WO2017090811A1 - Soap for make-up removal containing plant component extracts and method for manufacturing same - Google Patents

Abstract

The present invention relates to a soap for make - up removal containing plant component extracts, such as a Lycium chinense extract, a Saponaria officinalis extract, a Houttuynia cordata extract, an artichoke extract, and a licorice extract, and to a method for manufacturing the same and, specifically, to a method for manufacturing a soap for make - up removal containing plant component extracts, the method comprising the steps of: pulverizing, as plant materials, Lycium chinense , Saponaria officinalis , Houttuynia cordata , artichoke, and licorice, respectively; mixing an organic solvent and an inorganic solvent with the pulverized plant materials; homogenizing the plant materials mixed with the organic solvent and inorganic solvent; sonicating the homogenized plant materials; extracting the sonicated plant materials under vacuum decompression; filtering the extracted plant materials; concentrating and powdering the filtered plant extracts; adding soap noodles, titanium dioxide, and a flavoring to the respective powdered plant extracts, followed by mixing; and stirring the mixed mixture, followed by molding. More specifically, the present invention relates to a soap for make - up removal containing plant component extracts and a method for manufacturing the same, wherein the soap has a whitening effect, a pore minimizing effect, a moisturizing effect, and an anti-aging effect by adding the Lycium chinense extract, Saponaria officinalis extract, Houttuynia cordata extract, artichoke extract, and licorice extract, which are obtained by an extraction method under vacuum decompression using an organic solvent and an inorganic solvent; and the soap has an effect for sensitive skin, such as atopy and acne, through an anti-inflammatory action.

Description

Makeup remover soap containing plant extracts and preparation method thereof

The present invention relates to a make-up removal soap containing a plant extract such as goji extract, soap extract, Echo extract, artichoke extract, licorice extract and the like, and more specifically, as a plant material Grinding fish, artichoke and licorice, respectively; Mixing an organic solvent and an inorganic solvent with the pulverized plant material; Homogenizing the plant material in which the organic solvent and the inorganic solvent are mixed; Ultrasonically crushing the homogenized plant material; Vacuum-pressure extracting the ultrasonically crushed plant material; Filtering the extracted plant material; Concentrating and powdering the filtered plant extract; Adding and mixing Soap noodle, titanium dioxide and spices to each of the powdered plant extracts; And a step of forming the mixed mixture by stirring. It relates to a plant material-containing soap and a method for producing the same.

More specifically, gojija extract, soap paste extract, eochocho extract, artichoke extract and licorice extract extracted by vacuum decompression method using an organic solvent and an inorganic solvent, as well as whitening effect, pore convergence effect, moisturizing effect and anti-aging effect The present invention relates to a soap for removing makeup and a method for preparing the same, which contain plant extracts which are effective for sensitive skin such as atopy and acne through anti-inflammatory action.

As with the convenient living environment of modern people, environmental pollution, instant-oriented eating, stress and irregular lifestyles cause many skin problems. Due to this, skin diseases have recently increased rapidly, and according to this trend, development of soaps including natural products in soaps used for basic cleaning has been actively performed.

The general soap used for skin cleansing is alkali salt of higher fatty acid, which has been used for a long time with abundant bubbles and cleansing power. Soap is made of sodium hydroxide for various animal fats and vegetable fats and then saponified with sodium hydroxide. After making neat soap of degree, it adds fragrance to remove unpleasant odor, and adds various additives such as various softeners or moisturizers for the purpose of moisturizing and lubricity of the skin. Say what has been done.

The general soap manufacturing method used for skin cleaning can be largely divided into saponification, neutralization and methyl ester saponification. The saponification method is a method of obtaining soap and glycerin by hydrolyzing fats and oils with alkali. The neutralization method is obtained by refining fats and oils by using a catalyst such as an acid or a metal oxide at high temperature and high pressure to decompose the glycerol and fatty acids. It is then neutralized with alkali. The methyl ester saponification method is a method in which a fat or oil is treated with methanol to produce methyl ester, followed by reaction of methyl ester with alkali to obtain soap and methanol.

General soap prepared in this way contains chemical additives such as surfactants, EDTA (ethylenediaminetetraacetic acid), antioxidants, solids, preservatives, and artificial pigments. If you enter your eyes or mouth, it may be released little by little, but anything that enters through your skin will remain in your body. Surfactants in the chemical additives take blood through the skin cell membrane and travel throughout the body, causing disorders in cells such as the brain, heart, liver and spleen. Therefore, the body's immunity is weakened and various diseases occur, and it is presumed to be the main cause of atopic dermatitis.

