CN104922310A - Traditional Chinese medicine composition with bacteriostasis function and application of traditional Chinese medicine composition to daily necessities - Google Patents
Traditional Chinese medicine composition with bacteriostasis function and application of traditional Chinese medicine composition to daily necessities Download PDFInfo
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Abstract
The invention discloses a traditional Chinese medicine composition with a bacteriostasis function and the application of the traditional Chinese medicine composition to daily necessities. The traditional Chinese medicine composition is prepared from the following traditional Chinese medicines in parts by weight: 10 to 40 parts of heartleaf houttuynia herb, 5 to 35 parts of Chinese brake herb, 5 to 30 parts of Chinese fever vine, 5 to 25 parts of liquoric root and 5 to 20 parts of philippine violet herb. The traditional Chinese medicine composition is obtained by high-pressure homogeneous extraction, centrifugal separation, membrane concentration, macroporous resin adsorption separation and membrane concentration. The traditional Chinese medicine composition has a bacteriostasis effect, has an antiallergic function, an eczema treatment function and the like, and can be used for preparing the daily necessities such as anti-dandruff shampoo, antibacterial shower gel, an antibacterial hand-washing solution, acne-removing cosmetics and an antibacterial perfumed soap.
Description
Technical field
The present invention relates to a kind of Chinese medicine composition, the extract of said composition has bacteria resistance function, can be applied to preparation article of everyday use, belongs to article of everyday use technical field.
Background technology
In daily life, in particularly spring and summer, ambient humidity increases people, and the temperature rises, various antibacterial and virus active, antibacterial and virus are always along with the contact between article and other channels constantly propagate on the skin of human body." science " magazine ran according on May 29th, 2009: the skin of human body is antibacterial " ideal homeland ", and body surface is covered with about 1000 kinds of antibacterials altogether, the antibacterial resided on skin is that quantity or kind all reach astonishing degree.Particularly under humidity also grows crinite oxter and scalp, just look like be Tropical rain forest, for growing of antibacterial provides extraordinary living environment.These antibacterials on skin bring very large potential safety hazard to people's life, and cause some dermatosis, as dandruff, eczema, psoriasis, acne, antibiotic-resistant infectious disease etc.
Along with the raising of people's living standard, Personal hygiene more and more be familiar with by consumer and pay attention to, the personal care articles of antibiotic skin-care also becomes the necessary of people, as having the fancy soap, medicated soap, handwashing liquid, bath foam, shampoo etc. of antibacterial functions.But the bacteriostatic active ingredients of these products also antibacterial of mainly some chemosynthesis and antibacterial, has larger harm to human body skin at present.So find the developing direction that safe, nontoxic, efficient anti-virus activities bactericide is the daily chemical product with antibacterial functions.In addition, from market development situation and consumer psychology, daily chemical product is forming the new trend of naturalization, functionalization.The cry of " component naturalization ", " going back to nature " has become the trend of world's daily chemical industry.So the Chinese medicine with bacteria resistance function has been applied to current study hotspot in daily chemical product.As CN201310212388.7 discloses a kind of Fructus Cannabis antibacterial liquid and preparation method thereof and application; Patent CN201210126195.5 discloses Multi-herb antibacterial liquid, the compositions wherein containing plurality of Chinese such as Folium Artemisiae Argyi, Ramulus Mori, the Radix Angelicae Dahuricae, Rhizoma Alpiniae Officinarum; Patent CN200710003593.7 discloses a kind of Chinese medicinal herb antibiotic bacteriostat, is made up of Chinese medicines such as Herba Dianthi, Radix Sophorae Flavescentis, Herba Polygoni Avicularis, Radix Et Rhizoma Rhei, Radix Glycyrrhizae, Fructus Gardeniae, Rhizoma Bistortae, Cortex Phellodendris.
Summary of the invention
The object of the invention is the defect of the antibacterial in order to overcome chemosynthesis, providing a kind of Chinese medicine composition and preparation method thereof, this Chinese medicine composition has potent antibacterial function.
To achieve the object of the present invention, present invention employs following technical scheme:
A Chinese medicine composition for bacteria resistance function, is characterized in that being made up of the Chinese medicine of following weight portion: Herba Houttuyniae 10 ~ 40 parts; Herba Pteridis Multifidae 5 ~ 35 parts; Fevervine 5 ~ 30 parts; 5 ~ 25 parts, Radix Glycyrrhizae; Herba Violae 5 ~ 20 parts.
