CN107996630A - A kind of antimicrobial agent and preparation method thereof and the Antibacterial soaps prepared and method - Google Patents
A kind of antimicrobial agent and preparation method thereof and the Antibacterial soaps prepared and method Download PDFInfo
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- CN107996630A CN107996630A CN201711297743.XA CN201711297743A CN107996630A CN 107996630 A CN107996630 A CN 107996630A CN 201711297743 A CN201711297743 A CN 201711297743A CN 107996630 A CN107996630 A CN 107996630A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/42—Aloeaceae [Aloe family] or Liliaceae [Lily family], e.g. aloe, veratrum, onion, garlic or chives
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/005—Synthetic soaps
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/44—Perfumes; Colouring materials; Brightening agents ; Bleaching agents
- C11D9/442—Perfumes
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- Chemical & Material Sciences (AREA)
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Abstract
The invention discloses a kind of antimicrobial agent and preparation method thereof and the Antibacterial soaps prepared, antimicrobial agent to be made of following parts by weight material：30~36 parts of antibacterial peptide, 10~14 parts of radix glycyrrhizae, 12~16 parts of honeysuckle, 19~24 parts of peppermint, 2~8 parts of Aloe Vera Gel, 1~2 part of sulphur, 3~5 parts of sea salt.Contain antibacterial peptide in antimicrobial agent, antibacterial peptide biggest advantage is that microorganism can be killed quickly, has very high bactericidal activity, can effectively suppress the growth of a variety of pathogenetic bacterias and fungi.After being dissolved in water and grease by sodium hydroxide the reaction was complete, add antimicrobial agent and essential oil stirs evenly, Antibacterial soaps are made after solidification, method is simple, easy to operate；Invention raw material Chinese medicine convenient sources, it is cheap；Antibacterial substance and soap base raw material used is natural products, is had the advantages that safe and nontoxic, without side-effects；Lingering fragrance is left after washing；Perfumed soap of the present invention is adapted to young man to use, and for perspiration removing, antibacterial has good effects.
Description
Technical field
The invention belongs to household chemicals technical field, and in particular to a kind of antimicrobial agent and preparation method thereof and preparation
Antibacterial soaps and method.
Background technology
With the continuous development that modern civilization construction and business need, the continuous improvement of people's daily life level, to washing
The requirement of bath article is continuously improved.Traditionally people are used with sodium soap and other surfaces activating agent when washing and taking a shower
Quality improver and appearance modifying agents are added at the same time for primary raw material, manufactured perfumed soap product, this kind of production after machine-shaping
The pH value meta-alkalescence of product, it is uncoordinated with the acid pH value of human skin, thus irritation is larger, and stain removal bactericidal effect is bad.
Long-time service has skin certain harmful effect.
The content of the invention
In view of the above-mentioned deficiencies in the prior art, the technical problem to be solved by the present invention is that provide a kind of antimicrobial agent
And preparation method thereof and prepare Antibacterial soaps, contain traditional Chinese medicine ingredients, skin contactable, no chemical stimulation, add antibacterial peptide
Stain removal bactericidal effect has been lifted afterwards, and lingering fragrance is left after washing, and is adapted to young man to use, and for perspiration removing, antibacterial has good effects.
The present invention uses following technical scheme：
A kind of antimicrobial agent, is made of following parts by weight material：30~36 parts of antibacterial peptide, 10~14 parts of radix glycyrrhizae, honeysuckle
12~16 parts, 19~24 parts of peppermint, 2~8 parts of Aloe Vera Gel, 1~2 part of sulphur, 3~5 parts of sea salt.
Specifically, it is made of following parts by weight material：33 parts of antibacterial peptide, 12 parts of radix glycyrrhizae, 14 parts of honeysuckle, 22 parts of peppermint,
5 parts of Aloe Vera Gel, 1 part of sulphur, 4 parts of sea salt.