In addition, the chemical soap prepared by the general method does not disappear no matter how dilute, and the surface activity is the result of feeding the organic matter to the microorganisms, so the population will increase rapidly. This leads to dissolved oxygen, which causes red tides in rivers, lakes, and seas.

Due to these problems and the dangers associated with them, the use of natural soaps has soared and the population of natural soaps made at home has increased. Natural soaps, unlike chemical soaps prepared in the usual way, do not become a problem of environmental pollution when they are mixed with water and lose their surfactant activity and are decomposed by microorganisms in one day.

Therefore, the present invention was prepared by adding a gojija extract, soap paste extract, Echochocho extract, artichoke extract and licorice extract to natural soaps of colorless and preservative-free soaps and plant-containing soap suitable for atopic skin or sensitive skin and a preparation method thereof. .

Hereinafter, a brief look at the wolfberry, soap paste, eoseongcho, artichoke and licorice used as the material of the present invention.

Wolfberry ( Lycium chinense ) is a deciduous shrub belonging to the family Obsidian and is the fruit of goji berry and is distributed throughout Asia including Korea. Ingredients include Betaine, Zeaxanthin, Carotene, Thiamine, Vitamin A, B1, B2 and C, which contain a lot of vitamin C, which is good for skin care and is rich in fiber.

Soap ( Saponaria officinalis ) is a perennial plant of dianthus and distributed throughout Korea. The root contains saponin, which is used as a medicine and dried in the fall to be used as a treatment for chronic skin diseases. Plants and leaves can be used to wash wool or silk as a substitute for soap.

Eochocho ( Houttuynia cordata ) is a perennial plant of over three hundred years, distributed in Korea (Ulleungdo, Anmyeondo, Geoje), Japan, China, the Himalayas, and Java. It contains 0.005% of essential oils. Methyl nonyl ketone and myrcene are the main ingredients. Decanoyl acetaldehyde and Laurinaldehyd cause an unpleasant odor. Quercitrin is contained in leaves, and isoquercitrin is contained in flower and fruit ears.

Artichoke ( Cynara scolymus ) is a perennial plant of the Asteraceae family and enjoys a mild climate, so it can only be wintered in the southern part of Korea and can be easily grown on the southern coast of Korea or Jeju Island. Protein, vitamin A, C, calcium, iron, phosphorus, sugars, inulin, selenium (selenium) and the like is contained. Selenium acts on an enzyme system that lowers the concentration of peroxides in cells to prevent the production of free radicals, which is effective in preventing skin aging and treating inflammation.

Licorice ( Glycyrrhiza uralensis is a perennial herbaceous plant called Ural Licorice and Bent Licorice. It grows in Russia (Siberia), Iran, Afghanistan, Pakistan, China (Gamseong, Xinjiang) and Mongolia, and is also grown in Korea. European licorice is distributed in Southern Europe, Central Asia, and China. Glycyrrhizin, Sucrose, Glucose, Liquiritin, and Licoricidin are included. Glycyrrhizin is a detoxifying effect of diphtheria toxin, tetanus toxin, codeine hydrochloride, strychnine acetate, snake venom and puffer fish poison, and also has an anti-inflammatory action, which also suppresses edema. In addition, when the skin eczema and acne on the face is severe acne, such as gold and silver take a therapeutic effect.

Looking at the prior documents related to the present invention, Korean Patent Publication No. 10-1079915 (Previous Document 1) is described with respect to the mixed extract of soap paste, shiho and seaweed and the cosmetic composition containing it as a surfactant. Republic of Korea Patent Publication No. 10-1209189 (Prior Document 2) is described with respect to herbal soap to which herbal herbs are added. Korean Unexamined Patent Publication No. 10-2014-0071570 (Previous Document 3) describes a natural soap composition for skin improvement comprising a herbal extract and herbal powder.

Looking at the contents of the prior document 1, it is described with respect to the natural surfactant containing a mixed extract of soap paste, shiho and seaweed.

Looking at the contents of the prior document 2, the description of the herbal soap containing the extract of three hundred eoseongcho extract, centella, sewage, water-soluble phytoncide, machi, ginseng, cheongung, gold, Angelica and other herbal extracts extracted from herbs containing ginseng It is.

Looking at the contents of the prior document 3, herbal extracts and herbal powders, rosemary extract, pine extract, phytoncide, apricot seed extract, chamomile extract, evening primrose seed extract, bergamot extract, eucalyptus extract, mugwort extract, chaga extract, buckwheat extract, deflector Extract, Echochocho extract, Wolfberry extract, Angelica extract, Licorice extract, Dermis extract, Root-root extract, Aloe vera, Chitooligosaccharide, Xanthohumol, Germinated brown rice, Turmeric, Cheongung, Silkworm, Yulpi, Mulberry leaf, Yulmu, Mung bean and Green tea A natural soap composition for skin improvement is described.

