic solution, water can be chosen as inorganic solution.
Be 1: 9 ~ 9: 1 between the proportioning regulatory region of organic solution and inorganic solution, preferred proportioning regulates and is distinguished as between 3: 7 ~ 4: 6.
Further, the proportioning of organic solvent and inorganic solvent, according to the kind of raw material or can impose a condition, and carries out variation adjustment.
Such as, in order to extract the essential oil comprised in the raw material of Herba Houttuyniae, the blending ratio of organic solvent can be improved further.That is, can assign to regulate according to the one-tenth of the vegetable material that will extract the blending ratio of each solvent.
(3) homogenize the stage
The plant material being mixed with organic solution and inorganic solution is homogenized.
When the plant material being mixed with organic solution and inorganic solution is homogenized, high speed agitator (Homogenizer) is utilized to carry out the operation that homogenizes, carry out mechanical dispersion and add critical surface promoting agent according to condition, can use emulsion dispersion etc. method.
(4) crushing stage
Ultrasonic disruption is carried out to the plant material after homogenizing.
Crusher is utilized to carry out ultrasonic disruption.The broken time is 5 ~ 60 points, and the preferred broken time is 25 ~ 40 points.Further, according to imposing a condition, variation adjustment can be carried out.
Ultrasonic disruption machine molecular motion causes due to the acting in conjunction of Ultrasonic characteristics cavitation erosion (cavitation), molecular motion, and its effect keeps active-energy to extract, to improve the effect that reactive and concentration process is performed.If the unit-protein using ultrasonic disruption machine to upset the throughput rate of the protein contained in sample as being incorporated into sample is improved in process of production.
Ultrasonic disruption machine utilizes the distinctive cavitation erosion effect of ultrasonic wave, brings out the motion of molecule, and described molecular motion is as the sensitization energy, and its effect is the maintenance effect improving techniques such as extracting, concentrated.As for introducing the processing unit producing protein, using ultrasonic grinder to pulverize sample, proteinaceous production rate in sample can be increased.
(5) stage is extracted
Plant material after ultrasonic disruption is carried out vacuum decompression extraction.
Extracting method can adopt the multiple extracting method such as diversified extraction way extraction process such as microwave (microwave) technique extraction method, osmose process (percolation).When described vacuum decompression extracts, the inner extraction for carrying out 3 ~ 7 hours under the condition of 60-80 DEG C, preferably carries out the extraction of 5 hours at the temperature of 70 DEG C.
Further, according to imposing a condition, variation adjustment can be carried out.
(6) filtration stage
Filter the plant material extracted.
Filtration method comprises, filtration chromatography (Chromatography), suction strainer, natural filtration, filtration under diminished pressure, pressure filtration, ultrafiltration,
The methods such as micro-filtration and reverse osmosis filtration, and can select according to different design conditionss.
Filtration time, temperature and frequency also can be different according to design conditions, and at least two kinds of methods beyond above-mentioned filter method also can be used to filter.
(7) stage with powdered is concentrated
Plant extraction liquid after filtering is concentrated.
Concentration method can use, membrane concentration, freeze concentration, and dry concentrated, the multiple method such as evaporation concentration and concentrating under reduced pressure, preferably uses at concentrating under reduced pressure.
By Powdered for making of the plant extraction liquid after concentrated.
Drying means can use, warm air drying, cold air drying, far infrared drying, electric heating drying, the method such as microwave drying and lyophilize, preferably by the water in lyophilize removing solution.
After this, obtain after utilizing pulverizer again to pulverize adding the powder in soap to, preferably adopt pulverising mill to carry out powder making.
(8) mix stages
Increase in each plant extraction liquid after powdered and be mixed into soap component soap base (Soapnoodle), titanium dioxide (Titaniumdioxide) and spices.