The invention also discloses a kind of method for preparing antimicrobial agent, comprise the following steps：
Add water in S1, the radix glycyrrhizae to Jing Guo mechanical crushing, honeysuckle, peppermint, the heating extraction after Ultrasonic Pulverization, is filtered
Remove ethanol to extracting solution A and filter residue, then toward addition alcohol reflux extraction in filter residue, filtering, decompression and obtain extracting solution B, will carry
Liquid A and extracting solution B is taken to be concentrated to give concentrate after mixing；
S2, mix concentrate prepared by step S1 with Aloe Vera Gel, sulphur, sea salt and antibacterial peptide, and heating stirring is made anti-
Bacterium medicament.
Further, in step S1, radix glycyrrhizae, the water of 3~5 times of amounts of honeysuckle and peppermint total amount, ultrasonic grinder are added
After crushing, 98~102 DEG C, when extraction 1.8~2.2 is small are heated to.
Further, in step S1, the ethanol that 2~3 times of mass fractions of filter residue total amount are 83~87% is added into filter residue,
When refluxing extraction 1.9~2.1 is small.
Further, in step S1, concentrate concentration is 2.9~3.1 times of concentration after mixing.
Further, in step S2, heating-up temperature is 75~80 DEG C, and when 75~80 DEG C of stirrings 0.9~1.1 are small.
Further, in step S2, the particle diameter of sulphur and sea salt is 10~20 microns.
The invention also discloses a kind of Antibacterial soaps, including antimicrobial agent, essential oil, grease and sodium hydroxide, antimicrobial agent
Content be mass percent 30~40%, the content of essential oil is the weight of mass percent 0.1~1%, grease and sodium hydroxide
It is (10~15) to measure ratio：(1~1.5), accounts for remaining mass percent；
Essential oil is (0.8~1.2) including weight ratio：(1.8~2.2)：The lemon of (0.8~1.2), wormwood essential oil and
Lavender；
Grease is (4.8~5.2) including weight ratio：(1.8~2.2)：(1.8~2.2)：(0.4~0.6)：(0.8~
1.2)：The olive oil of (9.5~10.5), fiery sesame oil, castor oil, avocado oil, coconut oil and stearic acid.
The invention also discloses a kind of method for preparing Antibacterial soaps, by sodium hydroxide be dissolved in water postcooling to 40 DEG C with
Under, grease is added after the reaction was complete, adds antimicrobial agent and essential oil stirs evenly, Antibacterial soaps are made after solidification.
Compared with prior art, the present invention at least has the advantages that：
The present invention provides a kind of antimicrobial agent, antibacterial peptide is contained in antimicrobial agent, antibacterial peptide biggest advantage is can
To kill microorganism quickly, there is very high bactericidal activity, can effectively suppress the growth of a variety of pathogenetic bacterias and fungi.
The invention also discloses a kind of preparation method of antimicrobial agent, adds to the good radix glycyrrhizae of mechanical crushing, honeysuckle, peppermint
Water, heating extraction after Ultrasonic Pulverization are obtained by filtration extracting solution A and filter residue, then toward adding alcohol reflux extraction in filter residue, filtering,
Decompression removes ethanol and obtains extracting solution B, and extracting solution A and extracting solution B are concentrated to give concentrate after mixing；By concentrate with
Aloe Vera Gel, sulphur, sea salt and antibacterial peptide mixing, heating stirring are made antimicrobial agent, letter are not only operated using said extracted method
It is single, cost is saved, while can achieve the purpose that antibacterial pro-skin than more completely extracting the active ingredient in medicine.
Further, using Ultrasonic Pulverization heating extraction and alcohol reflux extraction can cause medicine it is fat-soluble with it is water-soluble
The effect of property component is more sufficiently extracted, gives full play to medicinal material.
Further, the mixing of extracting solution A and B can make antimicrobial agent synergy, active ingredient more horn of plenty；Concentration extraction
Liquid can greatly enhance antibacterial effect, while make the smell acceptance of antimicrobial agent more good.
The invention also discloses a kind of Antibacterial soaps, Chinese herbal antibacterial agent is with the addition of in Antibacterial soaps formula, wherein, aloe
With sterilization, anti-inflammatory and moistening beautification function；Peppermint can promote blood circulation, and have the function that antibacterial anti-inflammatory, in perfumed soap
Other traditional Chinese medicine ingredients, can directly contact skin, without chemical stimulation, play moisturizing beauty treatment, moisten moisturizing, stain removal bactericidal
Effect.
