CN101934059A - Preparation method of extract of traditional Chinese medicine composition with bacteriocidal function and application thereof in daily chemical products - Google Patents
Preparation method of extract of traditional Chinese medicine composition with bacteriocidal function and application thereof in daily chemical products Download PDFInfo
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Abstract
The invention discloses a preparation method of an extract of a traditional Chinese medicine composition with bacteriocidal function and application thereof in daily chemical products, relating to the technical field of traditional Chinese medicine formulations and the daily chemical field. The traditional Chinese medicine composition comprises the following traditional Chinese medicines in percentage by mass: 2-25 percent of honeysuckle, 2-10 percent of chrysanthemum indicum, 1-20 percent of taraxacum, 1-10 percent of liquorice, 1-20 percent of ginger, 2-20 percent of Chinese holly, 2-20 percent of herba andrographis, 2-20 percent of abelmoschus manihot, 1-20 percent of radix salviae miltiorrhizae, 2-30 percent of aloe and 2-20 percent of groundsel. The extract of the traditional Chinese medicine composition is prepared through measuring, mixing, pulverizing, extracting through high pressure homogenization and decoloring with active carbon. The extract of the traditional Chinese medicine composition does not contain chemically synthesized substances, has no toxicity or side effect, can effectively eliminate and kill bacteria on human skin and prevent the human skin from being infected by the bacteria at the same time and can be used for the daily chemical products, such as dandruff remover shampoo, antibacterial bath foam, antibacterial liquid soap, acne-removing cosmetics, antibacterial perfumed soap, and the like.
Description
Technical field
The present invention relates to a kind of method for preparing extractive of Chinese medicine composition, the extract of said composition has sterilizing function, can be applied to prepare cosmetics such as shampoo, bath foam, fancy soap, belongs to field of traditional Chinese, also belongs to the cosmetics technical field simultaneously.
Background technology
People in daily life, particularly spring and summer, ambient humidity increases, the temperature rises, various antibacterials and virus are enlivened, antibacterial and virus are always along with the contact between the article and other channels constantly propagate on the skin of human body." science " magazine according on May 29th, 2009: the skin of human body is antibacterial " desirable home ", and the body surface is covered with about 1000 kinds of antibacterials altogether, and the antibacterial that resides on the skin is that quantity or kind all reach astonishing degree.Under humidity and long crinite oxter and scalp, just look like to be Tropical rain forest, particularly for growing of antibacterial provides extraordinary living environment.These antibacterials on the skin have brought very big potential safety hazard to people's life, and cause some dermatosis, as dandruff, eczema, psoriasis, acne, antibiotic-resistant infectious disease etc.
Raising along with people's living standard, individual's sterilization is familiar with by consumer more and more and is paid attention to, the personal care articles of antibiotic skin-care also becomes people's necessary, as has fancy soap, medicated soap, handwashing liquid, bath foam, shampoo, Wei Lushi of antibacterial functions etc.But the fungicide active ingredient of these products also mainly is the antibacterial of some chemosynthesis at present, and human body skin is had bigger harm.So seek safe, nontoxic, antibacterial is the developing direction with daily chemical product of antibacterial functions efficiently.In addition, from market development situation and consumer psychology, daily chemical product is forming the new trend of naturalization, functionalization.The cry of " naturalization of component ", " going back to nature " has become the trend of world's daily chemical industry.So the Chinese medicine with sterilizing function has been applied to present research focus in daily chemical product.
About preparation method and more existing patents of the application in daily chemical product of Chinese medicine composition with sterilizing function, but the Chinese medicine composition extracting method of these patent introductions substantially all adopts infusion process or heating.And there is length consuming time in infusion process, the defective that effective component extraction rate is not high; And the heating rule can make some Chinese medicine ingredients lose activity because of being heated.Introduced a kind of preparation method of Chinese medicine preparation of disinfecting and sterilizing skin-cleaning as patent CN101744916A, said preparation adopts infusion process to extract Chinese medicine ingredients; Patent CN1398628 has introduced compound recipe dewiness lotion of a kind of cleaning and sterilization and preparation method thereof, and the composite mode of this lotion employing antibiotic and Chinese medicine reaches the sterilization purpose, and the extraction of Chinese medicine wherein also is the method that adopts dipping; Patent CN1439404 has introduced a kind of Chinese medicine preparation and production method of anti-inflammation and sterilization, also is to adopt infusion process to extract Chinese medicine ingredients; Patent CN101249190 has introduced a kind of anti-inflammation and sterilization Chinese medicine compound externally used coating liquid and preparation method thereof, adopts decocting method to extract Chinese medicine ingredients.