Preferably, a kind of Chinese medicine composition of bacteria resistance function, is characterized in that being made up of the Chinese medicine of following weight portion: Herba Houttuyniae 30 parts; Herba Pteridis Multifidae 20 parts; Fevervine 20 parts; 15 parts, Radix Glycyrrhizae; Herba Violae 15 parts.
Preferably, a kind of Chinese medicine composition of bacteria resistance function, is characterized in that being made up of the Chinese medicine of following weight portion: Herba Houttuyniae 25 parts; Herba Pteridis Multifidae 18 parts; Fevervine 22 parts; 20 parts, Radix Glycyrrhizae; Herba Violae 15 parts.
Preferably, a kind of Chinese medicine composition of bacteria resistance function, is characterized in that being made up of the Chinese medicine of following weight portion: Herba Houttuyniae 28 parts; Herba Pteridis Multifidae 20 parts; Fevervine 22 parts; 18 parts, Radix Glycyrrhizae; Herba Violae 12 parts.
Preferably, a kind of Chinese medicine composition of bacteria resistance function, is characterized in that being made up of the Chinese medicine of following weight portion: Herba Houttuyniae 25 parts; Herba Pteridis Multifidae 20 parts; Fevervine 15 parts; 25 parts, Radix Glycyrrhizae; Herba Violae 15 parts.
A kind of preparation method of Chinese medicine composition of bacteria resistance function, it is characterized in that following these steps to be prepared: Chinese medicine is pulverized, respectively with 20 ~ 100 mesh sieve screenings, mixing, be that 5:1 ~ 20:1 adds Extraction solvent by liquid material mass ratio, after soaking 1 ~ 5h, extract at room temperature is carried out with high pressure homogenization method machine under 10 ~ 100MPa extracts pressure, extracting solution is after centrifugalize, with membrance concentration, concentrated solution macroporous resin adsorption, be the ethanol repeatedly eluting of 10 ~ 95% again by volume fraction, collect eluent, membrance concentration is 1:0.5 ~ 1:5 to the mass ratio of extracting solution and Chinese medicine, add butanediol again to dissolve, filter, obtained Chinese medicine composition.Extraction solvent is water, ethanol or ethanol water.
Another object of the present invention is applied to by the Chinese medicine composition of above-mentioned a kind of bacteria resistance function to prepare article of everyday use.
For realizing this purpose of the present invention, present invention employs following technical scheme: be used for preparing article of everyday use by above-mentioned Chinese medicine composition, it is characterized in that the Chinese medicine composition containing above-mentioned bacteria resistance function in article of everyday use, its consumption is 0.01 ~ 20% by weight percentage, and preferable amount is 1 ~ 10% by weight percentage.
Beneficial effect of the present invention: human body skin has a lot of bacterium, some bacterium can make skin infection, and the lighter causes the symptom such as acne, eczema, allergy, inflammation, and severe one is threat to life even.In order to the infection of prevention and therapy skin, the present invention adopts the theory of Chinese medical science of monarch to design Chinese medicine composition, and Herba Houttuyniae is monarch drug, has very strong heat-clearing and toxic substances removing, antiinflammatory, antiviral efficacy; Herba Pteridis Multifidae and Herba Violae are ministerial drug, and both all have clearing away heat-damp and promoting diuresis, cooling blood for hemostasis, subduing swelling and detoxicating effect; Fevervine is adjuvant drug, has expelling wind and removing dampness, removing toxic substances and promoting subsidence of swelling, promoting blood circulation and stopping pain and antiallergic effect; Radix Glycyrrhizae is for making medicine, and coordinating the actions of various ingredients in a prescription, has effect of heat-clearing and toxic substances removing, dissipating blood stasis for subsidence of swelling, pain relieving and treatment ulcer.