The invention also discloses a kind of preparation method of Antibacterial soaps, and sodium hydroxide is dissolved in water, and the reaction was complete with grease
Afterwards, add antimicrobial agent and essential oil stirs evenly, Antibacterial soaps are made after solidification, method is simple, easy to operate；Invention raw material
Chinese medicine convenient sources, it is cheap；Antibacterial substance and soap base raw material used is natural products, has safe and nontoxic, nothing
The advantages of side effect；Lingering fragrance is left after washing；Perfumed soap of the present invention is adapted to young man to use, and for perspiration removing, antibacterial has good effects.
Below by drawings and examples, technical scheme is described in further detail.
Brief description of the drawings
Fig. 1 is flow diagram of the present invention；
Fig. 2 is that the biocidal property of antimicrobial agent of the present invention measures schematic diagram, wherein, (a) is staphylococcus aureus, and (b) is
Escherichia coli, (c) are bacillus subtilis.
Embodiment
Referring to Fig. 1, the present invention provides a kind of antimicrobial agent, it is made of following parts by weight material：Antibacterial peptide 30~36
Part, 10~14 parts of radix glycyrrhizae, 12~16 parts of honeysuckle, 19~24 parts of peppermint, 2~8 parts of Aloe Vera Gel, 1~2 part of sulphur, sea salt 3~5
Part.
Antimicrobial agent is made of following parts by weight material：33 parts of antibacterial peptide, 12 parts of radix glycyrrhizae, 14 parts of honeysuckle, 22 parts of peppermint,
5 parts of Aloe Vera Gel, 1 part of sulphur, 4 parts of sea salt.
A kind of preparation method of antimicrobial agent of the present invention：
1) water of 3~5 times of amounts is added into the radix glycyrrhizae Jing Guo mechanical crushing, honeysuckle, peppermint, using ultrasonic grinder
After crushing, be heated to 100 DEG C of extractions 2 it is small when after, be obtained by filtration extracting solution A and filter residue, then toward adding 2~3 times of heavys in filter residue
After when 85% alcohol reflux of amount fraction extraction 2 is small, filtering, decompression remove ethanol and obtain extracting solution B, by extracting solution A and extracting solution B
3 times of concentration after extracting solution mixes are concentrated into after mixing, obtain concentrate；
2) concentrate prepared by step 1 is mixed with Aloe Vera Gel, sulphur, sea salt and antibacterial peptide, is heated to 80 DEG C, at 80 DEG C
It is lower stirring 1 it is small when, obtain the antimicrobial agent.
Wherein, the particle diameter of sulphur and sea salt is 10~20 microns, and antibacterial peptide includes Magainin, streptococcus lactis peptide or plant breast
Bacillin etc..
The present invention provides a kind of Antibacterial soaps, raw material includes antimicrobial agent, essential oil, grease and sodium hydroxide, antimicrobial
The content of agent is mass percent 30~40%, and essential oil content is the weight of mass percent 0.1~1%, grease and sodium hydroxide
It is (10~15) to measure ratio：(1~1.5).
Essential oil includes lemon, wormwood essential oil, Lavender, its weight ratio is (0.8~1.2)：(1.8~2.2)：
(0.8~1.2).
Grease includes olive oil, fiery sesame oil, castor oil, avocado oil and coconut oil-stearic acid, olive oil, fiery sesame oil, castor-oil plant
Oil, avocado oil, coconut oil and stearic acid press (4.8~5.2)：(1.8~2.2)：(1.8~2.2)：(0.4~0.6)：(0.8~
1.2)：(9.5~10.5) weight ratio mixes.
A kind of preparation process of Antibacterial soaps：After being dissolved in water and grease by sodium hydroxide the reaction was complete, antimicrobial agent is added
Stirred evenly with essential oil, Antibacterial soaps are made after solidification.