The present invention adopts the high pressure homogenize extractive technique to carry out the extraction of Chinese medicine composition effective ingredient, this extractive technique is a kind of novel extractive technique, its principle is that homogenizer is under condition of high voltage, suspension is by decompression in the process of adjustable current limliting slit, expand, blast, comprehensive effects such as shearing and high-speed impact, granule in liquid is ground into very small size, about 0.1～2 μ m of diameter, this process collection ultrasonic grinding machine, colloid mill, spheroid mill function is in one, and the comprehensive effect that the granule area increases and high pressure brings in this work process has greatly quickened the infiltration and the diffusion of soluble substance.Serial advantage such as this extractive technique has extract at room temperature, extraction ratio height, the time is short, simple to operate and energy consumption is low, than the extract pharmacologically active height of conventional heating and refluxing extraction, microwave extraction, than the reduced investment of supercritical extraction, industrialization transforms easily, than infusion process weak point consuming time, efficient height.
Summary of the invention
The objective of the invention is the defective for the antibacterial that overcomes chemosynthesis, a kind of extract of Chinese medicine composition is provided, the extract of this Chinese medicine composition has sterilizing function.
According to purpose of the present invention, the inventor is by to the further investigation of Chinese medicine sterilization mechanism, carried out Chinese medicine and selected repeatedly and make up, and invented a kind of Chinese medicine composition with bactericidal activity, by weight percentage, is made up of following Chinese medicine: Flos Lonicerae 2～25; Flos Chrysanthemi Indici 2～10; Herba Taraxaci 1～20; Radix Glycyrrhizae 1～10; Rhizoma Zingiberis Recens 1～20; Ilex purpurea Hassk.[I.chinensis Sims 2～20; Herba Andrographis 2～20; Abelmoschus manihot 2～20; Radix Salviae Miltiorrhizae 1～20; Aloe 2～30; Herba Senecionis Scandentis 2～20.
According to purpose of the present invention, the present invention adopts the high pressure homogenize extractive technique that above Chinese medicine composition is extracted, investigated the bactericidal effect of factors on extraction rate such as Chinese medicine composition granularity, extractant type, solid-liquid mass ratio, extraction time, extraction pressure and extract, the extract preparation process condition that has obtained Chinese medicine composition is: the Chinese medicine composition granularity is 20～200 orders; Volume fraction is that 5%～80% ethanol is extractant, and extraction pressure is 10～80MPa, and the solid-liquid mass ratio is 1: 3～40, and extraction time is 5～80min.The extracting solution activated carbon decolorizing, active carbon and extracting solution mass ratio are 1: 10～100, bleaching time 10～180min.
Another object of the present invention is with the extract of this Chinese medicine composition effective ingredient as the daily chemical product with sterilizing function, makes stable in properties, daily chemical product that bactericidal effect is good.The consumption of the extract of this Chinese medicine composition in daily chemical product is 0.1%～20%.
The extract of the Chinese medicine composition with sterilizing function that the present invention obtains does not contain the material of chemosynthesis, and is nontoxic, have no side effect, safe and reliable, can be directly used in skin, effectively remove and kill the antibacterial on the human body skin, can effectively prevent human body skin simultaneously by bacterial infection.The extract of Chinese medicine composition of the present invention can be used to do have the sterilizing function material of the daily chemical product of sterilizing function, can join in the products such as anti-dandruff shampoo, antibacterial bath liquor, anti-bacterial hand lotion, acne-eliminating cosmetic, Antibacterial soaps.
The specific embodiment
Below come by specific embodiment that the present invention is further illustrated, but these embodiment are not limitations of the present invention just in order to illustrate.
One, the preparation of the extract of Chinese medicine composition
Embodiment 1:
A kind of Chinese medicine composition with sterilizing function, it is made up of according to percentage by weight following Chinese medicine: Flos Lonicerae 10; Flos Chrysanthemi Indici 10; Herba Taraxaci 10; Radix Glycyrrhizae 10; Rhizoma Zingiberis Recens 5; Ilex purpurea Hassk.[I.chinensis Sims 8; Herba Andrographis 6; Abelmoschus manihot 10; Radix Salviae Miltiorrhizae 6; Aloe 15; Herba Senecionis Scandentis 10.