The Chinese medicine composition of a kind of bacteria resistance function that the present invention obtains, not containing the material of chemosynthesis, nontoxic, have no side effect, safe and reliable, skin can be directly used in, effective removal and suppress the microorganisms such as antibacterial on human body skin, fungus and virus, can effectively prevent human body skin by effects such as infected by microbes, antiallergic and treatment eczemas simultaneously.Chinese medicine composition of the present invention may be used for the bacteria resistance function material of the article of everyday use making to have bacteria resistance function, can join in the article of everyday use such as shampoo, bath foam, handwashing liquid, cosmetics, fancy soap.
The present invention adopts high pressure homogenization method technology to carry out the extraction of Chinese medicine composition effective ingredient, this extractive technique is a kind of novel extractive technique, its principle be homogenizer under elevated pressure conditions, suspension is by decompression in adjustable current restricting slit process, expand, blast, the comprehensive effects such as shearing and high-speed impact, granular powder is in a liquid broken into very small size, diameter about 0.1 ~ 2 μm, this process collection ultrasonic grinder, colloid mill, ball grinding function is in one, the comprehensive effect that granule area increases and high pressure brings in this work process greatly accelerates infiltration and the diffusion of soluble substance.The number of advantages such as this extractive technique has extract at room temperature, extraction ratio is high, the time is short, simple to operate and energy consumption is low, higher than the extract pharmacologically active of conventional heating reflux, extract, microwave extraction, than the reduced investment of supercritical extraction, easy industrialization transforms, more consuming time than infusion process short, efficiency is high.
The concentrated employing membrance concentration of extracting solution of the present invention, overcomes the concentrated energy consumption height of heating and active matter destroys large defect.
Detailed description of the invention
Below by way of specific embodiment, the present invention is further illustrated, but these embodiments are just in order to illustrate, are not limitations of the present invention.
embodiment 1a kind of Chinese medicine composition (I) of bacteria resistance function
A Chinese medicine composition for bacteria resistance function, is made up of the Chinese medicine of following weight portion: Herba Houttuyniae 30 parts; Herba Pteridis Multifidae 20 parts; Fevervine 20 parts; 15 parts, Radix Glycyrrhizae; Herba Violae 15 parts.
The preparation method of this Chinese medicine composition is: pulverized by Chinese medicine, with 40 mesh sieve screenings, mixing, be the ethanol water that 10:1 adds that volume fraction is 60% by liquid material mass ratio, after soaking 2h, extract at room temperature is carried out with high pressure homogenization method machine under 50MPa extracts pressure, extracting solution is after centrifugalize, with membrance concentration, concentrated solution macroporous resin adsorption, be 50% by volume fraction again, ethanol twice eluting of 80%, collect eluent, membrance concentration is 1:1 to the mass ratio of extracting solution and Chinese medicine, add again and dissolve with the butanediol of the concentrated rear same weight of extracting solution, filter, obtained Chinese medicine composition.
comparative example 1-5
Comparative example 1 is for being used alone Herba Houttuyniae 100 parts;
Comparative example 2 is for being used alone Herba Pteridis Multifidae 100 parts;
Comparative example 3 is for being used alone fevervine 100 parts;
Comparative example 4 is for being used alone 100 parts, Radix Glycyrrhizae;
Comparative example 5 is for being used alone Herba Violae 100 parts;
Preparation method is consistent with embodiment 1.
embodiment 2a kind of Chinese medicine composition (II) of bacteria resistance function
A Chinese medicine composition for bacteria resistance function, is made up of the Chinese medicine of following weight portion: Herba Houttuyniae 25 parts; Herba Pteridis Multifidae 18 parts; Fevervine 22 parts; 20 parts, Radix Glycyrrhizae; Herba Violae 15 parts.
The preparation method of this Chinese medicine composition is: pulverized by Chinese medicine, with 60 mesh sieve screenings, mixing, be the ethanol water that 12:1 adds that volume fraction is 50% by liquid material mass ratio, after soaking 1.5h, extract at room temperature is carried out with high pressure homogenization method machine under 60MPa extracts pressure, extracting solution is after centrifugalize, with membrance concentration, concentrated solution macroporous resin adsorption, be 40% by volume fraction again, ethanol twice eluting of 80%, collect eluent, membrance concentration is 1:1 to the mass ratio of extracting solution and Chinese medicine, add again and dissolve with the butanediol of the concentrated rear same weight of extracting solution, filter, obtained Chinese medicine composition.
embodiment 3a kind of Chinese medicine composition (III) of bacteria resistance function
A Chinese medicine composition for bacteria resistance function, is made up of the Chinese medicine of following weight portion: Herba Houttuyniae 28 parts; Herba Pteridis Multifidae 20 parts; Fevervine 22 parts; 18 parts, Radix Glycyrrhizae; Herba Violae 12 parts.