To make the purpose, technical scheme and advantage of the embodiment of the present invention clearer, below in conjunction with the embodiment of the present invention
In attached drawing, the technical solution in the embodiment of the present invention is clearly and completely described, it is clear that described embodiment is
Part of the embodiment of the present invention, instead of all the embodiments.The present invention being described and shown in usually here in attached drawing is real
Applying the component of example can be arranged and be designed by a variety of configurations.Therefore, the present invention to providing in the accompanying drawings below
The detailed description of embodiment be not intended to limit the scope of claimed invention, but be merely representative of the selected of the present invention
Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are obtained without creative efforts
The every other embodiment obtained, belongs to the scope of protection of the invention.
Embodiment 1：
A kind of Antibacterial soaps, including following material are made：Antimicrobial agent, essential oil, grease, sodium hydroxide, water are solvent；
Wherein, the content of the antimicrobial agent is mass fraction 34.4%, and the essential oil content is mass fraction 0.1%,
The weight ratio of the grease and sodium hydroxide is 10：1, content 65.5%；
The antimicrobial agent is made of following parts by weight material：30 parts of antibacterial peptide, 10 parts of radix glycyrrhizae, 12 parts of honeysuckle, peppermint
19 parts, 2 parts of Aloe Vera Gel, 1 part of sulphur, 3 parts of sea salt；
The essential oil includes lemon, wormwood essential oil, Lavender, its weight ratio is 0.8：1.8：0.8.
The grease is olive oil, fiery sesame oil, castor oil, avocado oil, coconut oil, stearic acid are by weight 4.8：1.8：
1.8：0.4：0.8：9.5 mix.
The antimicrobial agent is made of following methods：
1) water of 3 times of amounts is added to the radix glycyrrhizae Jing Guo mechanical crushing, honeysuckle, peppermint, is crushed using ultrasonic grinder
Afterwards, be heated to 98 DEG C of extractions 1.8 it is small when after, be obtained by filtration extracting solution A and filter residue, then toward adding 2 times of weight mass fractions in filter residue
After when 83% alcohol reflux extraction 1.9 is small, filtering, decompression remove ethanol and obtain extracting solution B, and extracting solution A is mixed with extracting solution B
3 times of concentration after extracting solution mixes are concentrated into after uniformly, obtains concentrate；
2) concentrate obtained by upper step is mixed with Aloe Vera Gel, sulphur, sea salt and antibacterial peptide, is heated to 75 DEG C, at 75 DEG C
Stir 0.9 it is small when, obtain the antimicrobial agent.
The preparation method of the Antibacterial soaps：Raw material weighed up by proportioning, sodium hydroxide is dissolved in cold after water by the first step
But it is less than 40 DEG C to temperature, is slow added into room temperature grease, stirring is reacted, when liquid slowly becomes thick, reaction
Completely, stirred evenly after the antimicrobial agent weighed up and essential oil being added, up to the Antibacterial soaps after solidification.
Embodiment 2：
A kind of Antibacterial soaps, including following material are made：Antimicrobial agent, essential oil, grease, sodium hydroxide, water are solvent；
The content of wherein described antimicrobial agent is mass fraction 34%, and the essential oil content is mass fraction 1%, the oil
The weight ratio of fat and sodium hydroxide is 20：1.4, content 65%；
The antimicrobial agent is made of following parts by weight material：36 parts of antibacterial peptide, 14 parts of radix glycyrrhizae, 16 parts of honeysuckle, peppermint
24 parts, 8 parts of Aloe Vera Gel, 2 parts of sulphur, 5 parts of sea salt；
The essential oil includes lemon, wormwood essential oil, Lavender, its weight ratio is 1:2:1；
The grease is olive oil, fiery sesame oil, castor oil, avocado oil, coconut oil, stearic acid are by weight 5：2：2：0.5：
1：10 mix.