Prior literatures contain one or more of Goji berry extract, Soap paste extract, Echo extract, Artichoke extract and Licorice extract used in the present invention, but do not contain all, in particular does not contain artichoke extract as an active ingredient . Therefore, the efficacy in the preceding documents is not only excellent effect of antibacterial and moisturizing function, but also contain the artichoke extract skin whitening and pores convergence effect also can not reach the efficacy of the present invention excellent.

The purpose of the present invention is to remove the makeup ingredients, whitening effect, pore convergence effect, moisturizing effect, anti-aging effect, as well as anti-inflammatory effect Gojija extract, soap extract, Echo extract, Artie The present invention provides a soap for removing makeup containing a plant component extract such as choke extract and licorice extract, and a method for preparing the same.

The present invention comprises the steps of pulverizing wolfberry, soap paste, fish vinegar, artichoke and licorice as a plant material; Mixing an organic solvent and an inorganic solvent with the pulverized plant material; Homogenizing the plant material in which the organic solvent and the inorganic solvent are mixed; Ultrasonically crushing the homogenized plant material; Vacuum-pressure extracting the ultrasonically crushed plant material; Filtering the extracted plant material; Concentrating and powdering the filtered plant extract; Adding and mixing Soap noodle, titanium dioxide and spices to each of the powdered plant extracts; And a step of forming the mixed mixture by stirring; to solve the technical problem by providing a make-up removing soap and a method for producing the same containing a plant component extract comprising a.

The present invention is the addition of goji berry extract, soap paste extract, fish vinegar extract, artichoke extract and licorice extract extracted by vacuum pressure extraction method using organic and inorganic solvents, as well as anti-inflammatory effect, whitening effect, pore convergence effect, moisturizing effect, anti-aging effect By providing a plant material-containing soap and a method for producing the same that is effective for sensitive skin such as atopy and acne through the action to solve the technical problem.

Soap according to the present invention by containing a botanical extract such as goji extract, soap paste extract, Echochocho extract, artichoke extract and licorice extract, make-up removal effect, whitening effect, pore convergence effect, moisturizing effect, anti-aging effect Holds. In addition, there is an effect to improve sensitive skin, such as atopy and acne through anti-inflammatory action.

1 is a flow chart showing a preferred embodiment of a method for preparing a soap for removing makeup containing a plant extract such as wolfberry extract, soap extract, Echo extract, artichoke extract and licorice extract according to the present invention.

The terms or words used in this specification and claims are not to be construed as limiting in their usual or dictionary meanings, and the inventors may appropriately define the concept of terms in order to best describe their invention. It should be interpreted as meaning and concept corresponding to the technical idea of the present invention based on the principle that the present invention.

Therefore, the experimental examples and reference examples described herein are only one of the most preferred embodiments of the present invention and do not represent all of the technical idea of the present invention, and various equivalents and modifications that may be substituted for them at the time of the present application. It should be understood that there may be examples.

The present invention relates to a makeup removal soap containing Goji berry extract, soap paste extract, eochocho extract, artichoke extract and licorice extract extracted by vacuum decompression method using an organic solvent and an inorganic solvent, and a preparation method thereof.

First, the Goji extract, soap extract, Echo extract, artichoke extract and licorice extract is a plant material, pulverized wolfberry, soap paste, aeocho, artichoke and licorice, respectively, the organic solvent and inorganic solvent in the pulverized plant material Mixing step, homogenizing the plant material mixed with the organic solvent and inorganic solvent, ultrasonic crushing the homogenized plant material, vacuum pressure extraction of the ultrasonic crushed plant material, the extracted plant material It is obtained through the step of filtering and the step of concentrating and powdering the filtered plant extract.

Next, by adding and mixing soap noodle, titanium dioxide, and fragrance to each of the powdered plant extracts, the plant material-containing soap through stirring and molding the mixed mixture. To prepare.

Example 1 Soap Manufacturing Method

( 1) crushing step

As a plant material, it is pulverized wolfberry, soap paste, fish vinegar, artichoke and licorice.

Rotary crusher, jaw crusher, roll crusher, cone crusher, hammer crusher, impact crusher, hammer crusher mill, rod mill, ball mill, raymond mill, super mill, roll mill, pin mill, jet mill, konica It may be milled using a ball mill (Conical ball mill) or vibration mill (Vibration mill).