Now, the preferred blending ratio of each mixture of mix stages is soap base (Soapnoodle) 90 weight percent, medlar extract liquid 4 ~ 10 weight percent, Saponaria officinalis extracting solution 0.3 ~ 0.8 weight percent, Herba Houttuyniae extract 0.05 ~ 0.2 weight percent, arithoke extracting solution 0.05 ~ 0.2 weight percent, licorice extract 0.05 ~ 0.2 weight percent, titanium dioxide (Titaniumdioxide) 0.1 ~ 0.5 weight percent and spices 0.5 ~ 2 weight percent.
The present invention is it is further preferred that described soap base (Soapnoodle) is for extracting in coconut.
(9) shape the stage
Mixed mixture is stirred sizing.
After this, determine suitable shape and size and pack, completing a complete soap.
Reference example 1. carries out environmental performance evaluation for the use of soap
In order to carry out environmental performance evaluation to the use of soap of the present invention, evaluate from clean power, moisturizing power and pungency aspect.
Evaluation uses, and carries out control experiment, choose 25 and be grown up as object by 2 kinds of soap that the soap that obtains under condition described in embodiment 1 and market are sold.
Evaluation method is, has smeared the user of makeup, has cleaned respectively with often kind of soap, by the sensation after clean, carries out survey from clean power, moisturizing power and pungency angle.
Evaluation about clean power is the sensation after basis cleans, smooth feeling, the questionnaire assessment of the Abklingen of the makeup of thickness sense etc. and makeup removing degree etc.
Moisturizing power refers to the degree be tightened up the skin after clean, the questionnaire assessment of moisture sense etc.
Pungency refers to, to itching after washing one's face, shouting pain or the questionnaire assessment of the level of sensitivity of heating.
Environmental performance evaluation uses 5 points of full marks systems, using mark height person as the far-gone standard of identification.
[table 1]
Evaluation result is, in cleaning force, the soap that embodiment 1 provides is higher with the rank of general soap 2 than general soap 1.
In moisturizing power, contrasted by the soap that provides embodiment 1 and general soap 1 and general soap 2, the soap that embodiment 1 provides has very large advantage than general soap 1 with the moisturizing power aspect of general soap 2.
Pungency aspect, general soap 2, the soap that general soap 1 and embodiment 1 provide is evaluated, the pungency of the soap that embodiment 1 provides slightly lower than general soap 2, general soap 1.
That is, effect in general, known the present invention is compared to other soap not only in cleaning force, and also outstanding in moisturizing power, skin irritation is also less.
Claims (6)
1., containing a making method for the makeup removing soap of plant component extraction liquid, it is characterized in that, comprising:
Using the stage of pulverizing respectively as the wolfberry fruit of plant material, Saponaria officinalis, Herba Houttuyniae, arithoke, Radix Glycyrrhizae;
The mix stages of organic solution and inorganic solution is added in described chippy material of vegetable origin;
By the stage that the described plant material being mixed with organic solution and inorganic solution homogenizes;
Plant material after described homogenizing is carried out the stage of ultrasonic disruption;
Plant material after described ultrasonic disruption is carried out the stage of vacuum decompression extraction;
Plant material after described extraction is carried out the stage of filtering;
Plant extraction liquid after described filtration is carried out the stage that is concentrated and powdered;
Soap base (Soapnoodle) is added, the mix stages of titanium dioxide (Titaniumdioxide) and spices in each plant extraction liquid after described powdered; And
The stirring sizing stage of described mixed mixed solution.
2. the making method of the makeup removing soap containing plant component extraction liquid according to claim 1, is characterized in that, in the mix stages of described organic solution and inorganic solution, the ratio of mixture of organic solution and inorganic solution is 3: 7 ~ 4: 6.
3. the making method of the makeup removing soap containing plant component extraction liquid according to claim 1, is characterized in that, in the stage that described vacuum decompression extracts, extracts 3 ~ 7 hours at the temperature of 60 ~ 80 DEG C.
4. the making method of the makeup removing soap containing plant component extraction liquid according to claim 1, it is characterized in that, in described mix stages, the blending ratio of mixture is soap base (Soapnoodle) 90 weight percent, medlar extract liquid 4 ~ 10 weight percent, Saponaria officinalis extracting solution 0.3 ~ 0.8 weight percent, Herba Houttuyniae extract 0.05 ~ 0.2 weight percent, arithoke extracting solution 0.05 ~ 0.2 weight percent, licorice extract 0.05 ~ 0.2 weight percent, titanium dioxide (Titaniumdioxide) 0.1 ~ 0.5 weight percent and spices 0.5 ~ 2 weight percent.