The preparation method of this Chinese medicine composition is: pulverized by Chinese medicine, with 80 mesh sieve screenings, mixing, be the ethanol water that 8:1 adds that volume fraction is 70% by liquid material mass ratio, after soaking 1h, extract at room temperature is carried out with high pressure homogenization method machine under 40MPa extracts pressure, extracting solution is after centrifugalize, with membrance concentration, concentrated solution macroporous resin adsorption, be 30% by volume fraction again, 60%, ethanol three eluting of 95%, collect eluent, membrance concentration is 1:1 to the mass ratio of extracting solution and Chinese medicine, add again and dissolve with the butanediol of the concentrated rear same weight of extracting solution, filter, obtained Chinese medicine composition.
embodiment 4a kind of Chinese medicine composition (IV) of bacteria resistance function
A Chinese medicine composition for bacteria resistance function, is characterized in that being made up of the Chinese medicine of following weight portion: Herba Houttuyniae 25 parts; Herba Pteridis Multifidae 20 parts; Fevervine 15 parts; 25 parts, Radix Glycyrrhizae; Herba Violae 15 parts.
The preparation method of this Chinese medicine composition is: pulverized by Chinese medicine, with 40 mesh sieve screenings, mixing, be the ethanol water that 15:1 adds that volume fraction is 40% by liquid material mass ratio, after soaking 2h, extract at room temperature is carried out with high pressure homogenization method machine under 70MPa extracts pressure, extracting solution is after centrifugalize, with membrance concentration, concentrated solution macroporous resin adsorption, be 30% by volume fraction again, 50%, ethanol three eluting of 75%, collect eluent, membrance concentration is 1:1 to the mass ratio of extracting solution and Chinese medicine, add again and dissolve with the butanediol of the concentrated rear same weight of extracting solution, filter, obtained Chinese medicine composition.
the preparation of embodiment 5 antibacterial bath liquor
Table 1 provides the antibacterial bath liquor formula of the Chinese medicine composition containing bacteria resistance function, and the consumption of each material represents with mass fraction.
The preparation method of antibacterial bath liquor: the deionized water in component A is heated to 85 DEG C, add sodium chloride, EDTA-2Na, citric acid successively, after raw material is fully dissolved, add polyoxyethylenated alcohol sodium sulfate AES, cocamido propyl betaine CAB-35, alkanolamide 6501, after stirring and dissolving, temperature is adjusted to 75 DEG C, add pearlescent flake, stir, pass into cooling water, progressively cool to 45 DEG C, add all raw materials of B component, stir, continue to be cooled to 38 DEG C, can antibacterial bath liquor be obtained.
the preparation of embodiment 6 anti-bacterial hand lotion
Table 2 provides the anti-bacterial hand lotion formula of the Chinese medicine composition containing bacteria resistance function, and the consumption of each material represents with mass fraction.
The preparation method of anti-bacterial hand lotion: the deionized water in component A is heated to 85 DEG C, add sodium chloride, EDTA-2Na, citric acid successively, after raw material is fully dissolved, add polyoxyethylenated alcohol sodium sulfate AES, cocamido propyl betaine CAB-35, alkanolamide 6501, after stirring and dissolving, pass into cooling water, progressively cool to 45 DEG C, add all raw materials of B component, stir, continue to be cooled to 38 DEG C, can anti-bacterial hand lotion be obtained.
the preparation of embodiment 7 Antibiotic liquid detergent
Table 3 provides the Antibiotic liquid detergent formula of the Chinese medicine composition containing bacteria resistance function, and the consumption of each material represents with mass fraction.
The preparation method of Antibiotic liquid detergent: be dissolved in deionized water by the sodium hydroxide in component A, slowly adds DBSA and sodium hydroxide generation neutralization reaction in batches.After stirring and dissolving, add all raw materials of B component in order successively, stirring and dissolving is even, can obtain Antibiotic liquid detergent.
the preparation of embodiment 8 Antibacterial soaps
Table 4 provides the Antibacterial soaps formula of the Chinese medicine composition containing bacteria resistance function, and the consumption of each material represents with mass fraction.