The antimicrobial agent is made of following methods：
1) water of 4 times of amounts is added to the radix glycyrrhizae Jing Guo mechanical crushing, honeysuckle, peppermint, is crushed using ultrasonic grinder
Afterwards, be heated to 100 DEG C of extractions 2 it is small when after, be obtained by filtration extracting solution A and filter residue, then toward adding 2.5 times of weight mass fractions in filter residue
After when 85% alcohol reflux extraction 2 is small, filtering, decompression remove ethanol and obtain extracting solution B, and extracting solution A is mixed with extracting solution B
3 times of concentration after extracting solution mixes are concentrated into after even, obtains concentrate；
2) concentrate obtained by upper step is mixed with Aloe Vera Gel, sulphur, sea salt and antibacterial peptide, is heated to 77 DEG C, at 77 DEG C
Stir 1 it is small when, obtain the antimicrobial agent.
The preparation method of Antibacterial soaps, is weighed up raw material by proportioning, sodium hydroxide is dissolved in water postcooling to temperature by the first step
Degree is less than 40 DEG C, is slow added into room temperature grease, and stirring is reacted, and when liquid slowly becomes thick, the reaction was complete, will
The antimicrobial agent and essential oil weighed up stirs evenly after adding, up to the Antibacterial soaps after solidification.
Embodiment 3：
A kind of Antibacterial soaps, including following material are made：Antimicrobial agent, essential oil, grease, sodium hydroxide, water are solvent；
The content of wherein described antimicrobial agent is mass fraction 34.5%, and the essential oil content is mass fraction 0.5%, institute
The weight ratio for stating grease and sodium hydroxide is 15：1.2, content 65%；
The antimicrobial agent is made of following parts by weight material：33 parts of antibacterial peptide, 12 parts of radix glycyrrhizae, 14 parts of honeysuckle, peppermint
22 parts, 5 parts of Aloe Vera Gel, 1 part of sulphur, 4 parts of sea salt；
The essential oil includes lemon, wormwood essential oil, Lavender, its weight ratio is 1：2：1；
The grease is olive oil, fiery sesame oil, castor oil, avocado oil, coconut oil, stearic acid are by weight 5：2：2：0.5：
1：10 mix.
The antimicrobial agent is made of following methods：
1) radix glycyrrhizae, honeysuckle, peppermint are added into 5 times of heavy water, after being crushed using ultrasonic grinder, is heated to 102 DEG C and carries
Take 2.2 it is small when after, be obtained by filtration extracting solution A and filter residue, then toward adding 3 times of 87% alcohol refluxs of weight mass fraction extractions in filter residue
2 it is small when after, filtering, decompression remove ethanol and obtain extracting solution B, and extracting solution A and extracting solution B are concentrated into extracting solution after mixing
3 times of concentration, obtain concentrate after mixing；
2) concentrate obtained by upper step is mixed with Aloe Vera Gel, sulphur, sea salt and antibacterial peptide, is heated to 80 DEG C, at 80 DEG C
Stir 1.1 it is small when, obtain the antimicrobial agent.
The preparation method of the Antibacterial soaps：Raw material is weighed up by proportioning, sodium hydroxide is dissolved in water postcooling to temperature
Degree is less than 40 DEG C, is slow added into room temperature grease, and stirring is reacted, and when liquid slowly becomes thick, the reaction was complete, will
The antimicrobial agent and essential oil weighed up stirs evenly after adding, up to the Antibacterial soaps after solidification.
Referring to Fig. 2, wherein, (a) is staphylococcus aureus, (b) is Escherichia coli, and (c) is bacillus subtilis, figure
In 1 be this method antimicrobial agent, 2 be without addition antibacterial peptide antimicrobial agent, 3 be sterile water, when in antimicrobial agent resist
For bacterium peptide quality in 0.25ug/ul, its inhibition zone to staphylococcus aureus is 6mm, and the inhibition zone of bacillus coli DH 5 alpha is
5mm, the inhibition zone of bacillus subtilis is 10mm.
Above content is merely illustrative of the invention's technical idea, it is impossible to protection scope of the present invention is limited with this, it is every to press
According to technological thought proposed by the present invention, any change done on the basis of technical solution, each falls within claims of the present invention
Protection domain within.