5. the makeup removing soap containing plant component extraction liquid that the making method according to any one of claim 1-4 is made.
6. the making method of the makeup removing soap containing plant component extraction liquid according to claim 1, it is characterized in that, the extraction of described plant extraction liquid passes through,
Supercritical carbon dioxide extraction method, steam distillation, vacuum extraction method, decompression extraction method, microwave loss mechanisms, in diafiltration extraction method, any one extracting method extracts.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR10-2015-0163970 | 2015-11-23 | ||
| KR1020150163970A KR101880967B1 (en) | 2015-11-23 | 2015-11-23 | The makeup removal soap containing extract of plant component and manufacturing method of the same |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105543013A true CN105543013A (en) | 2016-05-04 |
| CN105543013B CN105543013B (en) | 2019-02-05 |
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| CN201510917328.4A Active CN105543013B (en) | 2015-11-23 | 2015-12-10 | Makeup removing soap of the liquid containing plant component extraction and preparation method thereof |
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| KR (1) | KR101880967B1 (en) |
| CN (1) | CN105543013B (en) |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105878323A (en) * | 2016-06-17 | 2016-08-24 | 湖南文理学院 | Method using ultrasonically-assisted supercritical extraction rectification to purify cynarin in globe artichoke |
| CN107456411A (en) * | 2016-06-02 | 2017-12-12 | 上海家化联合股份有限公司 | A kind of skin epidermal cells vitality improver and its application in skin preparations for extenal use |
| CN107468577A (en) * | 2017-09-03 | 2017-12-15 | 广州市花安堂生物科技有限公司 | A kind of crystal soda flower extract and its cosmetics containing crystal soda flower extract |
| CN107536753A (en) * | 2017-09-03 | 2018-01-05 | 广州市花安堂生物科技有限公司 | A kind of cosmetic material containing mineral matter |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108096172A (en) * | 2017-12-30 | 2018-06-01 | 蒋春霞 | A kind of makeup removing breast and preparation method thereof |
| KR102460827B1 (en) * | 2021-01-14 | 2022-10-31 | 우컴퍼니 주식회사 | Functional natural soap comprising complex fermented product of citrus peel and buckwheat and manufacturing methods thereof |
| CN115226894A (en) * | 2022-06-07 | 2022-10-25 | 广东药科大学 | Preparation method and application of lycium ruthenicum extract |
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- 2015-11-23 KR KR1020150163970A patent/KR101880967B1/en active IP Right Grant
- 2015-12-04 WO PCT/KR2015/013274 patent/WO2017090811A1/en active Application Filing
- 2015-12-10 CN CN201510917328.4A patent/CN105543013B/en active Active
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107456411A (en) * | 2016-06-02 | 2017-12-12 | 上海家化联合股份有限公司 | A kind of skin epidermal cells vitality improver and its application in skin preparations for extenal use |
| CN105878323A (en) * | 2016-06-17 | 2016-08-24 | 湖南文理学院 | Method using ultrasonically-assisted supercritical extraction rectification to purify cynarin in globe artichoke |
| CN107468577A (en) * | 2017-09-03 | 2017-12-15 | 广州市花安堂生物科技有限公司 | A kind of crystal soda flower extract and its cosmetics containing crystal soda flower extract |
| CN107536753A (en) * | 2017-09-03 | 2018-01-05 | 广州市花安堂生物科技有限公司 | A kind of cosmetic material containing mineral matter |
Also Published As
| Publication number | Publication date |
|---|---|
| WO2017090811A1 (en) | 2017-06-01 |
| CN105543013B (en) | 2019-02-05 |
| KR101880967B1 (en) | 2018-07-23 |
| KR20170059700A (en) | 2017-05-31 |
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