The preparation method of Antibacterial soaps: by even for material stirring and dissolving all in B component; Titanium dioxide in component A is mixed homogeneously with soap base, then the mixed liquor of B component is sprayed in component A, uniform mixing, after three-roll grinder grinding evenly, then through operations such as press strip, stripping and slicing, printings, can Antibacterial soaps be obtained.
the preparation of embodiment 9 anti-dandruff shampoo
Table 5 provides the anti-dandruff shampoo formula of the Chinese medicine composition containing bacteria resistance function, and the consumption of each material represents with mass fraction.
The preparation method of anti-dandruff shampoo: the deionized water in component A is heated to 85 DEG C, add ammonium chloride, EDTA-2Na, citric acid, cation guar gum successively, maintain the temperature at 80 ~ 85 DEG C, after raw material is fully dissolved, add AESA AESA, cocamido propyl betaine CAB-35, alkanolamide 6501, stirring and dissolving.Temperature is adjusted to 75 DEG C, add cetostearyl alcohol, pearlescent flake, after fusing, stir, pass into cooling water, progressively cool to 45 DEG C, add all raw materials of B component, stir, continue to be cooled to 38 DEG C, can anti-dandruff shampoo be obtained.
the preparation of embodiment 10 anti-acne moisturiser
Table 6 provides the anti-acne moisturiser formula of the Chinese medicine composition containing bacteria resistance function, and the consumption of each material represents with mass fraction.
The preparation method of anti-acne moisturiser: by the component A mixing in formula table, be heated to 85 DEG C, fusing stirs, as oil phase; By the B component mixing in formula table, be heated to 85 DEG C, stirring and dissolving is even, as aqueous phase.Added by oil phase in aqueous phase, stir, emulsifying, after 5 minutes, when stirring is cooled to below 45 DEG C, adds component C, stirs, be cooled to 35 DEG C, can obtain anti-acne moisturiser.
the preparation of the common moisturiser of comparative example 6
Table 7 provides the common moisturiser formula of the Chinese medicine composition containing bacteria resistance function, and the consumption of each material represents with mass fraction.
The preparation method of common moisturiser: by the component A mixing in formula table, be heated to 85 DEG C, fusing stirs, as oil phase; By the B component mixing in formula table, be heated to 85 DEG C, stirring and dissolving is even, as aqueous phase.Added by oil phase in aqueous phase, stir, emulsifying, after 5 minutes, when stirring is cooled to below 45 DEG C, adds component C, stirs, be cooled to 35 DEG C, can obtain anti-acne moisturiser.
experimental example 1 bacteriostatic experiment
1, strain
Be separated and screen and obtain mixed vaccine from the hands of human body, face, head, called after A4.
, culture medium
Nutrient agar, beef extract-peptone
3, main agents
Normal saline, 75% ethanol
4, sample
The compositions that embodiment 1-6 obtains and the single medicinal material extracting solution that comparative example 1-5 obtains.
, experimental technique
(1) activation of strain
Get test tube some, after loading the nutrient agar sterilizing of melting, be put into inclined-plane.Aseptically will move on the corresponding slant medium of access for examination strain by method of scoring, each actication of culture many, puts into incubator, antibacterial culturing 18 ~ 24h at 37 DEG C.
(2) preparation of strains tested suspension
Superclean bench carries out sterile working.Take out the strain activated, wash in sterilized triangular flask with appropriate physiological saline solution, bacteria suspension bacteria containing amount (colony forming unit, the CFU) antibacterial of making is 1.0 × 10
8.
(3) inhibition zone test
Adopt Odontothrips loti.The beef extract-peptone solid medium of sterilizing is poured in culture dish, in culture medium, the A4 bacteria suspension of 0.1ml is coated respectively equably after to be solidified, then aseptic Oxford cup is put thereon equidistantly, the extract of the different Chinese herbal medicine of 200 μ l is injected respectively in cup, 75% ethanol, normal saline in contrast, often organize do 3 parallel tests.After cultivating 24 h in 37 DEG C of calorstats, measure the antibacterial circle diameter of various medicine, get its meansigma methods.