Claims (10)
1. a kind of antimicrobial agent, it is characterised in that be made of following parts by weight material：30~36 parts of antibacterial peptide, radix glycyrrhizae 10~14
Part, 12~16 parts of honeysuckle, 19~24 parts of peppermint, 2~8 parts of Aloe Vera Gel, 1~2 part of sulphur, 3~5 parts of sea salt.
2. a kind of antimicrobial agent according to claim 1, it is characterised in that be made of following parts by weight material：Antibacterial peptide
33 parts, 12 parts of radix glycyrrhizae, 14 parts of honeysuckle, 22 parts of peppermint, 5 parts of Aloe Vera Gel, 1 part of sulphur, 4 parts of sea salt.
A kind of 3. method for preparing the antimicrobial agent of claim 1 or 2, it is characterised in that comprise the following steps：
Add water in S1, the radix glycyrrhizae to Jing Guo mechanical crushing, honeysuckle and peppermint, the heating extraction after Ultrasonic Pulverization, is obtained by filtration
Extracting solution A and filter residue, then remove ethanol toward addition alcohol reflux extraction in filter residue, filtering, decompression and obtain extracting solution B, will extract
Liquid A and extracting solution B is concentrated to give concentrate after mixing；
S2, mix concentrate prepared by step S1 with Aloe Vera Gel, sulphur, sea salt and antibacterial peptide, and antimicrobial is made in heating stirring
Agent.
A kind of 4. preparation method of antimicrobial agent according to claim 3, it is characterised in that in step S1, addition radix glycyrrhizae,
The water of 3~5 times of amounts of honeysuckle and peppermint total amount, after ultrasonic grinder crushes, is heated to 98~102 DEG C, extraction 1.8~2.2
Hour.
5. the preparation method of a kind of antimicrobial agent according to claim 4, it is characterised in that in step S1, into filter residue
The ethanol that 2~3 times of mass fractions of filter residue total amount are 83~87% is added, when refluxing extraction 1.9~2.1 is small.
6. the preparation method of a kind of antimicrobial agent according to claim 3, it is characterised in that in step S1, concentrate is dense
Spend for 2.9~3.1 times of concentration after mixing.
A kind of 7. preparation method of antimicrobial agent according to claim 3, it is characterised in that in step S2, heating-up temperature
For 75~80 DEG C, and when 75~80 DEG C of stirrings 0.9~1.1 are small.
A kind of 8. preparation method of antimicrobial agent according to claim 3, it is characterised in that in step S2, sulphur and sea
The particle diameter of salt is 10~20 microns.
9. a kind of Antibacterial soaps prepared using antimicrobial agent described in claim 1, it is characterised in that including antimicrobial agent, essence
Oil, grease and sodium hydroxide, the content of antimicrobial agent is mass percent 30~40%, and the content of essential oil is mass percent
0.1~1%, the weight ratio of grease and sodium hydroxide is (10~15)：(1~1.5), accounts for remaining mass percent；
Essential oil is (0.8~1.2) including weight ratio：(1.8~2.2)：The lemon of (0.8~1.2), wormwood essential oil and smoke clothing
Careless essential oil；
Grease is (4.8~5.2) including weight ratio：(1.8~2.2)：(1.8~2.2)：(0.4~0.6)：(0.8~1.2)：
The olive oil of (9.5~10.5), fiery sesame oil, castor oil, avocado oil, coconut oil and stearic acid.
A kind of 10. method for preparing Antibacterial soaps described in claim 9, it is characterised in that sodium hydroxide is dissolved in water postcooling
To less than 40 DEG C, grease is added after the reaction was complete, antimicrobial agent is added and essential oil stirs evenly, and it is fragrant that antibacterial is made after solidification
Soap.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109652239A (en) * | 2018-11-27 | 2019-04-19 | 安徽省玉兔日用化学品有限公司 | A kind of amino acid perfumed soap and its processing technology containing Rhizoma Polygonati extract |
| CN110742088A (en) * | 2019-11-07 | 2020-02-04 | 盛兆云 | Biological mixed liquor of taurine and preparation method thereof |
| CN111394204A (en) * | 2020-03-18 | 2020-07-10 | 卢喜 | Antibacterial medicated soap and preparation method thereof |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
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