Grinding may be performed in a size of 1 ~ 100 mesh, it can be set in various ways depending on the design conditions.

In the case of a plant material which is not easily crushed according to design conditions, it may be applied by repeating the grinding step two or more times.

(2) solvent mixing step

The organic and inorganic solvents are mixed with the ground plant material.

The step of using an organic solvent and an inorganic solvent was used to increase the extraction efficiency by selecting a solvent according to the components.

Organic solvents include ethanol, methanol, fatty oil, glycerin, propylene glycol, ether, chloroform, petroleum ether and hexane (hexane), benzene, methylene chloride, ethyl acetate, acetone, butanol and isopropanol, and the inorganic solvent may be selected from water, liquid ammonia (liquid ammonia), antimony trichloride, hydrogen fluoride and the like.

Preferably ethanol may be used as the organic solvent, water may be used as the inorganic solvent.

The blending ratio of the organic solvent and the inorganic solvent may be 1: 9 to 9: 1, preferably 3: 7 to 4: 6. In addition, the mixing ratio of the organic solvent and the inorganic solvent may be set in various ways depending on the type of material or design conditions.

For example, in order to extract essential oils contained in fish paste, the blending ratio of the organic solvent may be further increased. That is, each solvent blending ratio can be adjusted according to the components to be extracted from the plant material.

(3) homogenization step

Homogenize plant material mixed with organic and inorganic solvents.

When homogenizing a plant material mixed with an organic solvent and an inorganic solvent can be carried out using a high-speed homogenizer, depending on the conditions can be used to disperse emulsion dispersion by adding mechanical dispersion and surfactant. In addition, the conditions of the high speed homogenizer may be set in various ways.

(4) shredding step

Ultrasonic crushing of homogenized plant material.

Ultrasonic crushing may be performed using an ultrasonic crusher. The crushing time may be performed for 5 to 60 minutes, preferably 25 to 40 minutes. In addition, the crushing time can be set variously according to the design conditions.

Ultrasonic crushers cause molecular motions due to the unique cavitation of the ultrasonic waves, and the molecular motions act as an activation energy and thus have an effect of improving responsiveness when performing a process such as extraction and concentration. When the sample is crushed using an ultrasonic crusher as a device that has been introduced into the protein production process, the production rate of the protein contained in the sample may be improved.

(5) extraction step

Extract the plant extract from the ultrasonically crushed plant material.

The extraction may be a variety of extraction methods such as carbon dioxide supercritical extraction, steam distillation, vacuum extraction, reduced pressure extraction, microwave process extraction, percolation extraction, but may be preferably vacuum pressure extraction .

In the case of the vacuum decompression method, the internal conditions may be set to be extracted for 3 to 7 hours at a temperature of 60 ~ 80 ℃, preferably may be set to be extracted for 5 hours at a temperature of 70 ℃. In addition, it can be variously set according to the design conditions.

(6) filtration step

The extracted plant material is filtered.

Filtration includes chromatography, suction filtration, atmospheric filtration, reduced pressure filtration, pressure filtration, ultrafiltration, microfiltration, and reverse osmosis filtration, and may be variously selected and used according to design conditions.

Filtration time, temperature and frequency may also vary depending on the design conditions, and may be filtered using a method other than the above-described filtration method or using two or more methods.

(7) concentration and powdering step

The filtered plant extract is concentrated.

Concentration may be various concentration methods such as membrane concentration, freeze concentration, dry concentration, evaporation concentration, vacuum concentration and reduced pressure concentration, preferably concentrated under reduced pressure.

The concentrated plant extract may be dried to prepare a powder form.

Drying may be used in a variety of drying methods, such as hot air drying, cold air drying, far infrared drying, electric drying, microwave drying and freeze drying, preferably freeze-drying to remove the solvent and water.

Thereafter, when the powder is pulverized using a pulverizer, a powder used for soap can be obtained. Preferably, the powder can be prepared by pulverizing finely with a pulverizer.

(8) mixing step

Each powdered plant extract is mixed by adding soap soap noodle, titanium dioxide and flavorings.

At this time, the mixing ratio of the mixture in the mixing step (So) Noodle (Soap noodle) 90 parts by weight, 4 ~ 10 parts by weight of Goji berry extract, 0.3 ~ 0.8 parts by weight soap extract, 0.05 ~ 0.2 parts by weight Echochocho extract, artichoke extract 0.05 ~ It is preferably composed of 0.2 parts by weight, licorice extract 0.05-0.2 parts by weight, 0.1-0.5 parts by weight of titanium dioxide and 0.5-2 parts by weight of fragrance.