The preparation method of extract of this Chinese medicine composition is: earlier that above-mentioned Chinese medicine is good according to the percentage by weight weighing, behind the mix homogeneously, be crushed to 100 orders with pulverizer, according to the solid-liquid mass ratio is that 1: 15 adding 40% ethanol is extractant, extract under the pressure 40MPa extract 40min with high pressure homogenizer after, medicinal residues are removed in centrifugal filtration, obtain extracting solution.Be to add active carbon at 1: 30 according to active carbon and extracting solution mass ratio then, mix the 100min processing of decolouring, be the extract of the Chinese medicine composition after the decolouring.
Embodiment 2:
A kind of Chinese medicine composition with sterilizing function, it is made up of according to percentage by weight following Chinese medicine: Flos Lonicerae 5; Flos Chrysanthemi Indici 15; Herba Taraxaci 15; Radix Glycyrrhizae 15; Rhizoma Zingiberis Recens 5; Ilex purpurea Hassk.[I.chinensis Sims 5; Herba Andrographis 5; Abelmoschus manihot 5; Radix Salviae Miltiorrhizae 10; Aloe 10; Herba Senecionis Scandentis 10.
The preparation method of extract of this Chinese medicine composition is: earlier that above-mentioned Chinese medicine is good according to the percentage by weight weighing, behind the mix homogeneously, be crushed to 80 orders with pulverizer, according to the solid-liquid mass ratio is that 1: 8 adding 50% ethanol is extractant, extract under the pressure 60MPa extract 20min with high pressure homogenizer after, medicinal residues are removed in centrifugal filtration, obtain extracting solution.Be to add active carbon at 1: 40 according to active carbon and extracting solution mass ratio then, mix the 45min processing of decolouring, be the extract of the Chinese medicine composition after the decolouring.
Embodiment 3:
A kind of sterilization Chinese medicine composition, it is made up of according to percentage by weight following Chinese medicine: Flos Lonicerae 15; Flos Chrysanthemi Indici 8; Herba Taraxaci 15; Radix Glycyrrhizae 12; Rhizoma Zingiberis Recens 10; Ilex purpurea Hassk.[I.chinensis Sims 6; Herba Andrographis 4; Abelmoschus manihot 10; Radix Salviae Miltiorrhizae 10; Aloe 5; Herba Senecionis Scandentis 5.
The preparation method of extract of this Chinese medicine composition is: earlier that above-mentioned Chinese medicine is good according to the percentage by weight weighing, behind the mix homogeneously, be crushed to 60 orders with pulverizer, according to the solid-liquid mass ratio is that 1: 10 adding 60% ethanol is extractant, extract under the pressure 30MPa extract 35min with high pressure homogenizer after, medicinal residues are removed in centrifugal filtration, obtain extracting solution.Be to add active carbon at 1: 50 according to active carbon and extracting solution mass ratio then, mix the 120min processing of decolouring, be the extract of the Chinese medicine composition after the decolouring.
Two, the preparation that has the daily chemical product of sterilizing function
The preparation of embodiment 1 anti-acne moisturiser
Table 1 provides the anti-acne moisturiser prescription of the extract that contains the Chinese medicine composition that sterilizes, and the consumption of each material is represented with mass fraction.
Table 1
The preparation method of anti-acne moisturiser: the component A in the formula table is mixed, be heated to 85 ℃, fusing stirs, as oil phase; B component in the formula table is mixed, be heated to 85 ℃, stirring and dissolving is even, as water.Oil phase is added aqueous phase, stir, emulsifying was stirred when being cooled to below 45 ℃ after 5 minutes, added component C, stirred, and was cooled to 35 ℃, can make the anti-acne moisturiser.
The preparation of embodiment 2 anti-dandruff shampoos
Table 2 provides the anti-dandruff shampoo prescription of the extract that contains the Chinese medicine composition that sterilizes, and the consumption of each material is represented with mass fraction.
Table 2
The preparation method of anti-dandruff shampoo: the deionized water among the component A is heated to 85 ℃, add ammonium chloride, EDTA-2Na, citric acid, cation guar gum successively, maintain the temperature at 80～85 ℃, after raw material is fully dissolved, add AESA AESA, cocamido propyl betaine CAB-35, alkanolamide 6501, stirring and dissolving.Temperature is adjusted to 75 ℃, add 16 octadecanol, pearlescent flake, after the fusing, stir, feed cooling water, slowly be cooled to 45 ℃, add all raw materials of B component, stir, continue to be cooled to 38 ℃, can make anti-dandruff shampoo.
The preparation of embodiment 3 antibacterial bath liquors
Table 3 provides the antibacterial bath liquor prescription of the extract that contains the Chinese medicine composition that sterilizes, and the consumption of each material is represented with mass fraction.