, result
Experimental result is shown in Table 8.
Table 8
As shown in Table 8, be used alone Herba Houttuyniae, Herba Pteridis Multifidae, fevervine, Radix Glycyrrhizae, Herba Violae obtain extracting solution have certain bacteriostatic activity, particularly the antibacterial circle diameter of the extracting solution of Herba Houttuyniae, Herba Pteridis Multifidae, fevervine three kinds of Chinese medicines is all greater than 10mm, and bacteriostatic activity is stronger.By the Chinese medicine composition of the bacteria resistance function of the present invention of the composite acquisition of science, its bacteriostasis efficacy is more much better than being used alone the bacteriostasis efficacy of extracting solution that single medicinal material obtains, and illustrates to serve synergistic function after composite.
experimental example 2 zest evaluation experimental
With 30 women and 10 male for object, getting 0.03ml sample with syringe is placed in the coyote hole of speckle examination adhesive tape, longitudinally be affixed on the normal skin of left forearm by the speckle examination adhesive tape being equipped with sample from bottom immediately, light pressing room, to drive away air, and makes trier be uniformly distributed one by one simultaneously.Labelling is carried out, to observe in test position.Pasted skin once every 24 hours, open half an hour after paster, then check according to the term of CTFA guide (1981).Carrying out 6 patch experiments altogether, the 6th day after subsides skin terminates, in order to observe late response, having carried out additional inspection.Data then utilize last check result, compare.Identify with table 9 as standard is carried out.Substances is respectively the anti-acne moisturiser of embodiment 10 preparation and the common moisturiser of comparative example 6 preparation, and result is as shown in table 10.
Table 9 standard of perfection
Table 10 zest evaluation test result
By this result of the test, can recognize that blank experiment is non-stimulated, anti-acne moisturiser prepared by embodiment 10 is non-stimulated to skin, and the irritant reaction of common moisturiser to skin prepared by comparative example 6 still exists.Thus use after the anti-acne moisturiser prepared of the present invention to human body without any allergy and discomfort, illustrate that Chinese medicine composition of the present invention has certain antiallergic effect.
Claims (3)
1. a Chinese medicine composition for bacteria resistance function, is characterized in that being made up of the Chinese medicine of following weight portion: Herba Houttuyniae 10 ~ 40 parts, Herba Pteridis Multifidae 5 ~ 35 parts, fevervine 5 ~ 30 parts, 5 ~ 25 parts, Radix Glycyrrhizae, Herba Violae 5 ~ 20 parts.
2. the preparation method of the Chinese medicine composition of a kind of bacteria resistance function according to claim 1, it is characterized in that following these steps to be prepared: Chinese medicine is pulverized, respectively with 20 ~ 100 mesh sieve screenings, mixing, be that 5:1 ~ 20:1 adds Extraction solvent by liquid material mass ratio, after soaking 1 ~ 5h, extract at room temperature is carried out with high pressure homogenization method machine under 10 ~ 100MPa extracts pressure, extracting solution is after centrifugalize, with membrance concentration, concentrated solution macroporous resin adsorption, be the ethanol repeatedly eluting of 10 ~ 95% again by volume fraction, collect eluent, membrance concentration is 1:0.5 ~ 1:5 to the mass ratio of extracting solution and Chinese medicine, add butanediol again to dissolve, filter, obtained Chinese medicine composition, Extraction solvent is water, ethanol or ethanol water.
3. the Chinese medicine composition of a kind of bacteria resistance function according to claim 1 is preparing the application in article of everyday use, and it is characterized in that the Chinese medicine composition containing a kind of bacteria resistance function according to claim 1 in article of everyday use, its consumption is 0.01 ~ 20% by weight percentage.
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| CN112716867A (en) * | 2021-03-05 | 2021-04-30 | 孔静波 | Bath lotion containing Chinese herbal medicine components and preparation process thereof |
| CN115137676A (en) * | 2021-03-30 | 2022-10-04 | 海南师范大学 | Paederia scandens extract and application thereof in preparing toothpaste |
| CN115137676B (en) * | 2021-03-30 | 2024-03-26 | 海南师范大学 | Paederia scandens extract and application thereof in preparing toothpaste |
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