According to a more preferred feature of the invention, the Soap noodle is extracted from the palm.

(9) forming step

The mixed mixture is shaped by stirring.

Subsequently, one complete soap is completed by packaging the product into a suitable shape and size through molding.

Reference Example 1. Evaluation of effectiveness on using soap

In order to evaluate the effectiveness on the use of soap according to the present invention, the detergency, the moisturizing power and the degree of irritation were evaluated.

In the evaluation, soaps prepared under the conditions described in Example 1 and two commercially available soaps were used as controls, and the evaluation was performed on 25 adults.

The evaluation was conducted by the user applying the cosmetics using each soap, and the cleaning power, moisturizing power, and irritation felt after the cleaning were conducted through a questionnaire.

Evaluation of the cleaning power was evaluated through the questionnaire about the residual feeling of cosmetics such as slipperiness and stickiness after washing and the degree of cosmetic removal.

Moisturizing power was evaluated through a questionnaire about the degree of feeling of skin pulling after washing and moisture.

The irritability was evaluated by the questionnaire about the feeling of tickling, tingling or heat after washing the face.

The five-point scale was used to evaluate the effectiveness, and the higher the score was, the higher the degree was set.

soap	Cleaning power	Moisturizing	pepper
Soap according to Example 1	3.23 ± 0.31	4.32 ± 0.15	2.86 ± 0.33
Plain Soap 1	3.11 ± 0.42	3.40 ± 0.42	3.15 ± 0.38
Plain soap 2	3.02 ± 0.51	2.90 ± 0.64	3.21 ± 0.19

As a result of the evaluation, the cleaning power was evaluated as having high cleaning power in the order of soap, general soap 1 and soap 2 according to Example 1.

Moisturizing power was evaluated in the order of soap, general soap 1 and general soap 2 according to Example 1, it was evaluated that the moisturizing power of the soap according to Example 1 is superior to the moisturizing power of the general soap 1 and the general soap 2.

Stimulus was evaluated in the order of soap 2, soap 1 and soap in accordance with Example 1, the soap according to Example 1 was evaluated to be somewhat lower than the stimulation of soap 1 and soap 2.

In other words, it can be seen that the soap according to the present invention is excellent in moisturizing power as well as cleaning power and less skin irritation.

Claims (6)

1. Pulverizing wolfberry, soap paste, fish vinegar, artichoke and licorice as plant material, respectively;

   Mixing an organic solvent and an inorganic solvent with the pulverized plant material;

   Homogenizing the plant material in which the organic solvent and the inorganic solvent are mixed;

   Ultrasonically crushing the homogenized plant material;

   Extracting a plant extract from the ultrasonically crushed plant material;

   Filtering the extracted plant extracts;

   Concentrating and powdering the filtered plant extract;

   Adding and mixing Soap noodle, titanium dioxide and spices to each of the powdered plant extracts; And

   A method of manufacturing a soap for removing makeup comprising a plant component extract, characterized in that it comprises a; forming by stirring the mixed mixture.
2. The method according to claim 1,

   In the step of mixing the organic solvent and inorganic solvent, the mixing ratio of the organic solvent and the inorganic solvent is 3: 7 ~ 4: 6 manufacturing method of the makeup removal soap containing a plant component extract, characterized in that.
3. The method according to claim 1,

   The vacuum decompression step is a method for producing makeup soap containing a plant component extract, characterized in that extracted for 3 to 7 hours at a temperature of 60 ~ 80 ℃.
4. The method according to claim 1,

   The mixing ratio of the mixture in the mixing step is 솝 noodle (Soap noodle) 90 parts by weight, 4 ~ 10 parts by weight of Goji berry extract, 0.3 ~ 0.8 parts by weight soap extract, 0.05 ~ 0.2 parts by weight Echochocho extract, artichoke extract 0.05 ~ 0.2 parts by weight, licorice extract 0.05 ~ 0.2 parts by weight, titanium dioxide (titanium dioxide) 0.1 ~ 0.5 parts by weight and fragrance make-up soap containing a plant component extract, characterized in that 0.5 to 2 parts by weight.
5. Makeup removal soap containing the plant component extract manufactured by the manufacturing method of any one of Claims 1-4.
6. The method according to claim 1,

   Extraction of the plant extract is

   Soap for removing makeup containing plant extracts, characterized in that extracted by one of carbon dioxide supercritical extraction, steam distillation, vacuum extraction, reduced pressure extraction, microwave process extraction, percolation extraction method Manufacturing method.

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