Table 3
The preparation method of antibacterial bath liquor: the deionized water among the component A is heated to 85 ℃, add sodium chloride, EDTA-2Na, citric acid successively, after raw material is fully dissolved, add polyoxyethylenated alcohol sodium sulfate AES, cocamido propyl betaine CAB-35, alkanolamide 6501, after the stirring and dissolving, temperature is adjusted to 75 ℃, add pearlescent flake, stir, feed cooling water, slowly be cooled to 45 ℃, all raw materials that add B component, stir, continue to be cooled to 38 ℃, can make antibacterial bath liquor.
The preparation of embodiment 4 anti-bacterial hand lotions
Table 4 provides the anti-bacterial hand lotion prescription of the extract that contains the Chinese medicine composition that sterilizes, and the consumption of each material is represented with mass fraction.
Table 4
The preparation method of anti-bacterial hand lotion: the deionized water among the component A is heated to 85 ℃, add sodium chloride, EDTA-2Na, citric acid successively, after raw material is fully dissolved, add polyoxyethylenated alcohol sodium sulfate AES, cocamido propyl betaine CAB-35, alkanolamide 6501, after the stirring and dissolving, feed cooling water, slowly be cooled to 45 ℃, add all raw materials of B component, stir, continue to be cooled to 38 ℃, can make anti-bacterial hand lotion.
The preparation of embodiment 5 antibiotic liquid detergents
Table 5 provides the antibiotic liquid detergent prescription of the extract that contains the Chinese medicine composition that sterilizes, and the consumption of each material is represented with mass fraction.
The preparation method of antibiotic liquid detergent: the sodium hydroxide among the component A is dissolved in the deionized water, slowly adds DBSA and sodium hydroxide generation neutralization reaction in batches.After the stirring and dissolving, add all raw materials of B component in order successively, stirring and dissolving is even, can make antibiotic liquid detergent.
Table 5
The preparation of embodiment 6 Antibacterial soaps
Table 6 provides the Antibacterial soaps prescription of the extract that contains the Chinese medicine composition that sterilizes, and the consumption of each material is represented with mass fraction.
Table 6
The preparation method of Antibacterial soaps: all material stirring and dissolving in the B component are even; With titanium dioxide among the component A and soap base mix homogeneously, the mixed liquor with B component sprays among the component A then, and uniform mixing after three-roll grinder grinding evenly, is passed through operations such as press strip, stripping and slicing, printing again, can make Antibacterial soaps.
Claims (8)
1. the Chinese medicine composition that has sterilizing function is characterized in that by weight percentage, is made up of following Chinese medicine: Flos Lonicerae 2～25; Flos Chrysanthemi Indici 2～10; Herba Taraxaci 1～20; Radix Glycyrrhizae 1～10; Rhizoma Zingiberis Recens 1～20; Ilex purpurea Hassk.[I.chinensis Sims 2～20; Herba Andrographis 2～20; Abelmoschus manihot 2～20; Radix Salviae Miltiorrhizae 1～20; Aloe 2～30; Herba Senecionis Scandentis 2～20.
2. according to the described preparation method of extract of claim with Chinese medicine composition of sterilizing function, it is characterized in that: earlier that above-mentioned Chinese medicine is good according to the percentage by weight weighing, behind the mix homogeneously, be crushed to 20～200 orders with pulverizer, according to the solid-liquid mass ratio is that 1: 3～40 adding mass fractions are that 5%～80% ethanol is extractant, extract under pressure 10～80MPa extract 5～80min with high pressure homogenizer after, medicinal residues are removed in centrifugal filtration, obtain extracting solution.Be 1: 10～100 to add active carbons according to active carbon and extracting solution mass ratio then, mix 10～180min processing of decolouring, be the extract of the Chinese medicine composition after the decolouring with sterilizing function.
3. the described application of extract on the preparation acne-eliminating cosmetic of claim 1 with Chinese medicine composition of sterilizing function.
4. the described application of extract on the preparation anti-dandruff shampoo of claim 1 with Chinese medicine composition of sterilizing function.
5. the described application of extract on the preparation antibacterial bath liquor of claim 1 with Chinese medicine composition of sterilizing function.
6. the described application of extract on the preparation anti-bacterial hand lotion of claim 1 with Chinese medicine composition of sterilizing function.
7. the described application of extract on the antibiotic liquid detergent of preparation of claim 1 with Chinese medicine composition of sterilizing function.
8. the described application of extract on the preparation Antibacterial soaps of claim 1 with Chinese medicine composition of sterilizing function.
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